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CN114951674A - Continuous feeding mechanism for rotary electrode atomization powder making, powder making equipment and powder making method - Google Patents

Continuous feeding mechanism for rotary electrode atomization powder making, powder making equipment and powder making method Download PDF

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Publication number
CN114951674A
CN114951674A CN202210837922.2A CN202210837922A CN114951674A CN 114951674 A CN114951674 A CN 114951674A CN 202210837922 A CN202210837922 A CN 202210837922A CN 114951674 A CN114951674 A CN 114951674A
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China
Prior art keywords
electrode
transition bin
chamber
transmission chamber
bin
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CN202210837922.2A
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Chinese (zh)
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CN114951674B (en
Inventor
赵博
王健
赵博深
李永华
陈小龙
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Shangi Institute For Advanced Materials Nanjing Co ltd
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Shangi Institute For Advanced Materials Nanjing Co ltd
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Priority to CN202210837922.2A priority Critical patent/CN114951674B/en
Publication of CN114951674A publication Critical patent/CN114951674A/en
Priority to PCT/CN2022/124579 priority patent/WO2024016488A1/en
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F9/00Making metallic powder or suspensions thereof
    • B22F9/02Making metallic powder or suspensions thereof using physical processes
    • B22F9/14Making metallic powder or suspensions thereof using physical processes using electric discharge
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F1/00Metallic powder; Treatment of metallic powder, e.g. to facilitate working or to improve properties
    • B22F1/06Metallic powder characterised by the shape of the particles
    • B22F1/065Spherical particles
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B33ADDITIVE MANUFACTURING TECHNOLOGY
    • B33YADDITIVE MANUFACTURING, i.e. MANUFACTURING OF THREE-DIMENSIONAL [3-D] OBJECTS BY ADDITIVE DEPOSITION, ADDITIVE AGGLOMERATION OR ADDITIVE LAYERING, e.g. BY 3-D PRINTING, STEREOLITHOGRAPHY OR SELECTIVE LASER SINTERING
    • B33Y40/00Auxiliary operations or equipment, e.g. for material handling
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P10/00Technologies related to metal processing
    • Y02P10/25Process efficiency

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Manufacturing & Machinery (AREA)
  • Materials Engineering (AREA)
  • Nanotechnology (AREA)
  • Manufacture Of Metal Powder And Suspensions Thereof (AREA)

Abstract

The invention relates to the technical field of plasma rotary electrode atomization powder preparation, in particular to a continuous feeding mechanism, powder preparation equipment and a powder preparation method for rotary electrode atomization powder preparation, which comprise the following steps: the discharge port of the electrode transmission chamber is connected with the atomization chamber, a carrier roller for supporting an electrode bar is arranged in the electrode transmission chamber, the axis of the electrode bar is aligned with the discharge port, and the carrier roller is arranged to drive the electrode bar to rotate; and the pushing component is arranged in the electrode transmission chamber and used for moving the electrode bar on the carrier roller from a first position to a second position along the axis of the electrode bar. According to the invention, the gate valve is arranged between the transition bin and the electrode transmission chamber, when the gate valve is opened, the transition bin is communicated with the electrode transmission chamber, the bar material in the transition bin can be transferred into the electrode transmission chamber, and after the gate valve is closed, the transition bin can be communicated with the atmosphere, so that feeding is realized, and the protective atmosphere environment of the electrode transmission chamber is not interfered.

Description

Continuous feeding mechanism for rotary electrode atomization powder preparation, powder preparation equipment and powder preparation method
Technical Field
The invention relates to the technical field of plasma rotary electrode atomization powder preparation, in particular to a continuous feeding mechanism, powder preparation equipment and a powder preparation method for rotary electrode atomization powder preparation.
Background
In recent years, with the rapid development of technologies such as 3D printing, hot isostatic pressing, injection molding and the like, the demand for metal powder is gradually increased year by year, and the requirements for the quality of the metal powder are more and more strict; the 3D printing industry has high requirements on the fluidity of the metal powder, so that the metal powder is required to have high sphericity.
The plasma rotating electrode atomization powder manufacturing device has a great advantage for preparing spherical powder, but the existing plasma rotating electrode atomization powder manufacturing device uses a storage bin with limited volume, when electrode bars in the storage bin are completely manufactured into powder, an atomization chamber and the storage bin are communicated with the atmosphere, after a new batch of electrode bars are added, the storage bin is vacuumized again and filled with argon, and due to the fact that the volumes of the atomization chamber and the storage bin are large, and after each batch of electrode bars are manufactured into powder, cooling time is needed, the efficiency of the plasma rotating electrode atomization powder manufacturing device is reduced to a great extent, and the cost of metal powder is increased to a great extent; the use of a larger stock bin also cannot realize infinite continuous feeding in the true sense, and the larger the stock bin is, the higher the manufacturing cost is, and the bulkier the equipment is.
Disclosure of Invention
The invention provides a continuous feeding mechanism for atomizing and pulverizing by a rotary electrode, which comprises:
the discharge port of the electrode transmission chamber is connected with the atomization chamber, a carrier roller for supporting an electrode bar is arranged in the electrode transmission chamber, the axis of the electrode bar is aligned with the discharge port, and the carrier roller is arranged to drive the electrode bar to rotate;
the pushing component is arranged in the electrode transmission chamber and used for moving the electrode bar on the carrier roller from a first position to a second position along the axis of the electrode bar, and the electrode bar continuously enters the atomizing chamber to atomize and prepare powder with the plasma gun in the process of moving the electrode bar from the first position to the second position;
the turnover component is connected to the pushing component and used for driving the pushing component to be located at a pushing position and a feeding position, when the pushing component is located at the pushing position, the pushing component is provided with a part which is overlapped with the axis of the electrode bar, and when the pushing component is located at the feeding position, the pushing component deviates from the axis of the electrode bar;
the transition bin is connected with the feeding hole of the electrode transmission chamber and is provided with an air valve group for controlling the atmosphere of the cavity in the transition bin;
the feeding component is arranged at one end of the transition bin, which is far away from the electrode transmission chamber, and is used for conveying the electrode bars in the transition bin to a first position of the electrode transmission chamber;
the electrode transmission chamber is communicated with the transition bin through a gate valve, the gate valve is opened when materials in the transition bin are transmitted to the electrode transmission chamber, the electrode transmission chamber is communicated with the transition bin through the gate valve, and when new electrode bars are placed into the transition bin, the gate valve is closed to enable the electrode transmission chamber and the transition bin to be in an isolated state, and feeding is not performed under the condition that protective atmosphere in the electrode transmission chamber is not removed.
