CN112274437B - Massage cream and preparation method thereof - Google Patents
Massage cream and preparation method thereof Download PDFInfo
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- CN112274437B CN112274437B CN202011369062.1A CN202011369062A CN112274437B CN 112274437 B CN112274437 B CN 112274437B CN 202011369062 A CN202011369062 A CN 202011369062A CN 112274437 B CN112274437 B CN 112274437B
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- 239000006071 cream Substances 0.000 title claims abstract description 25
- 238000002360 preparation method Methods 0.000 title description 12
- 239000003921 oil Substances 0.000 claims abstract description 65
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims abstract description 57
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 44
- 239000003995 emulsifying agent Substances 0.000 claims abstract description 40
- 239000000839 emulsion Substances 0.000 claims abstract description 31
- 239000002562 thickening agent Substances 0.000 claims abstract description 31
- 239000000314 lubricant Substances 0.000 claims abstract description 27
- 239000012752 auxiliary agent Substances 0.000 claims abstract description 25
- 230000001804 emulsifying effect Effects 0.000 claims abstract description 21
- 239000003755 preservative agent Substances 0.000 claims abstract description 21
- 230000002335 preservative effect Effects 0.000 claims abstract description 21
- 239000008367 deionised water Substances 0.000 claims abstract description 19
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 19
- 239000002994 raw material Substances 0.000 claims abstract description 13
- XMWRBQBLMFGWIX-UHFFFAOYSA-N C60 fullerene Chemical compound C12=C3C(C4=C56)=C7C8=C5C5=C9C%10=C6C6=C4C1=C1C4=C6C6=C%10C%10=C9C9=C%11C5=C8C5=C8C7=C3C3=C7C2=C1C1=C2C4=C6C4=C%10C6=C9C9=C%11C5=C5C8=C3C3=C7C1=C1C2=C4C6=C2C9=C5C3=C12 XMWRBQBLMFGWIX-UHFFFAOYSA-N 0.000 claims description 37
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 33
- VBICKXHEKHSIBG-UHFFFAOYSA-N 1-monostearoylglycerol Chemical compound CCCCCCCCCCCCCCCCCC(=O)OCC(O)CO VBICKXHEKHSIBG-UHFFFAOYSA-N 0.000 claims description 22
- 238000003756 stirring Methods 0.000 claims description 21
- 229910003472 fullerene Inorganic materials 0.000 claims description 20
- 210000004080 milk Anatomy 0.000 claims description 16
- 235000013336 milk Nutrition 0.000 claims description 16
- 239000008267 milk Substances 0.000 claims description 15
- 238000010438 heat treatment Methods 0.000 claims description 14
- 238000005086 pumping Methods 0.000 claims description 14
- PKPOVTYZGGYDIJ-UHFFFAOYSA-N dioctyl carbonate Chemical compound CCCCCCCCOC(=O)OCCCCCCCC PKPOVTYZGGYDIJ-UHFFFAOYSA-N 0.000 claims description 11
- GLDOVTGHNKAZLK-UHFFFAOYSA-N octadecan-1-ol Chemical compound CCCCCCCCCCCCCCCCCCO GLDOVTGHNKAZLK-UHFFFAOYSA-N 0.000 claims description 10
- 229940075507 glyceryl monostearate Drugs 0.000 claims description 9
- 239000001788 mono and diglycerides of fatty acids Substances 0.000 claims description 9
- 229960005150 glycerol Drugs 0.000 claims description 8
- 229940100555 2-methyl-4-isothiazolin-3-one Drugs 0.000 claims description 7
- QCDWFXQBSFUVSP-UHFFFAOYSA-N 2-phenoxyethanol Chemical compound OCCOC1=CC=CC=C1 QCDWFXQBSFUVSP-UHFFFAOYSA-N 0.000 claims description 7
- HIQIXEFWDLTDED-UHFFFAOYSA-N 4-hydroxy-1-piperidin-4-ylpyrrolidin-2-one Chemical compound O=C1CC(O)CN1C1CCNCC1 HIQIXEFWDLTDED-UHFFFAOYSA-N 0.000 claims description 7
- 238000001816 cooling Methods 0.000 claims description 7
- 239000004205 dimethyl polysiloxane Substances 0.000 claims description 7
- BEGLCMHJXHIJLR-UHFFFAOYSA-N methylisothiazolinone Chemical compound CN1SC=CC1=O BEGLCMHJXHIJLR-UHFFFAOYSA-N 0.000 claims description 7
- 229960005323 phenoxyethanol Drugs 0.000 claims description 7
- 229920000435 poly(dimethylsiloxane) Polymers 0.000 claims description 7
- 229940081733 cetearyl alcohol Drugs 0.000 claims description 4
- LXCFILQKKLGQFO-UHFFFAOYSA-N methylparaben Chemical compound COC(=O)C1=CC=C(O)C=C1 LXCFILQKKLGQFO-UHFFFAOYSA-N 0.000 claims description 4
- QELSKZZBTMNZEB-UHFFFAOYSA-N propylparaben Chemical compound CCCOC(=O)C1=CC=C(O)C=C1 QELSKZZBTMNZEB-UHFFFAOYSA-N 0.000 claims description 4
- 238000000034 method Methods 0.000 claims description 2
- 235000010270 methyl p-hydroxybenzoate Nutrition 0.000 claims description 2
- 239000004292 methyl p-hydroxybenzoate Substances 0.000 claims description 2
- 229960002216 methylparaben Drugs 0.000 claims description 2
- -1 polydimethylsiloxane Polymers 0.000 claims description 2
- 235000010232 propyl p-hydroxybenzoate Nutrition 0.000 claims description 2
