CN103947967B - Double-colored dark red fruit matrimony vine sheet and preparation method thereof - Google Patents
Double-colored dark red fruit matrimony vine sheet and preparation method thereof Download PDFInfo
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- CN103947967B CN103947967B CN201410159905.3A CN201410159905A CN103947967B CN 103947967 B CN103947967 B CN 103947967B CN 201410159905 A CN201410159905 A CN 201410159905A CN 103947967 B CN103947967 B CN 103947967B
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- matrimony vine
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- dark red
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Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23P—SHAPING OR WORKING OF FOODSTUFFS, NOT FULLY COVERED BY A SINGLE OTHER SUBCLASS
- A23P20/00—Coating of foodstuffs; Coatings therefor; Making laminated, multi-layered, stuffed or hollow foodstuffs
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Mycology (AREA)
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Preparation Of Fruits And Vegetables (AREA)
- Medicinal Preparation (AREA)
Abstract
The present invention relates to a kind of double-colored dark red fruit matrimony vine sheet, it is with black fruit lyceum and haw matrimony vine raw material, to squeeze the juice through comprising, homogeneous, freeze drying, pulverizing and compressing tablet processing step prepare, and in all processing steps, all do not add any auxiliary material than water.The present invention adopts low-temperature grinding skilled worker skill, black fruit lyceum and haw matrimony vine cell membrane are broken, intracellular moisture, oil content and active ingredient come out all completely, make minuteness particle surface presentation half moisture state, this structure not only can make nutrition distribution pattern homogenising wherein, is conducive to improving food utilization; And combine low-temperature grinding and low temperature tablet forming technique, when not adding the binding agents such as starch, can obtain the matrimony vine sheet that hardness is suitable, thus without the need to adding any auxiliary material in described matrimony vine sheet, not only remain the complete local flavor of matrimony vine, also make food more safely with reliable.
Description
Technical field
The present invention relates to technical field prepared by food, more particularly, the present invention relates to a kind of double-colored dark red fruit matrimony vine sheet and preparation method thereof.
Background technology
Fruit of Chinese wolfberry another name FRUCTUS LYCII BARBARI, white thorn, mountain matrimony vine etc. are the ripening fruits of matrimony vine of solanaceae plant.Matrimony vine has consequence in China's traditional medicine, and its medical value enjoys the high praise of ancient Chinese medicine doctor, is traditional rare traditional Chinese medicine and tonic food.Containing several amino acids in matrimony vine, and containing special dietary compositions such as betaine, beautiful another name for Sichuan Province flavine, physalins.Modern study analysis shows, contained by matrimony vine, nutrition is very abundant, containing crude protein 4.49 grams in every hectogram FRUCTUS LYCII, crude fat 2.33 grams, 9.12 grams, carbohydrate, carotenoid 96 milligrams, thiamine 0.053 milligram, 0.137 milligram, riboflavin, 19.8 milligrams, ascorbic acid, betaine 0.26 milligram, also containing the abundant element such as potassium, sodium, calcium, magnesium, iron, copper, manganese, zinc, and 22 seed amino acid and multivitamin, there is abundant nutritive value and special medical care effect.
