CN114469825A - Bath foam special for pets and preparation method thereof - Google Patents
Bath foam special for pets and preparation method thereof Download PDFInfo
- Publication number
- CN114469825A CN114469825A CN202111682941.4A CN202111682941A CN114469825A CN 114469825 A CN114469825 A CN 114469825A CN 202111682941 A CN202111682941 A CN 202111682941A CN 114469825 A CN114469825 A CN 114469825A
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- extract
- pets
- bath foam
- special
- plant
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Classifications
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- A—HUMAN NECESSITIES
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Abstract
The invention discloses bath foam special for pets and a preparation method thereof, and relates to the technical field of pet products. The special bath foam for pets comprises the following raw material components in parts by mass: 15-30% of plant surfactant, 8-20% of Chinese herbal medicine plant acarus killing agent, 2-4% of complex enzyme preparation, 2-4% of hair softening and fluffing agent, 2-8% of biological enzyme stabilizer, 1-3% of thickening stabilizer, 0.5-2% of preservative and the balance of deionized water; wherein the compound enzyme agent comprises at least two of lipase, protease, cellulase and lysozyme. According to the invention, the plant surfactant and the complex enzyme preparation are compounded, and the two are synergistic, so that various stains on the pet can be quickly and efficiently cleaned; the special bath liquid for pets can sterilize and expel insects by adding the Chinese herbal medicine plant miticide; in addition, the plant surfactant and the Chinese herbal medicine plant acaricide are both plant sources, so that the safety is high, the components are mild and non-irritating, and the special bath foam for pets is safe, non-toxic and harmless to lick.
Description
Technical Field
The invention relates to the technical field of pet products, in particular to bath foam special for pets and a preparation method thereof.
Background
With the economic development and income level rising, the raised pets become a kind of spiritual trusting, many people regard the pets as family members, pet owners shift their own life style to favorite pets, and the demand upgrade and consumption upgrade are formed in the basic consumption field, so that in the process of raising the pets, the clean products of the pets pay more and more attention to the comfort, safety and functionality of the products.
At present, a plurality of pet bath products are available, in order to enable the pet bath products to have a cleaning effect, a surfactant is generally added into the bath products, and the selected surfactant is a chemical agent such as sodium dodecyl sulfate, ethoxylated alkyl sulfate and the like, and the chemical agent has large irritation to eyes and skin of pets and is easy to cause the discomfort and diseases of the pets. In addition, most bath products are mainly cleaned, rarely have a sterilization function, have the sterilization function, mostly contain chemical active ingredients, and have low sterilization efficiency, toxic, corrosive and pungent smells, certain damage to skin and hair, incapability of eliminating peculiar smell, and high irritation to pets, and are easy to cause dislike and diseases of pets.
Disclosure of Invention
The invention mainly aims to provide a special bath foam for pets and a preparation method thereof, and aims to provide the special bath foam for pets, which has good cleaning effect, can sterilize and expel insects, and has no irritation to component temperature.
In order to achieve the purpose, the invention provides a special bath foam for pets, which comprises the following raw material components in percentage by mass:
15-30% of plant surfactant, 8-20% of Chinese herbal medicine plant acarus killing agent, 2-4% of complex enzyme preparation, 2-4% of hair softening and fluffing agent, 2-8% of biological enzyme stabilizer, 1-3% of thickening stabilizer, 0.5-2% of preservative and the balance of deionized water;
wherein the compound enzyme agent comprises at least two of lipase, protease, cellulase and lysozyme.
Optionally, the plant surfactant comprises saponin extract of Gleditsia sinensis and pericarp extract of Sapindus mukorossi.
Optionally, the mass ratio of the gleditschia horrida saponin extract to the soapberry peel extract is 1-2: 1 to 4.
Optionally, the herbal plant mie xiaoling comprises at least one of stemona root extract, cnidium fruit extract, zanthoxylum bungeanum fruit extract, lilac flower extract, mint extract, ginger root extract and motherwort herb extract.
Optionally, the Chinese herbal medicine plant mie ling is the stemona tuberosa root extract, cnidium monnieri fruit extract, zanthoxylum bungeanum fruit extract, syringa caryophyllata flower extract, mint extract, ginger root extract and leonurus japonicus extract;
the mass ratio of the stemona sessilifolia root extract to the cnidium monnieri fruit extract to the zanthoxylum bungeanum fruit extract to the syringia flower extract to the mint extract to the ginger root extract to the motherwort herb extract is 7-9: 3.5-4.5: 3.5-4.5: 3: 3: 3: 2.
optionally, the complex enzyme preparation is obtained by compounding the lipase, the protease, the cellulase and the lysozyme, and the mass ratio of the lipase, the protease, the cellulase and the lysozyme is 0.5-1.2: 0.8-2.5: 0.1-0.5: 0.05 to 0.5; and/or the presence of a gas in the gas,
the hair softening and fluffing agent comprises at least one of bionic phospholipid, hair care grease, hydrolyzed wheat protein, guar gum and polyquaternium-7.
Optionally, the bio-enzyme stabilizer includes a metal compound, a saccharide, and a polyol.
Optionally, the metal compound comprises at least one of ferrous sulfate, calcium chloride, magnesium sulfate, zinc sulfate, and potassium chloride; and/or the presence of a gas in the gas,
the saccharide comprises at least one of glucose, trehalose and sucrose; and/or the presence of a gas in the gas,
the polyhydric alcohol comprises at least one of glycerol, 1, 3-propylene glycol, tripropylene glycol, sorbitol, mannitol and polyethylene glycol.
Optionally, the thickening stabilizer comprises at least one of PEG-120 methyl glucose dioleate, cocamide methyl MEA, polyethylene glycol distearate, and fatty alcohol polyoxyethylene ether acrylic acid copolymer; and/or the presence of a gas in the gas,
the antiseptic comprises cason and phenoxyethanol.
