CN115216363B - Essence formula for increasing aroma of cigarettes and improving smoke quality - Google Patents
Essence formula for increasing aroma of cigarettes and improving smoke quality Download PDFInfo
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- CN115216363B CN115216363B CN202211022862.5A CN202211022862A CN115216363B CN 115216363 B CN115216363 B CN 115216363B CN 202211022862 A CN202211022862 A CN 202211022862A CN 115216363 B CN115216363 B CN 115216363B
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- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 43
- 239000000779 smoke Substances 0.000 title claims abstract description 17
- 241000208125 Nicotiana Species 0.000 claims abstract description 90
- 235000002637 Nicotiana tabacum Nutrition 0.000 claims abstract description 90
- 239000003205 fragrance Substances 0.000 claims abstract description 68
- 238000002360 preparation method Methods 0.000 claims abstract description 16
- 230000002708 enhancing effect Effects 0.000 claims abstract description 13
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims description 72
- 239000002304 perfume Substances 0.000 claims description 50
- 239000002904 solvent Substances 0.000 claims description 42
- 238000000605 extraction Methods 0.000 claims description 37
- WRMNZCZEMHIOCP-UHFFFAOYSA-N 2-phenylethanol Chemical compound OCCC1=CC=CC=C1 WRMNZCZEMHIOCP-UHFFFAOYSA-N 0.000 claims description 32
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 26
- 239000000463 material Substances 0.000 claims description 21
- SATCULPHIDQDRE-UHFFFAOYSA-N piperonal Chemical compound O=CC1=CC=C2OCOC2=C1 SATCULPHIDQDRE-UHFFFAOYSA-N 0.000 claims description 18
- 239000002994 raw material Substances 0.000 claims description 18
- 235000014443 Pyrus communis Nutrition 0.000 claims description 15
- 238000001914 filtration Methods 0.000 claims description 15
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 15
- 239000007788 liquid Substances 0.000 claims description 14
- 239000000203 mixture Substances 0.000 claims description 14
- UHEPJGULSIKKTP-UHFFFAOYSA-N sulcatone Chemical compound CC(C)=CCCC(C)=O UHEPJGULSIKKTP-UHFFFAOYSA-N 0.000 claims description 13
- KWOLFJPFCHCOCG-UHFFFAOYSA-N Acetophenone Chemical compound CC(=O)C1=CC=CC=C1 KWOLFJPFCHCOCG-UHFFFAOYSA-N 0.000 claims description 12
- CFAKWWQIUFSQFU-UHFFFAOYSA-N 2-hydroxy-3-methylcyclopent-2-en-1-one Chemical compound CC1=C(O)C(=O)CC1 CFAKWWQIUFSQFU-UHFFFAOYSA-N 0.000 claims description 11
- MWOOGOJBHIARFG-UHFFFAOYSA-N vanillin Chemical compound COC1=CC(C=O)=CC=C1O MWOOGOJBHIARFG-UHFFFAOYSA-N 0.000 claims description 11
- FGQOOHJZONJGDT-UHFFFAOYSA-N vanillin Natural products COC1=CC(O)=CC(C=O)=C1 FGQOOHJZONJGDT-UHFFFAOYSA-N 0.000 claims description 11
- 235000012141 vanillin Nutrition 0.000 claims description 11
- LCZUOKDVTBMCMX-UHFFFAOYSA-N 2,5-Dimethylpyrazine Chemical compound CC1=CN=C(C)C=N1 LCZUOKDVTBMCMX-UHFFFAOYSA-N 0.000 claims description 10
- DBZAKQWXICEWNW-UHFFFAOYSA-N 2-acetylpyrazine Chemical compound CC(=O)C1=CN=CC=N1 DBZAKQWXICEWNW-UHFFFAOYSA-N 0.000 claims description 10
- OVBFMEVBMNZIBR-UHFFFAOYSA-N 2-methylvaleric acid Chemical compound CCCC(C)C(O)=O OVBFMEVBMNZIBR-UHFFFAOYSA-N 0.000 claims description 10
- XPCTZQVDEJYUGT-UHFFFAOYSA-N 3-hydroxy-2-methyl-4-pyrone Chemical compound CC=1OC=CC(=O)C=1O XPCTZQVDEJYUGT-UHFFFAOYSA-N 0.000 claims description 10
- INAXVXBDKKUCGI-UHFFFAOYSA-N 4-hydroxy-2,5-dimethylfuran-3-one Chemical compound CC1OC(C)=C(O)C1=O INAXVXBDKKUCGI-UHFFFAOYSA-N 0.000 claims description 10
- 240000008042 Zea mays Species 0.000 claims description 10
- 235000005824 Zea mays ssp. parviglumis Nutrition 0.000 claims description 10
- 235000002017 Zea mays subsp mays Nutrition 0.000 claims description 10
- HUMNYLRZRPPJDN-UHFFFAOYSA-N benzaldehyde Chemical compound O=CC1=CC=CC=C1 HUMNYLRZRPPJDN-UHFFFAOYSA-N 0.000 claims description 10
- ISAOCJYIOMOJEB-UHFFFAOYSA-N benzoin Chemical compound C=1C=CC=CC=1C(O)C(=O)C1=CC=CC=C1 ISAOCJYIOMOJEB-UHFFFAOYSA-N 0.000 claims description 10
- POIARNZEYGURDG-FNORWQNLSA-N beta-damascenone Chemical compound C\C=C\C(=O)C1=C(C)C=CCC1(C)C POIARNZEYGURDG-FNORWQNLSA-N 0.000 claims description 10
- POIARNZEYGURDG-UHFFFAOYSA-N beta-damascenone Natural products CC=CC(=O)C1=C(C)C=CCC1(C)C POIARNZEYGURDG-UHFFFAOYSA-N 0.000 claims description 10
- 238000001816 cooling Methods 0.000 claims description 10
- 235000005822 corn Nutrition 0.000 claims description 10
- SHZIWNPUGXLXDT-UHFFFAOYSA-N ethyl hexanoate Chemical compound CCCCCC(=O)OCC SHZIWNPUGXLXDT-UHFFFAOYSA-N 0.000 claims description 10
- MMKRHZKQPFCLLS-UHFFFAOYSA-N ethyl myristate Chemical compound CCCCCCCCCCCCCC(=O)OCC MMKRHZKQPFCLLS-UHFFFAOYSA-N 0.000 claims description 10
- 239000000706 filtrate Substances 0.000 claims description 10
- 239000000796 flavoring agent Substances 0.000 claims description 10
- 235000019634 flavors Nutrition 0.000 claims description 10
- JVTAAEKCZFNVCJ-UHFFFAOYSA-N lactic acid Chemical compound CC(O)C(O)=O JVTAAEKCZFNVCJ-UHFFFAOYSA-N 0.000 claims description 10
- CDOSHBSSFJOMGT-UHFFFAOYSA-N linalool Chemical compound CC(C)=CCCC(C)(O)C=C CDOSHBSSFJOMGT-UHFFFAOYSA-N 0.000 claims description 10
- YLYBTZIQSIBWLI-UHFFFAOYSA-N octyl acetate Chemical compound CCCCCCCCOC(C)=O YLYBTZIQSIBWLI-UHFFFAOYSA-N 0.000 claims description 10
- ZRSNZINYAWTAHE-UHFFFAOYSA-N p-methoxybenzaldehyde Chemical compound COC1=CC=C(C=O)C=C1 ZRSNZINYAWTAHE-UHFFFAOYSA-N 0.000 claims description 10
- MDHYEMXUFSJLGV-UHFFFAOYSA-N phenethyl acetate Chemical compound CC(=O)OCCC1=CC=CC=C1 MDHYEMXUFSJLGV-UHFFFAOYSA-N 0.000 claims description 10
- 229960000380 propiolactone Drugs 0.000 claims description 10
- 239000006188 syrup Substances 0.000 claims description 10
- 235000020357 syrup Nutrition 0.000 claims description 10