- 239000004405 propyl p-hydroxybenzoate Substances 0.000 claims description 2
- 229960003415 propylparaben Drugs 0.000 claims description 2
- 230000000694 effects Effects 0.000 abstract description 24
- 238000004519 manufacturing process Methods 0.000 abstract description 9
- 239000000686 essence Substances 0.000 abstract 1
- 230000000052 comparative effect Effects 0.000 description 28
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 8
- 229940082500 cetostearyl alcohol Drugs 0.000 description 6
- 235000013870 dimethyl polysiloxane Nutrition 0.000 description 6
- OULAJFUGPPVRBK-UHFFFAOYSA-N tetratriacontyl alcohol Natural products CCCCCCCCCCCCCCCCCCCCCCCCCCCCCCCCCCO OULAJFUGPPVRBK-UHFFFAOYSA-N 0.000 description 6
- 239000000654 additive Substances 0.000 description 5
- 230000000996 additive effect Effects 0.000 description 5
- 230000002421 anti-septic effect Effects 0.000 description 5
- 229940008099 dimethicone Drugs 0.000 description 5
- 239000011248 coating agent Substances 0.000 description 4
- 238000000576 coating method Methods 0.000 description 4
- 230000007480 spreading Effects 0.000 description 4
- 238000003892 spreading Methods 0.000 description 4
- 239000000725 suspension Substances 0.000 description 4
- 238000012360 testing method Methods 0.000 description 4
- 239000004408 titanium dioxide Substances 0.000 description 4
- 239000000341 volatile oil Substances 0.000 description 4
- 239000002537 cosmetic Substances 0.000 description 3
- 238000011161 development Methods 0.000 description 3
- 210000003205 muscle Anatomy 0.000 description 3
- BANXPJUEBPWEOT-UHFFFAOYSA-N 2-methyl-Pentadecane Chemical compound CCCCCCCCCCCCCC(C)C BANXPJUEBPWEOT-UHFFFAOYSA-N 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- 238000010521 absorption reaction Methods 0.000 description 2
- 238000001035 drying Methods 0.000 description 2
- 238000001914 filtration Methods 0.000 description 2
- YQEMORVAKMFKLG-UHFFFAOYSA-N glycerine monostearate Natural products CCCCCCCCCCCCCCCCCC(=O)OC(CO)CO YQEMORVAKMFKLG-UHFFFAOYSA-N 0.000 description 2
- SVUQHVRAGMNPLW-UHFFFAOYSA-N glycerol monostearate Natural products CCCCCCCCCCCCCCCCC(=O)OCC(O)CO SVUQHVRAGMNPLW-UHFFFAOYSA-N 0.000 description 2
- 239000004615 ingredient Substances 0.000 description 2
- 238000004898 kneading Methods 0.000 description 2
- 230000001050 lubricating effect Effects 0.000 description 2
- 238000005461 lubrication Methods 0.000 description 2
- 239000000244 polyoxyethylene sorbitan monooleate Substances 0.000 description 2
- 235000010482 polyoxyethylene sorbitan monooleate Nutrition 0.000 description 2
- 229940068968 polysorbate 80 Drugs 0.000 description 2
- 229920000053 polysorbate 80 Polymers 0.000 description 2
- 238000009210 therapy by ultrasound Methods 0.000 description 2
- PQUXFUBNSYCQAL-UHFFFAOYSA-N 1-(2,3-difluorophenyl)ethanone Chemical compound CC(=O)C1=CC=CC(F)=C1F PQUXFUBNSYCQAL-UHFFFAOYSA-N 0.000 description 1
- IIZPXYDJLKNOIY-JXPKJXOSSA-N 1-palmitoyl-2-arachidonoyl-sn-glycero-3-phosphocholine Chemical class CCCCCCCCCCCCCCCC(=O)OC[C@H](COP([O-])(=O)OCC[N+](C)(C)C)OC(=O)CCC\C=C/C\C=C/C\C=C/C\C=C/CCCCC IIZPXYDJLKNOIY-JXPKJXOSSA-N 0.000 description 1
- 229940043268 2,2,4,4,6,8,8-heptamethylnonane Drugs 0.000 description 1
- 208000003556 Dry Eye Syndromes Diseases 0.000 description 1
- 206010013774 Dry eye Diseases 0.000 description 1
- 239000004909 Moisturizer Substances 0.000 description 1
- 229920001214 Polysorbate 60 Polymers 0.000 description 1
- 239000002671 adjuvant Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000017531 blood circulation Effects 0.000 description 1
- 229920001577 copolymer Polymers 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- 230000007794 irritation Effects 0.000 description 1
- KUVMKLCGXIYSNH-UHFFFAOYSA-N isopentadecane Natural products CCCCCCCCCCCCC(C)C KUVMKLCGXIYSNH-UHFFFAOYSA-N 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 230000003340 mental effect Effects 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 230000001333 moisturizer Effects 0.000 description 1
- 235000016709 nutrition Nutrition 0.000 description 1
- 230000035764 nutrition Effects 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 230000019612 pigmentation Effects 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 230000005808 skin problem Effects 0.000 description 1
- 229940047670 sodium acrylate Drugs 0.000 description 1
- 208000024891 symptom Diseases 0.000 description 1
- 210000002435 tendon Anatomy 0.000 description 1
- 238000010998 test method Methods 0.000 description 1
- 230000008719 thickening Effects 0.000 description 1
- 230000000007 visual effect Effects 0.000 description 1