Black fruit lyceum (LyciumruthenicumMurr) is the perennial shrub plant of Solanaceae Lycium, black fruit lyceum taste is sweet, property is put down, detect through science, its calcium, iron, niacin content are respectively 2.3,4.6,16.7 times of haw matrimony vine, and especially OPC (OPC) exceedes blueberry (black fruit lyceum is containing OPC3690mg/100g; Blueberry is containing OPC330 ~ 3380mg/100g); In addition, black fruit lyceum contains abundant aliphatic acid, protein, free amino acid, mineral element and polysaccharide etc., and being conducive to human body directly absorbs, and the content of its procyanidins, up to 3.45%, is the plant berry that natural procyanidins content is the highest.Black fruit lyceum finds the wild fruit that OPC content is the highest up to now, is also the most effective natural, and its effect is 20 times of Vc, 50 times of VE, the tonic effect have superpower develop immunitypty, delaying senility.Black fruit lyceum taste is sweet, property is put down, clear away heart-fire heat, can nourishing liver and kidney, benefiting shrewd head, be applicable to soreness and weakness of waist and knees, have a dizzy spell, the symptom such as bleary-eyed, the Tibetan medicine and pharmacology classical Four-Volume Medical Code, " Jingzhubencao " etc. are recorded black fruit lyceum and are cured mainly cardiopyretic disease, heart disease, irregular menstruation, menelipsis etc." Uygur medicine will " is recorded Uygur medicine and is commonly used lycium ruthenicum fruit and root skin treatment urethral calculus, tinea scabies, the diseases such as gingiva bleeding gingival hemorrhage, among the peoplely make strengthening by means of tonics and depressor modern scientific research confirms above-mentioned saying, and think that black fruit lyceum can reduce cholesterol, excited cerebral nerve, strengthen immunologic function, anti-curing cancers, anti-ageing and beauty treatment, black fruit lyceum extract can promote cellular immune function, strengthen the generation of lymphopoiesis and TNF, two-way conciliation effect is had to interleukins II, can eat by the many drinks of diabetes-alleviating patient more, lose weight disease.
At present, the matrimony vine series products on domestic market mainly contains drinks, medicine class, food beverages and Normal juice class etc.The matrimony vine food be developed into have Red beer contg. Chinese wolf-berry wine, soft sweets matrimony vine dried apricot dried meat, join wolfberry juice, Aloe-medlar Beverage, matrimony vine Walnut Milk and matrimony vine honey milk etc.Wherein the exploitation of lycium barbarum product has defined five large series more than 30 kind, matrimony vine series products extend to wine-making industry by traditional Chinese medicine category, the industry such as beverage/food and nutrient and healthcare products, successively develop dried fruit of lycium barbarum, fresh juice beverage of matrimony vine, Lycium chinense wine, wolfberry fruit sauce, matrimony vine extra dry red wine, Chinese wolfberry tea, matrimony vine toffee, Wolf-berry capsules, matrimony vine shortcake volume, Chinese wolfberry soyabean milk powder, instant Chinese wolfberry-soya-bean milk granules, Chinese wolfberry and coffee, wolfberry juice, amino acid selenium-enriched wolfberry fruit phospholipid wine, Boxthorn Seed Oil, LBP-X, matrimony vine freeze-dried powder, the products such as matrimony vine normal-temperature fresh-keeping Normal juice and matrimony vine crystal sugar.Along with the raising of people's living standard and the progress of science and technology, matrimony vine, on the basis of traditional market, will have more wide application prospect.According to the nature,taste and action of matrimony vine, its market orientation answers emphasis based on old man, women and sub-health population, expands new market development space.Along with the adjustment of people's food configuration and consumption habit, the range of application of matrimony vine will be more extensive, answer focus development to delay senility, anti-oxidant, radioresistance, adjusting blood lipid, blood sugar, improve the matrimony vine product of alimentary anemia, immunological regulation and beautifying face and moistering lotion; With the matrimony vine of integration of drinking and medicinal herbs for raw material, through scientific compatibility, the formulation products (as oral liquid, capsule, dripping pill, tablet, electuary etc.) that exploitation is suitable, meets relevant consumer demand.
In the prior art, the preparation method of multiple matrimony vine lozenge has been disclosed, such as CN200910082329.6, CN201310392078.8, CN201310206949.2; But, in prior art, no matter be compound medlar lozenge, or black fruit lyceum lozenge, in order to shaping compressing tablet, all need to add the adhesives such as such as starch, carboxymethyl cellulose, maltose and microcrystalline cellulose when preparing burden; Or need to carry out Cotton seeds; In addition, for the preparation of matrimony vine lozenge in prior art, be all adopt wolfberry fruit extract as raw material, often need to add the chemical reagent such as ethanol, citric acid in extraction process, and likely introduce the materials such as unsafe heavy metal; And extraction process is also often along with the destruction of active component, and the nutritional labeling be rich in insoluble matter is wherein wasted.
