CN110205200B

CN110205200B - Myrtle-flavored essence and myrtle-flavored electronic cigarette liquid and preparation method thereof

Info

Publication number: CN110205200B
Application number: CN201910484783.8A
Authority: CN
Inventors: 赵旭; 温志勇; 温育青
Original assignee: Guangdong Shennong Yanke Technology Co ltd
Current assignee: Guangdong Shennong Yanke Technology Co ltd
Priority date: 2019-05-31
Filing date: 2019-05-31
Publication date: 2023-01-06
Anticipated expiration: 2039-05-31
Also published as: CN110205200A

Abstract

The invention relates to the technical field of electronic cigarettes, in particular to a myrtle-flavored essence and myrtle-flavored electronic cigarette liquid and a preparation method thereof. The essence with vivid myrtle fragrance is obtained by a fragrance blending technology and scientific proportioning, and the essence is rich, pleasant and full in fragrance. The prepared electronic cigarette liquid has a special myrtle aroma style, is comfortable in taste and pleasant in aroma, and has good experience and satisfaction. Meanwhile, the myrtle essence disclosed by the invention can also be applied to smoking products which are not combusted when being heated, and are blown to be beaded by cigarettes.

Description

Myrtle-flavored essence and myrtle-flavored electronic cigarette liquid and preparation method thereof

Technical Field

The invention relates to the technical field of electronic cigarettes, in particular to myrtle-flavor essence, myrtle-flavor electronic cigarette liquid and a preparation method thereof.

Background

The electronic cigarette controls the output quantity and the working state of smoke through a high-tech silicon chip and an airflow inductor, so that tobacco tar is atomized, smoke liquid containing extracts, essence, nicotine and smoke agent is atomized into particles, the particles are absorbed through the lung, simulated smoke is discharged at the same time, however, the electronic cigarette does not contain tar and other harmful ingredients in the cigarette, cannot generate second-hand smoke, and cannot be diffused or awkwardly in a closed space. Electronic cigarettes, as a form of new tobacco products, on the one hand provide consumption habits and satisfaction similar to traditional cigarettes, and on the other hand the hazard index of electronic cigarettes is greatly reduced compared to traditional cigarettes. Therefore, electronic cigarettes present a huge market prospect.

The myrtle is an evergreen shrub, and has a plurality of wild species in Guangdong and Minshan, and opposite leaves. Myrtle essential oil is generally extracted from the leaves of myrtle, and has a pungent and pleasant aroma and a pungent taste, which are very specific. The myrtle essential oil is added into the electronic cigarette liquid to obtain the electronic cigarette liquid with special taste, so that the taste of the electronic cigarette liquid can be enriched, and the electronic cigarette liquid product is enriched. However, the content of natural myrtle essential oil is low, the extraction process is complex, and the large-scale industrial application is limited.

Disclosure of Invention

The invention provides a myrtle-flavored essence, an electronic cigarette liquid with vivid myrtle fragrance and a preparation method thereof by a fragrance blending technology aiming at the existing electronic cigarette liquid without myrtle fragrance.

In order to achieve the purpose, the invention adopts the following technical scheme.

The myrtle-flavored essence consists of the following components in percentage by mass: 0.1-2% of beta-pinene, 0.1-2% of alpha-myrcene, 0.1-5% of geraniol, 1-20% of alpha-pinene, 0.1-10% of p-cymene, 0.1-5% of menthol, 1-50% of D-limonene, 0.1-2% of citral, 0.1-3% of borneol, 1-70% of 1, 8-cineole, 0.1-10% of caryophyllene and 0.1-3% of eugenol.

The cigarette liquid of the myrtle-flavored electronic cigarette contains the myrtle-flavored essence, and the mass percentage of the myrtle-flavored essence is less than or equal to 30%.

Preferably, the myrtle-flavored electronic cigarette liquid also contains 10-99% of a smoke agent and 0-5% of a nicotine component by mass percent.

Preferably, the smoke agent is at least one selected from the group consisting of glycerin, propylene glycol, butylene glycol, isopropyl alcohol, and erythritol.

Preferably, the smoke agent contains glycerin and/or propylene glycol.

Preferably, the mass percent of the glycerol or the propylene glycol in the smoke agent is 10-80%.

Preferably, the nicotine component is selected from at least one of nicotine and nicotine salt.

The preparation method of the myrtle-flavored electronic cigarette liquid comprises the following steps:

s1, weighing the components according to the using ratio of the components, and uniformly mixing the components to obtain a mixed solution.

Preferably, the components are mixed together and subjected to at least one of heating, stirring and ultrasonic assisting to obtain a mixed solution.

S2, filtering the mixed liquid to obtain the electronic cigarette liquid.

Preferably, the mixed liquor is filtered using 80-120 mesh filter cloth.