- 239000000230 xanthan gum Substances 0.000 description 1
- 229920001285 xanthan gum Polymers 0.000 description 1
- 229940082509 xanthan gum Drugs 0.000 description 1
- 235000010493 xanthan gum Nutrition 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/04—Dispersions; Emulsions
- A61K8/06—Emulsions
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/29—Titanium; Compounds thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/31—Hydrocarbons
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/342—Alcohols having more than seven atoms in an unbroken chain
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
- A61K8/375—Esters of carboxylic acids the alcohol moiety containing more than one hydroxy group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/4993—Derivatives containing from 2 to 10 oxyalkylene groups
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
- A61K8/8158—Homopolymers or copolymers of amides or imides, e.g. (meth) acrylamide; Compositions of derivatives of such polymers
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/48—Thickener, Thickening system
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/56—Compounds, absorbed onto or entrapped into a solid carrier, e.g. encapsulated perfumes, inclusion compounds, sustained release forms
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
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- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Veterinary Medicine (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Chemical & Material Sciences (AREA)
- Emergency Medicine (AREA)
- Inorganic Chemistry (AREA)
- Dermatology (AREA)
- Dispersion Chemistry (AREA)
- Cosmetics (AREA)
Abstract
The invention discloses a massage cream which is prepared from the following raw materials: propylene glycol, an emulsifier, a lubricant, white oil, an auxiliary agent, a thickening agent, a preservative, essence and deionized water. The massage emulsion has the appearance of emulsion, and when in use, the massage emulsion can be rapidly demulsified, so that the massage emulsion has a good oil production effect; the emulsifier and the thickener jointly form the emulsifying system of the invention, the emulsifier and the thickener have good applicability, the prepared emulsion has very thin, fine and smooth interface film between water and oil, the grain size of oil drops is small, and the emulsion can be spread rapidly after demulsification; the addition of the auxiliary agent can obviously improve the oil production effect, reduce the greasy feeling, obviously reduce the friction force during massage, improve the lubricity, further improve the spreadability and enhance the fitting property between the massage cream and the skin.
Description
Technical Field
The invention relates to the technical field of cosmetics, in particular to massage milk and a preparation method thereof.
Background
With the development of society, the pace of modern life is continuously accelerated, the living competition is fierce day by day, the work and study pressure is higher and higher, and particularly business people, white-collar workers and students often feel tired and faint. As people age, the skin of people is injured to different degrees, such as exposure to severely polluted air, ultraviolet irradiation or eating polluted food and other factors, the skin loses water, pigmentation, dullness, elasticity loss and the like to different degrees, or various problems of high working and living pressure, mental stress, fatigue, weakness and the like can be solved through massage, the massage can relax muscles and tendons and promote blood circulation, muscles are relaxed, and massage products are matched in the massage process, so that the resistance in the massage can be reduced, the nutrition can be supplemented to the skin, and various skin problems can be repaired.
The massage product for cosmetics mainly comprises massage essential oil and massage emulsion, the massage essential oil is most widely applied in the market at present, the massage essential oil can relax tension muscles of eyes and relieve symptoms of dry eyes and painful eyes, but the massage essential oil is high in cost and high in price, has certain irritation and is not suitable for being used in large quantities. Therefore, massage emulsion has entered the visual field of people, but the massage emulsion on the market at present has disadvantages, such as poor oil-yielding effect, and therefore, the problem of providing massage emulsion with good oil-yielding effect is a great challenge to the workers in the field.