Preferably, the feeding part comprises a feeding cylinder and an expansion link connected to the output end of the feeding cylinder, and the axis of the expansion link coincides with the axis of the discharge port and the axis of the feed port.
Preferably, the transition bin is provided with a detachable bin cover, and when the bin cover is opened, new electrode bars can be placed into the transition bin.
Preferably, the powder making time of a single electrode material rod is defined as T, T1 is the time for opening the cover of the transition bin, T2 is the time for adding a new electrode material rod into the transition bin, T3 is the time for closing the cover of the transition bin, T4 is the time for vacuumizing the transition bin, and T5 is the time for filling the inert gas into the transition bin;
wherein T is greater than T1+ T2+ T3+ T4+ T5, the volume of the transition bin is defined as Q, the vacuumizing speed is a, and the inert gas filling speed is b, so that T4+ T5 is Q/a + Q/b;
the volume of the transition bin is Q < (T-T1-T2-T3). ((a + b)/ab).
Preferably, the gate valve comprises a valve body, a valve plate and an electromagnetic driving part, the valve body is provided with a circular channel, the valve plate is controlled by the electromagnetic driving part and extends into the circular channel or slides out of the circular channel, and when the valve plate is positioned in the circular channel, the valve plate completely covers the circular channel so that the circular channel is closed.
Preferably, the pushing mechanism comprises a driving part, a screw rod, a threaded sleeve and a push rod, bearing seats are arranged at two ends of the screw rod, the bearing seats are fixed to the outer wall of the turnover shaft through bolts, the screw rod is driven by the driving part to rotate relative to the bearing seats, the threaded sleeve is arranged to move in the opposite direction along the axis of the screw rod, and the push rod is fixed to the outer wall of the threaded sleeve and used for pushing the electrode bar to move along the axial direction of the feeding port and move from a first position to a second position.
Preferably, the push rod is arranged to be driven by the turning part so that the push rod is in a pushing position and a feeding position.
Preferably, the upset part includes trip shaft, upset cylinder, upset arm, the upset cylinder is fixed to the electrode transmission room, just the first end of upset arm articulates the output of upset cylinder, the second end of upset arm is fixed to the first end of trip shaft, the trip shaft with the electrode transmission room rotates to be connected, works as when the upset cylinder is flexible, the upset arm winds the trip shaft axis rotates, makes the trip shaft upset.
Preferably, the driving part comprises a motor and a universal coupling, a first end of the universal coupling is connected to the screw, a second end of the universal coupling is connected to an output shaft of the motor, and the motor is fixed with the electrode transmission chamber.
Preferably, a supporting groove is arranged at the bottom of the transition bin, when the electrode is placed in the supporting groove in the transition bin, the electrode is limited at a third position, the telescopic rod at the contraction position is attached to the end face of the electrode, when the telescopic rod is at the feeding position, the electrode is at a first position, and at the moment, the right end face of the electrode is flush with the left end face of the push rod.
Preferably, the gas valve group comprises a first valve and a second valve, the first valve is used for vacuumizing the transition bin, and the second valve is used for filling inert gas into the transition bin so as to construct a protective atmosphere in the transition bin.
Preferably, the electrode transfer chamber is provided with a removable cover for projecting electrode rod stock into the electrode transfer chamber when the cover is opened.
The second aspect of the invention provides a technical scheme that the rotary electrode atomization powder making equipment comprises the continuous feeding mechanism and the plasma gun, wherein one end of the plasma gun is positioned in the atomization chamber, a plasma arc is formed between the plasma gun and the electrode charge bar, and atomized particles are formed in the atomization chamber.
Preferably, the idler comprises a first idler and a second idler, the electrode bar stock is placed between the first idler and the second idler and is in contact with surfaces of the first idler and the second idler, the first idler and the second idler are driven to rotate by a drive means, and the direction of rotation of the first idler and the second idler is opposite.
The third aspect of the present invention provides a technical solution, a method for pulverizing powder by atomization with a rotary electrode, which uses the above-mentioned powder pulverizing apparatus by atomization with a rotary electrode, comprising the following steps:
step 1, respectively filling an electrode bar into an electrode transmission chamber and a transition bin;
2, communicating the electrode transmission chamber with a transition bin, vacuumizing the transition bin and filling inert gas into the transition bin to ensure that the electrode transmission chamber, the transition bin and the atomization chamber reach protective atmosphere;
step 3, controlling the electrode bar stock in the electrode transmission chamber to move to the atomizing chamber at a preset speed and a preset rotating speed, and contacting with a plasma arc emitted by a plasma gun to atomize and prepare powder;
step 4, when the electrode bar stock is consumed, transferring the electrode bar stock in the transition stock bin into the electrode transmission chamber, and isolating the electrode transmission chamber from the transition stock bin;
and 5, realizing continuous atomization powder preparation through the following actions 1 and 2:
action 1: opening a transition bin, filling a new electrode bar material into the transition bin, closing the transition bin, independently vacuumizing the transition bin and filling inert gas into the transition bin to ensure that the protective atmosphere of the transition bin is the same as that of an electrode transmission chamber, and communicating the electrode transmission chamber with the transition bin;
and action 2: electrode bar stock in the electrode transmission chamber is moved into the atomization chamber at a preset speed and a preset rotating speed and is contacted with plasma arcs emitted by a plasma gun to atomize and prepare powder;
the actions in the step are carried out synchronously, and the action time is longer than the action time;
and (5) repeating the step (4) and the step (5) to realize continuous atomization powder preparation.