Compared with the prior art, the invention has the beneficial effects that:

according to the invention, through adjusting the components forming the myrtle essence and the proportion of the components, the aroma of the myrtle essence is natural, coordinated, elegant and pleasant, so that the electronic cigarette liquid with vivid myrtle aroma can be further obtained, and the aroma is rich, pleasant and full. In addition, the content of nicotine components, smoke agents and myrtle flavor essence in the electronic cigarette liquid is optimized, and particularly the composition of the smoke agents enables the electronic cigarette liquid to better present the aroma of myrtle oil and meanwhile the electronic cigarette liquid is comfortable in taste. Meanwhile, the myrtle essence can also be applied to smoking products which are not combusted when heated, and explode cigarette beads and the like.

Detailed Description

In order to more fully understand the technical contents of the present invention, the technical solutions of the present invention will be further described and illustrated with reference to the following specific embodiments.

Examples 1 to 14

Examples 1 to 14 each provide a myrtle-flavored essence, and the components constituting the myrtle-flavored essence are shown in table 1 below.

Table 1 composition of the components of the myrtle-flavored essence and mass percentages (%)

The preparation method of the myrtle-flavored essence of examples 1 to 14: weighing the components according to the components and the dosage proportion shown in the table 1, and then uniformly mixing the components to prepare the myrtle-flavored essence for later use. The myrtle-flavored essences prepared in examples 1-14 are respectively and sequentially labeled as essences 1-14.

Examples 15 to 28

Examples 15 to 28 respectively provide an electronic cigarette liquid, which is prepared from nicotine, a smoking agent, and a myrtle-flavored essence, and the nicotine, the smoking agent, and the myrtle-flavored essence are, by mass: 5% of nicotine, 90% of smoke agent and 5% of myrtle flavor essence; wherein the smoke agent consists of 50wt.% of glycerin and 50wt.% of propylene glycol. The difference between the electronic cigarette liquid of the examples 15-28 is that the myrtle flavor used is different, and the myrtle flavor used in the electronic cigarette liquid of the examples 15-28 is respectively 1-14 flavors. The e-cigarette smoke solutions prepared in examples 15-28 are labeled as smoke solutions 15-28, respectively, in order.

The preparation of the e-cigarette smoke solutions of examples 15-28 was as follows: weighing the components according to the using ratio of the components, mixing the components together, and performing dissolution assistance by at least one of heating, stirring and ultrasound to obtain a mixed solution; and filtering the mixed solution by using filter cloth of 80-120 meshes to obtain the electronic cigarette liquid.

Examples 29 to 32

Examples 29-32 each provide an electronic cigarette liquid, the electronic cigarette liquids of examples 29-32 differ from the electronic cigarette liquid of example 18 in the composition of the smoke agent, and the compositions of the smoke agents of examples 29-32 are as follows:

example 29: the smoke agent consisted of 60wt.% glycerin and 40wt.% propylene glycol.

Example 30: the smoke agent consisted of 10wt.% glycerin, 80wt.% propylene glycol and 10wt.% butylene glycol.

Example 31: the smoke agent consisted of 25wt.% erythritol, 60wt.% propylene glycol and 15wt.% butylene glycol.

Example 32: the smoke agent consisted of 25wt.% erythritol, 25wt.% isopropanol, 10wt.% propylene glycol and 40wt.% butylene glycol.

The preparation method of the e-cigarette smoke solutions of examples 29-32 is the same as that of example 18, and the e-cigarette smoke solutions prepared in examples 29-32 are respectively labeled as smoke solutions 29-32 in sequence.

Example 33

Embodiment 33 provides an electronic cigarette liquid, which is prepared from nicotine, a smoking agent, and a myrtle-flavored essence in a ratio of: 5% of nicotine, 65% of smoke agent and 30% of myrtle flavor essence; wherein the smoke agent consists of 80wt.% of glycerin and 20wt.% of propylene glycol, and the myrtle-flavored essence is selected from essence 4. The e-cigarette smoke solution prepared in this example is labeled as smoke solution 33.

The method for preparing the electronic cigarette liquid of example 33 is the same as the method for preparing the electronic cigarette liquid of example 18, and the electronic cigarette liquids prepared in example 33 are respectively and sequentially labeled as liquid 33.

In other embodiments, the nicotine can be replaced by nicotine salt, and the electronic cigarette liquid can also be made of only the smoke agent and the myrtle flavor essence without adding a nicotine component.

The electronic cigarette liquids (15-33) of examples 15-33 were added to electronic cigarette devices as samples to evaluate sensory effects. The sensory evaluation method was as follows.