Based on the above purpose, the invention also provides a preparation method of the bath foam special for pets, which comprises the following steps:
dissolving a plant surfactant in deionized water to obtain a mixed solution;
adding the Chinese herbal medicine acarus-killing pesticide into the mixed solution, and uniformly stirring at 50-60 ℃ to obtain a mixed solution;
under the condition of stirring, sequentially adding a thickening stabilizer, a hair softening and fluffing agent and a biological enzyme stabilizer into the mixed solution to obtain a solution A;
and cooling the solution A to 33-37 ℃, and sequentially adding a complex enzyme preparation and a preservative into the solution A under the stirring condition to obtain the special bath foam for pets, wherein the pH value of the bath foam is 6.5-7.8, and the viscosity of the bath foam is 3500-8000 cps.
According to the technical scheme provided by the invention, the special bath foam for pets is prepared by taking a plant surfactant, a Chinese herbal medicine plant acarus killing agent, a complex enzyme preparation, a hair softening and fluffing agent, a biological enzyme stabilizer, a thickening stabilizer, a preservative and deionized water as raw materials, and the plant surfactant and the complex enzyme preparation are compounded to realize synergistic interaction, so that various stains on pets can be quickly and efficiently cleaned; the special bath liquid for pets can sterilize and expel insects by adding the Chinese herbal medicine plant miticide; in addition, the plant surfactant and the Chinese herbal medicine plant acaricide are both plant sources, so that the safety is high, the components are mild and non-irritating, and the special bath foam for pets is safe, non-toxic and harmless to lick.
Detailed Description
In order to make the objects, technical solutions and advantages of the embodiments of the present invention clearer, the technical solutions in the embodiments of the present invention will be clearly and completely described below. The examples, in which specific conditions are not specified, were conducted under conventional conditions or conditions recommended by the manufacturer. The reagents or instruments used are not indicated by the manufacturer, and are all conventional products available commercially.
In addition, the meaning of "and/or" appearing throughout includes three juxtapositions, exemplified by "A and/or B" including either A or B or both A and B. In addition, technical solutions between various embodiments may be combined with each other, but must be realized by a person skilled in the art, and when the technical solutions are contradictory or cannot be realized, such a combination should not be considered to exist, and is not within the protection scope of the present invention. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
The invention provides bath foam special for pets, and aims to provide the bath foam special for pets, which can sterilize and expel insects and has no irritation to component temperature. In one embodiment, the bath foam special for pets comprises the following raw material components in parts by mass:
15-30% of plant surfactant, 8-20% of Chinese herbal medicine plant acarus killing agent, 2-4% of complex enzyme preparation, 2-4% of hair softening and fluffing agent, 2-8% of biological enzyme stabilizer, 1-3% of thickening stabilizer, 0.5-2% of preservative and the balance of deionized water.
Wherein the compound enzyme agent comprises at least two of lipase, protease, cellulase and lysozyme. At least two of the substances are selected, so that the complex enzyme preparation can be added to cooperate with the plant surfactant for synergism, and the cleaning effect is good. Meanwhile, the addition amount of the plant surfactant and the complex enzyme preparation is designed, so that the synergistic effect is better.
According to the technical scheme provided by the invention, the special bath foam for pets is prepared by taking a plant surfactant, a Chinese herbal medicine plant acarus killing agent, a complex enzyme preparation, a hair softening and fluffing agent, a biological enzyme stabilizer, a thickening stabilizer, a preservative and deionized water as raw materials, and the plant surfactant and the complex enzyme preparation are compounded to realize synergistic interaction, so that various stains on pets can be quickly and efficiently cleaned; the special bath liquid for pets can sterilize and expel insects by adding the Chinese herbal medicine plant miticide; in addition, the plant surfactant and the Chinese herbal medicine acarus-killing pesticide are both plant sources, so that the safety is high, and the components are mild and are not irritant.
The present invention does not limit the specific choice of the plant surfactant as long as it can function as a surfactant, and preferably, the plant surfactant includes Gleditsia sinensis saponin extract and soapberry pericarp extract.
The Gleditsia sinensis saponin extract is natural product of Gleditsia sinensis seed of Leguminosae, and has the basic structure of combined natural product formed by triterpene aglycon, structural sugar and organic acid, wherein the aglycon ligand structure belongs to pentacyclic triterpene compounds, and the most main is five glycoside compounds. The gleditschia horrida saponin molecule consists of hydrophilic glycosyl and hydrophobic saponin coordination group, so that the gleditschia horrida saponin has various surface active properties of emulsification, dispersion, wetting, decontamination, foaming and the like, and is a nonionic natural surfactant with good performance. In addition, the gleditschia horrida saponin also has the obvious functions of resisting inflammation, diminishing inflammation, eliminating phlegm, relieving pain, killing bacteria, killing insect and the like.
The soapberry (Sapindus MUKOROSSI) peel extract contains rich glycoside substances, mainly triterpenoid saponins (I) and sesquiterpene glycosides (II), has strong surface activity, is a natural nonionic surfactant, has strong decontamination capability, is easy to degrade, has no harmful residue, is easy to wash, has rich foam, fine hand feeling and strong detergency, and has the characteristics of antibiosis, environmental protection, no public nuisance, rich foam, dirt removal, antibiosis, beauty treatment, skin tendering, freckle removal, acne removal, skin disease prevention and treatment and the like; meanwhile, the hair conditioner contains a large amount of natural nutrition conditioning substances, has no stimulation to hair and skin, and has the effects of conditioning, removing dandruff, relieving itching and the like.
According to the invention, the gleditsia sinensis saponin extract and the soapberry peel extract are compounded, so that the plant surfactant has a good cleaning effect, low foam and easy cleaning, and has a certain sterilization and insect expelling effect; in addition, the substances are easy to degrade, and the degraded substances are safe and environment-friendly.
Preferably, the mass ratio of the gleditschia horrida saponin extract to the soapberry peel extract is 1-2: 1-4, so that the cleaning effect of the compounded plant surfactant is better.
