CN111743189A

CN111743189A - Preparation method of herbal plant solid spice for cigarettes

Info

Publication number: CN111743189A
Application number: CN202010582789.1A
Authority: CN
Inventors: 王启宇; 贾发聚
Original assignee: Xianglong Biotechnology Co ltd
Current assignee: Xianglong Biotechnology Co ltd
Priority date: 2020-06-23
Filing date: 2020-06-23
Publication date: 2020-10-09

Abstract

The invention relates to the technical field of solid spices for cigarettes, in particular to a preparation method of a herbal plant solid spice for cigarettes, which comprises the following steps: (1) mixing: weighing raw materials including fructus momordicae, lotus plumule, rose, mint and tobacco powder, crushing the lotus plumule, the rose and the mint, and uniformly mixing the crushed lotus plumule, rose and mint with the tobacco powder to obtain a mixture; (2) soaking: respectively adding water and ethanol into the mixture to soak the mixture to obtain mixed solution; (3) enzymolysis: pouring the mixed solution into an enzymolysis device with a stirring device, and adding cellulase for enzymolysis to obtain an enzymolysis solution; (4) extraction: adding the enzymatic hydrolysate into an extraction container, and heating with water bath to obtain extractive solution and insoluble substance. (5) Concentrating and forming: the extracting solution is put in an evaporator for reduced pressure concentration to obtain a concentrate, and the concentrate and insoluble substances are uniformly mixed to obtain the herbal plant solid spice for the cigarettes.

Description

Preparation method of herbal plant solid spice for cigarettes

Technical Field

The invention relates to the technical field of solid spices for cigarettes, in particular to a preparation method of a herbal plant solid spice for cigarettes.

Background

With the continuous improvement of living standard and the continuous improvement of the requirements on living quality of people, the living goods are expected to reach the maximum use value for human bodies and environment, have no toxicity and harm, return to nature, pursue harmonious development in all aspects and use of essence and spice. At this time, the traditional Chinese medicine enters the sight of people, Chinese herbal medicines have three thousand years of history of application and practice, 11164 kinds of medicinal plants are proved to be effective clinically, and the Chinese herbal medicine has a complete Chinese medicine theory basis and a complete medical system. There are many herbs in the world: indian herbs, European herbs, south American herbs, Indian herbs, Thailand herbs, Chinese herbs (Miao ethnic group, Tibetan herbs as well) are unique and none of the herbs are comparable with respect to their application history, variety, theoretical system, etc. The Chinese herbal medicine system with profound bouquet and rich resources is an important direction for the research and development of essences and spices. Under the advance of the function of adding Chinese herbal medicines, the technical problem of always researching and solving how to make up the loss of the tobacco fragrance and improve the quality of the tobacco fragrance is needed.

Through search, the Chinese patent with the patent number CN108936792A discloses a preparation method of a herbal plant solid spice for cigarettes, which comprises the following steps: (1) leaching the herbal spice plants with water, and separating leaching liquor and insoluble substances; (2) preparing the insoluble substance obtained in the step (1) into a substrate; (3) dipping and coating the leaching liquor obtained in the step (1) on the substrate obtained in the step (2) after low-temperature vacuum concentration, wherein the following defects are mostly existed in the use process: the preparation method in the prior art solves the problem of how to prepare the herbal plant solid spice for cigarettes by a pulping method, and does not achieve the effects of clearing away the heart fire, soothing the nerves and relieving throat discomfort.

Disclosure of Invention

The invention aims to provide a preparation method of a herbal plant solid spice for cigarettes, so as to solve the problems in the background technology.

In order to achieve the purpose, the invention provides the following technical scheme:

a preparation method of a herbal plant solid spice for cigarettes comprises the following steps:

(1) mixing: weighing raw materials including fructus momordicae, lotus plumule, rose, mint and tobacco powder, crushing the lotus plumule, the rose and the mint, sieving the crushed lotus plumule, the rose and the mint by a 20-30-mesh sieve, and uniformly mixing the crushed lotus plumule, the rose and the mint with the tobacco powder to obtain a mixture;

(2) soaking: respectively adding water and ethanol into the mixture obtained in the step (1), and soaking for 8-20H to obtain a mixed solution;

(3) enzymolysis: pouring the mixed solution obtained in the step (2) into an enzymolysis device with a stirring device, adding cellulase accounting for 0.1-0.3% of the mixed solution by mass, and carrying out enzymolysis for 6-10H to obtain an enzymolysis solution;

(4) extraction: adding the enzymolysis liquid obtained in the step (3) into an extraction container, heating by using a water bath, and performing reflux extraction on the enzymolysis liquid for 2-4H in a boiling state to obtain an extracting solution and insoluble substances;

(5) concentrating and forming: and (4) putting the extracting solution obtained in the step (4) into an evaporator for reduced pressure concentration, wherein the operating pressure at room temperature is 0.08-0.105Mpa to obtain a concentrate, and uniformly mixing the concentrate and insoluble substances to obtain the herbal plant solid spice for the cigarettes.