Summary of the invention
In order to utilize the nutritional labeling of matrimony vine more efficiently, all sidedly, and obtaining the matrimony vine lozenge of high finished product rate, the object of the present invention is to provide a kind of double-colored dark red fruit matrimony vine sheet and preparation method thereof.Double-colored dark red fruit matrimony vine sheet of the present invention is not only nutritious, and owing to not adding any auxiliary material, product quality is also more safe and reliable, and remains the pure local flavor of matrimony vine.
In order to realize foregoing invention object, the technical solution adopted in the present invention is as follows:
A kind of double-colored dark red fruit matrimony vine sheet, it is with black fruit lyceum and haw matrimony vine raw material, squeeze the juice through comprising, homogeneous, freeze drying, pulverizing and compressing tablet processing step prepare, and in all processing steps, all do not add any auxiliary material than water.
Wherein, described pulverizing and tablet forming technique are all carry out at low temperatures; Wherein, described pulverizing carries out under the condition of-20 DEG C ~ 0 DEG C, and described tablet forming technique carries out under the condition of-10 DEG C ~ 10 DEG C.
Wherein, in described double-colored dark red fruit matrimony vine sheet, the mass ratio of black fruit lyceum and haw matrimony vine, for can be any proportioning, as preferably, such as, can be 1:9 ~ 9:1; More preferably, the mass ratio of described black fruit lyceum and haw matrimony vine is 3:7 ~ 7:3.
Wherein, described double-colored dark red fruit matrimony vine sheet is the double-colored dark red fruit matrimony vine sheet of Tai Ji shape or dark red double color plate.
Wherein, described homogeneous refers to and is carried out grinding and obtain the fruit juice that pulp diameter is 1 ~ 150 μm by the fruit juice colloid mill obtained after squeezing the juice, and carries out homogeneous with homogenizer;
Wherein, described freeze drying refers to that the fruit juice after by homogeneous carries out precooling and freezing; And the time of precooling is 1 ~ 12 hour, temperature is-30 ~-60 DEG C; The freezing time is 1 ~ 12 hour, and temperature is 0 ~-60 DEG C.
Wherein, described pulverizing refers to that under cryogenic the solids after freeze drying being carried out pulverizing obtains the matrimony vine freeze-dried powder that particle diameter is 1 ~ 150 μm.
Wherein, described compressing tablet refers to and adds in layering tablet press machine by black fruit lyceum freeze-dried powder and haw matrimony vine freeze-dried powder, is carry out compressing tablet under the condition of 10 ~ 60KN at pressure.
A second aspect of the present invention, also relate to a kind of preparation method of double-colored dark red fruit matrimony vine sheet, it is characterized in that described method comprise squeeze the juice, homogeneous, freeze drying, pulverizing and compressing tablet processing step prepare, and in all processing steps, all do not add any auxiliary material than water; Further, described pulverizing and tablet forming technique are all carry out at low temperatures, and described pulverizing carries out under the condition of-20 DEG C ~ 0 DEG C, and described tablet forming technique carries out under the condition of-10 DEG C ~ 10 DEG C.
Wherein, described method specifically comprises the following steps:
(1) squeeze the juice: fresh fruit or the dry fruit after getting damp are squeezed the juice;
(2) homogeneous: the fruit juice colloid mill that step (1) obtains carried out grinding and obtains the fruit juice that pulp diameter is 1 ~ 150 μm, and carrying out homogeneous with homogenizer;
(3) freeze drying: the fruit juice freeze drier that step (2) obtains is carried out freeze drying; And the time of precooling is 1 ~ 12 hour, temperature is-30 ~-60 DEG C; The freezing time is 1 ~ 12 hour, and temperature is 0 ~-60 DEG C;
(4) pulverize, solids step (3) obtained carries out pulverizing and obtains the matrimony vine freeze-dried powder that particle diameter is 1 ~ 150 μm under the condition of-10 ~-30 DEG C.
(5) compressing tablet, the black fruit lyceum freeze-dried powder obtain step (4) and haw matrimony vine freeze-dried powder add in layering tablet press machine or bi-layer tablet press, temperature be-10 DEG C ~ 10 DEG C, pressure carries out compressing tablet under being the condition of 10 ~ 60KN.