- IAEGWXHKWJGQAZ-UHFFFAOYSA-N trimethylpyrazine Chemical compound CC1=CN=C(C)C(C)=N1 IAEGWXHKWJGQAZ-UHFFFAOYSA-N 0.000 claims description 10
- 229930007850 β-damascenone Natural products 0.000 claims description 10
- VEZXCJBBBCKRPI-UHFFFAOYSA-N beta-propiolactone Chemical compound O=C1CCO1 VEZXCJBBBCKRPI-UHFFFAOYSA-N 0.000 claims description 9
- 235000019198 oils Nutrition 0.000 claims description 9
- 230000035807 sensation Effects 0.000 claims description 9
- 235000019615 sensations Nutrition 0.000 claims description 9
- FKUPPRZPSYCDRS-UHFFFAOYSA-N Cyclopentadecanolide Chemical compound O=C1CCCCCCCCCCCCCCO1 FKUPPRZPSYCDRS-UHFFFAOYSA-N 0.000 claims description 8
- XINCECQTMHSORG-UHFFFAOYSA-N Isoamyl isovalerate Chemical compound CC(C)CCOC(=O)CC(C)C XINCECQTMHSORG-UHFFFAOYSA-N 0.000 claims description 8
- JBFHTYHTHYHCDJ-UHFFFAOYSA-N gamma-caprolactone Chemical compound CCC1CCC(=O)O1 JBFHTYHTHYHCDJ-UHFFFAOYSA-N 0.000 claims description 8
- 244000028419 Styrax benzoin Species 0.000 claims description 7
- 235000000126 Styrax benzoin Nutrition 0.000 claims description 7
- XYHKNCXZYYTLRG-UHFFFAOYSA-N 1h-imidazole-2-carbaldehyde Chemical compound O=CC1=NC=CN1 XYHKNCXZYYTLRG-UHFFFAOYSA-N 0.000 claims description 6
- GWYFCOCPABKNJV-UHFFFAOYSA-M 3-Methylbutanoic acid Natural products CC(C)CC([O-])=O GWYFCOCPABKNJV-UHFFFAOYSA-M 0.000 claims description 6
- 240000008866 Ziziphus nummularia Species 0.000 claims description 6
- GWYFCOCPABKNJV-UHFFFAOYSA-N beta-methyl-butyric acid Natural products CC(C)CC(O)=O GWYFCOCPABKNJV-UHFFFAOYSA-N 0.000 claims description 6
- 229940119429 cocoa extract Drugs 0.000 claims description 6
- 235000019382 gum benzoic Nutrition 0.000 claims description 6
- 238000002156 mixing Methods 0.000 claims description 6
- 229940081310 piperonal Drugs 0.000 claims description 6
- PINIEAOMWQJGBW-FYZOBXCZSA-N tenofovir hydrate Chemical compound O.N1=CN=C2N(C[C@@H](C)OCP(O)(O)=O)C=NC2=C1N PINIEAOMWQJGBW-FYZOBXCZSA-N 0.000 claims description 6
- NOOLISFMXDJSKH-KXUCPTDWSA-N (-)-Menthol Chemical compound CC(C)[C@@H]1CC[C@@H](C)C[C@H]1O NOOLISFMXDJSKH-KXUCPTDWSA-N 0.000 claims description 5
- 239000001490 (3R)-3,7-dimethylocta-1,6-dien-3-ol Substances 0.000 claims description 5
- CDOSHBSSFJOMGT-JTQLQIEISA-N (R)-linalool Natural products CC(C)=CCC[C@@](C)(O)C=C CDOSHBSSFJOMGT-JTQLQIEISA-N 0.000 claims description 5
- BJEPYKJPYRNKOW-REOHCLBHSA-N (S)-malic acid Chemical compound OC(=O)[C@@H](O)CC(O)=O BJEPYKJPYRNKOW-REOHCLBHSA-N 0.000 claims description 5
- UFLHIIWVXFIJGU-ARJAWSKDSA-N (Z)-hex-3-en-1-ol Chemical compound CC\C=C/CCO UFLHIIWVXFIJGU-ARJAWSKDSA-N 0.000 claims description 5
- 239000001934 2,5-dimethylpyrazine Substances 0.000 claims description 5
- DXLUAQMRYDUZCJ-UHFFFAOYSA-N 2-(methoxymethyl)pyrazine Chemical compound COCC1=CN=CC=N1 DXLUAQMRYDUZCJ-UHFFFAOYSA-N 0.000 claims description 5
- AJKVQEKCUACUMD-UHFFFAOYSA-N 2-Acetylpyridine Chemical compound CC(=O)C1=CC=CC=N1 AJKVQEKCUACUMD-UHFFFAOYSA-N 0.000 claims description 5
- IEMMBWWQXVXBEU-UHFFFAOYSA-N 2-acetylfuran Chemical compound CC(=O)C1=CC=CO1 IEMMBWWQXVXBEU-UHFFFAOYSA-N 0.000 claims description 5
- VMUXSMXIQBNMGZ-UHFFFAOYSA-N 3,4-dihydrocoumarin Chemical compound C1=CC=C2OC(=O)CCC2=C1 VMUXSMXIQBNMGZ-UHFFFAOYSA-N 0.000 claims description 5
- KBEBGUQPQBELIU-CMDGGOBGSA-N Ethyl cinnamate Chemical compound CCOC(=O)\C=C\C1=CC=CC=C1 KBEBGUQPQBELIU-CMDGGOBGSA-N 0.000 claims description 5
- 235000003368 Ilex paraguariensis Nutrition 0.000 claims description 5
- 244000188472 Ilex paraguariensis Species 0.000 claims description 5
- 235000007688 Lycopersicon esculentum Nutrition 0.000 claims description 5
- HYMLWHLQFGRFIY-UHFFFAOYSA-N Maltol Natural products CC1OC=CC(=O)C1=O HYMLWHLQFGRFIY-UHFFFAOYSA-N 0.000 claims description 5
- 240000003768 Solanum lycopersicum Species 0.000 claims description 5
- 235000008411 Sumatra benzointree Nutrition 0.000 claims description 5
- 244000269722 Thea sinensis Species 0.000 claims description 5
- 235000006468 Thea sinensis Nutrition 0.000 claims description 5
- 235000013832 Valeriana officinalis Nutrition 0.000 claims description 5
- 244000126014 Valeriana officinalis Species 0.000 claims description 5
- BJEPYKJPYRNKOW-UHFFFAOYSA-N alpha-hydroxysuccinic acid Natural products OC(=O)C(O)CC(O)=O BJEPYKJPYRNKOW-UHFFFAOYSA-N 0.000 claims description 5
- 235000015197 apple juice Nutrition 0.000 claims description 5
- 125000003118 aryl group Chemical group 0.000 claims description 5
- 229960002130 benzoin Drugs 0.000 claims description 5
- 235000020279 black tea Nutrition 0.000 claims description 5
- KBEBGUQPQBELIU-UHFFFAOYSA-N cinnamic acid ethyl ester Natural products CCOC(=O)C=CC1=CC=CC=C1 KBEBGUQPQBELIU-UHFFFAOYSA-N 0.000 claims description 5
- 235000008504 concentrate Nutrition 0.000 claims description 5
- 239000012141 concentrate Substances 0.000 claims description 5
- DMSHWWDRAYHEBS-UHFFFAOYSA-N dihydrocoumarin Natural products C1CC(=O)OC2=C1C=C(OC)C(OC)=C2 DMSHWWDRAYHEBS-UHFFFAOYSA-N 0.000 claims description 5
- 235000013399 edible fruits Nutrition 0.000 claims description 5
- 235000020765 fenugreek extract Nutrition 0.000 claims description 5
- HIGQPQRQIQDZMP-UHFFFAOYSA-N geranil acetate Natural products CC(C)=CCCC(C)=CCOC(C)=O HIGQPQRQIQDZMP-UHFFFAOYSA-N 0.000 claims description 5
- HIGQPQRQIQDZMP-DHZHZOJOSA-N geranyl acetate Chemical compound CC(C)=CCC\C(C)=C\COC(C)=O HIGQPQRQIQDZMP-DHZHZOJOSA-N 0.000 claims description 5
- NFLGAXVYCFJBMK-UHFFFAOYSA-N isomenthone Natural products CC(C)C1CCC(C)CC1=O NFLGAXVYCFJBMK-UHFFFAOYSA-N 0.000 claims description 5
- 239000004310 lactic acid Substances 0.000 claims description 5
- 235000014655 lactic acid Nutrition 0.000 claims description 5
- 229940069445 licorice extract Drugs 0.000 claims description 5
- 229930007744 linalool Natural products 0.000 claims description 5