The invention does not limit the specific source of the gleditschia horrida saponin extract, and the gleditschia horrida saponin extract can be obtained by purchasing or self-preparing, and when the gleditschia horrida saponin extract is prepared by self-preparing, the steps are as follows: pulverizing Gleditsia sinensis seed, water extracting (ultrasonic assisted extraction), sequentially centrifuging, hydrolyzing with enzyme method, decolorizing, centrifuging, evaporating, concentrating, and drying to obtain Gleditsia sinensis saponin extract.
The invention also does not limit the concrete source of the soapberry peel extract, and the soapberry peel extract can be obtained by purchase or prepared by self, and when prepared by self, the preparation method is as follows: 1. selecting soapberry peel, drying at 60 ℃, and crushing for later use; 2. soaking the soapberry peel powder in methanol, and extracting with ultrasonic wave; 3. reducing pressure, concentrating and separating methanol to obtain soapberry peel extract; 4. freezing the extractive solution at 4 deg.C for 24 hr, cooling for crystallization, and centrifuging to obtain Sapindus mukurossi pericarp extract.
In this embodiment, the gleditsia sinensis saponin extract and the soapberry peel extract are extracted by using an ultrasonic-assisted extraction technology, so that the solvent can be more easily permeated into the plant under the ultrasonic condition, the effective components can be completely dissolved in the solvent, the extraction is more thorough, and the active components of the extracting solution are higher and more effective.
The special bath foam for pets has the functions of sterilization and insect expelling by adding the Chinese herbal medicine plant miticide. In this embodiment, the Chinese herbal medicine plant miticide includes at least one of stemona root extract, cnidium fruit extract, zanthoxylum bungeanum fruit extract, clove flower extract, mint extract, ginger root extract and motherwort herb extract, so that the Chinese herbal medicine plant miticide has mild and non-irritant components and good effects of killing and expelling parasites.
In a preferred embodiment, the Chinese herbal medicine plant mie xian ling is composed of the stemona sessilifolia root extract, the cnidium monnieri fruit extract, the zanthoxylum bungeanum fruit extract, the syringa flos extract, the mint extract, the ginger root extract and the motherwort herb extract, and the mass ratio of the stemona sessilifolia root extract, the cnidium monnieri fruit extract, the syringa flos extract, the mint extract, the ginger root extract and the motherwort herb extract is 7-9: 3.5-4.5: 3.5-4.5: 3: 3: 3:2, preferably, the mass ratio is 8: 4: 4: 3: 3: 3: 2.
the Chinese herbal medicine plant miticide can be obtained by purchasing or self-preparing, and when the self-preparing is carried out, the steps are as follows: (1) sorting: removing impurities and bad parts such as old rot, mildew or insect eating in medicinal materials; (2) cleaning and airing: rinsing the medicinal materials with clear water, and drying in the sun; (3) sterilization and disinfection: sterilizing the dried medicinal materials with ultraviolet light; (4) and (3) crushing treatment: putting the sterilized medicinal materials into a pulverizer to perform pulverizing treatment until the medicinal materials are sieved by a 50-mesh sieve; (5) primary soaking: soaking the crushed medicinal materials into white vinegar for 12 hours, wherein the mass ratio of the medicinal materials to the white vinegar is 1: 2-1: 3; boiling the soaked mixed solution with strong fire, and stewing with slow fire until the white vinegar is boiled to be dry; (6) secondary soaking: soaking the medicinal materials after boiling the white vinegar for 8 hours by using deionized water as a solvent, wherein the dosage of the solvent is 6-8 times of that of the medicinal materials, and the extraction temperature is 65 ℃; (7) concentration: precipitating the obtained medicinal liquid for 5 hr, filtering, and concentrating the filtrate to obtain extract with relative density of 1.2-1.35; (8) preparing a product: and (3) placing the prepared extract into a freezer at the temperature of 50 ℃ below zero for freeze drying for 0.5 to 5 hours, and performing vacuum drying to obtain the plant extract.
In order to enable the cleaning effect of the bath foam special for pets to be better, in a preferred embodiment, the compound enzyme preparation is prepared by compounding the lipase, the protease, the cellulase and the lysozyme, and the mass ratio of the lipase, the protease, the cellulase and the lysozyme is 0.5-1.2: 0.8-2.5: 0.1-0.5: 0.05 to 0.5. In addition, the lysozyme can also play a certain role in sterilization.
The enzymes in the complex enzyme preparation are easy to inactivate, and in order to enable the enzymes in the complex enzyme preparation to fully exert the functions, the special bath foam for pets is added with a biological enzyme stabilizer. In this embodiment, the bio-enzyme stabilizer includes a metal compound, a saccharide, and a polyol. In a preferred embodiment, the biological enzyme stabilizer is composed of metal compounds, saccharides and polyols, so that the enzyme is stabilized well.
Wherein the metal compound comprises at least one of ferrous sulfate, calcium chloride, magnesium sulfate, zinc sulfate and potassium chloride; and/or, the saccharide comprises at least one of glucose, trehalose and sucrose; and/or the polyol comprises at least one of glycerol, 1, 3-propanediol, propylene glycol, tripropylene glycol, sorbitol, mannitol and polyethylene glycol.
In a preferred embodiment, the metal compound is calcium chloride, the saccharide is glucose, and the polyol is a mixture of glycerol and polyethylene glycol. Further, the polyethylene glycol (PEG) has a molecular weight of 1000.
The addition of the hair softening and fluffing agent enables the special bath foam for pets to have the effect of hair maintenance, and enables the hair of pets to be easily combed and smooth. In this embodiment, the hair softening and relaxing agent comprises at least one of bionic phospholipid, hair care grease, hydrolyzed wheat protein, guar gum and polyquaternium-7, and the substances are selected to achieve a good hair care effect and make the components of the bath foam special for pets mild and non-irritant.
By adding the thickening stabilizer, the prepared special bath foam for pets is stable in system and is not easy to be turbid, precipitate or delaminate. In this embodiment, the thickening stabilizer includes at least one of PEG-120 methyl glucose dioleate, cocamide methyl MEA, polyethylene glycol distearate, and fatty alcohol polyoxyethylene ether acrylic acid copolymer.