Wherein, described method, also comprises the sterilization steps after compressing tablet, and described sterilization steps refers to and utilizes wavelength to be that the ultraviolet of 100 ~ 120nm irradiates, and to irradiate irradiation be 1mWcm
-2below.
Compared with prior art, double-colored dark red fruit matrimony vine sheet of the present invention and preparation method thereof has following outstanding beneficial effect:
(1) matrimony vine freeze-dried powder and black fruit lyceum freeze-dried powder are carried out scientific compatibility by the present invention, rationally prepare, and are matrimony vine freeze-dried powder, and another side is black fruit lyceum freeze-dried powder; In addition not containing any adjunct ingredient, double-colored dark red matrimony vine sheet has namely been prepared.
(2) adopt the extract of the squeeze the juice fruit juice instead of ethanol that obtain or water as raw material, not only nutrition is abundanter to make the food made, and mouthfeel is also better.
(3) low-temperature grinding skilled worker skill is adopted, black fruit lyceum and haw matrimony vine cell membrane are broken, intracellular moisture, oil content and active ingredient come out all completely, make minuteness particle surface presentation half moisture state, semistable particle cluster can be formed between particle and particle, each particle cluster all includes the active component of same ratio, and this structure not only can make nutrition distribution pattern homogenising wherein, is conducive to improving food utilization.
(4) applicant is surprised to find, associating low-temperature grinding and low temperature tablet forming technique, can when not adding the binding agents such as starch, the matrimony vine sheet that hardness is suitable can be obtained, thus without the need to adding any auxiliary material in described matrimony vine sheet, not only remain the complete local flavor of matrimony vine, also make food more safely with reliable.
(5) applicant is also surprised to find, associating low-temperature grinding and low temperature tablet forming technique, only need take the ultraviolet radiation of low-light (level) (needing under the ultraviolet condition that 100 ~ 120nm wavelength is shorter), worm's ovum and bacteria inactivation can be made, and the content of microorganisms of product is controlled in safe range, also do not damage the active component in matrimony vine sheet and local flavor simultaneously.
Detailed description of the invention
Below with reference to specific embodiment, double-colored dark red fruit matrimony vine sheet of the present invention and preparation method thereof is further elaborated, has more complete, accurate and deep understanding to help those skilled in the art to inventive concept of the present invention, technical scheme; It is to be noted that the description of related materials and performance etc. is all exemplary in embodiment, and do not refer to the restriction to invention protection domain.
embodiment 1
Double-colored dark red matrimony vine sheet described in the present embodiment, is prepared by following steps: fresh black fruit lyceum and haw matrimony vine are cleaned respectively, and remove carpopodium, impurity and wormy fruit etc.; Then juice extractor is utilized to squeeze the juice to black fruit lyceum and haw matrimony vine respectively; Then the fruit juice colloid mill obtained carried out grinding and obtain the fruit juice that pulp diameter is 1 ~ 150 μm, and carrying out homogeneous with homogenizer; Then the fruit juice freeze drier after homogeneous is carried out freeze drying; And the time of precooling is 3 hours, and temperature is-30 DEG C; Carrying out freezing, the freezing time is afterwards 30 hours, and temperature is-50 DEG C; Then be warming up to-20 DEG C, and utilize pulverizer to carry out pulverizing and obtain the matrimony vine freeze-dried powder that particle diameter is 1 ~ 150 μm.By the black fruit lyceum freeze-dried powder that obtains and haw matrimony vine freeze-dried powder according to a certain percentage afterwards, such as 3:7 adds respectively in rotary three-tier tablet press machine and carries out compressing tablet, rotating speed is 20 ~ 30r/min, humidity≤70%, temperature be 0 DEG C, pressure carries out compressing tablet under being the condition of 40KN.The double-colored dark red matrimony vine sheet that the present embodiment obtains according to the shape formable of design, such as, can form traditional black and white Tai Ji shape shape; And the double-colored dark red matrimony vine sheet obtained has the distinctive flavour of matrimony vine and fragrance, and delicate mouthfeel, hardness is moderate, and fragrance is pure; And described double-colored dark red matrimony vine sheet smooth surface, fractography are fine and smooth closely; The sheet of described double-colored dark red matrimony vine sheet is heavily generally 0.6 ~ 1.0g, and hardness is 3.5 ~ 3.8kg/mm, and crisp hardness is less than 0.5%.