- 239000001630 malic acid Substances 0.000 claims description 5
- 235000011090 malic acid Nutrition 0.000 claims description 5
- 229940043353 maltol Drugs 0.000 claims description 5
- 238000000034 method Methods 0.000 claims description 5
- QNGNSVIICDLXHT-UHFFFAOYSA-N para-ethylbenzaldehyde Natural products CCC1=CC=C(C=O)C=C1 QNGNSVIICDLXHT-UHFFFAOYSA-N 0.000 claims description 5
- 238000003860 storage Methods 0.000 claims description 5
- 229940062013 tamarind extract Drugs 0.000 claims description 5
- 229940098465 tincture Drugs 0.000 claims description 5
- 235000016788 valerian Nutrition 0.000 claims description 5
- IPBFYZQJXZJBFQ-UHFFFAOYSA-N gamma-octalactone Chemical compound CCCCC1CCC(=O)O1 IPBFYZQJXZJBFQ-UHFFFAOYSA-N 0.000 claims description 4
- 238000004804 winding Methods 0.000 claims description 4
- WLJVXDMOQOGPHL-PPJXEINESA-N 2-phenylacetic acid Chemical compound O[14C](=O)CC1=CC=CC=C1 WLJVXDMOQOGPHL-PPJXEINESA-N 0.000 claims description 3
- QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 claims description 3
- XYIBRDXRRQCHLP-UHFFFAOYSA-N ethyl acetoacetate Chemical compound CCOC(=O)CC(C)=O XYIBRDXRRQCHLP-UHFFFAOYSA-N 0.000 claims description 3
- 230000006911 nucleation Effects 0.000 claims description 3
- 238000010899 nucleation Methods 0.000 claims description 3
- 235000015511 Liquidambar orientalis Nutrition 0.000 claims description 2
- 239000004870 Styrax Substances 0.000 claims description 2
- 238000007710 freezing Methods 0.000 claims description 2
- 230000008014 freezing Effects 0.000 claims description 2
- 150000002596 lactones Chemical class 0.000 claims description 2
- 239000001730 (5R)-5-butyloxolan-2-one Substances 0.000 claims 1
- 244000018436 Coriandrum sativum Species 0.000 claims 1
- 235000002787 Coriandrum sativum Nutrition 0.000 claims 1
- 241000732800 Cymbidium Species 0.000 claims 1
- 235000015112 vegetable and seed oil Nutrition 0.000 claims 1
- 238000011156 evaluation Methods 0.000 description 14
- 238000000227 grinding Methods 0.000 description 12
- 238000009472 formulation Methods 0.000 description 9
- 239000000047 product Substances 0.000 description 8
- 239000003921 oil Substances 0.000 description 7
- 230000001953 sensory effect Effects 0.000 description 7
- 230000000694 effects Effects 0.000 description 6
- WLJVXDMOQOGPHL-UHFFFAOYSA-N phenylacetic acid Chemical compound OC(=O)CC1=CC=CC=C1 WLJVXDMOQOGPHL-UHFFFAOYSA-N 0.000 description 6
- OHEFFKYYKJVVOX-UHFFFAOYSA-N sulcatol Natural products CC(O)CCC=C(C)C OHEFFKYYKJVVOX-UHFFFAOYSA-N 0.000 description 6
- 235000013599 spices Nutrition 0.000 description 5
- 241000233855 Orchidaceae Species 0.000 description 4
- 239000001072 coriandrum sativum l. fruit oil Substances 0.000 description 4
- IMKHDCBNRDRUEB-UHFFFAOYSA-N dihydroactinidiolide Chemical compound C1CCC(C)(C)C2=CC(=O)OC21C IMKHDCBNRDRUEB-UHFFFAOYSA-N 0.000 description 3
- 229960003424 phenylacetic acid Drugs 0.000 description 3
- 239000003279 phenylacetic acid Substances 0.000 description 3
- UBLAMKHIFZBBSS-UHFFFAOYSA-N 3-Methylbutyl pentanoate Chemical compound CCCCC(=O)OCCC(C)C UBLAMKHIFZBBSS-UHFFFAOYSA-N 0.000 description 2
- 244000024873 Mentha crispa Species 0.000 description 2
- 235000014749 Mentha crispa Nutrition 0.000 description 2
- 241000745768 Pluchea carolinensis Species 0.000 description 2
- FMFHUEMLVAIBFI-BQYQJAHWSA-N [(e)-2-phenylethenyl] acetate Chemical compound CC(=O)O\C=C\C1=CC=CC=C1 FMFHUEMLVAIBFI-BQYQJAHWSA-N 0.000 description 2
- WDJHALXBUFZDSR-UHFFFAOYSA-M acetoacetate Chemical compound CC(=O)CC([O-])=O WDJHALXBUFZDSR-UHFFFAOYSA-M 0.000 description 2
- 235000011869 dried fruits Nutrition 0.000 description 2
- 239000000523 sample Substances 0.000 description 2
- 230000000391 smoking effect Effects 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- PHOQVHQSTUBQQK-SQOUGZDYSA-N D-glucono-1,5-lactone Chemical compound OC[C@H]1OC(=O)[C@H](O)[C@@H](O)[C@@H]1O PHOQVHQSTUBQQK-SQOUGZDYSA-N 0.000 description 1
- 241001060310 Styracaceae Species 0.000 description 1
- 235000001361 Styrax officinalis Nutrition 0.000 description 1
- 150000001299 aldehydes Chemical class 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 239000013068 control sample Substances 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- NIJJYAXOARWZEE-UHFFFAOYSA-N di-n-propyl-acetic acid Natural products CCCC(C(O)=O)CCC NIJJYAXOARWZEE-UHFFFAOYSA-N 0.000 description 1
- 230000003031 feeding effect Effects 0.000 description 1
- 230000007794 irritation Effects 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000003607 modifier Substances 0.000 description 1
- 239000000178 monomer Substances 0.000 description 1
- 230000035515 penetration Effects 0.000 description 1
- 238000012797 qualification Methods 0.000 description 1
- 210000000697 sensory organ Anatomy 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- MSRILKIQRXUYCT-UHFFFAOYSA-M valproate semisodium Chemical compound [Na+].CCCC(C(O)=O)CCC.CCCC(C([O-])=O)CCC MSRILKIQRXUYCT-UHFFFAOYSA-M 0.000 description 1
- 229960000604 valproic acid Drugs 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/12—Steaming, curing, or flavouring tobacco
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Fats And Perfumes (AREA)
- Manufacture Of Tobacco Products (AREA)
Abstract
The invention discloses an essence formula for increasing the aroma of cigarettes and improving the quality of smoke, which comprises the following components in parts by weight: fragrant base: 1-4 parts; improve the fine and smooth fragrance base: 2-5 parts; enhancing the rich fragrance base of the tobacco fragrance: 0.2 to 1 part; reducing heat dryness feeling fragrance base: 1-4 parts; flue-cured tobacco fragrance base: 0.5-2 parts. The invention also discloses a preparation method and application of the essence formula.