Preferably, the thickening stabilizer is formulated from PEG-120 methyl glucose dioleate and cocamide methyl MEA. Further, the molecular weight of the polyethylene glycol distearate was 6000.
In this embodiment, the preservative comprises cason and phenoxyethanol. Preferably, the preservative is prepared by compounding the cason and the phenoxyethanol, so that the prepared special bath foam for pets has longer preservation time.
The special bath foam for pets provided by the invention can be used for most animals, and cats and dogs are taken as an example here in view of the largest pet market in scale. The thickness of cat skin is 0.4-2 mm, and the thickness of dog skin is 0.5-5 mm (the thickness of human skin is 0.5-4 mm); the skin tissue structure of the cats and dogs is simple, and 3-5 layers (10-15 layers) of the epidermis layer are adopted, namely, the skin tissue structure of the cats and dogs is single, fragile and easy to damage; meanwhile, the pH value of the skin of the cat and the dog is about 7.0. The pH value of the bath foam special for a plurality of current pets is 5.5-6.4, the difference between the pH value of the bath foam and the pH value of skin of cats and dogs is large, the skin sebaceous glands of the cats and dogs are easily damaged by using the current bath foam, the protection force of the cats and dogs is reduced, the cats and dogs are easily susceptible to skin diseases, and the hairs of the cats and dogs are rough and dull or even fall off. In the embodiment, through the design of the components and the proportion of the bath foam special for pets, the pH value of the prepared bath foam special for pets is about 6.5-7.8, and is closer to the pH value of pet skin, so that the bath foam special for pets is mild and does not irritate the pet skin.
In addition, cats and dogs tend to lick their fur, and thus the residual components of the care product are also important to the safety of pets. The special substances are selected, so that the selected natural raw materials are high in safety and easy to degrade, and the special bath foam for pets is safe, non-toxic and harmless to lick.
In conclusion, the special bath foam for pets, provided by the invention, has the advantages that through the design of the raw material components and the proportion, the pH of the product is 6.5-7.8, is closer to the pH of the skin of pets, and is mild and non-irritating to the skin of pets; the natural green surfactant is compounded with the biological enzyme to play a synergistic role, quickly and efficiently remove various stains such as proteins, fats, saccharides, sweat, excrement and the like on the pet body, and play a certain role in sterilization and insect expelling; on the basis of cleaning, the theory formula principle of 'monarch, minister, assistant and guide' of the traditional Chinese medicine is followed, and the Chinese herbal medicine plant mite-killing and mite-expelling agent is added to prevent and treat demodex, sterilize and expel insects; in addition, the special bath foam for the pets, which is prepared from natural raw materials which are high in safety and easy to degrade, does not contain alcohol, a synthetic spice masking agent and a chemical disinfectant, and is safe, non-toxic and harmless to lick.
Further, the invention also provides a preparation method of the special bath foam for pets, which comprises the following steps:
s10, dissolving the plant surfactant in deionized water to obtain a mixed solution;
s20, adding the Chinese herbal medicine acarus killing agent into the mixed solution, and uniformly stirring at 50-60 ℃ to obtain a mixed solution;
s30, sequentially adding a thickening stabilizer, a hair softening and fluffing agent and a biological enzyme stabilizer into the mixed solution under the stirring condition to obtain a solution A;
s40, cooling the solution A to 33-37 ℃, and sequentially adding a complex enzyme preparation and a preservative into the solution A under the stirring condition to obtain the special bath foam for pets, wherein the pH value of the bath foam is 6.5-7.8, and the viscosity of the bath foam is 3500-8000 cps.
In one embodiment, the bath foam special for pets is prepared by the following steps: adding 50% of the total mass of the deionized water into the batching pot, and slowly starting a stirrer, wherein the stirring frequency is 15-30 r/min; putting the plant surfactant into a mixing pot, and stirring until the plant surfactant is completely dissolved; putting the Chinese herbal medicine plant miticide into a mixing pot, starting a heater to heat to 50-60 ℃, stirring at the frequency of 45-65 r/min, and stirring until the materials are uniformly mixed; adding the thickening stabilizer into a mixing pot, and stirring until the thickening stabilizer is completely dissolved uniformly; putting the hair softening and fluffing agent into a mixing pot, and stirring until the hair softening and fluffing agent is uniformly mixed; adding the biological enzyme stabilizer into a proportioning pot, and stirring until the biological enzyme stabilizer and the proportioning pot are uniformly mixed; adding the rest deionized water, and starting cooling; when the temperature of the materials in the pot is reduced to be lower than 35 ℃, accurately weighing the complex enzyme preparation, putting the complex enzyme preparation into a proportioning pot, and reducing the stirring speed, wherein the stirring frequency is 10-20 r/min; putting the preservative into a mixing pot, and stirring until the preservative is uniformly mixed to obtain the special bath foam for the pets, wherein the bath foam is light yellow transparent liquid, the pH value of the bath foam is 6.5-7.8, and the viscosity of the bath foam is 3500-8000 cps.
The technical solutions of the present invention are further described in detail with reference to the following specific examples, which should be understood as merely illustrative and not limitative.
In the following examples, some of the raw material source information used is as follows:
in the hair relaxer: the bionic phospholipid is British CRODA, and has a product trade name of SAPILUB PTC and a chemical name of cocamidopropyl PG-dimethyl ammonium chloride phosphate; the hair care oil is CROMOLLITE SCE-LQ- (MH) which is a product of British CRODA and has a chemical name of di (PPG-2 myristyl polyether-10) adipate; hydrolyzed wheat protein is Chongqing Haiman Biochemical technology Co., Ltd, chemical name is undecylenoylHydrolyzing wheat protein potassium; guar gum is a product of Soervin and has the trade name of
Excel, chemical name guar hydroxypropyl trimonium chloride; polyquaternary ammonium salt-7 is a product of Solvay and has the trade name of
550SBF。
In the thickening agent: the manufacturer of PEG-120 methyl glucose dioleate is Luoborun, under the trade name Glutamate DOE-120; the manufacturer of cocoamide methyl MEA is Guangzhou Huayun Fine chemical Co., Ltd, under the trade name CMMEA.