embodiment 2
Double-colored dark red matrimony vine sheet described in the present embodiment, is prepared by following steps: black dried fruit of lycium barbarum and red dried fruit of lycium barbarum are carried out process of getting damp, and the ratio of wherein said black dried fruit of lycium barbarum and red dried fruit of lycium barbarum and water is 1:2, and the time of getting damp is 1 ~ 12 hour; Then juice extractor is utilized to squeeze the juice to black fruit lyceum and haw matrimony vine respectively; Then the fruit juice colloid mill obtained carried out grinding and obtain the fruit juice that pulp diameter is 1 ~ 150 μm, and carrying out homogeneous with homogenizer; Then the fruit juice freeze drier after homogeneous is carried out freeze drying; And the time of precooling is 2 hours, and temperature is-30 DEG C; Carrying out freezing, the freezing time is afterwards 40 hours, and temperature is-40 DEG C; Then be warming up to 0 DEG C, and utilize pulverizer to carry out pulverizing and obtain the matrimony vine freeze-dried powder that particle diameter is 1 ~ 150 μm.By the black fruit lyceum freeze-dried powder that obtains and haw matrimony vine freeze-dried powder according to a certain percentage afterwards, such as 1:1 also adds respectively in rotary three-tier tablet press machine and carries out compressing tablet, rotating speed is 20 ~ 30r/min, humidity≤70%, temperature be 0 DEG C, pressure carries out compressing tablet under being the condition of 40KN.The double-colored dark red matrimony vine sheet that the present embodiment obtains according to the shape formable of design, such as, can form traditional black and white Tai Ji shape shape; And the double-colored dark red matrimony vine sheet obtained has the distinctive flavour of matrimony vine and fragrance, and delicate mouthfeel, hardness is moderate, and fragrance is pure; And described double-colored dark red matrimony vine sheet smooth surface, fractography are fine and smooth closely; The sheet of described double-colored dark red matrimony vine sheet is heavily generally 0.6 ~ 1.0g, and hardness is 3.5 ~ 3.8kg/mm, and crisp hardness is less than 0.5%.
embodiment 3
The ultraviolet that double-colored dark red matrimony vine sheet embodiment 2 obtained utilizes wavelength to be 100nm carries out sterilization treatment, and the illumination of irradiation is 0.5mWcm
-2; Then by the matrimony vine sheet through ultraviolet disinfection process and the matrimony vine sheet (monolithic) without sterilization treatment, on aseptic operating platform, carry out dilution respectively to matrimony vine sheet sample to cultivate, dilution gradient is 1:100, then the cultivation of beef-protein medium and bile salt lactose fermentation tube is utilized, then constant temperature culture 48 hours and 36 hours in the incubator of 37 DEG C; Experimental result show undressed sample through cultivation after total plate count between 5 ~ 150,000/gram; And through the sample total plate count of above-mentioned process within 1000/gram.
