CN113425663A

CN113425663A - Preparation method of dendrobium flower soybean skin-beautifying mask

Info

Publication number: CN113425663A
Application number: CN202110947460.5A
Authority: CN
Inventors: 张珍林; 陈乃富; 韩邦兴; 刘�东; 殷智超; 何晓梅; 汪学军; 邓辉; 祁明雪
Original assignee: West Anhui University
Current assignee: West Anhui University
Priority date: 2021-08-18
Filing date: 2021-08-18
Publication date: 2021-09-24

Abstract

The invention discloses a preparation method of a dendrobium flower soybean skin-beautifying facial mask, which relates to the field of daily cosmetics, and the facial mask liquid mainly comprises dendrobium flower extract, soybean extract, glycerol, micromolecular hyaluronic acid, EDTA disodium, carbomer, xanthan gum, a pH regulator (triethanolamine), a small amount of parabens, a small amount of essence and deionized water; the dendrobium flower soybean skin-beautifying facial mask prepared by the invention contains the dendrobium flower extracting solution with various effects of whitening, nourishing, antioxidation, anti-aging and the like, and also contains the soybean isoflavone component with antioxidation and anti-aging, and according to the synergistic effect, the dendrobium flower soybean skin-beautifying facial mask prepared by the invention can greatly enhance the effects of antioxidation and anti-aging, nourish skin cells, restore the moisture and luster and delay the skin aging, is prepared by using pure natural extraction essence, and is pollution-free and pollution-free. The glycerin and the small molecular hyaluronic acid can also increase the moisture retention property and make the skin more moist.

Description

Preparation method of dendrobium flower soybean skin-beautifying mask

Technical Field

The invention relates to the field of daily cosmetics, and particularly relates to a dendrobium flower and soybean skin-beautifying facial mask and a preparation method thereof.

Background

On a special mask cabinet, a paste mask is mostly mainly used, and the paste mask with various efficacies can be seen, such as elastic moistening, after-sun repairing, fair and fine, and the like. The patch type facial mask mainly comprises facial mask cloth and essence, wherein the facial mask cloth is mainly used for adsorbing the essence and is used as a medium capable of being fixed on the face to isolate air to form a sealing layer, so that nutrient substances in the essence can be effectively absorbed, and the effect of caring the skin is achieved. The mask cloth with the essence is used for covering the face for 15-20min generally, sweat evaporation can be reduced, sufficient moisture and nutrient substances of the face skin can be maintained, the skin can quickly absorb nutrients in dendrobium flower components, facial metabolism is promoted, free radicals are eliminated, skin aging is delayed, and accordingly the skin can recover moisture elasticity and presents bright and good skin color.

The dendrobium officinale contains various active ingredients, such as polysaccharide, flavonoid, phenols, vitamins, amino acid and the like, has special effects on skin, can achieve the effects of moistening and moisturizing, resisting aging and treating certain diseases, has quite obvious effects on interfaces due to plant extract ingredients, has the medicinal values and health-care effects of resisting tumors, resisting blood coagulation, reducing blood fat, reducing blood pressure and improving immunity, and can effectively delay skin aging and keep skin elasticity through skin absorption. Researches show that the dendrobium officinale aqueous extract and the soybean isoflavone have obvious antioxidant effect when being used independently, have obvious synergistic effect when being used together, and can enable the anti-wrinkle and anti-aging effects of the product to be more excellent. Many commercial companies in the market publicize masks capable of whitening skin in a short period, and most masks contain heavy metal substances such as lead and mercury. Since mercury can inhibit the generation of melanocytes, the skin can be whitened quickly, but mercury is a toxic substance and is difficult to remove in vivo, and mercury poisoning of the skin can occur, so that serious skin problems can be caused, and the safety of the mercury can be affected.

201911341412.0A high affinity gel mask and its preparation method, comprising the following components by weight: 6 parts of sodium polyacrylate, 3-3.5 parts of polyacrylamide, 0.1-0.3 part of dihydroxyaluminium aminoacetate, 0.1-0.3 part of tartaric acid, 21.3-28.8 parts of glycerol, 45-55 parts of water and 10-20 parts of dendrobium flower composition. The high-affinity gel mask disclosed by the invention contains sodium polyacrylate and polyacrylamide, the sodium polyacrylate and the polyacrylamide have a multi-crosslinked multidimensional network structure, and the obtained gel mask is strong in viscosity and high in affinity and is beneficial to being attached to the face. There is no base cloth mask containing the extract of dendrobium flowers.

Disclosure of Invention

Aiming at the existing problems, the invention aims to provide a dendrobium flower soybean skin-beautifying facial mask which fully utilizes active ingredients in dendrobium flowers and soybeans, can achieve the effects of increasing skin elasticity and delaying skin aging, has an obvious moisturizing effect, and also has the effects of resisting bacteria, inflammation, aging, sun and the like.