(1) Evaluation standard of sensory quality of electronic cigarette:

wholly set up 6 evaluation items, include: fragrant quality, fragrant amount, sweet and greasy feeling, irritation, miscellaneous gas, and aftertaste. The maximum scale of each evaluation item is 9 points, each evaluation item is divided into scoring units by 1, and the specific evaluation criteria are shown in table 2.

(2) The evaluation method comprises the following steps: and providing a sample and a sensory quality evaluation standard table for 15 smoking technical experts, and smoking each index according to the requirements of the table.

(3) And (4) counting results: the results of all 15 technical experts were effective, the arithmetic mean of the individual results of each expert was calculated, the results were retained to 1 decimal place, and the arithmetic mean of the individual results was summed to obtain the total score, the results are shown in table 3.

TABLE 2 evaluation criteria for sensory quality of electronic cigarette

Score value

Quality of fragrance

Amount of fragrance

Sweet and greasy feeling

Irritation property

Miscellaneous qi

Aftertaste

9

Is very good

Sufficient (sufficient)

Is very light

Very small

Is very light

Is very good

8

Good taste

Foot

Bland taste

Small

Light and lightweight

Good taste

7

Is better

Relatively big foot

Is relatively light

Is smaller

Is lighter

Is preferably used

6

Slightly better

Little foot

Slightly bland

Is slightly smaller

Is slightly light

Slightly better

5

In

In (1)

In

4

A little bit worse

Is slightly provided with

Slightly concentrated

Slightly larger

Is a little heavier

A little bit worse

3

Is poor

Is relatively light

Is thicker

Is larger than

Heavy weight

Poor quality

2

Difference (D)

Bland

Concentrated

Big (a)

Heavy load

Difference (D)

1

Is very poor

Is very light

Is very dense

Is very big

Is very heavy

Is very poor

TABLE 3 sensory quality evaluation results

According to the invention, through adjusting the components forming the myrtle essence and the proportion of the components, the aroma of the myrtle essence is naturally coordinated, elegant and pleasant, so that the electronic cigarette liquid with vivid myrtle aroma can be further obtained, and the aroma is rich, pleasant and full. In addition, by optimizing the content of nicotine component, smoke agent and myrtle flavor essence in the electronic cigarette liquid, especially the composition of the smoke agent, the electronic cigarette liquid can better present the aroma of myrtle oil, and meanwhile, the electronic cigarette liquid can present better aftertaste, has light miscellaneous gas and comfortable mouthfeel.

The technical contents of the present invention are further illustrated by the examples, so as to facilitate the understanding of the reader, but the embodiments of the present invention are not limited thereto, and any technical extension or re-creation based on the present invention is protected by the present invention.

Claims

1. The myrtle-flavored essence is characterized by comprising the following components in percentage by mass: 0.1-2% of beta-pinene, 0.1-2% of alpha-myrcene, 0.1-5% of geraniol, 1-20% of alpha-pinene, 0.1-10% of p-cymene, 0.1-5% of menthol, 1-50% of D-limonene, 0.1-2% of citral, 0.1-3% of borneol, 1-70% of 1, 8-cineole, 0.1-10% of caryophyllene and 0.1-3% of eugenol.

2. The myrtle-flavored electronic cigarette liquid is characterized by comprising the myrtle-flavored essence of claim 1, wherein the content of the myrtle-flavored essence is 5% by mass.

3. The E-cigarette liquid with the myrtle flavor according to claim 2, further comprising 10-99% of a smoke agent and 0-5% of a nicotine component by mass, wherein the sum of the raw materials of the E-cigarette liquid with the myrtle flavor is 100%.

4. The E-liquid of claim 3, wherein the smoking agent is at least one of glycerin, propylene glycol, butylene glycol, isopropyl alcohol, and erythritol.

5. The E-liquid cigarette with a myrtle flavor according to claim 4, wherein the smoking agent contains glycerin and/or propylene glycol.

6. The E-liquid cigarette with a myrtle flavor according to claim 5, wherein the smoking agent contains 10-80% of glycerin or propylene glycol by mass.

7. A myrtle-flavored electronic cigarette liquid according to claim 3, wherein said nicotine component is at least one selected from nicotine and nicotine salt.

8. A method of preparing a myrtle-flavored electronic cigarette liquid according to any one of claims 2 to 7, comprising the steps of:

s1, weighing each component according to the using amount ratio of each component, and uniformly mixing the components to obtain a mixed solution;

s2, filtering the mixed liquid to obtain the electronic cigarette liquid.

9. The method for preparing a myrtle-flavored electronic cigarette liquid according to claim 8, wherein in the step S1, the components are mixed together and subjected to dissolution assistance by at least one of heating, stirring and ultrasonic treatment to obtain a mixed liquid.

10. The method for preparing the myrtle-flavored electronic cigarette liquid according to claim 8, wherein in the step S2, the mixed liquid is filtered by using a filter cloth of 80-120 meshes.