comparative example 1
Double-colored dark red matrimony vine sheet described in this comparative example, is prepared by following steps: fresh black fruit lyceum and haw matrimony vine are cleaned respectively, and remove carpopodium, impurity and wormy fruit etc.; Then juice extractor is utilized to squeeze the juice to black fruit lyceum and haw matrimony vine respectively; Then the fruit juice colloid mill obtained carried out grinding and obtain the fruit juice that pulp diameter is 1 ~ 150 μm, and carrying out homogeneous with homogenizer; Then the fruit juice freeze drier after homogeneous is carried out freeze drying; And the time of precooling is 3 hours, and temperature is-30 DEG C; Carrying out freezing, the freezing time is afterwards 30 hours, and temperature is-50 DEG C; Then be warming up to 0 DEG C, and utilize pulverizer to carry out pulverizing and obtain the matrimony vine freeze-dried powder that particle diameter is 1 ~ 150 μm.By the black fruit lyceum freeze-dried powder that obtains and haw matrimony vine freeze-dried powder according to a certain percentage afterwards, such as 3:7 adds respectively in rotary three-tier tablet press machine and carries out compressing tablet, rotating speed is 20 ~ 30r/min, humidity≤70%, temperature be 20 DEG C, pressure carries out compressing tablet under being the condition of 40KN.The double-colored dark red matrimony vine sheet obtained according to the shape formable of design, such as, can form traditional black and white Tai Ji shape shape; And the sheet of the double-colored dark red matrimony vine sheet obtained is heavily 0.6 ~ 1.0g, hardness is 2.5 ~ 2.8kg/mm, and crisp hardness is 12 ~ 15%, and the double-colored dark red matrimony vine sheet obtained is easily broken, is difficult to long-term preservation.The ultraviolet that the double-colored dark red matrimony vine sheet obtained by this comparative example utilizes wavelength to be 100nm carries out sterilization treatment, and the illumination of irradiation is 0.5mWcm
-2; Then by the matrimony vine sheet sample through ultraviolet disinfection process on aseptic operating platform, carry out dilution respectively to matrimony vine sheet sample to cultivate, dilution gradient is 1:100, then the cultivation of beef-protein medium and bile salt lactose fermentation tube is utilized, then constant temperature culture 48 hours and 36 hours in the incubator of 37 DEG C; Experimental result show undressed sample through cultivation after total plate count between 2 ~ 100,000/gram.Experiment shows to only have and the illumination of irradiation is increased to 50mWcm further
-2, sample total plate count could be controlled within 1000/gram.
comparative example 2
Double-colored dark red matrimony vine sheet described in this comparative example, is prepared by following steps: fresh black fruit lyceum and haw matrimony vine are cleaned respectively, and remove carpopodium, impurity and wormy fruit etc.; Then juice extractor is utilized to squeeze the juice to black fruit lyceum and haw matrimony vine respectively; Then the fruit juice colloid mill obtained carried out grinding and obtain the fruit juice that pulp diameter is 1 ~ 150 μm, and carrying out homogeneous with homogenizer; Then the fruit juice freeze drier after homogeneous is carried out freeze drying; And the time of precooling is 3 hours, and temperature is-30 DEG C; Carrying out freezing, the freezing time is afterwards 30 hours, and temperature is-50 DEG C; Then be warming up to 20 DEG C, and utilize pulverizer to carry out pulverizing and obtain the matrimony vine freeze-dried powder that particle diameter is 1 ~ 150 μm.By the black fruit lyceum freeze-dried powder that obtains and haw matrimony vine freeze-dried powder according to a certain percentage afterwards, such as 3:7 adds respectively in rotary three-tier tablet press machine and carries out compressing tablet, rotating speed is 20 ~ 30r/min, humidity≤70%, temperature be 10 DEG C, pressure carries out compressing tablet under being the condition of 40KN.The double-colored dark red matrimony vine sheet obtained according to the shape formable of design, such as, can form traditional black and white Tai Ji shape shape; And the sheet of the double-colored dark red matrimony vine sheet obtained is heavily 0.6 ~ 1.0g, hardness is 2.8 ~ 3.0kg/mm, and crisp hardness is 20 ~ 25%, and the double-colored dark red matrimony vine sheet obtained is easily broken, is difficult to long-term preservation.The ultraviolet that the double-colored dark red matrimony vine sheet obtained by this comparative example utilizes wavelength to be 100nm carries out sterilization treatment, 0.5mWcm
-2; Then by the matrimony vine sheet sample through ultraviolet disinfection process on aseptic operating platform, carry out dilution respectively to matrimony vine sheet sample to cultivate, dilution gradient is 1:100, then the cultivation of beef-protein medium and bile salt lactose fermentation tube is utilized, then constant temperature culture 48 hours and 36 hours in the incubator of 37 DEG C; Experimental result show undressed sample through cultivation after total plate count between 2 ~ 100,000/gram.Experiment shows to only have and the illumination of irradiation is increased to 50mWcm further
-2, sample total plate count could be controlled within 1000/gram.