As a further scheme of the invention: weighing the raw materials in the step (1) in parts by weight as follows: 3-7 parts of momordica grosvenori, 2-5 parts of lotus plumule, 7-11 parts of rose, 4-9 parts of mint and 1-3 parts of tobacco powder.

As a further scheme of the invention: the water and the ethanol in the step (2) are respectively in parts by weight: 4-6 parts of water and 1-3 parts of ethanol.

As a further scheme of the invention: the enzymolysis temperature in the step (3) is 55-75 ℃.

As a further scheme of the invention: the stirring speed of the enzymatic hydrolysis device is 50-60 revolutions per minute.

As a further scheme of the invention: the temperature of the water bath in the step (4) is 95-100 ℃.

As a further scheme of the invention: the evaporator in the step (5) is a rotary evaporator.

As a still further scheme of the invention: the mass ratio of the concentrate to the insoluble matter is 1:5-1: 7.

The efficacy of the herbal plant solid spice for the cigarette is as follows:

momordica grosvenori: belongs to the cucurbitaceae family, and is called as good medicine and good fruit. The fruits contain abundant glucose, fructose, various vitamins and the like, have wide application, are sold in domestic and foreign markets, are cool in nature and sweet in taste. Enters lung and large intestine channels, clears heat and moistens lung, relieves cough, relieves sore throat, and smoothes intestine and relieves constipation. Can be used for treating cough due to lung fire dryness, pharyngalgia, aphonia, and constipation due to intestinal dryness.

Lotus plumule: the lotus plumule is green plumule in the kernel of the mature lotus seed, is frequently drunk in folk by tea making, has the effects of clearing heart fire, calming liver fire, purging spleen fire and reducing lung fire, can reduce fat, clear heat, tranquilize mind and strengthen heart, is most suitable for insomnia patients with heart-kidney disharmony and yin deficiency and fire excess, is bitter in taste and cold in nature, and can also be used for treating dysphoria, obnubilation, nocturnal emission and spermatorrhea and other symptoms caused by high fever. Lian Xin contains alkaloid and can also reduce blood pressure.

And (3) rose: the rose contains more than 300 chemical components, such as aromatic alcohol, aldehyde, fatty acid, phenol and oil and fat containing essence, and the rose product is usually eaten to soften liver and wake stomach, relax qi and activate blood, maintain beauty and keep young and refresh people.

Mint: also called as Yindan, is a labiate plant and is one of the common Chinese traditional medicines. It is a pungent and cool sweating and antipyretic medicine, and can be used for treating influenza, headache, conjunctival congestion, fever, sore throat, and gum swelling, and clearing lung-heat and moistening lung. The external application can be used for treating neuralgia, skin pruritus, rash, eczema and the like, can be used as spice, also has the effects of antisepsis and sterilization, diuresis, phlegm reduction, stomach strengthening, digestion promotion and the like, and the insomnia can be caused by eating a large amount of mint, but the sleep is facilitated by eating a small dose of mint.

Compared with the prior art, the invention has the beneficial effects that: the preparation method is simple, the steps are easy to operate, the momordica grosvenori, the lotus plumule, the rose and the mint are reasonably matched with the tobacco, so that the aroma components of the rose and the mint and the original aroma of the tobacco can be mutually coordinated, the aroma quality, the aroma quantity and the harmony of the tobacco product are improved, meanwhile, the momordica grosvenori and the lotus plumule are matched in a matching mode, the effects of clearing away heart fire and soothing the nerves and relieving throat discomfort can be achieved, the strength and the stimulation of the tobacco product are reduced, and the quality of the tobacco product is improved.

Detailed Description

The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.

The present invention will be described in detail with reference to examples.

Example one

(1) mixing: weighing raw materials including fructus momordicae, lotus plumule, rose, mint and tobacco powder, crushing the lotus plumule, the rose and the mint, sieving the crushed lotus plumule, the rose and the mint with a 20-mesh sieve, and uniformly mixing the crushed lotus plumule, the rose and the mint with the tobacco powder to obtain a mixture, wherein the raw materials are weighed according to the following parts by weight: 3 parts of momordica grosvenori, 2 parts of lotus plumule, 7 parts of rose, 4 parts of mint and 1 part of tobacco powder;

(2) soaking: respectively adding water and ethanol into the mixture obtained in the step (1), and soaking for 8H to obtain a mixed solution, wherein the water and the ethanol are respectively in parts by weight: 4 parts of water and 1 part of ethanol;