Preferably, the electrode bar stock is transferred from the electrode transfer chamber into the atomization chamber by a pusher member, and when a new electrode bar stock is transferred from the transition bin into the electrode transfer chamber, the pusher member is arranged to be offset from the axis of the electrode bar stock to avoid the moving track of the electrode bar stock.
Compared with the prior art, the invention has the advantages that:
according to the invention, the gate valve is arranged between the transition bin and the electrode transmission chamber, when the gate valve is opened, the transition bin is communicated with the electrode transmission chamber, the bar material in the transition bin can be transferred into the electrode transmission chamber, and after the gate valve is closed, the transition bin can be communicated with the atmosphere, so that feeding is realized, and the protective gas atmosphere of the electrode transmission chamber is not interfered;
the transition bin can be independently vacuumized and filled with argon gas, so that the transition bin can reestablish the same protective atmosphere as the atomizing chamber; when the transition bin and the atomizing chamber have the same protective atmosphere, the gate valve can be opened to ensure that the transition bin is communicated with the electrode transmission chamber again, the electrode bar material in the transition bin can enter the electrode transmission chamber, and the continuous feeding can be realized by repeating the steps; because the feeding is only carried out the environmental reconstruction to the transition feed bin, and does not need to carry out the environmental reconstruction (vacuumizing and inert gas protection) to the electrode transmission chamber, the needed inert gas consumption is less, the reconstruction process is short, the production interruption time is greatly reduced, the processing efficiency is improved, and the production cost is reduced.
Drawings
The drawings are not intended to be drawn to scale. In the drawings, each identical or nearly identical component that is illustrated in various figures may be represented by a like numeral. For purposes of clarity, not every component may be labeled in every drawing.
Fig. 1 is a schematic structural view of a continuous feeding mechanism for atomizing and pulverizing by a rotary electrode in an embodiment of the present invention.
Fig. 2 is a schematic structural diagram of a continuous feeding mechanism for atomizing and pulverizing by a rotary electrode in the embodiment of the present invention.
Figure 3 is a left side view of the electrode transfer chamber (the pusher mechanism is in the electrode bar axis).
Figure 4 is a left side view of the electrode transfer chamber (the pusher mechanism is offset from the electrode bar axis).
Fig. 5 is a schematic structural diagram of a transition bin.
Fig. 6 is a schematic structural diagram of electrode bars placed in the electrode transmission chamber and the transition bin.
Fig. 7 is a dynamic diagram of electrode rod pushing milling in the electrode driving chamber according to the present invention.
Figure 8 is a schematic view of the pusher mechanism of the present invention shown offset from the feed axis.
Fig. 9 is a schematic diagram of the process of the electrode bar stock entering the electrode driving chamber from the transition bin according to the invention.
Fig. 10 is a schematic view of the electrode rod material entering the electrode transfer chamber from the transition bin according to the present invention.
FIG. 11 is a schematic view of electrode rod stock of the present invention externally added to a transition bin.
Fig. 12 is a schematic diagram illustrating the filling of the transition bin with the shielding gas according to the present invention.
Fig. 13 is a schematic diagram of the electrode bar stock waiting for feeding in the transition bin according to the invention.
Detailed Description
In order to better understand the technical content of the present invention, specific embodiments are described below with reference to the accompanying drawings.
In order to realize continuous feeding in the electrode transmission chamber 10 and atomization preparation of the continuous rotating electrode, the electrode bar stock 100 enters into atomization powder preparation environment from the atmospheric environment, in the process, the relief of the vacuum environment and the protective atmosphere environment in the equipment is involved, so that the vacuum environment and the protective atmosphere environment of a feeding link and an electrode transmission link need to be reestablished, the consumed time is long, energy and gas are wasted, the interruption time of powder making is long, and the efficiency and the capacity of atomized powder making are influenced, therefore, the invention solves the problem by introducing a transition bin, as shown in FIG. 1, the first aspect of the present invention provides a technical solution, a continuous feeding mechanism for atomizing and pulverizing by a rotary electrode, comprising an electrode transmission chamber 10 and a transition bin 50, a gate valve 60 is arranged between the transition bin 50 and the electrode transmission chamber 10, the control electrode transmission chamber 10 and the cavities in the transition bin 50 are independent or communicated with each other.
Therefore, when the electrode transmission chamber 10 is used, and the electrode bar stock in the electrode transmission chamber 10 is consumed by the atomization powder making process, can be supplemented by electrode bars in a transition bin 50 which is communicated with the electrode transmission chamber 10 and establishes a vacuum protective atmosphere environment, in the normal milling process of the electrode bar, the connection between the electrode transmission chamber 10 and the cavity of the transition bin 50 is cut off, the vacuum protective atmosphere environment is normally maintained in the electrode transmission chamber 10, the vacuum protective atmosphere in the transition bin 50 is independently removed, electrode bar materials are supplemented into the cavity of the transition bin, then the vacuum protective atmosphere environment in the transition bin 50 is reestablished to be the same as that of the electrode transmission chamber 10, the transition storage bin 50 can be communicated with the electrode transmission chamber 10 again through a control component such as a gate valve, so that feeding from the transition storage bin 50 into the electrode transmission chamber 10 is realized. The above-mentioned two-chamber division-transition bin environment release-transition bin environment reconstruction-two-chamber communication process is repeated, so that the continuous feeding into the electrode transmission chamber 10 is realized.
In the process, only the transition bin is subjected to environment reconstruction, and the electrode transmission chamber is not required to be subjected to environment reconstruction (vacuumizing and inert gas protection), so that the required inert gas consumption is less, the reconstruction process is short, and the production interruption time is greatly reduced.
Electrode transmission chamber
Electrode transmission room 10 includes electrode transmission storehouse 11 and lid, forms confined cavity in electrode transmission storehouse 11 and the lid, atomizing chamber 101 is connected to the one end that transition feed bin 50 was kept away from in electrode transmission room 10, electrode transmission room 10 passes through pay-off mouth and atomizing chamber 101 intercommunication, the inside of electrode transmission room 10 is equipped with bearing roller 12 for bearing the electrode, and make electrode axis and pay-off mouth axis align, wherein, bearing roller 12 is driven by the motor, make electrode bar 100 on the bearing roller 12 rotate.