The present invention solves the above problems with the following embodiments:

a method for preparing a dendrobium flower soybean skin-beautifying mask is characterized by comprising the following steps: comprises herba Dendrobii flower extractive solution.

The method for preparing the dendrobium flower soybean skin-beautifying facial mask is characterized by comprising the following steps of:

the facial mask liquid comprises the following components in percentage by weight:

2-4% of dendrobium flower extract, 0.7-1.5% of soybean extract, 3-5% of glycerol, 1-3% of butanediol, 0.01-0.03% of micromolecular hyaluronic acid, 0.1% of EDTA disodium, 0.1-0.3% of carbomer, 0.1-0.3% of xanthan gum, a proper amount of pH regulator, a proper amount of parabens, 0.01-0.02% of essence and the balance of deionized water;

the preparation of the facial mask liquid comprises the following steps:

the method comprises the following steps: taking a proper amount of deionized water, adding EDTA disodium, adding carbomer under a rapid stirring state, dispersing uniformly, adding a premix of glycerol and xanthan gum, adding a premix of micromolecular hyaluronic acid, essence and butanediol, and adding a proper amount of parabens to obtain a mixture;

step two: adding the dendrobium flower extract and the soybean extract into the mixture obtained in the step one, uniformly stirring and mixing, and homogenizing in a homogenizer for 20-30min to obtain a uniformly emulsified mixture;

step three: adjusting the pH value of the mixture obtained in the third step to 5.5-6.5 by using a pH regulator to obtain facial mask liquid;

step four: placing the facial mask solution in a disinfection cabinet, sterilizing for 25-30min, soaking the facial mask base cloth in the sterilized facial mask for 20-25min, and finally packaging and sealing the facial mask.

the preparation method of the dendrobium flower extract comprises the following steps:

accurately weighing 1 part of dried dendrobium flower, adding 80-120 parts of boiled distilled water for soaking, transferring all mixed liquid to squeeze juice, adding a proper amount of methyl paraben into the obtained sample, filtering out solid impurities from the obtained mixed liquid, and keeping filtrate, namely the dendrobium flower essence for later use.

the soybean extract is prepared by the following steps:

crushing soybeans, putting 50g of crushed soybean powder into a beaker, adding 150mL of 100-mL water, heating, collecting every 20min, adding 100mL of water, and repeating the operation for 10-12 times. Collecting, and storing in refrigerator at 4 deg.C.

accurately weighing 1 part of dried dendrobium flower, adding 99 parts of distilled water which is just boiled into the dried dendrobium flower, soaking for 1h, transferring all mixed liquor into a juicer to squeeze juice for 10min, adding a proper amount of methyl hydroxybenzoate into the obtained sample, filtering out solid impurities from the obtained mixed liquor through gauze, and putting the obtained filtrate, namely the dendrobium flower essence liquid, into a refrigerator at 4 ℃ for later use.

the soybean extract is prepared by the following steps:

crushing semen glycines into 0.3cm thick, adding 50g semen glycines powder into 250 mL beaker, adding 120mL water, heating in 50 deg.C water bath, collecting once every 20min, adding 100mL water, and repeating the above operation for 12 times. Collecting, and storing in refrigerator at 4 deg.C.

The dendrobium flower is dendrobium officinale flower.

Specifically, the dendrobium officinale used in the invention contains various active ingredients, such as polysaccharide, flavonoid, amino acid, phenols, vitamins and the like, wherein the flavonoid and the phenol are purely natural antioxidant substances and can remove excessive free radicals in vivo, so that the effects of antioxidation and anti-aging are generated; the amino acids can nourish the skin, promote the skin to absorb nutrition and moisture, show good moisturizing effect and enable a user to have good use experience; the dendrobium officinale can also effectively keep the water in the body, accelerate the metabolism of the skin and generate good effects of oxidation resistance and aging resistance.

Preferably, soy. The soybean isoflavone has certain physiological effects, including antioxidation, aging delaying, anticancer, cancer inhibition, etc. The antioxidant mechanism of the compound mainly shows that: (1) inhibiting free radical effect. The phenolic hydroxyl group in soybean isoflavone can bind with in vivo surplus free radical, and can inhibit fat peroxidation, so that the reaction can be blocked to produce antioxidant effect. (2) The effect of altering the activity of an oxidase. The soybean isoflavone can improve the activity of some antioxidant enzymes in vivo, promote the action of superoxide dismutase in vivo, and generate antioxidant effect. (3) Helping to regulate the signal path. Soybean isoflavone can protect tissue from oxidative damage and regulate specific sites on cell signaling pathway. Thereby, an antioxidant effect is produced.