Disclosure of Invention
The invention provides massage cream and a preparation method thereof.
The invention adopts the following technical scheme for solving the technical problems:
a massage cream is prepared from the following raw materials in parts by weight: 2 to 5 portions of propylene glycol, 5 to 9 portions of emulsifier, 4 to 10 portions of lubricant, 40 to 55 portions of white oil, 1 to 3 portions of auxiliary agent, 0.2 to 0.6 portion of thickener, 0.2 to 0.6 portion of preservative, 0.03 to 0.08 portion of essence and 30 to 45 portions of deionized water.
As a preferable scheme, the massage milk is prepared from the following raw materials in parts by weight: 3 to 5 portions of propylene glycol, 6 to 9 portions of emulsifier, 5 to 10 portions of lubricant, 45 to 55 portions of white oil, 1 to 2.5 portions of auxiliary agent, 0.2 to 0.5 portion of thickener, 0.3 to 0.6 portion of preservative, 0.04 to 0.08 portion of essence and 30 to 40 portions of deionized water.
As a most preferable scheme, the massage milk is prepared from the following raw materials in parts by weight: 4 parts of propylene glycol, 8 parts of emulsifier, 8 parts of lubricant, 46 parts of white oil, 2 parts of auxiliary agent, 0.35 part of thickening agent, 0.58 part of preservative, 0.05 part of essence and 35 parts of deionized water.
As a preferred scheme, the emulsifier is prepared from cetearyl alcohol, glyceryl monostearate and glycerol according to the weight ratio of 1:1 to 4:2 to 5.
The inventor of the present invention has surprisingly found in a great deal of research that, under the system of the present invention, namely, when white oil and water are used as base materials, cetearyl alcohol, glyceryl monostearate and glycerol are selected as emulsifiers, wherein glyceryl monostearate is a main emulsifier, and cetearyl alcohol and glycerol (which are used as moisturizers in conventional cosmetic formulations and are creatively added into an emulsifying system) are selected as auxiliary emulsifiers to form a main emulsifying system of the present invention, so that the massage emulsion state of the present invention is emulsion state, and the massage emulsion can be rapidly broken when in use, thereby having good oil output effect.
Preferably, the preservative is one or more of methylisothiazolinone, phenoxyethanol, methyl paraben and propyl paraben.
Preferably, the lubricant is polydimethylsiloxane, cyclopentadimethylsiloxane and isopropyl myristate according to a weight ratio of 1:1-3:3-6.
The addition of the lubricant can reduce viscosity and improve lubrication, improve the fluidity and surface tension of an emulsion system and improve the dispersibility of the powdery raw materials.
Preferably, the auxiliary agent is fullerene and dioctyl carbonate, and the weight ratio of the fullerene to the dioctyl carbonate is 1:2-5.
Preferably, the auxiliary agent is modified fullerene and dioctyl carbonate, and the weight ratio of the modified fullerene to the dioctyl carbonate is 1:2-5.
The preparation method of the modified fullerene comprises the following steps:
adding 10 parts of fullerene into 87 parts of absolute ethyl alcohol, carrying out ultrasonic treatment for 25min at 400W to obtain a fullerene suspension, adding 3 parts of titanium dioxide and the fullerene suspension into a kneader, kneading for 15 min, filtering, and drying to obtain the modified fullerene.
The titanium dioxide is loaded on the fullerene, so that the biocompatibility of the modified fullerene can be effectively improved, the biological performance of the fullerene can not be damaged, when the modified fullerene massage emulsion is used, the massage emulsion is demulsified rapidly, the absorption of oil phase components is increased by the modified fullerene, the oil outlet effect can be improved when the modified fullerene massage emulsion is smeared, the greasy feeling is reduced, the friction force during massage can be obviously reduced, the lubricating property is improved, the spreadability is further improved, and the adhesiveness between the massage emulsion and the skin is enhanced.
Preferably, the thickener is SIMULGEL TM EG。
Said SIMULGEL TM EG was purchased from Baihabo Co, guangzhou under the standard inci name sodium acrylate/sodium acryloyldimethyl taurate copolymer (and) isohexadecane (and) polysorbate-80.
SIMULGEL TM EG in the emulsion system of the present invention can improve the stability of the system and is composed of SIMULGEL TM EG also contains polysorbate-80, so that the EG also has certain emulsifying performance under the thickening effect, and the emulsifier jointly form the emulsifying system, so that the oil yielding effect and the spreadability can be improved to a certain extent, and the emulsifying system has very good applicability.