comparative example 3
Double-colored dark red matrimony vine sheet described in this comparative example, is prepared by following steps: fresh black fruit lyceum and haw matrimony vine are cleaned respectively, and remove carpopodium, impurity and wormy fruit etc.; Then juice extractor is utilized to squeeze the juice to black fruit lyceum and haw matrimony vine respectively; Then the fruit juice colloid mill obtained carried out grinding and obtain the fruit juice that pulp diameter is 1 ~ 150 μm, and carrying out homogeneous with homogenizer; Then the fruit juice freeze drier after homogeneous is carried out freeze drying; And the time of precooling is 3 hours, and temperature is-30 DEG C; Carrying out freezing, the freezing time is afterwards 30 hours, and temperature is-50 DEG C; Then be warming up to 20 DEG C, and utilize pulverizer to carry out pulverizing and obtain the matrimony vine freeze-dried powder that particle diameter is 1 ~ 150 μm.By the black fruit lyceum freeze-dried powder that obtains and haw matrimony vine freeze-dried powder according to a certain percentage afterwards, such as 3:7 adds respectively in rotary three-tier tablet press machine and carries out compressing tablet, rotating speed is 20 ~ 30r/min, humidity≤70%, temperature be-10 DEG C, pressure carries out compressing tablet under being the condition of 40KN.The double-colored dark red matrimony vine sheet obtained according to the shape formable of design, such as, can form traditional black and white Tai Ji shape shape; And the sheet of the double-colored dark red matrimony vine sheet obtained is heavily 0.6 ~ 1.0g, hardness is 2.5 ~ 2.8kg/mm, and crisp hardness is 12 ~ 15%, and the double-colored dark red matrimony vine sheet obtained is easily broken, is difficult to long-term preservation.
comparative example 4
Double-colored dark red matrimony vine sheet described in this comparative example, is prepared by following steps: fresh black fruit lyceum and haw matrimony vine are cleaned respectively, and remove carpopodium, impurity and wormy fruit etc.; Then black fruit lyceum and haw matrimony vine are pulverized respectively, obtain 50 ~ 400 objects screening things, then utilize the alcohol extract 3 ~ 5 times of 30 ~ 50%, concentrate after merging extract, obtain extract and concentrate slurry, then utilize homogenizer to carry out homogeneous; Then by the concentrated slurry after homogeneous; Then, utilize freeze drier to carry out freeze drying, wherein the time of precooling is 3 hours, and temperature is-30 DEG C; Carrying out freezing, the freezing time is afterwards 30 hours, and temperature is-50 DEG C; Then be warming up to 10 DEG C, and utilize pulverizer to carry out pulverizing and obtain the matrimony vine freeze-dried powder that particle diameter is 1 ~ 150 μm.By the black fruit lyceum freeze-dried powder that obtains and haw matrimony vine freeze-dried powder according to a certain percentage afterwards, such as 3:7 adds respectively in rotary three-tier tablet press machine and carries out compressing tablet, rotating speed is 20 ~ 30r/min, humidity≤70%, temperature be 0 DEG C, pressure carries out compressing tablet under being the condition of 40KN.The double-colored dark red matrimony vine sheet obtained according to the shape formable of design, such as, can form traditional black and white Tai Ji shape shape; And the sheet of the double-colored dark red matrimony vine sheet obtained is heavily 0.6 ~ 1.0g, hardness is 3.0 ~ 3.2kg/mm, and crisp hardness is 10 ~ 12%, and the double-colored dark red matrimony vine sheet obtained is same easily broken, is difficult to long-term preservation.
comparative example 5
The ultraviolet that double-colored dark red matrimony vine sheet embodiment 2 obtained utilizes wavelength to be 200nm carries out sterilization treatment, and the illumination of irradiation is 0.5mWcm
-2; Then by the matrimony vine sheet sample through ultraviolet disinfection process on aseptic operating platform, carry out dilution to it to cultivate, dilution gradient is 1:100, then utilizes the cultivation of beef-protein medium and bile salt lactose fermentation tube, then constant temperature culture 48 hours and 36 hours in the incubator of 37 DEG C; Experimental result show this sample through cultivation after total plate count between 2 ~ 100,000/gram.