Description
Technical Field
The invention belongs to the technical field of essence and spice, and particularly relates to an essence formula for increasing the aroma of cigarettes and improving the quality of smoke.
Background
The traditional cigarette consumption experience is mainly concerned with physiological satisfaction, and modern cigarette consumption is more focused on comfort and individuation characteristics of cigarette products besides the traditional characteristic experience. The development of cigarette brands has reached the stage of enhancing the market competitiveness of products by highlighting the style characteristics of cigarettes and improving the technical level so as to meet the demands of different consumer groups on cigarette products. The cigarette flavoring and feeding can effectively improve the smoking quality of the cigarette and endow the cigarette product with certain style characteristics, and based on the principle, the formed fragrance base module and the formed essence formula are finally designed and optimized and are applied to the cigarette product.
The formulation of cigarette flavors is generally divided into several parts: firstly, determining the flavor type and the flavor of the prepared essence and determining the flavor blending target; selecting main spice and matched spice with corresponding quality grades according to the application requirements of the essence; preparing a main part of essence base of the essence according to different spice effect evaluation effects; after determining that the bases meet the requirements, the modifier, the perfume fixing agent and the solvent can be added according to actual conditions; repeating the fitting, and trial-preparing 5-10 g essence sample for evaluating the fragrance quality; after evaluation and approval, preparing 500-1000 g of essence big sample, verifying and evaluating in the cigarette product, and finally finishing the formulation of the essence.
The variety of the prior art perfume is complex and various. When a certain characteristic essence and spice is configured, the selection of the perfume raw materials is difficult to determine; the proportioning and blending after the determination of the fragrance raw materials and the testing requires a great deal of work.
The invention is proposed for this purpose.
Disclosure of Invention
Aiming at the characteristics of slightly single aroma, sinking smoke and slightly large smoke irritation and coarseness of a part of leaf groups of Chinese cigarettes, the invention provides an essence formula with strong aroma layering sense and aroma intensity and harmonious overall penetration, which can enrich the aroma of cigarettes and improve the quality of smoke with less consumption.
The technical scheme of the invention is as follows:
the invention discloses an essence formula for increasing the aroma of cigarettes and improving the quality of smoke, which comprises the following components in parts by weight:
fragrant base: 1-4 parts;
improve the fine and smooth fragrance base: 2-5 parts;
enhancing the rich fragrance base of the tobacco fragrance: 0.2 to 1 part;
reducing heat dryness feeling fragrance base: 1-4 parts;
flue-cured tobacco fragrance base: 0.5-2 parts; wherein,,
the fragrant base comprises the following components in parts by weight: 2 to 5 per mill of absolute oil of the tobacco, 1 to 3 per mill of tincture of the orchid, 10 to 25 per mill of distillate of the candied date, 0.1 to 0.5 per mill of coriander seed oil, 0.25 to 1.0 per mill of valerian oil, 5 to 20 per mill of ethyl caproate, 2 to 8 per mill of octyl acetate, 0.25 to 0.75 per mill of styryl acetate, 15 to 30 per mill of isopentyl valerate, 2 to 7 per mill of ethyl acetoacetate, 1 to 5 per mill of beta-damascenone (10%), 0.5 to 2 per mill of leaf alcohol, 2.5 to 7.5 per mill of phenethyl alcohol, 2 to 5 per mill of ethyl myristate, 3 to 40 per mill of geranyl acetate, 3 to 6 per mill of lactic acid, 0.4 to 1.0 per mill of benzaldehyde, 3 to 7 per mill of dihydrocoumarin, 1 to 5.0 per mill of 1% of cyclotrididelactone, 2 to 5 per mill of 1% 2-acetylpyrazine, 1 to 3.0 per mill of 2-acetyl furan, 1 to 3.0 per mill of 1% of 1-6 per mill of 1.0 v of glucolactone, 1 to 0.0 per mill of 1% of gamma-propiolactone and 0 to 0.100 per mill of ethanol;
the improving fine fragrance comprises the following components in parts by weight: 75-150 per mill of apple juice concentrate, 10-30 per mill of tamarind extract, 5-10 per mill of tomato extract, 75-150 per mill of corn syrup, 20-40 per mill of licorice extract, 10-20 per mill of Spirachica black tea extract, 15-40 per mill of plum extract, 0.01-0.1 per mill of 2, 5-dimethyl pyrazine, 1-3 per mill of malic acid, 1-5 per mill of 5% 2-acetylpyridine and 700-750 per mill of solvent propylene glycol;
the heat dryness sensation reducing incense base comprises the following components in parts by weight: 15 to 25 per mill of L-menthone, 0.1 to 1.0 per mill of linalool, 10 to 30 per mill of L-menthol, 0.10 to 0.40 per mill of phenethyl acetate, 2.0 to 5.0 per mill of phenethyl alcohol, 0.5 to 3 per mill of maltol, 0.1 to 1.0 per mill of pineapple ketone/4-hydroxy-2, 5-dimethyl-3 (2H) furanone, 0.25 to 0.75 per mill of ethyl cinnamate, 1 to 5 per mill of dihydroactinolide, 0.2 to 0.5 per mill of 2,3, 5-trimethyl pyrazine, 0.01 to 0.10 per mill of methyl methoxy pyrazine, 0.5 to 2.0 per mill of beta-damascenone, 3 to 5 per mill of vanillin and 100 to 150 per mill of solvent propylene glycol;
the flue-cured tobacco fragrance base comprises the following components in parts by weight: 0.5 to 2 per mill of fenugreek extract, 1 to 5 per mill of yerba mate extract, 30 to 50 per mill of jujube extract, 0.1 to 0.5 per mill of benzoin extract, 1 to 3 per mill of mixed dry fruit extract, 3 to 10 per mill of burley extract, 5 to 10 per mill of aromatic tobacco extract, 30 to 60 per mill of Virginia tobacco extract, 75 to 150 per mill of flue-cured tobacco extract, 80 to 120 per mill of plateau pear extract, 150 to 300 per mill of corn syrup, 150 to 300 per mill of solvent propylene glycol and 200 to 350 per mill of water;
the rich perfume base for enhancing the tobacco fragrance is prepared by using thirteen perfume raw materials, and the relation between the perfume base and the existing thirteen perfume raw materials is as follows:wherein Y is Richness of The value range of (2) is 6.34-9.24; the existing thirteen perfume raw materials and the weight proportion ranges thereof are respectively as follows: x is X 1 :10 to 15 per mill of cocoa extract and X 2 : 110 to 130 per mill of Methyl Cyclopentenolone (MCP) and X 3 : 35 to 50 per mill of isoamyl phenylacetate and X 4 : 30-45%o of propiolactone and X 5 : 25 to 50 per mill of 6-methyl-5-hepten-2-one and X 6 : vanillin 20-40% 7 : 12.5 to 30 per mill of gamma-heptolactone and X 8 : 15 to 30 per mill of phenethyl alcohol and X 9 : heliotropin/piperonal 10-30% 10 :5 to 15 per mill of isovaleric acid and X 11 : acetophenone 5-20% 12 : phenylacetic acid 1-5% 13 :10 to 20 per mill of 2-methyl valeric acid; the balance of propylene glycol solvent, the weight range is: 600 to 700 per mill.