The invention also provides a preparation method of the massage cream, which comprises the following steps:
(1) Adding white oil, a lubricant, an emulsifier and an auxiliary agent into an oil phase pot, heating to 75-90 ℃, and uniformly stirring to obtain an oil phase;
(2) Adding deionized water and propylene glycol into a water phase pot, heating to 75-90 ℃, and uniformly stirring to obtain a water phase;
(3) Pumping the water phase into an emulsifying pot, pumping the oil phase into the emulsifying pot, homogenizing and uniformly dispersing;
(4) Adding a thickening agent, homogenizing, and uniformly dispersing;
(5) Cooling to 35-45 ℃, adding preservative and essence, and stirring uniformly to obtain the massage milk.
The invention has the beneficial effects that: (1) The massage emulsion is in an emulsion state, and when the massage emulsion is used, the massage emulsion is rapidly demulsified, so that the massage emulsion has a good oil production effect; (2) The emulsifier and thickener (SIMULGEL) of the present invention TM EG) together form the emulsifying system of the invention, the two have good applicability, and the prepared emulsion has very thin and fine interface film between water and oilGreasiness and lubrication, small particle size of oil drops, and rapid spreading after demulsification when being smeared; (3) The addition of the auxiliary agent can obviously improve the oil production effect, reduce the greasy feeling, obviously reduce the friction force during massage, improve the lubricity, further improve the spreadability and enhance the bonding property between the massage cream and the skin.
Detailed Description
In order to make the objects, technical solutions and advantages of the embodiments of the present invention clearer, the technical solutions in the embodiments of the present invention will be clearly and completely described below, and it is obvious that the described embodiments are some, but not all embodiments of the present invention. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
In the present invention, the "parts" are parts by weight unless otherwise specified.
Example 1
The massage cream is prepared from the following raw materials in parts by weight: 4 parts of propylene glycol, 8 parts of emulsifier, 8 parts of lubricant, 46 parts of white oil, 2 parts of auxiliary agent, 0.35 part of thickening agent, 0.58 part of preservative, 0.05 part of essence and 35 parts of deionized water.
In this example, the emulsifier is composed of cetostearyl alcohol, glyceryl monostearate, glycerol in a weight ratio of 1:3: 4.
In this embodiment, the preservative is methylisothiazolinone and phenoxyethanol in a weight ratio of 4: 25.
In this example, the lubricant is dimethicone, cyclopentadimethicone, isopropyl myristate in a weight ratio of 1:2: 5.
In this embodiment, the additive is fullerene, dioctyl carbonate, in a weight ratio of 1: 4.
In this embodiment, the thickener is SIMULGEL TM EG。
The preparation method of the massage milk comprises the following steps:
(1) Adding white oil, lubricant, emulsifier and auxiliary agent into an oil phase pot, heating to 85 ℃, and uniformly stirring to obtain an oil phase;
(2) Adding deionized water and propylene glycol into a water phase pot, heating to 85 ℃, and uniformly stirring to obtain a water phase;
(3) Pumping the water phase into an emulsifying pot, pumping the oil phase into the emulsifying pot, homogenizing and uniformly dispersing;
(4) Adding a thickening agent, homogenizing, and uniformly dispersing;
(5) Cooling to 40 deg.C, adding antiseptic and essence, and stirring to obtain massage cream.
Example 2
The massage cream is prepared from the following raw materials in parts by weight: 4 parts of propylene glycol, 8 parts of emulsifier, 8 parts of lubricant, 46 parts of white oil, 2 parts of auxiliary agent, 0.35 part of thickening agent, 0.58 part of preservative, 0.05 part of essence and 35 parts of deionized water.
In this example, the emulsifier is composed of cetostearyl alcohol, glyceryl monostearate, glycerol in a weight ratio of 1:3: 4.
In this embodiment, the preservative is methylisothiazolinone and phenoxyethanol in a weight ratio of 4: 25.
In this example, the lubricant is dimethicone, cyclopentadimethicone, isopropyl myristate in a weight ratio of 1:2:5, the components are mixed.
In this embodiment, the additive is a modified fullerene, dioctyl carbonate, in a weight ratio of 1: 4.
In this embodiment, the preparation method of the modified fullerene comprises:
adding 10 parts of fullerene into 87 parts of absolute ethyl alcohol, carrying out ultrasonic treatment for 25min by 400W to obtain fullerene suspension, adding 3 parts of titanium dioxide and the fullerene suspension into a kneader, kneading for 15 min, filtering, and drying to obtain the modified fullerene.
The titanium dioxide is loaded on the fullerene, so that the biocompatibility of the modified fullerene can be effectively improved, the biological performance of the fullerene can not be damaged, when the modified fullerene massage emulsion is used, the massage emulsion is demulsified rapidly, the absorption of oil phase components is increased by the modified fullerene, the oil outlet effect can be improved when the modified fullerene massage emulsion is smeared, the greasy feeling is reduced, the friction force during massage can be obviously reduced, the lubricating property is improved, the spreadability is further improved, and the adhesiveness between the massage emulsion and the skin is enhanced.