comparative example 6
The ultraviolet that double-colored dark red matrimony vine sheet embodiment 2 obtained utilizes wavelength to be 300nm carries out sterilization treatment, 0.5mWcm
-2; Then by the matrimony vine sheet sample through ultraviolet disinfection process on aseptic operating platform, carry out dilution to it to cultivate, dilution gradient is 1:100, then utilizes the cultivation of beef-protein medium and bile salt lactose fermentation tube, then constant temperature culture 48 hours and 36 hours in the incubator of 37 DEG C; Experimental result show this sample through cultivation after total plate count between 2 ~ 120,000/gram.
comparative example 7
The ultraviolet that double-colored dark red matrimony vine sheet embodiment 2 obtained utilizes wavelength to be 200nm carries out sterilization treatment, and the illumination of irradiation is 20mWcm
-2; Then by the matrimony vine sheet sample through ultraviolet disinfection process on aseptic operating platform, carry out dilution to it to cultivate, dilution gradient is 1:100, then utilizes the cultivation of beef-protein medium and bile salt lactose fermentation tube, then constant temperature culture 48 hours and 36 hours in the incubator of 37 DEG C; Experimental result show this sample through cultivation after total plate count between 2 ~ 80,000/gram.
For the ordinary skill in the art; specific embodiment is just to invention has been exemplary description; obvious specific implementation of the present invention is not subject to the restrictions described above; as long as have employed the improvement of the various unsubstantialities that method of the present invention is conceived and technical scheme is carried out; or design of the present invention and technical scheme directly applied to other occasion, all within protection scope of the present invention without to improve.
Claims (4)
1. a preparation method for double-colored dark red fruit matrimony vine sheet, is characterized in that: described method with black fruit lyceum and haw matrimony vine raw material, to squeeze the juice through comprising, homogeneous, freeze drying, pulverizing and compressing tablet processing step prepare; Any auxiliary material than water is not all added in all processing steps; And described preparation method specifically comprises the following steps:
(1) squeeze the juice: fresh fruit or the dry fruit after getting damp are squeezed the juice;
(2) homogeneous: the fruit juice colloid mill obtained of step (1) being squeezed the juice carries out grinding and obtains the fruit juice that pulp diameter is 1 ~ 150 μm, and carries out homogeneous with homogenizer;
(3) freeze drying: the fruit juice freeze drier that step (2) obtains is carried out freeze drying; And the time of precooling is 1 ~ 12 hour, temperature is-30 ~-60 DEG C; The freezing time is 1 ~ 12 hour, and temperature is 0 ~-60 DEG C;
(4) pulverize, solids step (3) obtained carries out pulverizing and obtains the matrimony vine freeze-dried powder that particle diameter is 1 ~ 150 μm under the condition of 0 ~-20 DEG C;
(5) compressing tablet, the black fruit lyceum freeze-dried powder obtain step (4) and haw matrimony vine freeze-dried powder add in layering tablet press machine or bi-layer tablet press, temperature be-10 DEG C ~ 0 DEG C, pressure carries out compressing tablet under being the condition of 10 ~ 60KN.
2. the preparation method of double-colored dark red fruit matrimony vine sheet according to claim 1, is characterized in that: in described double-colored dark red fruit matrimony vine sheet, the mass ratio of black fruit lyceum and haw matrimony vine is 1:9 ~ 9:1.
3. the preparation method of double-colored dark red fruit matrimony vine sheet according to claim 1, is characterized in that: described double-colored dark red fruit matrimony vine sheet is the double-colored dark red fruit matrimony vine sheet of Tai Ji shape or dark red matrimony vine double-layer tablets.
4. the preparation method of double-colored dark red fruit matrimony vine sheet according to claim 1, is characterized in that: also comprise the sterilization steps after compressing tablet, and described sterilization steps refers to and utilizes wavelength to be that the ultraviolet of 100 ~ 120nm irradiates, and to irradiate irradiation be 1mWcm
-2below.
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| CN103932081B (en) * | 2014-03-25 | 2016-05-18 | 金诃藏药股份有限公司 | Red-black matrimony vine double-layer tablet and preparation method thereof |
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| CN104382176B (en) * | 2014-12-03 | 2016-08-24 | 铁顺良 | A kind of Qaidam Lycium ruthenicum Murr. dew |
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