Optionally, two carrier rollers 12 are arranged side by side, a space for holding the electrode bar stock 100 is formed between the two carrier rollers 12, and the electrode bar stock 100 is attached to the surfaces of the two carrier rollers 12, wherein the rotation directions of the two carrier rollers 12 are opposite, so that the electrode bar stock 100 between the two carrier rollers 12 is driven to rotate.
The electrode driving chamber 10 is further provided with a material pushing mechanism 30 and a turnover mechanism 20, the material pushing mechanism 30 is used for feeding the electrode on the carrier roller 12 into the atomizing chamber 101 from the feeding port along the axis of the electrode, and the turnover mechanism 20 is used for controlling the material pushing mechanism 30 to turn over so that the material pushing mechanism deviates from the axis of the feeding port.
Thus, when the electrode bar 100 is on the carrier roller 12, the electrode bar 100 is pushed by the pushing mechanism 30 to move towards the feeding port, and meanwhile, the electrode bar 100 is in high-speed rotation and reacts with the plasma arc of the plasma gun 102 arranged in the atomizing chamber 101, so that the electrode bar 100 can be uniformly consumed, atomized powder is formed, and the electrode bar 100 needs to be fed into the electrode transmission chamber 10 again along with the continuous feeding and consumption of the electrode bar 100.
Turnover mechanism
Since the electrode bar 100 needs to be fed along the moving direction of the pushing mechanism 30 in the process of transferring the electrode bar 100 from the transition bin 50 to the electrode transmission chamber 10, if the pushing mechanism 30 is kept on the moving path of the electrode bar 100, interference can be caused on smooth transfer of the electrode bar 100, and therefore, in order to avoid interference caused by the pushing mechanism 30 on feeding of the electrode bar 100, the turnover mechanism 20 is used for controlling the pushing mechanism 30 to turn over, so that the pushing mechanism 30 deviates from the moving path of the electrode bar 100, namely, deviates from the axis of the feeding port.
Specifically, as shown in fig. 1, fig. 3 and fig. 4, the turnover mechanism 20 includes a turnover shaft 23, a turnover cylinder 21 and a turnover arm 22, the turnover cylinder 21 is fixed to the electrode transmission chamber 10, a first end of the turnover arm 22 is hinged to an output end of the turnover cylinder 21, a second end of the turnover arm 22 is fixed to a first end of the turnover shaft 23, the turnover shaft 23 is rotatably connected to the electrode transmission chamber 10, and when the turnover cylinder 21 is extended and retracted, the turnover arm 22 rotates around an axis of the turnover shaft 23 to turn over the turnover shaft 23.
Further, a material pushing mechanism 30 is fixed to the surface of the turnover shaft 23, as shown in fig. 3, when the turnover cylinder 21 is in the extended state, the material pushing mechanism 30 can push the electrode bar 100, as shown in fig. 4, when the turnover cylinder 21 is in the compressed state, the left end of the turnover arm 22 moves downward, and the right end rotates around the axis of the turnover shaft 23, so that the turnover shaft 23 rotates, and at this time, the material pushing mechanism 30 deviates from the axis of the feeding port, so that the electrode bar 100 can be pushed into the electrode transmission chamber 10 through the transition bin 50.
Pushing mechanism
Referring to fig. 1, the pushing mechanism 30 includes a driving member, a screw 33, a threaded sleeve 34 and a push rod 35, wherein bearing seats are disposed at two ends of the screw 33, the bearing seats are fixed to an outer wall of the turnover shaft 23 through bolts, the screw 33 is driven by the driving member to rotate relative to the bearing seats, the threaded sleeve 34 is arranged to move in a reverse direction along an axis of the screw 33, and the push rod 35 is fixed to an outer wall of the threaded sleeve 34 and used for pushing the electrode to move along an axial direction of the feeding port.
In a preferred embodiment, in order to provide better support for the pushing mechanism 30, a slide rail 331 is provided on one side of the screw 33, and a fixing ring is provided on one side of the slide rail 331 and welded to the surface of the turning shaft 23, so that when the turning shaft 23 rotates, the slide rail 331 rotates around the axis of the turning shaft 23.
Specifically, two ends of the slide rail 331 are provided with two bearing seats on one side away from the turning shaft 23, two ends of the screw 33 are respectively connected to the bearing seats, the screw sleeve 34 is sleeved on the surface of the screw 33, a slide block is arranged on one side of the screw sleeve 34, the slide block is slidably connected with the slide rail 331 along the length direction of the screw 33, and when the drive part drives the screw 33 to rotate, the screw sleeve 34 slides on the surface of the screw 33 and drives the push rod 35 to push the electrode bar 100 to advance.
Optionally, the driving component includes a motor 31 and a universal joint 32, a first end of the universal joint 32 is connected to the screw 33, a second end is connected to an output shaft of the motor 31, and the motor 31 is fixed with the electrode driving chamber 10.
In this way, when the screw 33 is driven by the turning shaft 23 to rotate reversely, the motor 31 can still be connected with the screw 33 through the universal joint 32.
Transition bin
Referring to fig. 2 and 5, the transition bin 50 includes a bin body 51 and an upper cover 52, the bin body 51 is hermetically connected with the upper cover 52, a feeding cavity 53 is formed inside the transition bin 50, a first end 531 of the feeding cavity 53 is communicated with the electrode transmission chamber 10, and a second end 532 of the feeding cavity 53 is communicated with the feeding component 40.
The bin body 51 and the upper cover 52 are detachably arranged, and a sealing ring is arranged between the bin body 51 and the upper cover 52 to ensure the sealing after the cover is closed.
The volume of the transition bin 50 should be as small as possible to reduce the time to re-establish the protective atmosphere.