In the preservative: the commercial name of cason is mulberry K15(SupGuard K15); the trade name of phenoxyethanol is
PE 9010。
Example 1
The special bath foam for pets comprises the following raw material components in parts by mass:
15% of plant surfactant, wherein the plant surfactant is obtained by compounding a gleditsia sinensis saponin extract and a soapberry peel extract in a mass ratio of 2: 1;
15% of a Chinese herbal medicine plant miticide, wherein the Chinese herbal medicine plant miticide is prepared from stemona root extract, fructus cnidii extract, zanthoxylum fruit extract, clove flower extract, mint extract, ginger root extract and motherwort extract according to the mass ratio of 8: 4: 4: 3: 3: 3:2, compounding to obtain;
2% of a complex enzyme preparation, wherein the complex enzyme preparation is prepared by compounding lipase, protease, cellulase and lysozyme according to the mass ratio of 1:0.8:0.1: 0.1;
2% of hair softening and fluffing agent, wherein the hair softening and fluffing agent is prepared by compounding bionic phospholipid, hair care grease and hydrolyzed wheat protein according to the mass ratio of 0.6:0.4: 1;
4% of a biological enzyme stabilizer, wherein the biological enzyme stabilizer is obtained by compounding calcium chloride, glucose, glycerol and polyethylene glycol according to the mass ratio of 0.01:1:8: 2;
thickening stabilizer 3%, specifically PEG-120 methyl glucose dioleate;
0.75% of preservative, wherein the preservative is prepared by compounding cason and phenoxyethanol according to the mass ratio of 0.1: 0.65;
and 58.25% of deionized water.
Example 2
The special bath foam for pets comprises the following raw material components in parts by mass:
23% of plant surfactant, wherein the plant surfactant is prepared from the following components in a mass ratio of 1.875: 1, compounding the gleditschia horrida saponin extract and the soapberry peel extract;
the Chinese herbal medicine plant miticide is 20 percent, wherein the Chinese herbal medicine plant miticide is prepared from stemona root extract, fructus cnidii extract, zanthoxylum fruit extract, clove flower extract, mint extract, ginger root extract and motherwort extract according to the mass ratio of 8: 4: 4: 3: 3: 3:2, compounding to obtain;
2.35% of a complex enzyme preparation, wherein the complex enzyme preparation is prepared from lipase, protease, cellulase and lysozyme according to a mass ratio of 0.5: 1.5: 0.1: 0.25 is obtained by compounding;
3% of hair softening and fluffing agent, wherein the hair softening and fluffing agent is prepared by compounding bionic phospholipid, hair care grease and hydrolyzed wheat protein according to the mass ratio of 1:1: 1;
8% of a biological enzyme stabilizer, wherein the biological enzyme stabilizer is obtained by compounding calcium chloride, glucose, glycerol and polyethylene glycol according to the mass ratio of 0.01:5:2: 5;
thickening stabilizer 1%, specifically PEG-120 methyl glucose dioleate;
1.65% of preservative, wherein the preservative is prepared by compounding cason and phenoxyethanol according to the mass ratio of 0.3: 1.35;
and 41% of deionized water.
Example 3
The special bath foam for pets comprises the following raw material components in parts by mass:
25% of a plant surfactant, wherein the plant surfactant is obtained by compounding a Chinese honeylocust saponin extract and a soapberry pericarp extract in a mass ratio of 1: 4;
the Chinese herbal medicine plant miticide is 8 percent, wherein the Chinese herbal medicine plant miticide is prepared from stemona root extract, fructus cnidii extract, zanthoxylum fruit extract, clove flower extract, mint extract, ginger root extract and motherwort herb extract according to the mass ratio of 8: 4: 4: 3: 3: 3:2, compounding to obtain;
4% of a complex enzyme preparation, wherein the complex enzyme preparation is prepared by compounding lipase, protease, cellulase and lysozyme according to the mass ratio of 1:2.5:0.35: 0.05;
4% of hair softening and fluffing agent, wherein the hair softening and fluffing agent is prepared by compounding bionic phospholipid, hair care grease and polyquaternium-7 according to the mass ratio of 1.5:1: 1.5;
2% of a biological enzyme stabilizer, wherein the biological enzyme stabilizer is obtained by compounding calcium chloride, glucose, glycerol and polyethylene glycol according to the mass ratio of 0.05:5:2: 5;
2% of thickening stabilizer, specifically polyethylene glycol distearate;
2% of preservative, wherein the preservative is obtained by compounding cason and phenoxyethanol according to the mass ratio of 0.15: 1.85;
and 53 percent of deionized water.
Example 4
The special bath foam for pets comprises the following raw material components in parts by mass:
30% of plant surfactant, wherein the plant surfactant is obtained by compounding a small fruit gleditsia sinensis saponin extract and a soapberry peel extract in a mass ratio of 1: 1;
10% of a Chinese herbal medicine plant miticide, wherein the Chinese herbal medicine plant miticide is prepared from stemona root extract, fructus cnidii extract, zanthoxylum fruit extract, clove flower extract, mint extract, ginger root extract and motherwort herb extract according to the mass ratio of 8: 4: 4: 3: 3: 3:2, compounding to obtain;
3.4% of a complex enzyme preparation, wherein the complex enzyme preparation is obtained by compounding lipase, protease, cellulase and lysozyme according to the mass ratio of 1.2:1.2:0.5: 0.5;
2.8% of hair softening and fluffing agent, wherein the hair softening and fluffing agent is prepared by compounding bionic phospholipid, guar gum and polyquaternium-7 according to the mass ratio of 1.5:0.3: 1;
6% of a biological enzyme stabilizer, wherein the biological enzyme stabilizer is obtained by compounding calcium chloride, glucose, glycerol and polyethylene glycol according to the mass ratio of 0.05:2:6: 2;
3% of thickening stabilizer, wherein the thickening stabilizer is obtained by compounding polyethylene glycol distearate and cocamide methyl MEA according to the mass ratio of 2: 1;
0.5% of preservative, wherein the preservative is prepared by compounding cason and phenoxyethanol according to the mass ratio of 0.08: 0.42;
44.3 percent of deionized water.