In this embodiment, the thickener is simulgel.
The preparation method of the massage milk comprises the following steps:
(1) Adding white oil, lubricant, emulsifier and auxiliary agent into an oil phase pot, heating to 85 ℃, and uniformly stirring to obtain an oil phase;
(2) Adding deionized water and propylene glycol into a water phase pot, heating to 85 ℃, and uniformly stirring to obtain a water phase;
(3) Pumping the water phase into an emulsifying pot, pumping the oil phase into the emulsifying pot, homogenizing and uniformly dispersing;
(4) Adding a thickening agent, homogenizing, and uniformly dispersing;
(5) Cooling to 40 deg.C, adding antiseptic and essence, and stirring to obtain massage cream.
Example 3
The massage cream is prepared from the following raw materials in parts by weight: 2 parts of propylene glycol, 5 parts of emulsifier, 4 parts of lubricant, 40 parts of white oil, 1 part of auxiliary agent, 0.2 part of thickening agent, 0.2 part of preservative, 0.03 part of essence and 30 parts of deionized water.
In this example, the emulsifier is composed of cetostearyl alcohol, glyceryl monostearate, glycerol in a weight ratio of 1:3: 4.
In this embodiment, the preservative is methylisothiazolinone and phenoxyethanol in a weight ratio of 4: 25.
In this example, the lubricant is dimethicone, cyclopentadimethicone, isopropyl myristate in a weight ratio of 1:2: 5.
In this embodiment, the assistant is fullerene, dioctyl carbonate in a weight ratio of 1: 4.
In this embodiment, the thickener is SIMULGEL TM EG。
The preparation method of the massage milk comprises the following steps:
(1) Adding white oil, lubricant, emulsifier and auxiliary agent into an oil phase pot, heating to 85 ℃, and uniformly stirring to obtain an oil phase;
(2) Adding deionized water and propylene glycol into a water phase pot, heating to 85 ℃, and uniformly stirring to obtain a water phase;
(3) Pumping the water phase into an emulsifying pot, pumping the oil phase into the emulsifying pot, homogenizing and uniformly dispersing;
(4) Adding a thickening agent, homogenizing, and uniformly dispersing;
(5) Cooling to 40 deg.C, adding antiseptic and essence, and stirring to obtain massage cream.
Example 4
The massage cream is prepared from the following raw materials in parts by weight: 5 parts of propylene glycol, 9 parts of emulsifier, 10 parts of lubricant, 55 parts of white oil, 2.2 parts of auxiliary agent, 0.6 part of thickening agent, 0.6 part of preservative, 0.08 part of essence and 45 parts of deionized water.
In this example, the emulsifier is composed of cetostearyl alcohol, glyceryl monostearate, glycerol in a weight ratio of 1:3: 4.
In this embodiment, the preservative is methylisothiazolinone and phenoxyethanol in a weight ratio of 4: 25.
In this example, the lubricant is dimethicone, cyclopentadimethicone, isopropyl myristate in a weight ratio of 1:2: 5.
In this embodiment, the additive is fullerene, dioctyl carbonate, in a weight ratio of 1: 4.
In this embodiment, the thickener is SIMULGEL TM EG。
The preparation method of the massage milk comprises the following steps:
(1) Adding white oil, lubricant, emulsifier and auxiliary agent into an oil phase pot, heating to 85 ℃, and uniformly stirring to obtain an oil phase;
(2) Adding deionized water and propylene glycol into a water phase pot, heating to 85 ℃, and uniformly stirring to obtain a water phase;
(3) Pumping the water phase into an emulsifying pot, pumping the oil phase into the emulsifying pot, homogenizing and uniformly dispersing;
(4) Adding a thickening agent, homogenizing, and uniformly dispersing;
(5) Cooling to 40 deg.C, adding antiseptic and essence, and stirring to obtain massage milk.
Example 5
The massage cream is prepared from the following raw materials in parts by weight: 5 parts of propylene glycol, 9 parts of emulsifier, 10 parts of lubricant, 55 parts of white oil, 2.2 parts of auxiliary agent, 0.6 part of thickening agent, 0.6 part of preservative, 0.08 part of essence and 45 parts of deionized water.
In this example, the emulsifier is composed of cetostearyl alcohol, glyceryl monostearate, glycerol in a weight ratio of 1:3: 4.
In this embodiment, the preservative is methylisothiazolinone and phenoxyethanol in a weight ratio of 4: 25.
In this example, the lubricant is dimethicone, cyclopentadimethicone, isopropyl myristate in a weight ratio of 1:2: 5.
In this embodiment, the additive is fullerene, dioctyl carbonate, in a weight ratio of 1: 4.