Specifically, the powder making time of a single electrode material rod is defined as T, T1 is the time for opening the cover of the transition bin (50), T2 is the time for adding a new electrode rod material (100) into the transition bin (50), T3 is the time for closing the cover of the transition bin (50), T4 is the time for vacuumizing the transition bin (50), and T5 is the time for filling inert gas into the transition bin (50);
wherein T is greater than T1+ T2+ T3+ T4+ T5, the volume of the transition bin (50) is defined as Q, the vacuumizing speed is a, and the inert gas filling speed is b, so that T4+ T5 is Q/a + Q/b;
the volume Q of the transition bin (50) satisfies Q < (T-T1-T2-T3) ((a + b)/ab).
Further, the transition bin 50 is provided with two valves, a first valve 54 is used for vacuumizing the transition bin 50, and a second valve 55 is used for filling the transition bin 50 with inert gas. In this way, the first valve 54 and the second valve 55 are controlled to perform operations of evacuating and filling argon gas into the charging chamber 53.
In a specific embodiment, after materials are put into the transition bin 50 and the electrode transmission chamber 10 for the first time, the cavities of the electrode transmission chamber 10 and the transition bin 50 are in a mutually communicated state, the cavities of the transition bin 50 and the electrode transmission chamber 10 are vacuumized through the first valve 54, and then argon is filled into the transition bin 50 and the electrode transmission chamber 10 through the second valve 55 to establish a protective atmosphere of inert gas;
before a new material is put into the transition bin 50, the cavity of the transition bin 50 and the cavity of the electrode transmission chamber 10 are separated through the gate valve 60, so that the cavities of the transition bin 50 and the electrode transmission chamber 10 are independent, at the moment, a new electrode bar 100 is put into the transition bin 50, the original protective atmosphere environment is relieved, after the operations of vacuumizing and argon filling are carried out, the protective atmosphere in the transition bin 50 is identical to the protective atmosphere in the electrode transmission chamber 10 again, at the moment, the gate valve 60 is opened, and the transition bin 50 is communicated with the electrode transmission chamber 10.
Wherein, the transition feed bin 50 is equipped with feeding cylinder 41 far away from the one end of electrode transmission room 10, and the telescopic link 42 of feeding cylinder 41 includes contraction position and pay-off position, when telescopic link 42 was in the pay-off position, made the electrode in the transition feed bin 50 pass push-pull valve 60 and move to in the electrode transmission room 10.
In a preferred embodiment, the bottom of the transition bin 50 is provided with a support slot, when the electrode is placed in the support slot in the transition bin 50, the electrode is defined in a first position, in which the telescopic rod 42 in the retracted position engages the end face of the electrode, and when the telescopic rod 42 is in the feeding position, the electrode is in a second position, in which the right end face of the electrode is flush with the left end face of the push rod 35.
Preferably, the push rod 35 includes a start position and an end position, when the push rod 35 is located at the start position, the end surface of the pushing end of the push rod 35 and the end surface of the telescopic rod 42 located at the feeding position are located on the same plane, and when the push rod 35 is located at the end position, the end surface of the pushing end of the push rod 35 extends to the inside of the feeding port.
Preferably, a circular channel is arranged inside the gate valve 60, and the axis of the circular channel is coincident with the axis of the telescopic rod 42 and the axis of the feeding port.
In a specific embodiment, the gate valve 60 comprises a valve body and a valve plate, the valve body is provided with a round opening, the gate is opened and closed by the control of the electromagnetic valve, the gate and the round opening on the gate body perform the action of complete separation and fit, so that the gate valve 60 is opened or closed, when the gate valve 60 is opened, the electrode transmission chamber 10 and the transition bin 50 are communicated with each other, and when the gate valve 60 is closed, the electrode transmission chamber 10 and the transition bin 50 are isolated from each other.
As described above, by the alternate operation of the telescopic rod 42 and the push rod 35, the electrode bar 100 can be pushed from the first position to the second position by using the telescopic rod 42 in the first stage, and the electrode bar 100 can be pushed from the second position to the feed port of the electrode transmission chamber 10 by using the push rod 35 in the second stage.
Further, a first end of the gate valve 60 is connected with the electrode transmission chamber 10 through a transition flange, and a second end of the gate valve 60 is connected with the transition bin 50 through a corrugated pipe.
In this way, the communication state of the electrode driving chamber 10 and the transition bin 50 can be controlled by opening and closing the gate valve 60.
Specifically, after the gate valve 60 is closed, the transition bin 50 can be communicated with the atmosphere to realize feeding; the transition bin 50 can be independently vacuumized and filled with argon, and after feeding is completed, the transition bin 50 is vacuumized and filled with argon, so that the transition bin 50, the electrode transmission chamber 10 and the atomization chamber 101 have the same atmosphere; after the transition bin 50 and the atomizing chamber 101 have the same atmosphere, the gate valve 60 is opened, the electrode bar 100 in the transition bin 50 can enter the atomizing chamber 101, and the process is repeated, so that continuous feeding is realized.
[ ROTARY ELECTRODE ATOMIZED POWDER-MAKING APPARATUS ]
The second aspect of the present invention provides a technical solution, and a rotary electrode atomization powder manufacturing apparatus, which includes the above continuous feeding mechanism and a plasma gun 102, wherein one end of the plasma gun is located in the atomization chamber 101, and a plasma arc is formed between the plasma gun and an electrode, so as to form atomized particles in the atomization chamber 101.
The atomization powder manufacturing equipment can realize continuous feeding, and operations of vacuumizing and filling argon into the atomization chamber 101 and the electrode transmission chamber 10 are not required to be stopped, so that the production interruption time is greatly reduced.
Preferably, the idler 12 comprises a first idler and a second idler, the electrode bar stock 100 being placed between and in contact with surfaces of the first and second idlers, the first and second idlers being driven in rotation by the drive means, the first and second idlers being counter-rotating.