Example 5
Except that the Chinese herbal medicine plant of the acaricide is replaced by the Chinese herbal medicine plant of stemona tuberosa root extract, cnidium fruit extract and zanthoxylum fruit extract according to the mass ratio of 8: 4: 4, and the rest components and the mixture ratio are the same as those of the embodiment 1.
Example 6
Except that the Chinese herbal medicine miticide is replaced by compounding radix stemonae leaf extract, fructus cnidii extract, flos caryophylli extract and mint extract according to the mass ratio of 3:2:4:2, and the other components and the proportion are the same as those in the embodiment 1.
Example 7
(1) The formula of the bath foam special for pets is the same as that of the example 1;
(2) adding 50% of the total mass of the deionized water into the batching pot, and slowly starting a stirrer, wherein the stirring frequency is 15-30 r/min; putting the plant surfactant into a mixing pot, and stirring until the plant surfactant is completely dissolved; putting the Chinese herbal medicine plant miticide into a mixing pot, starting a heater to heat to 50-60 ℃, stirring at the frequency of 45-65 r/min, and stirring until the materials are uniformly mixed; adding the thickening stabilizer into a mixing pot, and stirring until the thickening stabilizer is completely dissolved uniformly; putting the hair softening and fluffing agent into a mixing pot, and stirring until the hair softening and fluffing agent is uniformly mixed; adding the biological enzyme stabilizer into a proportioning pot, and stirring until the biological enzyme stabilizer and the proportioning pot are uniformly mixed; adding the rest deionized water, and starting cooling; when the temperature of the materials in the pot is reduced to be lower than 35 ℃, accurately weighing the complex enzyme preparation, putting the complex enzyme preparation into a proportioning pot, and reducing the stirring speed, wherein the stirring frequency is 10-20 r/min; putting the preservative into a mixing pot, and stirring until the preservative is uniformly mixed to obtain the special bath foam for the pets, wherein the bath foam is light yellow transparent liquid, the pH value of the bath foam is 6.5-7.8, and the viscosity of the bath foam is 3500-8000 cps.
Example 8
The procedure of example 7 was followed except that the formulation of the pet-specific bath foam was replaced with the formulation of example 2.
Example 9
The procedure of example 7 was followed except that the formulation of the bath foam for pet use was replaced with the formulation of example 3.
Example 10
The procedure of example 7 was followed except that the formulation of the pet-specific bath foam was replaced with the formulation of example 4.
Example 11
The procedure of example 7 was followed except that the formulation of the bath foam for pet use was replaced with the formulation of example 5.
Example 12
The procedure of example 7 was followed except that the formulation of the bath foam for pet use was replaced with the formulation of example 6.
Example 13
(1) The formula is the same as that in example 1 except that the complex enzyme preparation is replaced by a compound of lipase and protease in a ratio of 1:2.
(2) Same as in step (2) in example 7.
Comparative example 1
Except that the plant surfactant was replaced with a chemical surfactant obtained by compounding sodium lauryl sulfate and ethoxylated alkyl sodium sulfate in a mass ratio of 4:1, the other components and the ratio and the preparation steps were the same as those in example 7.
Comparative example 2
Except that the plant surfactant was replaced with the conventional surfactants sodium fatty alcohol polyoxyethylene ether sulfate (AES) and sodium alpha-alkenyl sulfonate (AOS), wherein the mass ratio of AES to AOS was 3:2, and the remaining components, the compounding ratio, and the preparation steps were the same as those in example 7.
Comparative example 3
Except that no complex enzyme preparation was added, the addition amount of deionized water was changed to 60.25%, and the remaining components and the compounding ratio and the preparation steps were the same as those in example 7.
The bath liquids for exclusive use for pets prepared in examples 7 to 10 and comparative example 1 were subjected to the following tests:
firstly, safety test
1. The test method comprises the following steps: in vitro eye stimulation test-modified CAMVA method.
2. The evaluation method comprises the following steps:
(1) CAMVA stimulation responses include ghosting, engorgement, bleeding, etc., with phenomena and stimulation scores as given in Table 1 below.
TABLE 1CAMVA stimulus response phenomenon and its score table
(2) According to the scores in the table 1, 60 effective chick embryos are divided into 6 groups of 10 chick embryos, the irritation evaluation of the samples is recorded, the average value is calculated, and the irritation Average Score (AS) of the samples is obtained, wherein the correspondence between the AS value and the eye irritation of the samples is shown in the table 2 below.
TABLE 2 evaluation criteria for eye irritation
| Stimulation scoring | Stimulation level |
| 0≤AS＜0.5 | Has no irritation |
| 0.5≤AS＜1.5 | Micro-stimulation property |
| 1.5≤AS＜3.5 | Light irritation |
| 3.5≤AS＜5 | Moderate irritation |
| 5.0≤AS＜6.0 | Strong irritation/corrosion |
(3) The bath liquids for pet prepared in examples 7 to 10 and the bath liquids prepared in comparative examples 1 and 2 were applied to 6 groups of chick embryos (10 per group), respectively, and the results of the CAMVA test are shown in Table 3 below.
TABLE 3CAMVA test observations
Based on the evaluation criteria of tables 1 and 2 and the results of the CAMVA test observation of Table 3, the CAMVA test observation score table shown in Table 4 below was obtained.
TABLE 4 CAMVA test observation and scoring table
As can be seen from Table 4, the results of the in vitro eye irritation test show that the bath foam for pets, prepared in any example of the invention, has an average stimulation score on eyes of less than 1.1, and is micro-irritant, while the average stimulation scores on eyes of the bath foams prepared in comparative examples 1 and 2 are respectively 2.8 and 2.3, which are light irritants, and the invention shows that the components of the prepared bath foam for pets are mild, the stimulation is small, and the safety is high by selecting the plant surfactant.