(3) enzymolysis: pouring the mixed solution obtained in the step (2) into an enzymatic hydrolysis device with a stirring device, adding cellulase accounting for 0.1% of the mixed solution by mass, and carrying out enzymatic hydrolysis for 6H to obtain an enzymatic hydrolysis solution, wherein the enzymatic hydrolysis temperature is 55 ℃, and the stirring speed of the enzymatic hydrolysis device is 50 r/min;

(4) extraction: adding the enzymolysis liquid obtained in the step (3) into an extraction container, heating the enzymolysis liquid by using a water bath, and performing reflux extraction on the enzymolysis liquid for 2H in a boiling state to obtain an extracting solution and insoluble substances, wherein the temperature of the water bath is 95 ℃;

(5) concentrating and forming: and (3) putting the extracting solution obtained in the step (4) into an evaporator for reduced pressure concentration, wherein the operating pressure at room temperature is 0.08Mpa, so as to obtain a concentrate, and uniformly mixing the concentrate and the insoluble substances, so as to obtain the herbal plant solid spice for the cigarettes, wherein the evaporator is a rotary evaporator, and the mass ratio of the mixture of the concentrate and the insoluble substances is 1: 5.

Example two

(1) mixing: weighing raw materials including fructus momordicae, lotus plumule, rose, mint and tobacco powder, crushing the lotus plumule, the rose and the mint, sieving the crushed lotus plumule, rose and mint with a 30-mesh sieve, and uniformly mixing the crushed lotus plumule, rose and mint with the tobacco powder to obtain a mixture, wherein the raw materials are weighed according to the following parts by weight: 7 parts of momordica grosvenori, 5 parts of lotus plumule, 11 parts of rose, 9 parts of mint and 3 parts of tobacco powder;

(2) soaking: respectively adding water and ethanol into the mixture obtained in the step (1), and soaking for 20H to obtain a mixed solution, wherein the water and the ethanol are respectively in parts by weight: 6 parts of water and 3 parts of ethanol;

(3) enzymolysis: pouring the mixed solution obtained in the step (2) into an enzymatic hydrolysis device with a stirring device, adding cellulase accounting for 0.3% of the mixed solution by mass, and carrying out enzymatic hydrolysis for 10H to obtain an enzymatic hydrolysis solution, wherein the enzymatic hydrolysis temperature is 75 ℃, and the stirring speed of the enzymatic hydrolysis device is 60 r/min;

(4) extraction: adding the enzymolysis liquid obtained in the step (3) into an extraction container, heating the enzymolysis liquid by using a water bath, and performing reflux extraction on the enzymolysis liquid for 4H in a boiling state to obtain an extracting solution and insoluble substances, wherein the temperature of the water bath is 100 ℃;

(5) concentrating and forming: and (3) putting the extracting solution obtained in the step (4) into an evaporator for reduced pressure concentration, wherein the operating pressure at room temperature is 0.105Mpa, so as to obtain a concentrate, and uniformly mixing the concentrate and the insoluble substances, so as to obtain the herbal plant solid spice for the cigarettes, wherein the evaporator is a rotary evaporator, and the mass ratio of the mixture of the concentrate and the insoluble substances is 1: 7.

EXAMPLE III

(1) mixing: weighing raw materials including fructus momordicae, lotus plumule, rose, mint and tobacco powder, crushing the lotus plumule, the rose and the mint, sieving the crushed lotus plumule, the rose and the mint with a 20-30-mesh sieve, and uniformly mixing the crushed lotus plumule, the rose and the tobacco powder to obtain a mixture, wherein the raw materials are weighed according to the following parts by weight: 5 parts of momordica grosvenori, 4 parts of lotus plumule, 9 parts of rose, 7 parts of mint and 2 parts of tobacco powder;

(2) soaking: respectively adding water and ethanol into the mixture obtained in the step (1), and soaking for 12H to obtain a mixed solution, wherein the water and the ethanol are respectively in parts by weight: 5 parts of water and 2 parts of ethanol;

(3) enzymolysis: pouring the mixed solution obtained in the step (2) into an enzymatic hydrolysis device with a stirring device, adding cellulase accounting for 0.2% of the mixed solution by mass, and carrying out enzymatic hydrolysis for 8H to obtain an enzymatic hydrolysis solution, wherein the enzymatic hydrolysis temperature is 65 ℃, and the stirring speed of the enzymatic hydrolysis device is 55 revolutions per minute;

(4) extraction: adding the enzymolysis liquid obtained in the step (3) into an extraction container, heating the enzymolysis liquid by using a water bath, and performing reflux extraction on the enzymolysis liquid for 3H in a boiling state to obtain an extracting solution and insoluble substances, wherein the temperature of the water bath is 98 ℃;

(5) concentrating and forming: and (3) putting the extracting solution obtained in the step (4) into an evaporator for reduced pressure concentration, wherein the operating pressure at room temperature is 0.095Mpa, so as to obtain a concentrate, and uniformly mixing the concentrate and the insoluble substances, so as to obtain the herbal plant solid spice for the cigarettes, wherein the evaporator is a rotary evaporator, and the mass ratio of the mixture of the concentrate and the insoluble substances is 1: 6.