Preferably, the thirteen kinds of incense raw materials for enhancing the richness of the smoke incense comprise the following components in parts by weight: x is X 1 : cocoa extract 13.6% 2 : methyl Cyclopentenolone (MCP) 110% 3 : 44%o of isoamyl phenylacetate, X 4 : 35% 5 : 6-methyl-5-hepten-2-one 30% 6 : vanillin 28% 7 : 25 per mill of gamma-heptolactone and X 8 : phenethyl alcohol 25% 9 : heliotropin/piperonal 18% 10 : isovaleric acid 8% 11 : acetophenone 6% 12 : phenylacetic acid 3% 13 : 2-methylpentanoic acid 16%; propylene glycol 638.4 per mill.
In the method for enhancing the richness of the tobacco fragrance, the 6-methyl-5-hepten-2-one is mainly expressed as oil fragrance, green fragrance and herb fragrance, has certain fresh fragrance and fruit fragrance, can endow the tobacco with the green fragrance in cigarettes, soft the tobacco fragrance, and enable the tobacco fragrance to be plump, but when the dosage is too high, the tobacco fragrance is easy to bring roughness and green smell, and is mainly used for softening and plumping the tobacco fragrance in a formula without positively influencing the richness of the tobacco fragrance.
Preferably, the preparation method of the Virginia tobacco extract comprises the following steps: according to the ratio of feed liquid to liquid of 1 (10-15), the materials are crushed tobacco leaves of Virginia, the solvent is water, and the crushed tobacco leaves are added into an extraction tank; the extraction temperature is 80-100 ℃ and the extraction time is 50-75 min; extracting for two times respectively, collecting filtrate obtained by the two extraction, and concentrating at 50-70deg.C and pressure of 80-100 mbar; controlling the relative density of the concentrated paste (d 20 20 ) 1.1-1.2, dissolving the paste back by using 20v/v% ethanol, storing the solution in a storage tank at-15 ℃, freezing and settling for 8h, and filtering to obtain dark red clarified solution; concentrating again to obtain the Virginia tobacco extract.
Preferably, the preparation method of the plateau pear extract comprises the following steps: according to the ratio of feed liquid to material of 1 (5-10), the materials are Gao Yuanli after stoning and crushing, the solvent is water, and the materials are added into an extraction tank; the extraction temperature is 85-100 ℃ and the extraction time is 30-55 min; filtering with a filter screen and a duplex filter after extraction, cooling with a heat exchange device, extracting for two times, filtering, cooling, and collecting the filtrate of the two times to obtain the plateau pear extract.
The invention discloses a preparation method of the essence formula, which comprises the following steps: respectively dissolving the perfume raw materials with different solubilities to obtain target perfume bases, mixing 5 perfume base systems according to a proportion, and preserving for 48-96 hours to obtain the perfume compound.
In a third aspect the invention discloses the use of said flavour formulation for perfuming a tobacco leaf set.
Preferably, the essence formula is added according to the proportion of 0.25-0.50% of the mass of the tobacco shreds.
Compared with the prior art, the invention has the following beneficial effects:
1. the enhanced tobacco aroma abundant perfume base in the essence formula provides guidance for the use of the existing thirteen perfume raw materials and the weight range of the enhanced tobacco aroma abundant perfume base in the enhanced tobacco aroma abundant perfume base through the relationship between the enhanced tobacco aroma abundant perfume base and the existing thirteen perfume raw materials. Under the guidance of the relation, the method ensures that the fragrance raw materials have higher blending speed, and the obtained result of enhancing the richness of the smoke fragrance is accurate and reliable.
2. The formula of the essence for the cigarettes is prepared by blending a fragrant aroma base, a fine and smooth aroma base, a rich aroma base for enhancing the cigarette aroma, a heat dryness sensation reducing aroma base, a flue-cured tobacco aroma base and a common essence solvent for the cigarettes. The tobacco essence formula is used as the flavoring essence to be applied to tobacco shreds of a tobacco group, so that the aroma concentration and fullness of tobacco can be enhanced, the aroma is more elegant, fresh and natural, and the comprehensive taste of Chinese cigarette products is improved. The obtained essence formula can endow blank cigarettes with faint scent, fruit sweet scent and spicy sweet scent, and the tobacco-baking herbal scent, and plays a role in harmonizing the tobacco scent and transmitting smoke.
3. The perfume raw materials used in the essence formula are common perfume raw materials, are easy to obtain, accord with international and national laws and regulations and related regulations, and have simple production process.
3. The essence formula disclosed by the invention is added into a blank cigarette leaf group, and has good universality and popularization in tobacco industry. Compared with the existing commercial functional essence, the essence formula provided by the invention is prepared from monomer perfume raw materials, and has obvious advantages in cost.
The specific embodiment is as follows:
the invention will be further illustrated with reference to specific examples. For convenience of explanation, the sources of the raw materials used in the following examples of the present invention are as follows, respectively, but are not intended to limit the scope of the present invention. Other reagents, materials, methods and apparatus employed in the present invention are those conventionally used in the art unless otherwise specified.
Example 1
The embodiment provides an essence formula for increasing the aroma of cigarettes and improving the quality of smoke, which comprises the following components in percentage by mass: 1 part of delicate fragrance base; 2 parts of fine fragrance base; 1 part of enhanced tobacco fragrance rich fragrance base; 3 parts of a heat dryness sensation reducing base; 0.5 parts of flue-cured tobacco fragrance base.
The fragrant perfume comprises, by weight, 3 parts of tobacco absolute, 2 parts of orchid tincture, 12.5 parts of candied date distillate, 0.25 parts of coriander seed oil, 0.75 parts of valerian oil, 10 parts of ethyl caproate, 5 parts of octyl acetate, 0.75 parts of storax acetate, 20 parts of isopentyl isovalerate, 5 parts of acetoacetate, 2 parts of beta-damascenone (10%), 1.0 part of leaf alcohol, 5 parts of phenethyl alcohol, 3 parts of ethyl myristate, 10 parts of geranyl acetate, 4 parts of lactic acid, 0.6 parts of benzaldehyde, 5 parts of dihydrocoumarin, 3.5 parts of 1% cyclopentadecanolide, 1% 2-acetylpyrazine, 1.5 parts of 1% 2-acetylfuran, 0.75 parts of anisyl aldehyde/p-methoxybenzaldehyde, 0.2 parts of gamma-caprolactone, 0.6 parts of gamma-octanolide and 98.800% of propylene glycol as solvents.
The fine-improving perfume base comprises, by weight, 100 parts of apple juice concentrate, 20 parts of tamarind extract, 10 parts of tomato extract, 75 parts of corn syrup, 25 parts of licorice extract, 10 parts of Spearmint black tea extract, 20 parts of plum extract, 0.03 part of 2, 5-dimethyl pyrazine, 2 parts of malic acid, 3 parts of 5% 2-acetylpyridine and 734.97 parts of solvent propylene glycol.
The rich perfume base for enhancing the tobacco fragrance comprises 10 per mill of cocoa extract, 110 per mill of Methyl Cyclopentenolone (MCP), 35 per mill of isoamyl phenylacetate, 40 per mill of propiolactone, 30 per mill of 6-methyl-5-hepten-2-one, 30 per mill of vanillin, 17.5 per mill of propiolactone/gamma-heptolactone, 25 per mill of phenethyl alcohol, 15 per mill of heliotropin/piperonal, 7.5 per mill of isovaleric acid, 17.5 per mill of acetophenone, 3 per mill of phenylacetic acid, 18.5 per mill of 2-methyl valeric acid and 641 per mill of solvent propylene glycol, and sensory score Y of the tobacco fragrance richness Richness of 7.25.