It should be noted that, the preparation principles of examples 11-13 are similar to those of examples 7-10, and the pH values are also similar to 6.5-7.8, so the irritation is similar to that of examples 7-10, and further description is omitted here.
Secondly, testing the mite killing performance
1. The mite killing performance test is carried out according to the pesticide indoor pesticide effect test method for pesticide registration sanitation and evaluation part 2 of NY/T1151.2-2006: mite killing and expelling agent.
2. Mite killing test:
(1) taking 7 culture dishes, wherein 6 of the culture dishes are placed with the special bath foam for pets prepared in examples 7-12 according to the using method, the other culture dish is not placed with the bath foam to be tested as a control, and the upper edge of the inner wall of each culture dish is uniformly coated with a mixture of white oil and vaseline.
(2) 200 test insects are put in the center of each culture dish, 0.5g of mite feed is put in the center of each culture dish when 30min is needed, and then the culture dish is placed in a water-proof culture box.
(3) The dead mites were examined and recorded at 48 h.
3. Calculation of results
The mite control rate was calculated according to the formula and expressed as a percentage (%):
P＝R/N×100.................(1)
in the formula:
p-mite killing rate;
r is death number of tested insects;
n-number of tested insects.
When the death rate of the mites in the control group is less than 5%, no correction is needed; when the mite mortality of the control group is between 5% and 20%, the corrected mortality is calculated according to the following formula (2) and expressed as a percentage (%) ratio; when the death rate of the mites in the control group is more than 20 percent, the test is carried out again.
Pt＝(Py-Px)/(1-Px)..............(2)
In the formula:
pt-corrected mite kill rate;
py-mite eradication rate in test group;
px-control group acaricidal ratio.
Test insects: dust mites (Dermatophagoides farinae), male and female adults
The test conditions are as follows:
temperature: 25 ℃ plus or minus 2 DEG C
Relative humidity: 75% +/-5%
4. The results of the mite killing rate test are shown in table 5 below.
TABLE 5 Deacarid Rate test results
| Examples | Example 7 | Example 8 | Example 9 | Example 10 | Example 11 | Example 12 |
| Mite eradication Rate (%) | 96.8 | 98.2 | 97.6 | 99.1 | 95.6 | 95.4 |
5. The evaluation criteria of the acaricidal effect are shown in the following table 6.
TABLE 6 evaluation criteria for efficacy of miticidal agents
As can be seen from tables 5 and 6, the mite killing rate of the bath foam special for pets prepared in the embodiments 7 to 12 of the invention reaches B level, which shows that the prepared bath foam special for pets has good mite killing effect by designing the components and the proportion of the raw materials.
The mite killing rate of the special bath foam for pets in examples 7-10 is more than 96.8%, the mite killing rate of the special bath foam for pets prepared in examples 11 and 12 is 95.6% and 95.4% respectively, and the Chinese herbal medicine mite killing agent is prepared by compounding the stemona tuberosa root extract, the fructus cnidii extract, the zanthoxylum bungeanum fruit extract, the clove flower extract, the mint extract, the ginger root extract and the motherwort herb extract, and the mass ratio of the extract to the extract is 7-9: 3.5-4.5: 3.5-4.5: 3: 3: 3: and 2, the mite killing effect is better.
Third, antibacterial property test
The tests for killing of Escherichia coli (ATCC25922), Staphylococcus aureus (ATCC6538) and Candida albicans (ATCC10231) were carried out according to the test method of the sterilization specification (2002 edition) suspension quantitative sterilization test, and the test method of each example was: setting two identical culture dishes (containing culture medium), placing equal amount of test bacteria, taking one culture dish as an experimental group, adding special bath foam diluent for pets (the special bath foam diluent for pets is obtained by mixing the special bath foam for pets prepared in the embodiment with deionized water according to the mass ratio of 1: 5), taking the other culture dish as a control group (not adding the special bath foam for pets, and adding the deionized water with the same amount as the special bath foam diluent for pets of the experimental group), culturing for the same time under the same culture conditions, and then testing the viable bacteria of the control group and the experimental group respectively, wherein the action time is as follows: 5 min; the test results are given in table 7 below.
TABLE 7 antibacterial property test results
As can be seen from Table 7, the bath foam for pets prepared in examples 7-12 all showed a bactericidal rate of 99% or more against Escherichia coli, Staphylococcus aureus and Candida albicans, and thus the bath foam for pets provided by the present invention has an excellent antibacterial effect through the design of the components and the ratio. The sterilization rates of the examples 7 to 10 are higher than those of the examples 11 and 12, and the sterilization rate of the example 12 is higher than that of the example 11, which indicates that the Chinese herbal medicine miticide is prepared by compounding the stemona tuberosa root extract, the cnidium fruit extract, the zanthoxylum bungeanum fruit extract, the clove flower extract, the mint extract, the ginger root extract and the motherwort herb extract, and the mass ratio of the stemona tuberosa root extract, the cnidium fruit extract, the zanthoxylum bungeanum flower extract, the mint extract, the ginger root extract and the motherwort herb extract is 7 to 9: 3.5-4.5: 3.5-4.5: 3: 3: 3: and 2, the sterilization effect is better.
Fourth, testing detergency
The detergency test is carried out according to GB/T13174-2008 test of detergency and circulating washing performance of the detergent for clothing, the detergency test concentration is 0.1% (the bath foam is diluted by 1000 times), and the pH value is 6.8-7.2. JB-01-carbon black soiled cloth; JB-02-protein stain cloth; JB-03-sebum-stained cloth; and according to the standard parameter index requirements, the JB-01 test polluted cloth, the JB-02 test polluted cloth and the JB-03 test polluted cloth are all greater than or equal to the standard liquid and are qualified.