[ METHOD FOR MAKING POWDER BY ATOMIZING WITH ROTARY ELECTRODE ]
Referring to fig. 6-13, a third aspect of the present invention provides a technical solution, a method for pulverizing powder by atomization with a rotary electrode, comprising the following steps:
the method comprises the following steps:
step 1, as shown in fig. 6, filling an electrode bar 100 into the electrode transmission chamber 10 and the transition bin 50 respectively;
step 2, as shown in fig. 7, communicating the electrode transmission chamber 10 with the transition bin 50, vacuumizing the transition bin 50, and filling inert gas into the transition bin to make the electrode transmission chamber 10, the transition bin 50 and the atomization chamber 101 reach a protective atmosphere;
step 3, as shown in fig. 8, controlling the electrode bar 100 in the electrode transmission chamber 10 to move into the atomization chamber at a predetermined speed and a predetermined rotation speed, and contacting the electrode bar with the plasma arc emitted by the plasma gun 50 to atomize and prepare powder;
step 4, as shown in fig. 9-11, when the electrode bar stock 100 is exhausted, the electrode bar stock 100 in the transition bin 50 is transferred into the electrode transmission chamber 10, and the electrode transmission chamber 10 is isolated from the transition bin 50;
step 5, as shown in fig. 11-13, continuously atomizing to prepare powder through the following actions 1 and 2:
action 1: opening a transition bin 50, filling a new electrode bar material 100 into the transition bin 50, closing the transition bin 50, independently vacuumizing the transition bin 50 and filling inert gas into the transition bin, so that the protective atmosphere of the transition bin 50 is the same as that of the electrode transmission chamber 10, and the electrode transmission chamber 10 is communicated with the transition bin 50;
and action 2: the electrode bar stock 100 in the electrode transmission chamber 10 is moved into the atomizing chamber 101 at a preset speed and rotating speed, and contacts with the plasma arc emitted by the plasma gun 102 to atomize and prepare powder;
wherein, the action 1 and the action 2 in the step 5 are synchronously performed, and the time of the action 1 is longer than that of the action 2;
and (5) repeating the step (4) and the step (5) to realize continuous milling.
Preferably, the electrode bar stock 100 is transferred from the electrode transfer chamber 10 to the atomization chamber 101 through the pushing member 30, and when a new electrode bar stock 100 is transferred from the transition bin 50 to the electrode transfer chamber 10, the pushing member 30 is disposed to be offset from the axis of the electrode bar stock 100 so as to avoid the moving track of the electrode bar stock 100.
Preferably, a flashboard valve is used to control the isolation or communication between the electrode drive chamber 10 and the transition bin 50.
In a specific embodiment, the gate valve 60 comprises a valve body and a valve plate, the valve body is provided with a round opening, the gate is opened and closed by the control of the electromagnetic valve, the gate and the round opening on the gate body perform the action of complete separation and fit, so that the gate valve 60 is opened or closed, when the gate valve 60 is opened, the electrode transmission chamber 10 and the transition bin 50 are communicated with each other, and when the gate valve 60 is closed, the electrode transmission chamber 10 and the transition bin 50 are isolated from each other.
Process for making powders
1. Establishing a protective atmosphere and pushing materials to prepare powder: before atomization powder manufacturing is started, the feeding cylinder 41 retracts to a proper position, the overturning cylinder 21 extends to a proper position, the push rod 35 is located on a feeding central line at the moment, one electrode bar 100 is respectively placed in the electrode transmission chamber 10 and the transition bin 50, the top cover and the upper cover 52 of the electrode transmission chamber 10 are closed, the gate valve 60 is opened, the transition bin 50 is communicated with the electrode transmission chamber 10 at the moment, the electrode transmission chamber 10 is vacuumized and filled with argon through the first valve 54 and the second valve 55, and after the pressure of the argon reaches a set value, the plasma gun 102 is started to atomize and manufacture the electrode bar 100 rotating at a high speed;
2. feeding electrode bars in an electrode transmission chamber: the motor 31 positively drives and drives the screw rod 33 to rotate, so that the push rod 35 pushes the electrode bar to move forward along the feeding central line from the initial position, the electrode bar 100 enters the atomizing chamber 101 and contacts with a plasma arc emitted by the plasma gun 102 to atomize and prepare powder, wherein the moving speed of the electrode bar is matched with the powder preparing speed;
3. the pusher 30 is offset from the feed axis: when the electrode bar stock 100 in the electrode transmission chamber 10 is consumed to a certain extent, the motor 31 rotates reversely and drives the screw rod 33 to rotate, so that the push rod 35 returns to the initial position along the feeding center line; the overturning cylinder 21 retracts and transmits a retraction in-place signal to an upper computer, and the overturning arm 22 and the overturning shaft 23 drive the pushing structure to overturn integrally, so that the push rod 35 deviates from a feeding central line (as shown in fig. 4);
4. the electrode bar stock 100 in the transition bin 50 is fed into the electrode transmission chamber 10: the upper computer controls the feeding cylinder 41 to extend according to the retraction in-place signal of the turnover cylinder 21, pushes the electrode bar 100 in the transition bin 50 into a designated position (shown in fig. 2) in the electrode transmission chamber 10, and retracts the feeding cylinder 41 immediately after the electrode bar reaches the designated position;
5. the electrode transmission chamber is separated from the transition bin; closing the gate valve 60;
6. pushing and milling newly fed bars: the overturning cylinder 21 extends out, and drives the pushing structure to overturn integrally through the overturning arm 22 and the overturning shaft 23, so that the push rod 35 returns to a feeding central line (as shown in fig. 3), and 2-3 times of the inside of the electrode transmission chamber 10 are repeated;
7. the environment of the transition bin is removed, and a new electrode bar is added: opening the upper cover 52, putting an electrode bar, closing the upper cover 52 and locking by using a locking assembly;
8. and (3) rebuilding the environment of the transition bin: opening a first valve 54 for vacuumizing the transition bin 50, measuring the vacuum degree by a vacuum gauge and transmitting the vacuum degree to an upper computer, and closing the first valve 54 when the vacuum degree reaches a set value; opening a second valve 55 for filling inert gas such as argon gas into the transition bin 50, measuring the argon gas pressure by a pressure sensor 56 and transmitting the argon gas pressure to an upper computer, and closing the second valve 55 when the argon gas pressure reaches a set value;
in the process of the step 7-8, electrode bars in the electrode transmission chamber 10 are pushed by the push rod 35 to continuously atomize and prepare powder;
9. and (3) communicating the electrode transmission chamber and the transition bin again: the gate valve 60 is opened to wait for the turning cylinder 21 to retract to the in-place signal;
10. after the tumble cylinder 21 is retracted to its position, repeat 5-9.