The heat dryness sensation reducing perfume base comprises, by weight, 22.5 per mill of L-menthone, 0.75 per mill of linalool, 23 per mill of L-menthol, 0.35 per mill of phenethyl acetate, 3.0 per mill of phenethyl alcohol, 0.65 per mill of maltol, 0.8 per mill of pineapple ketone/4-hydroxy-2, 5-dimethyl-3 (2H) furanone, 0.50 per mill of ethyl cinnamate, 3 per mill of dihydroactinolide, 0.4 per mill of 2,3, 5-trimethyl pyrazine, 0.07 per mill of methyl methoxy pyrazine, 1.35 per mill of beta-damascenone, 3.5 per mill of vanillin and 115.13 per mill of solvent propylene glycol 825 per mill of 95v/v% ethanol.
The flue-cured tobacco fragrance base comprises, by weight, 1.75% of fenugreek extract, 3% of yerba mate extract, 35% of jujube extract, 0.4% of benzoin extract, 2% of mixed dry fruit extract, 4% of burley extract, 8% of aromatic tobacco extract, 35% of Virginia tobacco extract (self-grinding), 130% of flue-cured tobacco extract, 95% of plateau pear extract (self-grinding), 250% of corn syrup and 235% of solvent propylene glycol and 200.85% of water.
The preparation method of the Virginia tobacco extract (self-grinding) comprises the following steps: according to the ratio of the feed liquid to the liquid of 1:10, the materials are crushed tobacco leaves of Virginia, the solvent is water, and the materials are added into an extraction tank; the extraction temperature is 100 ℃ and the extraction time is 60min; extracting twice respectively, collecting the filtrates, concentrating at 70deg.C under pressure of 80mbar. Controlling the relative density of the concentrated paste (d 20 20 ) Dissolving the paste with 20v/v% ethanol at about 1.2, storing the solution in a storage tank at-15deg.C, freeze-settling for 8 hr, and filtering to obtain dark red clarified solution; concentrating again to obtain extract.
The preparation method of the plateau pear extract (self-grinding) comprises the following steps: according to the ratio of 1:5 of the feed liquid, the materials are Gao Yuanli after the nucleation and the crushing, the solvent is water, and the materials are added into an extraction tank; the extraction temperature is 100 ℃ and the extraction time is 30min; filtering with a filter screen and a duplex filter after extraction, cooling with a heat exchange device, extracting twice, filtering, cooling, and collecting the filtrate of the two times to obtain the plateau pear extract.
The preparation method of the essence formula comprises the following steps: the 5 different perfume bases are respectively mixed with corresponding solvents, namely, the perfume raw materials with different solubilities in the perfume base modules are respectively dissolved in the solvents, then the 5 perfume base systems are mixed, and the mixed perfume base systems are stored for 72 hours for use.
Application in tobacco leaf winding: the prepared essence is applied to tobacco shreds as a flavoring formula, and the dosage is 0.30% of the mass of the tobacco shreds.
Example 2
The embodiment provides an essence formula for increasing the aroma of cigarettes and improving the quality of smoke, which comprises the following components in percentage by mass: 3 parts of delicate fragrance base; 5 parts of fine fragrance base; 0.6 part of enhanced tobacco aroma rich fragrance base; 2 parts of a heat dryness sensation base; 0.5 parts of flue-cured tobacco fragrance base.
The fragrant perfume base comprises, by weight, 3.5% of a net oil of Yunnan tobacco, 2% of a tincture of tree orchid, 13.5% of a distillate of candied jujube, 0.4% of coriander seed oil, 0.65% of valerian oil, 13% of ethyl caproate, 7% of octyl acetate, 0.50% of styryl acetate, 17.5% of isoamyl isovalerate, 4% of ethyl acetoacetate, 2.5% of beta-damascenone (10%), 1% of leaf alcohol, 3.5% of phenethyl alcohol, 3.5% of ethyl myristate, 10% of geranyl acetate, 4% of lactic acid, 0.6% of benzaldehyde, 4% of dihydrocoumarin, 2.0% of 1% of cyclopentadecanolide, 3% of 2-acetylpyrazine, 2.5% of 1% of 2-acetylfuran, 0.6% of anisaldehyde/p-methoxybenzaldehyde, 0.3% of gamma-caprolactone, 3% of gamma-octanolide and 0.3% of 0.5% of ethanol/95% of a solvent, and 75% to 95% of ethanol.
The fine-improving perfume base comprises, by weight, 100 parts of apple juice concentrate, 25 parts of tamarind extract, 6 parts of tomato extract, 80 parts of corn syrup, 35 parts of licorice extract, 13 parts of Spearmint black tea extract, 18 parts of plum extract, 0.06 part of 2, 5-dimethyl pyrazine, 2.5 parts of malic acid, 3 parts of 5% 2-acetylpyridine and 717.44 parts of solvent propylene glycol.
The rich perfume base for enhancing the tobacco fragrance comprises, by weight, 14.9% of cocoa extract, 117.3% of Methyl Cyclopentenolone (MCP), 46% of isoamyl phenylacetate, 38% of propiolactone, 38.6% of 6-methyl-5-hepten-2-one, 33.2% of vanillin, 28% of propiolactone/gamma-heptolactone, 25% of phenethyl alcohol, 13.3% of heliotropin/piperonal, 12.6% of isovaleric acid, 8.8% of acetophenone, 3.8% of phenylacetic acid, 19.5% of 2-methyl valeric acid and 601% of solvent propylene glycol, and the sensory score Y of the rich tobacco fragrance Richness of 8.061.
The heat dryness sensation reducing perfume base comprises, by weight, 22.5 per mill of L-menthone, 0.6 per mill of linalool, 12.5 per mill of L-menthol, 0.30 per mill of phenethyl acetate, 3.0 per mill of phenethyl alcohol, 1.2 per mill of maltol, 0.6 per mill of pineapple ketone/4-hydroxy-2, 5-dimethyl-3 (2H) furanone, 0.60 per mill of ethyl cinnamate, 3 per mill of dihydroactinolide, 0.4 per mill of 2,3, 5-trimethyl pyrazine, 0.07 per mill of methyl methoxy pyrazine, 1.25 per mill of beta-damascenone, 4 per mill of vanillin and 150 per mill of solvent propylene glycol 800 per mill, 95v/v% ethanol.
The cured tobacco fragrance base comprises, by weight, 1% of fenugreek extract, 4% of yerba mate extract, 12.5% of jujube extract, 0.35% of benzoin extract, 2.5% of mixed dried fruit extract, 5.5% of burley extract, 6% of aromatic tobacco extract, 45% of Virginia tobacco extract (self-grinding), 80% of cured tobacco extract, 100% of plateau pear extract (self-grinding), 225% of corn syrup, 300% of solvent propylene glycol and 218.15% of water.
The preparation method of the Virginia tobacco extract (self-grinding) comprises the following steps: according to the ratio of the feed liquid to the liquid of 1:12, the materials are crushed tobacco leaves of Virginia, the solvent is water, and the materials are added into an extraction tank; the extraction temperature is 90 ℃ and the extraction time is 65min; extracting twice respectively, collecting the filtrates, concentrating at 60deg.C under 100mbar. Controlling the relative density of the concentrated paste (d 20 20 ) Dissolving the paste with 20v/v% ethanol at about 1.15, storing the solution in a storage tank at-15deg.C, freeze-settling for 8 hr, and filtering to obtain dark red clarified solution; concentrating again to obtain extract.