In this example, the thickener is xanthan gum.
The preparation method of the massage milk comprises the following steps:
(1) Adding white oil, lubricant, emulsifier and auxiliary agent into an oil phase pot, heating to 85 ℃, and uniformly stirring to obtain an oil phase;
(2) Adding deionized water and propylene glycol into a water phase pot, heating to 85 ℃, and uniformly stirring to obtain a water phase;
(3) Pumping the water phase into an emulsifying pot, pumping the oil phase into the emulsifying pot, homogenizing and uniformly dispersing;
(4) Adding a thickening agent, homogenizing, and uniformly dispersing;
(5) Cooling to 40 deg.C, adding antiseptic and essence, and stirring to obtain massage cream.
Comparative example 1
Comparative example 1 differs from example 1 in that comparative example 1 does not contain the described auxiliary agent, the other things being equal.
Comparative example 2
Comparative example 2 differs from example 1 in that the additive described in comparative example 2 is a single fullerene, and the rest is the same.
Comparative example 3
Comparative example 3 differs from example 1 in that comparative example 3 describes the adjuvant as dioctyl carbonate alone, all other things being equal.
Comparative example 4
Comparative example 4 differs from example 1 in that the emulsifier of comparative example 4 is glycerol monostearate, glycerol, in a weight ratio of 4: 4.
Comparative example 5
Comparative example 5 differs from example 1 in that the emulsifier described in comparative example 5 is prepared from cetostearyl alcohol, glycerol monostearate in a weight ratio of 1:3, and (3).
Comparative example 6
Comparative example 6 differs from example 1 in that the emulsifier described in comparative example 6 is hydrogenated lecithin, tween 60, glycerol, in a weight ratio of 1:3: 4.
To further demonstrate the effect of the present invention, the following test methods were provided:
1. 30 volunteers (20-25 years old), 20 women and 10 men, were selected for the test.
2. Volunteers pick up 0.2g +/-0.1 g of the massage cream described in examples 1-5 and comparative examples 1-6 with hands, smear the massage cream on the back of the hand clockwise uniformly, record the number of the smeared circles, observe the oil condition and make a record, and judge the following: the oil yield is very obvious: the number of coating turns is 0-5 circles, and a relatively obvious oil outlet effect is observed; obvious oil production: the number of coating turns is 5-10, and a relatively obvious oil production effect is observed; the oil yielding is general: the number of coating turns is 10-15, and the oil outlet effect can be observed; the oil is not obvious: the number of coating turns is more than 15 turns, no oil-out effect can be observed, and the test results are shown in table 1.
TABLE 1 oil-out effect
As can be seen from Table 1, the massage emulsion of the invention has good oil production effect, can be used for demulsifying quickly and has good oil production effect.
It is understood from comparative examples 1 and 2 that the modified fullerene can further improve the oil-yielding effect as compared with fullerene.
It can be seen from comparison of examples 1, 3 and 4 that different proportions of massage cream can affect the oil-yielding effect, wherein example 1 is the best proportion.
Comparative examples 1 and 5 show that the thickener (SIMULGEL) TM EG) can improve oil production.
Comparing example 1 with comparative examples 1 to 3, it can be seen that the assistant of the present invention can significantly improve the oil-yielding effect.
It can be seen from the comparison of example 1 with comparative examples 4 to 6 that the emulsifier of the present invention can significantly improve the oil-yielding effect, and the oil-yielding effect is significantly reduced when the emulsifier of the present invention is partially replaced or the ingredients are not three combinations.
3. The volunteers respectively dip 0.2g +/-0.1 g of the massage milk described in examples 1-5 and comparative examples 1-6 with hands, and apply the massage milk on the back of the hand clockwise, and evaluate the spreading feeling of application, and the spreading is easy to spread: the sample development time is less than 2s; the deployment is general: the sample unfolding time is 2-5 s; difficult expansion: the sample development time was greater than 5s and the smear spread test results are shown in table 2.
TABLE 2 test results
As can be seen from Table 2, the massage cream of the invention has good spreadability and is easy to spread.
It is understood from comparative examples 1 and 2 that the modified fullerene can further improve spreadability as compared with fullerene.
It can be seen from comparison of examples 1, 3 and 4 that different ratios of massage milks can affect spreadability, with example 1 being the best ratio.
Comparative examples 1 and 5 show that the thickener (SIMULGEL) TM EG) does not substantially affect spreadability.
Comparing example 1 with comparative examples 1 to 3, it can be seen that the spreading property of the auxiliary of the present invention can be significantly improved.
It can be seen from comparison of example 1 with comparative examples 4 to 6 that the emulsifier of the present invention can significantly improve spreadability, and when the emulsifier of the present invention is partially replaced or the ingredients are not combined in three, the spreadability is significantly reduced.