The above two-chamber division-transition bin environment release-transition bin environment reconstruction-two-chamber communication process is repeated, continuous feeding into the electrode transmission chamber 10 is realized, and continuous electrode bar supplementing in the electrode transmission chamber 10 can be continuously pushed by the push rod 35 to prepare powder in the atomization chamber.
By combining the embodiment, the gate valve is arranged between the transition bin and the electrode transmission chamber, when the gate valve is opened, the transition bin is communicated with the electrode transmission chamber, the bar material in the transition bin can be transferred into the electrode transmission chamber, and after the gate valve is closed, the transition bin can be communicated with the atmosphere, so that feeding is realized, and the protective gas atmosphere of the electrode transmission chamber is not interfered;
the transition bin can be independently vacuumized and filled with argon gas, so that the transition bin can reestablish the same protective atmosphere as the atomizing chamber; when the transition bin and the atomizing chamber have the same protective atmosphere, the gate valve can be opened to ensure that the transition bin is communicated with the electrode transmission chamber again, the electrode bar material in the transition bin can enter the electrode transmission chamber, and the continuous feeding can be realized by repeating the steps;
because the feeding is only carried out the environmental reconstruction to the transition feed bin, and does not need to carry out the environmental reconstruction (vacuumizing and inert gas protection) to the electrode transmission chamber, the needed inert gas consumption is less, the reconstruction process is short, the production interruption time is greatly reduced, the processing efficiency is improved, and the production cost is reduced.
Although the invention has been described with reference to preferred embodiments, it is not intended to be limited thereto. Those skilled in the art can make various changes and modifications without departing from the spirit and scope of the invention. Therefore, the protection scope of the present invention should be determined by the appended claims.

Claims (16)

1. The utility model provides a rotary electrode atomizing powder process is with continuous feed mechanism which characterized in that includes:
the electrode driving chamber (10) is connected with the atomizing chamber (101) through a discharge hole of the electrode driving chamber (10), a carrier roller (12) used for supporting an electrode bar (100) is arranged in the electrode driving chamber (10), the axis of the electrode bar (100) is aligned with the discharge hole, and the carrier roller (12) is arranged to drive the electrode bar (100) to rotate;
the pushing component (30) is arranged in the electrode transmission chamber (10) and used for moving the electrode bar (100) on the carrier roller (12) from a first position to a second position along the axis of the electrode bar (100), and in the process that the electrode bar (100) moves from the first position to the second position, the electrode bar (100) continuously enters the atomizing chamber (101) to atomize and prepare powder with the plasma gun (102);
the turnover component (20) is connected to the pushing component (30) and is used for driving the pushing component (30) to be in a pushing position and a feeding position, when the pushing component (30) is in the pushing position, the pushing component (30) is provided with a part which is overlapped with the axis of the electrode bar (100), and when the pushing component (30) is in the feeding position, the pushing component (30) deviates from the axis of the electrode bar (100);
the transition bin (50) is connected with a feeding hole of the electrode transmission chamber (10), and the transition bin (50) is provided with an air valve group for controlling the atmosphere environment of the cavity in the transition bin (50);
the feeding part (40) is arranged at one end of the transition bin (50) far away from the electrode transmission chamber (10) and is used for conveying the electrode bars (100) in the transition bin (50) to a first position of the electrode transmission chamber (10);
wherein, be equipped with push-pull valve (60) between electrode transmission room (10) and transition feed bin (50), be used for controlling be in between electrode transmission room (10) and the transition feed bin (50) communicate/isolation state:
when the materials in the transition bin (50) are transmitted into the electrode transmission chamber (10), the gate valve (60) is opened to enable the electrode transmission chamber (10) and the transition bin (50) to be in a communicated state, when new electrode bars (100) are placed in the transition bin (50), the gate valve (60) is closed to enable the electrode transmission chamber (10) and the transition bin (50) to be in an isolated state, and feeding does not release the protective atmosphere in the electrode transmission chamber (10).
2. The continuous feeding mechanism for pulverizing by atomizing with rotating electrode as claimed in claim 1, wherein said feeding member (40) comprises a feeding cylinder (41) and a telescopic rod (42) connected to the output end of said feeding cylinder (41), the axis of said telescopic rod (42) is coincident with the axis of said outlet and the axis of said inlet.
3. The continuous feeding mechanism for pulverizing by atomizing rotary electrode as claimed in claim 1, wherein said transition bin (50) is provided with a detachable lid, and when said lid is opened, a new electrode bar stock (100) can be put into said transition bin (50).
4. The continuous feeding mechanism for pulverizing powder by atomizing a rotary electrode as claimed in claim 3, wherein the pulverizing time of a single electrode bar is defined as T, T1 is the time for opening the cover of the transition bin (50), T2 is the time for adding a new electrode bar (100) into the transition bin (50), T3 is the time for closing the cover of the transition bin (50), T4 is the time for vacuumizing the transition bin (50), and T5 is the time for filling the transition bin (50) with inert gas;
wherein, T is greater than T1+ T2+ T3+ T4+ T5, the volume of the transition bin (50) is defined as Q, the vacuumizing speed is a, and the inert gas filling speed is b, so that T4+ T5 is Q/a + Q/b;
the volume Q of the transition bin (50) satisfies: q < (T-T1-T2-T3) ((a + b)/ab).
5. The continuous feeding mechanism for pulverizing by atomizing rotary electrode as claimed in claim 1, wherein said gate valve (60) comprises a valve body and a valve plate and an electromagnetic driving member, said valve body is provided with a circular passage, said valve plate is controlled by said electromagnetic driving member to protrude into or slide out of said circular passage, and when said valve plate is in said circular passage, said valve plate completely covers said circular passage, so that said circular passage is closed.