The preparation method of the plateau pear extract (self-grinding) comprises the following steps: according to the ratio of 1:7, the materials are Gao Yuanli after stoning and crushing, the solvent is water, and the materials are added into an extraction tank; the extraction temperature is 85 ℃ and the extraction time is 45min; filtering with a filter screen and a duplex filter after extraction, cooling with a heat exchange device, extracting twice, filtering, cooling, and collecting the filtrate of the two times to obtain the plateau pear extract.
The preparation method of the essence formula comprises the following steps: the 5 different perfume bases are respectively mixed with corresponding solvents, namely, the perfume raw materials with different solubilities in the perfume base modules are respectively dissolved in the solvents, then the 5 perfume base systems are mixed, and the mixed perfume base systems are stored for 96 hours for use.
Application in tobacco leaf winding: the prepared essence is applied to tobacco shreds as a flavoring formula, and the usage amount is 0.50% of the mass of the tobacco shreds.
Example 3
The embodiment provides an essence formula for increasing the aroma of cigarettes and improving the quality of smoke, which comprises the following components in percentage by mass: 2 parts of delicate fragrance and fragrant base; 5 parts of fine fragrance base; 0.4 part of enhanced tobacco aroma rich fragrance base; 2 parts of a heat dryness sensation base; 0.75 parts of flue-cured tobacco fragrance base.
The fragrant perfume base comprises, by weight, 5 parts of tobacco absolute, 2 parts of tree orchid tincture, 20 parts of candied date distillate, 0.3 part of coriander seed oil, 0.75 part of valerian oil, 15 parts of ethyl caproate, 5 parts of octyl acetate, 0.50 part of styrax acetate, 20 parts of isopentyl isovalerate, 5 parts of acetoacetate, 4 parts of beta-damascenone (10%), 1 part of leaf alcohol, 5 parts of phenethyl alcohol, 4 parts of ethyl myristate, 5 parts of geranyl acetate, 4 parts of lactic acid, 0.75 part of benzaldehyde, 4.5 parts of dihydrocoumarin, 1.5 parts of 1% cyclopentadecanolide, 1% 2-acetylpyrazine, 1.5 parts of 1% 2-acetylfuran, 0.6 part of anisaldehyde/p-methoxybenzaldehyde, 0.3 part of gamma-caprolactone, 0.15 part of gamma-octanolide and 871.15 parts of solvent propylene glycol/95% v.
The aroma base for improving the fineness comprises, by weight, 100 parts of apple juice concentrate, 20 parts of tamarind extract, 5 parts of tomato extract, 100 parts of corn syrup, 30 parts of licorice extract, 15 parts of Spearkacha black tea extract, 20 parts of plum extract, 0.1 part of 2, 5-dimethyl pyrazine, 2 parts of malic acid, 2 parts of 5% 2-acetylpyridine and 705.9 parts of solvent propylene glycol.
The rich fragrance base for enhancing the smoke fragrance comprises 13.6 per mill of cocoa extract, 110 per mill of Methyl Cyclopentenolone (MCP), 44 per mill of isoamyl phenylacetate, 35 per mill of propiolactone, 30 per mill of 6-methyl-5-hepten-2-one, 28 per mill of vanillin, 25 per mill of propiolactone/gamma-heptolactone, 25 per mill of phenethyl alcohol, 18 per mill of heliotropin/piperonal, 8 per mill of isovaleric acid, 6 per mill of acetophenone, 3 per mill of phenylacetic acid and 2-methyl16 per mill of valproic acid and 638.4 per mill of propylene glycol as solvent, and sensory score Y of richness of smoke Richness of 7.7133.
The heat dryness sensation reducing perfume base comprises, by weight, 22.5 per mill of L-menthone, 0.5 per mill of linalool, 25 per mill of L-menthol, 0.25 per mill of phenethyl acetate, 2.5 per mill of phenethyl alcohol, 1 per mill of maltol, 0.5 per mill of pineapple ketone/4-hydroxy-2, 5-dimethyl-3 (2H) furanone, 0.5 per mill of ethyl cinnamate, 3 per mill of dihydro-kiwi lactone, 0.4 per mill of 2,3, 5-trimethyl pyrazine, 0.07 per mill of methyl methoxy pyrazine, 1 per mill of beta-damascenone, 4.4 per mill of vanillin and 142 per mill of solvent propylene glycol 796.38 per mill of 95v/v% ethanol.
The flue-cured tobacco fragrance base comprises, by weight, 1% of fenugreek extract, 1% of yerba mate extract, 40% of jujube extract, 0.2% of benzoin extract, 2% of mixed dried fruit extract, 4% of burley extract, 6% of aromatic tobacco extract, 40% of Virginia tobacco extract (self-grinding), 100% of flue-cured tobacco extract, 100% of plateau pear extract (self-grinding), 200% of corn syrup and 200% of solvent propylene glycol, and 305.8% of water.
The preparation method of the Virginia tobacco extract (self-grinding) comprises the following steps: according to the ratio of the feed liquid to the liquid of 1:10, the materials are crushed tobacco leaves of Virginia, the solvent is water, and the materials are added into an extraction tank; the extraction temperature is 100 ℃ and the extraction time is 65min; extracting twice respectively, collecting the filtrates, concentrating at 70deg.C under 90mbar. Controlling the relative density of the concentrated paste (d 20 20 ) Dissolving the paste with 20v/v% ethanol at about 1.15, storing the solution in a storage tank at-15deg.C, freeze-settling for 8 hr, and filtering to obtain dark red clarified solution; concentrating again to obtain extract.
The preparation method of the plateau pear extract (self-grinding) comprises the following steps: according to the ratio of 1:6 of the feed liquid, the materials are Gao Yuanli after the nucleation and the crushing, the solvent is water, and the materials are added into an extraction tank; the extraction temperature is 95 ℃ and the extraction time is 35min; filtering with a filter screen and a duplex filter after extraction, cooling with a heat exchange device, extracting twice, filtering, cooling, and collecting the filtrate of the two times to obtain the plateau pear extract.
The preparation method of the essence formula comprises the following steps: the 5 different perfume bases are respectively mixed with corresponding solvents, namely, the perfume raw materials with different solubilities in the perfume base modules are respectively dissolved in the solvents, then the 5 perfume base systems are mixed, and the mixed perfume base systems are stored for 84 hours for use.
Application in tobacco leaf winding: the prepared essence is applied to tobacco shreds as an essence formula, and the usage amount is 0.40% of the mass of the tobacco shreds.
Example 4 application evaluation
The application test was performed using the same leaf formulation with any one of the flavor formulations of examples 1-3 as the cigarette flavor formulation. For convenience of description, in this example, a blank cigarette with a certain brand without flavoring is used as an evaluation carrier, and sensory comparison is performed, and the comparison situation is shown in table 1. Evaluation of the vector: a certain brand of blank cigarettes provided by Yunnan medium cigarettes are used as an evaluation carrier.
The evaluation method comprises the following steps: aiming at developing the flavoring effect and style evaluation of the designed and developed essence formula, the evaluation control sample is the same blank cigarette. Cigarette flavoring and feeding effects and style evaluation: the method mainly comprises the fragrance characteristic, the taste characteristic and the fragrance style of the flavored cigarettes, wherein the fragrance and the taste are quantified in a manner of-5 to 5 minutes, the score unit is 1 minute, the fragrance style is quantified in a manner of 0 to 3 minutes, the score unit is 1 minute, and the evaluation result is the arithmetic average value (accurate to 0.1) of each panelist. The personnel involved in the evaluation needs to have the special fragrance smelling capability and the sensory cigarette smoking qualification evaluation, and the number of the participants is 5.