TABLE 8 detergency test results
| Detergency (%) JB-01 | Detergency (%) JB-02 | Detergency (%) JB-03 | |
| Standard liquid | 1.0 | 1.0 | 1.0 |
| Comparative example 1 | 1.9 | 1.5 | 1.7 |
| Comparative example 2 | 1.5 | 1.0 | 0.9 |
| Comparative example 3 | 1.8 | 1.3 | 1.1 |
| Example 7 | 2.2 | 1.8 | 2.0 |
| Example 8 | 2.1 | 1.6 | 2.5 |
| Example 9 | 2.5 | 2.2 | 1.9 |
| Example 10 | 2.1 | 3.2 | 2.0 |
| Example 13 | 2.0 | 1.6 | 1.8 |
As can be seen from Table 8, the pet-specific bath foam prepared in any of the examples has higher detergency on JB-01, JB-02 and JB-03 test soiled cloths than the comparative examples, which shows that the pet-specific bath foam has excellent cleaning effect through the design of the components and the proportion of the plant surfactant. Comparing the example 7 with the example 13, it can be seen that when the complex enzyme preparation is obtained by compounding lipase, protease, cellulase and lysozyme, the mass ratio of the lipase to the protease is 0.5-1.2: 0.8-2.5: 0.1-0.5: when the content of the surfactant is 0.05-0.5, the prepared special bath foam for pets has the best detergency.
Comparing the comparative example 3 with the example 7 of the invention, it can be seen that the complex enzyme preparation and the plant surfactant are used together to play an important role in improving the detergency, and if the complex enzyme preparation is lacked, the detergency is reduced, which indicates that the plant surfactant and the complex enzyme in the bath lotion special for pets of the invention have a synergistic interaction effect, and can rapidly and efficiently remove various stains such as proteins, fats, saccharides, sweat, excrement and the like on the pets.
The above is only a preferred embodiment of the present invention, and it is not intended to limit the scope of the invention, and various modifications and changes will occur to those skilled in the art. Any modification, equivalent replacement, or improvement made within the spirit and principle of the present invention shall be included in the scope of the present invention.
Claims (10)
1. The bath foam special for pets is characterized by comprising the following raw material components in parts by mass:
15-30% of plant surfactant, 8-20% of Chinese herbal medicine plant acarus killing agent, 2-4% of complex enzyme preparation, 2-4% of hair softening and fluffing agent, 2-8% of biological enzyme stabilizer, 1-3% of thickening stabilizer, 0.5-2% of preservative and the balance of deionized water;
wherein the compound enzyme agent comprises at least two of lipase, protease, cellulase and lysozyme.
2. The special bath foam for pets according to claim 1, wherein said plant surfactants comprise saponin extract of Gleditsia sinensis and pericarp extract of Sapindus mukorossi.
3. The bath foam special for pets as claimed in claim 2, wherein the mass ratio of the gleditschia horrida saponin extract to the soapberry peel extract is 1-2: 1 to 4.
4. The bath foam special for pets as claimed in claim 1, wherein the Chinese herbal medicine miticide comprises at least one of stemona tuberosa root extract, cnidium monnieri fruit extract, zanthoxylum bungeanum fruit extract, lilac flower extract, mint extract, ginger root extract and motherwort herb extract.
5. The bath foam special for pets as claimed in claim 4, wherein the Chinese herbal medicine acanthopanax senticosus is the stemona tuberosa root extract, the cnidium monnieri fruit extract, the zanthoxylum bungeanum fruit extract, the lilac flower extract, the mint extract, the ginger root extract and the motherwort herb extract;
the mass ratio of the stemona sessilifolia root extract to the cnidium monnieri fruit extract to the zanthoxylum bungeanum fruit extract to the syringia flower extract to the mint extract to the ginger root extract to the motherwort herb extract is 7-9: 3.5-4.5: 3.5-4.5: 3: 3: 3: 2.
6. the special bath foam for pets as claimed in claim 1, wherein the complex enzyme preparation is obtained by compounding the lipase, the protease, the cellulase and the lysozyme, and the mass ratio of the lipase, the protease, the cellulase and the lysozyme is 0.5-1.2: 0.8-2.5: 0.1-0.5: 0.05 to 0.5; and/or the presence of a gas in the gas,
the hair softening and fluffing agent comprises at least one of bionic phospholipid, hair care grease, hydrolyzed wheat protein, guar gum and polyquaternium-7.
7. The special purpose body wash for pet of claim 1, wherein said bio-enzyme stabilizer comprises metal compounds, saccharides and polyols.
8. The special pet bath according to claim 7, wherein said metal compound comprises at least one of ferrous sulfate, calcium chloride, magnesium sulfate, zinc sulfate, and potassium chloride; and/or the presence of a gas in the atmosphere,
the saccharide comprises at least one of glucose, trehalose and sucrose; and/or the presence of a gas in the gas,
the polyhydric alcohol comprises at least one of glycerol, 1, 3-propylene glycol, tripropylene glycol, sorbitol, mannitol and polyethylene glycol.
9. The special pet bath foam according to claim 1, wherein the thickening stabilizer comprises at least one of PEG-120 methyl glucose dioleate, cocamide methyl MEA, polyethylene glycol distearate, and fatty alcohol polyoxyethylene ether acrylic acid copolymer; and/or the presence of a gas in the gas,
the antiseptic comprises cason and phenoxyethanol.
10. The preparation method of the bath foam special for pets as claimed in any one of claims 1 to 9, characterized by comprising the following steps:
dissolving a plant surfactant in deionized water to obtain a mixed solution;
adding the Chinese herbal medicine acarus-killing pesticide into the mixed solution, and uniformly stirring at 50-60 ℃ to obtain a mixed solution;
under the condition of stirring, sequentially adding a thickening stabilizer, a hair softening and fluffing agent and a biological enzyme stabilizer into the mixed solution to obtain a solution A;
and cooling the solution A to 33-37 ℃, and sequentially adding a complex enzyme preparation and a preservative into the solution A under the stirring condition to obtain the special bath foam for pets, wherein the pH value of the bath foam is 6.5-7.8, and the viscosity of the bath foam is 3500-8000 cps.
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| CN116115517A (en) * | 2022-11-28 | 2023-05-16 | 媞颂日化用品(广州)有限公司 | Cat tail oil-dispelling composition containing biological ferment and application thereof |
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| CN114469825B (en) | 2023-12-12 |
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