Comparative example 1

Except that the fructus momordicae, the lotus plumule, the rose and the mint are not contained, the other formulas and the preparation process are the same as the third embodiment.

The method comprises the steps of naming a cigarette manufactured according to the first embodiment as a No. 1 cigarette, naming a cigarette manufactured according to the second embodiment as a No. 2 cigarette, naming a cigarette manufactured according to the third embodiment as a No. 3 cigarette, naming a cigarette manufactured according to the first comparative example as a No. 4 cigarette, respectively rolling control cigarettes on the same production line, and evaluating by an evaluation expert group according to the sensory quality technical requirements of 3.1.2 mixed type cigarettes of GB 5606.4-1996 cigarette sensory technical requirements when the relative change of the quality of a sample is not more than 0.2% within 3h according to the requirements of GB/T16447-2004 tobacco and the regulated and tested atmospheric environment of tobacco products under the conditions of temperature (22 +/-1) DEG C and relative humidity (60 +/-5)%. The evaluation criteria are shown in table 1, 100 smokers are randomly selected, the specific senses are scored, the average value is taken, and the specific sense score is shown in table 2.

TABLE 1

Gloss of

Fragrance

Tuning by hand

Miscellaneous qi

Irritation property

Aftertaste

A（75-100）

Glossy and oily

Strong, fine and plump fragrance

Tuning by hand

Without miscellaneous gas

Has no irritation

Clean and comfortable

B（50-75）

The luster is more oily

Rich fragrance and slightly coarse

Relatively harmonious

Slight miscellaneous qi

Slight irritation

Cleaner and more comfortable

C（30-50）

Glossy and oily

The fragrance is thin and coarse

Shang harmony

Slight miscellaneous qi

Slight stimulation

Clear and comfortable

TABLE 2

As can be seen from the sensory scores in Table 2, the score of the No. 4 cigarette prepared according to the preparation method of the comparative example is the lowest and is respectively lower than the scores of the No. 1 cigarette, the No. 2 cigarette and the No. 3 cigarette prepared according to the preparation methods of the example I, the example II and the example III, so that the herbal plant solid spice for the cigarettes can remarkably improve the cigarette fragrance, harmonize the smoke, increase the sweet feeling of the smoke, reduce the irritation of the cigarette smoke and improve the comfort of the throat of a user when being added into the cigarettes, can increase the fullness and the fineness of the cigarette fragrance, and has better cigarette application effect.

Claims

1. A preparation method of a herbal plant solid spice for cigarettes is characterized by comprising the following steps:

(5) concentrating and forming: and (4) putting the extracting solution obtained in the step (4) into an evaporator for reduced pressure concentration, wherein the operating pressure at room temperature is 0.08-0.105Mpa to obtain a concentrate, and uniformly mixing the concentrate and insoluble substances to obtain the herbaceous plant solid spice for cigarettes.

2. The preparation method of the herbal plant solid spice for the cigarettes according to claim 1, wherein the raw materials in the step (1) are weighed according to the following parts by weight: 3-7 parts of momordica grosvenori, 2-5 parts of lotus plumule, 7-11 parts of rose, 4-9 parts of mint and 1-3 parts of tobacco powder.

3. The preparation method of the herbaceous plant solid spice for the cigarette as claimed in claim 1, wherein the water and the ethanol in the step (2) are respectively in parts by weight: 4-6 parts of water and 1-3 parts of ethanol.

4. The preparation method of the herbal plant solid spice for the cigarette as claimed in claim 1, wherein the enzymolysis temperature in the step (3) is 55-75 ℃.

5. The method for preparing the herbaceous plant solid spice for the cigarette as claimed in claim 4, wherein the stirring speed of the enzymatic hydrolysis device is 50-60 rpm.

6. The method for preparing the herbaceous plant solid spice for the cigarette as claimed in claim 1, wherein the water bath temperature in the step (4) is 95-100 ℃.

7. The method for preparing the herbaceous plant solid spice for the cigarette as claimed in claim 1, wherein the evaporator in the step (5) is a rotary evaporator.

8. The preparation method of the herbaceous plant solid spice for the cigarette as claimed in claim 7, wherein the mass ratio of the mixture of the concentrate and the insoluble substances is 1:5-1: 7.