6. The continuous feeding mechanism for atomizing powder by using the rotary electrode as claimed in claim 1, wherein the pushing mechanism comprises a driving member, a screw rod (33), a threaded sleeve (34) and a push rod (35), the two ends of the screw rod (33) are provided with bearing seats, the bearing seats are fixed to the outer wall of the turnover shaft (23) through bolts, the screw rod (33) is driven by the driving member to rotate relative to the bearing seats, the threaded sleeve (34) is arranged to move along the axis of the screw rod (33) in the opposite direction, and the push rod (35) is fixed to the outer wall of the threaded sleeve (34) and used for pushing the electrode bar stock to move along the axis direction of the feeding port from a first position to a second position.
7. The continuous feeding mechanism for pulverizing by atomizing with rotary electrode as claimed in claim 6, wherein said pushing rod (35) is configured to be driven by said turning member to make said pushing rod (35) at a pushing position and a feeding position.
8. The continuous feeding mechanism for pulverizing by atomizing rotary electrode as claimed in claim 7, wherein said turning member comprises a turning shaft (23), a turning cylinder (21), and a turning arm (22), said turning cylinder (21) is fixed to said electrode transmission chamber (10), and a first end of said turning arm (22) is hinged to an output end of said turning cylinder (21), a second end of said turning arm (22) is fixed to a first end of said turning shaft (23), said turning shaft (23) is rotatably connected to said electrode transmission chamber (10), when said turning cylinder (21) is extended, said turning arm (22) rotates around an axis of said turning shaft (23) to turn said turning shaft (23).
9. The continuous feeding mechanism for pulverizing by rotary electrode atomization as claimed in claim 8, wherein the driving member comprises a motor (31) and a universal coupling (32), a first end of the universal coupling (32) is connected to the screw (33), a second end is connected to an output shaft of the motor (31), and the motor (31) is fixed with the electrode transmission chamber (10).
10. The continuous feeding mechanism for atomizing and powdering by using the rotary electrode as claimed in claim 6, wherein said transition bin (50) is provided with a receiving slot at the bottom thereof, when said electrode is placed in said receiving slot of said transition bin (50), said electrode is confined to a third position, in which said telescopic rod (42) in a retracted position is engaged with said electrode end face, and when said telescopic rod (42) is in a feeding position, said electrode is in a first position, in which a right end face of said electrode is flush with a left end face of said pushing rod (35).
11. The continuous feeding mechanism for pulverizing by atomizing rotary electrode according to any one of claims 1-10, wherein the valve set comprises a first valve (54) and a second valve (55), the first valve (54) is used for evacuating the transition bin (50), and the second valve (55) is used for filling inert gas into the transition bin (50) to form a protective atmosphere in the transition bin (50).
12. A continuous feed mechanism for atomizing and powdering by rotating electrode according to any of claims 1-10, wherein said electrode drive chamber (10) is provided with a removable cover for feeding electrode rod into said electrode drive chamber (10) when said cover is opened.
13. A rotary electrode atomization powder manufacturing device, which comprises the continuous feeding mechanism and the plasma gun of any one of claims 1 to 12, wherein one end of the plasma gun is positioned in the atomization chamber (101) and forms a plasma arc with the electrode material rod, and atomized particles are formed in the atomization chamber (101).
14. The rotary electrode atomizing powder manufacturing apparatus as set forth in claim 13, said idler (12) including a first idler and a second idler, said electrode bar stock (100) being interposed between and in contact with surfaces of said first and second idlers, said first and second idlers being driven to rotate by a drive means, said first and second idlers being turned in opposite directions.
15. A method for pulverizing by atomizing with rotating electrode as claimed in claim 13, which comprises the steps of:
step 1, filling an electrode bar stock (100) into an electrode transmission chamber (10) and a transition bin (50) respectively;
step 2, communicating the electrode transmission chamber (10) with a transition bin (50), vacuumizing the transition bin (50) and filling inert gas into the transition bin to enable the electrode transmission chamber (10), the transition bin (50) and the atomization chamber (101) to reach a protective atmosphere;
step 3, controlling the electrode bar stock (100) in the electrode transmission chamber (10) to move into the atomization chamber at a preset speed and a preset rotating speed, and contacting with a plasma arc emitted by the plasma gun (50) to atomize and prepare powder;
step 4, when the electrode bar stock (100) is completely consumed, transferring the electrode bar stock (100) in the transition stock bin (50) into the electrode transmission chamber (10), and isolating the electrode transmission chamber (10) from the transition stock bin (50);
and 5, realizing continuous atomization powder preparation through the following actions 1 and 2:
action 1: opening a transition bin (50), filling a new electrode bar material (100) into the transition bin (50), closing the transition bin (50), independently vacuumizing the transition bin (50) and filling inert gas into the transition bin, enabling the protective atmosphere of the transition bin (50) to be the same as that of an electrode transmission chamber (10), and enabling the electrode transmission chamber (10) to be communicated with the transition bin (50);
and action 2: an electrode bar stock (100) in the electrode transmission chamber (10) is moved into the atomization chamber (101) at a preset speed and a preset rotating speed and is contacted with a plasma arc emitted by a plasma gun (102) to carry out atomization and powder making;
wherein, the action 1 and the action 2 in the step 5 are synchronously performed, and the time of the action 1 is longer than that of the action 2;
and (5) repeating the step (4) and the step (5) to realize continuous atomization powder preparation.
16. The method of claim 15, wherein the electrode rod material (100) is transferred from the electrode driving chamber (10) to the atomizing chamber (101) by a pushing member (30), and when a new electrode rod material (100) is transferred from the transition bin (50) to the electrode driving chamber (10), the pushing member (30) is disposed to be offset from the axis of the electrode rod material (100) to avoid the moving track of the electrode rod material (100).
CN202210837922.2A 2022-07-16 2022-07-16 Continuous feeding mechanism for rotary electrode atomization powder preparation, powder preparation equipment and powder preparation method Active CN114951674B (en)

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