Preferably, triethanolamine is selected as the pH adjusting agent in the present invention, because triethanolamine can neutralize carbomer used to form a stable high molecular structure substance, exhibiting an effect of increasing moisture retention and consistency.

Preferably, the thickening agent may be carbomer and/or xanthan gum to increase the consistency of the mask base.

The micromolecular hyaluronic acid has the advantages of rapid absorption and rapid penetration, can rapidly synthesize hyaluronic acid of skin under the catalysis of skin fiber cells, increases the content of endogenous hyaluronic acid of facial skin, and makes the skin moist and glossy.

The scheme also adopts various components such as the humectant, the thickener and the additive, so that the facial mask essence has the effects of whitening, resisting oxidation, supplementing water and the like, and simultaneously, the matrix system of the facial mask is more stable, and the facial mask has good experience and skin beautifying effects.

Compared with the prior art, the dendrobium flower soybean skin-beautifying mask has the following characteristics: 1. effectively delay skin aging and keep skin elasticity. Because the dendrobium officinale is rich in abundant nutrient substances, the dendrobium officinale has obvious nourishing effect on skin, and can play the effects of moistening, moisturizing, resisting oxidation and aging and treating certain facial acnes.

2. According to the data, only the dendrobium extract or the soybean isoflavone can generate oxidation resistance, but the experiment combines the dendrobium extract and the soybean isoflavone by utilizing the synergistic effect, so that the oxidation resistance is obviously improved, and the remarkable effects of resisting oxidation and aging are achieved; 3. The dendrobium health care tea is prepared from pure natural pollution-free dendrobium traditional Chinese medicinal materials and soybean crops, is more healthy and safe, and is comfortable and relieved to use. The preparation process is simple and quick, and industrial production and sale can be carried out.

Detailed Description

The experiment will be further described below by way of specific examples, but the experiment is not limited thereto.

Example 1

The weight percentage formula of the mask liquid is as follows: 2% of dendrobium flower extract, 0.7% of soybean extract, 5% of glycerol, 1% of butanediol, 0.01% of micromolecular hyaluronic acid, 0.1% of EDTA disodium, 0.1% of carbomer, 0.3% of xanthan gum, a proper amount of pH regulator, a proper amount of parabens, 0.01% of essence and the balance of deionized water;

the manufacturing method of the invention comprises the following steps:

the method comprises the following steps: taking a little amount of deionized water, adding EDTA disodium, adding carbomer under a rapid stirring state, dispersing uniformly, adding a premix of glycerol and xanthan gum, adding a premix of micromolecular hyaluronic acid, essence and butanediol, and adding an appropriate amount of parabens to obtain a mixture;

step two: adding the dendrobium flower extract and the soybean extract into the mixture obtained in the step one, uniformly stirring and homogenizing in a homogenizer for 20-30min to obtain a uniformly emulsified mixture;

step three: dropwise adding a little triethanolamine, and adjusting the pH value of the mixture obtained in the step two to 5.5-6.5 by using a pH regulator triethanolamine to obtain a mask liquid;

step four: placing the facial mask liquid in a disinfection cabinet, sterilizing for 25-30min, soaking the facial mask base cloth in the sterilized facial mask liquid for 20-25min, and finally packaging and sealing to obtain the dendrobium flower soybean skin-beautifying facial mask.

Example 2

The formula is as follows: 3% of dendrobium flower extract, 1.5% of soybean extract, 4% of glycerol, 2% of butanediol, 0.02% of small molecular hyaluronic acid, 0.1% of EDTA disodium, 0.2% of carbomer, 0.2% of xanthan gum, a proper amount of pH regulator, a proper amount of parabens, 0.02% of essence and the balance of deionized water;

step three: dropwise adding a little triethanolamine, and adjusting the pH value of the mixture obtained in the second step to 5.5-6.5 to obtain a mask liquid;

Example 3

The formula is as follows: 4% of dendrobium flower extract, 1.3% of soybean extract, 3% of glycerol, 3% of butanediol, 0.03% of micromolecular hyaluronic acid, 0.1% of EDTA disodium, 0.3% of carbomer, 0.1% of xanthan gum, a proper amount of pH regulator, a proper amount of parabens, 0.01% of essence and the balance of deionized water;

Example 4

The formula is as follows: 4% of dendrobium flower extract, 1.5% of soybean extract, 5% of glycerol, 5% of butanediol, 0.03% of micromolecular hyaluronic acid, 0.1% of EDTA disodium, 0.3% of carbomer, 0.1% of xanthan gum, a proper amount of pH regulator, a proper amount of parabens, 0.02% of essence and the balance of deionized water;

In the above examples, the extract solution of dendrobii flowers is prepared by:

The soybean extract is prepared by the following steps:

The above is only a part of the experimental implementation means, the protection scope of the present invention is not limited to the above operation, and various operation schemes which are not different from the concept of the present invention are within the protection scope of the present invention.