Table 1 table of the flavoring effect and style evaluation records of cigarettes before and after applying the essence formulation of the present invention
As can be seen from Table 1, the essence formulation of example 3 has the best effect of improving the sensory effect of cigarettes, and the proper addition amount of the essence formulation in the leaf group is 0.40%, which shows that the sensory score Y for enhancing the richness of the tobacco fragrance when the fragrance base module is designed Richness of When the design is about 7.7, the compatibility with the blank cigarette leaf group is good. Effect on cigarette sense organ:the aroma concentration and fullness of the tobacco are enhanced, so that the aroma is more elegant, fresh and natural, and the comprehensive taste and aroma feeling of Chinese cigarette products is improved.
The foregoing is only a preferred embodiment of the present invention, but the scope of the present invention is not limited thereto, and any person skilled in the art, who is within the scope of the present invention, should make equivalent substitutions or modifications according to the technical scheme of the present invention and the inventive concept thereof, and should be covered by the scope of the present invention.
Claims (4)
1. The essence composition for increasing the aroma of cigarettes and improving the quality of smoke is characterized by comprising the following components in percentage by mass:
fragrant base: 2 parts;
improve the fine and smooth fragrance base: 5 parts;
enhancing the rich fragrance base of the tobacco fragrance: 0.4 parts;
reducing heat dryness feeling fragrance base: 2 parts;
flue-cured tobacco fragrance base: 0.75 parts; wherein,,
the fragrant base comprises the following components in parts by weight: 5 per mill of net oil of tobacco, 2 per mill of tincture of cymbidium, 20 per mill of distillate of candied date, 0.3 per mill of seed oil of coriander, 0.75 per mill of valerian oil, 15 per mill of ethyl caproate, 5 per mill of octyl acetate, 0.50 per mill of styrax acetate, 20 per mill of isoamyl isovalerate, 5 per mill of ethyl acetoacetate, 4 per mill of 10% beta-damascenone, 1 per mill of leaf alcohol, 5 per mill of phenethyl alcohol, 4 per mill of ethyl myristate, 5 per mill of geranyl acetate, 4 per mill of lactic acid, 0.75 per mill of benzaldehyde, 4.5 per mill of dihydrocoumarin, 1.5 per mill of 1% cyclopentadecanolide, 1% 2-acetylpyrazine, 1.5 per mill of 2-acetylfuran, 0.6 per mill of anisaldehyde/p-methoxybenzaldehyde, 0.3 per mill of gamma-caprolactone, 0.15 per mill of gamma-octalactone and 871.15 per mill of solvent propylene glycol, 95v/v% of 20 per mill of ethanol;
the improving fine fragrance comprises the following components in parts by weight: 100 per mill of apple juice concentrate, 20 per mill of tamarind extract, 5 per mill of tomato extract, 100 per mill of corn syrup, 30 per mill of licorice extract, 15 per mill of Spirachica black tea extract, 20 per mill of plum extract, 0.1 per mill of 2, 5-dimethyl pyrazine, 2 per mill of malic acid, 2 per mill of 5% 2-acetylpyridine and 705.9 per mill of solvent propylene glycol;
the heat dryness sensation reducing incense base comprises the following components in parts by weight: 22.5 per mill of L-menthone, 0.5 per mill of linalool, 25 per mill of L-menthol, 0.25 per mill of phenethyl acetate, 2.5 per mill of phenethyl alcohol, 1 per mill of maltol, 0.5 per mill of pineapple ketone/4-hydroxy-2, 5-dimethyl-3 (2H) furanone, 0.5 per mill of ethyl cinnamate, 3 per mill of dihydrokiwi lactone, 0.4 per mill of 2,3, 5-trimethylpyrazine, 0.07 per mill of methyl methoxy pyrazine, 1 per mill of beta-damascenone, 4.4 per mill of vanillin and 796.38 per mill of solvent propylene glycol, and 142 per mill of 95v/v% ethanol;
the flue-cured tobacco fragrance base comprises the following components in parts by weight: 1 per mill of fenugreek extract, 1 per mill of yerba mate extract, 40 per mill of jujube extract, 0.2 per mill of benzoin extract, 2 per mill of mixed dry fruit extract, 4 per mill of burley tobacco extract, 6 per mill of aromatic tobacco extract, 40 per mill of virginia tobacco extract, 100 per mill of flue-cured tobacco extract, 100 per mill of plateau pear extract, 200 per mill of corn syrup, 200 per mill of solvent propylene glycol and 305.8 per mill of water; the preparation method of the Virginia tobacco extract comprises the following steps: according to the ratio of the feed liquid to the liquid of 1:10, the materials are crushed tobacco leaves of Virginia, the solvent is water, and the materials are added into an extraction tank; the extraction temperature is 100 ℃ and the extraction time is 65min; extracting for two times respectively, collecting the filtrate obtained by the two extraction, and concentrating at 70deg.C under 90mbar; controlling the relative density of the concentrated pasted 20 20 ) 1.15, dissolving the paste back with 20v/v% ethanol, storing the solution in a storage tank at-15 ℃, freezing and settling for 8h, and filtering to obtain dark red clarified solution; concentrating again to obtain the Virginia tobacco extract; the preparation method of the plateau pear extract comprises the following steps: according to the ratio of 1:6 of the feed liquid, the materials are Gao Yuanli after the nucleation and the crushing, the solvent is water, and the materials are added into an extraction tank; the extraction temperature is 95 ℃ and the extraction time is 35min; filtering with a filter screen and a duplex filter after extraction, cooling with a heat exchange device, extracting for two times, filtering, cooling, and collecting the filtrate of the two times to obtain the plateau pear extract;
the enhanced tobacco fragrance rich fragrance base comprises the following components in parts by weight: 13.6 per mill of cocoa extract, 110 per mill of methyl cyclopentenolone, 44 per mill of isoamyl phenylacetate, 35 per mill of propiolactone, 30 per mill of 6-methyl-5-heptene-2-one, 28 per mill of vanillin, 25 per mill of propiolactone/gamma-heptanone, 25 per mill of phenethyl alcohol, 18 per mill of heliotropin/piperonal, 8 per mill of isovaleric acid, 6 per mill of acetophenone, 3 per mill of phenylacetic acid, 16 per mill of 2-methylpentanoic acid and 638.4 per mill of solvent propylene glycol.
2. A process for the preparation of a flavour composition according to claim 1, comprising the steps of: respectively dissolving the perfume raw materials with different solubilities to obtain target perfume base, mixing 5 perfume base systems according to a certain proportion, and storing 48-96h to obtain the perfume composition.
3. A perfuming application of a flavour composition according to claim 1, in a tobacco leaf winding group.
4. The use according to claim 3, wherein the flavour composition is added in a proportion of 0.25 to 0.50% by mass of tobacco.
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| CN114516797B (en) * | 2022-03-10 | 2023-09-08 | 安徽中烟工业有限责任公司 | Methyl cyclopentenolone menthol carbonate spice and synthetic method and application thereof |
| CN114587003B (en) * | 2022-03-24 | 2023-04-21 | 江苏中烟工业有限责任公司 | Development method of medium and thin cigarette formula tobacco shreds with characteristic aroma |
| CN115813010A (en) * | 2023-01-09 | 2023-03-21 | 福建中烟工业有限责任公司 | Tobacco functional additive, tobacco shred and cigarette |
| CN116548654B (en) * | 2023-04-26 | 2024-02-20 | 广州科百欣香料有限公司 | Tobacco essence capable of reducing smoke stimulation and preparation method and application thereof |
| CN116463171B (en) * | 2023-04-27 | 2024-04-12 | 广州科百欣香料有限公司 | Essence for enhancing cigarette aroma and preparation method and application thereof |
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