In light of the foregoing description of preferred embodiments according to the invention, it is clear that many changes and modifications can be made by the person skilled in the art without departing from the scope of the invention. The technical scope of the present invention is not limited to the contents of the specification, and must be determined according to the scope of the claims.
Claims (5)
1. The massage milk is characterized by being prepared from the following raw materials in parts by weight: 2 to 5 portions of propylene glycol, 5 to 9 portions of emulsifier, 4 to 10 portions of lubricant, 40 to 55 portions of white oil, 1 to 3 portions of auxiliary agent, 0.2 to 0.6 portion of thickener, 0.2 to 0.6 portion of preservative, 0.03 to 0.08 portion of essence and 30 to 45 portions of deionized water;
the emulsifier is prepared from cetearyl alcohol, glyceryl monostearate and glycerol according to the weight ratio of 1:1 to 4: 2-5;
the lubricant consists of polydimethylsiloxane, cyclopentadimethylsiloxane and isopropyl myristate according to the weight ratio of 1:1-3:3-6;
the auxiliary agent consists of fullerene and dioctyl carbonate according to the weight ratio of 1:2-5;
the thickener is SIMULGEL TM EG。
2. The massage cream according to claim 1, wherein the massage cream is prepared from the following raw materials in parts by weight: 3 to 5 portions of propylene glycol, 6 to 9 portions of emulsifier, 5 to 10 portions of lubricant, 45 to 55 portions of white oil, 1 to 2.5 portions of auxiliary agent, 0.2 to 0.5 portion of thickener, 0.3 to 0.6 portion of preservative, 0.04 to 0.08 portion of essence and 30 to 40 portions of deionized water.
3. The massage cream according to claim 1, wherein the massage cream is prepared from the following raw materials in parts by weight: 4 parts of propylene glycol, 8 parts of emulsifier, 8 parts of lubricant, 46 parts of white oil, 2 parts of auxiliary agent, 0.35 part of thickening agent, 0.58 part of preservative, 0.05 part of essence and 35 parts of deionized water.
4. The massage milk of claim 1, wherein the preservative is one or more of methylisothiazolinone, phenoxyethanol, methylparaben, propylparaben.
5. A method for preparing massage milk according to any one of claims 1 to 4, comprising the steps of:
(1) Adding white oil, a lubricant, an emulsifier and an auxiliary agent into an oil phase pot, heating to 75-90 ℃, and uniformly stirring to obtain an oil phase;
(2) Adding deionized water and propylene glycol into a water phase pot, heating to 75-90 ℃, and uniformly stirring to obtain a water phase;
(3) Pumping the water phase into an emulsifying pot, pumping the oil phase into the emulsifying pot, homogenizing and uniformly dispersing;
(4) Adding a thickening agent, homogenizing, and uniformly dispersing;
(5) Cooling to 35-45 ℃, adding the preservative and the essence, and uniformly stirring to obtain the massage emulsion.
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| JP3641697B2 (en) * | 1997-08-07 | 2005-04-27 | 株式会社ノエビア | External preparation for skin massage and cleaning |
| JP5107560B2 (en) * | 2006-11-22 | 2012-12-26 | 日本精化株式会社 | Cyclohexanedicarboxylic acid diester and cosmetic or skin external preparation containing the same |
| CN101647760B (en) * | 2009-07-24 | 2012-04-25 | 广州市白云联佳精细化工厂 | Massage emulsion |
| JP2012077044A (en) * | 2010-10-05 | 2012-04-19 | Ezaki Glico Co Ltd | Skin care preparation |
| CN105496866A (en) * | 2015-12-22 | 2016-04-20 | 广州潮徽化工科技有限公司 | Massage emulsion oil containing plant extraction ingredients and preparation method of massage emulsion oil |
| CN105963156B (en) * | 2016-06-23 | 2019-03-05 | 虞琼斐 | Pregnant line massage lotion and preparation method thereof |
| CN106389162A (en) * | 2016-09-29 | 2017-02-15 | 广州暨南生物医药研究开发基地有限公司 | Massage oil emulsion containing argy wormwood leaf essential oil and preparation method of massage oil emulsion |
| CN111821222A (en) * | 2020-07-17 | 2020-10-27 | 茂名市瑜丰沉香创意产业有限公司 | Agilawood massage oil and preparation method thereof |
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| AU2009222500A1 (en) * | 2009-10-01 | 2011-04-21 | Manoj Jain | A green emulsifying system for cosmetic and/or pharmaceutical emulsion composition |
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Denomination of invention: A massage milk and its preparation method Effective date of registration: 20230609 Granted publication date: 20230411 Pledgee: Guangdong Fogang Rural Commercial Bank Co.,Ltd. Pledgor: GUANGZHOU BAIFEI COSMETICS Co.,Ltd. Registration number: Y2023980043381 |
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