Secondly, performance detection 1, and an experiment for removing hydroxyl free radicals by the dendrobium flower soybean skin-beautifying facial mask.

Hydroxyl radical prepared by electrocatalytic oxidation method, the dendrobium flower soybean skin-beautifying facial masks prepared in examples 1 to 4 were immersed in a hydroxyl radical solution and injected into a quartz capillary for about 10 minutes for ESR detection, and the results are shown in table one

Table 1 effect of the dendrobe flower soybean skin care mask of the present invention on removal of hydroxyl radical

Serial number	Clearance rate%
		Example 1	92
Example 2	94
		Example 3	94
Example 4	95

2. The invention discloses a dendrobium flower soybean skin beautifying mask whitening effect experiment.

Selecting 50 female college students, wherein the female college students are 25-35 years old and randomly divided into 10 groups, each group comprises 5 individuals, measuring the skin brightness of the face by using a colorimeter, recording as S1, using the facial masks of the embodiments 1-4 respectively for each group, applying the facial masks twice a day for 3 weeks, measuring the skin brightness of the face by using the colorimeter, recording as S2, and measuring the whitening efficacy of the facial masks of the embodiments, wherein when the difference is more than 2, the facial masks can obviously relieve pigmentation and play a whitening role, and the experimental results are as follows:

table 2 whitening effect experiment of dendrobium flower soybean skin-beautifying mask of the present invention

Group of	Difference value
		Example 1	4.12
Example 2	4.35
		Example 3	4.47
Example 4	4.55

As can be seen from table 2, after 3 weeks using the mask products of embodiments 1 to 4 of the present invention, the chromaticity difference of the facial skin of the volunteers reached 4.12 or more, which indicates that the mask prepared in embodiments 1 to 4 of the present invention can significantly improve the pigmentation of the facial skin, and has a good whitening effect.

Third, probation investigation of dendrobium flower soybean skin-beautifying mask

In order to verify the efficacy of the dendrobium flower soybean skin-beautifying facial mask, 80 questionnaires are issued, evaluation indexes comprise after-use feelings such as appearance feeling, moisturizing, difficulty and easiness in smearing, skin smoothness and the like, and the evaluation results are shown in the following table 3. The evaluation results were obtained by using a 5-point scale, from 1 point to 5 points, and were poor, bad, normal, good and good in order.

TABLE 3 questionnaire statistics

Index (I)	Appearance feeling	Moisturizing and moisture-preserving water	Is difficult to apply	Feeling of skin lubrication
					Example 1	3.40	3.86	4.00	3.45
Example 2	3.20	3.45	3.06	4.00
					Example 3	5.00	4.00	3.68	3.67
Example 4	4.00	4.12	4.16	5.00

As can be seen from the questionnaire statistical table in table 3, the evaluation ratings of example 4 are all higher than 4 points, and are more popular than others, and have good after-use feelings such as appearance feeling, moisturizing, difficulty in application, and skin smoothness.

Claims

1. A preparation method for preparing a dendrobium flower soybean skin-beautifying mask is characterized by comprising the following steps: comprises herba Dendrobii flower extractive solution.

2. The preparation method of the dendrobium flower soybean skin-beautifying mask according to claim 1, which is characterized by comprising the following steps of:

the preparation of the facial mask liquid comprises the following steps:

3. The preparation method of the dendrobium flower soybean skin-beautifying mask according to claim 1, which is characterized by comprising the following steps of:

4. The preparation method of the dendrobium flower soybean skin-beautifying mask according to claim 1, which is characterized by comprising the following steps of:

the soybean extract is prepared by the following steps:

crushing soybeans, putting 50g of crushed soybean powder into a beaker, adding 150mL of 100-mL water, heating, collecting once every 20min, adding 100mL of water, repeating the operation for 10-12 times, collecting, and storing at 4 ℃ in a refrigerator for later use.

5. The preparation method of the dendrobium flower soybean skin-beautifying mask according to claim 1, which is characterized by comprising the following steps of:

6. The preparation method of the dendrobium flower soybean skin-beautifying mask according to claim 1, which is characterized by comprising the following steps of:

the soybean extract is prepared by the following steps:

crushing semen glycines to 0.3cm thickness, adding 50g semen glycines powder into 250 mL beaker, adding 120mL water, heating in 50 deg.C water bath, collecting once every 20min, adding 100mL water, repeating the above steps for 12 times, collecting, and storing in refrigerator at 4 deg.C for use.

7. The preparation method of the dendrobium flower soybean skin-beautifying mask according to claim 1, which is characterized by comprising the following steps of: the dendrobium flower is dendrobium officinale flower.