CN103773617B - A kind of footgear personal cleansing liquid and preparation method thereof - Google Patents
A kind of footgear personal cleansing liquid and preparation method thereof Download PDFInfo
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Abstract
The invention discloses a kind of footgear personal cleansing liquid and preparation method thereof, belong to daily washing composition technical field, the present invention is compounded with the humic acids/salt with sterilizing and deodorizing function and the tensio-active agent etc. with soil removability, thus sterilization, deodorizing and decontamination is organically combined together.The present invention by antibacterial deodorant, tensio-active agent, white dyes, other add auxiliary agent and deionized waters etc. formulated.Compared with prior art, the present invention except the traditional advantages such as have gentle delicate fragrance, anti-hard water, antistatic, clean effect is remarkable, and has the new feature of good sterilizing and deodorizing function; In addition the waste water after washing flows into water drain or urinal etc. can do sewage deodorizing agent, also can be used as the natural plant fertilizer such as fruit tree; Preparation technology of the present invention is simple, cost is lower, practical value is high, environmental protection, be applicable to suitability for industrialized production.
Description
Technical field
The present invention relates to a kind of footgear personal cleansing liquid and preparation method thereof, specifically a kind of containing humic acids/salt can the footgear personal cleansing liquid and preparation method thereof of simultaneously deodorization and sterilization, belong to daily washing composition technical field.
Background technology
Along with improving constantly of people's living standard, Personal hygiene and health come into one's own day by day.People have not rested in the single pattern of tradition to the requirement of cleaning product, having sold washing of various dedicated functions on the market protects product at present, as underwear pants clean-out system, down jackets detergent for woollen sweater, leather and fur fur washing composition etc., and according to the singularity of footgear spot and the washing composition researched and developed specially is relatively less.
Sweaty feet and pin smelly be a lot of people's of a puzzlement difficult problem always, radical cure sweaty feet and pin smelly except medicine and other sanitary products, more to notice that the duty of daily footgear is changed clothes; But remove the function such as multiple intractable spot and deodorization and sterilization because ordinary liquid laundry detergent can not possess simultaneously, therefore there is a part of spot or bacterium continues to adhere on footgear, particularly on socks, this will produce negative influence to sweaty feet and the smelly radical cure of pin, therefore need a kind of footgear that is specifically designed to wash the product protected, accomplish rapidly and efficiently, the effect such as strong dirt-removing, deodorization and sterilization.
The sodium salt that humate refers generally to be refined by natural product humic acids and obtains or sylvite, prove through pharmacological evaluation, it is without any side effects to human body, in addition, along with going deep into of research, effect of its deodorization and sterilization gradually by people cognition, as patent: CN 102864624.A discloses a kind of fabric bactericidal deodorant, patent: CN 103043802.A discloses a kind of water purification reodorant and preparation method thereof, for another example patent: CN 1607009.A discloses a kind of Sodium salts humic acids/potassium as biochemical deodorant for rubbish deodorizing, reodorant preparation and deodorizing method, above-mentioned patent has all rationally suitably used the function of humic acids or humate deodorization and sterilization.In addition, humic acids and salt thereof can be used as natural anion surfactant, the effects such as emulsification, wetting, solubilising, moisturizing, lubrication, softness, antistatic, foaming, froth breaking can be played and possess other synthetic surfactants alternative performance washing function, the use of synthetic surfactant can be reduced to a certain extent, reduce the pungency of washings.Humic acids and salt thereof also can be used as natural chelators, replace the sequestrants such as the disodium ethylene diamine tetraacetate of traditional difficult for biological degradation, strengthen washings resistance to hard water.But, at present by humic acids/salt and other cleaning ingredients are composite is made as a kind of footgear special efficient washings having deodorization and sterilization dirt-removing functions concurrently and have not been reported, be therefore necessary to invent this type of product innovation to meet the growing demand in market.
Summary of the invention
The object of the present invention is to provide a kind of footgear personal cleansing liquid, this washings possesses the advantages such as sterilization, deodorizing, decontamination, anti-hard water, and preparation technology is simple, and cost is lower, and practical value is high, and face of promoting is large, is applicable to suitability for industrialized production.
Footgear personal cleansing liquid of the present invention, its constituent and weight percent are: antibacterial deodorant 12 ~ 20%, anion surfactant 15 ~ 20%, nonionogenic tenside 10 ~ 15%, wetting Agent for Printing Inks 3 ~ 6%, thickening material 1 ~ 4%, pH adjusting agent 1 ~ 10%, softener 0.5 ~ 3%, white dyes 0.05 ~ 1%, essence 0.05 ~ 0.5% and deionized water 35 ~ 50%.
Described antibacterial deodorant is humic acids and/or humate.
Described humic acids is xanthohumic acid and/or ulmic acid; Humate is that SODLUM FULVATE, potassium fulvate, ulmic acid sodium, ulmic acid potassium wherein one or more are arbitrarily than mixture; The humic acids that in its reference patent CN 200810233669.X " oxidation and degradation of brown coal produces the method for humic acids and salt thereof ", method is obtained and humate, commercial refining humic acids and humate, after heavy metal analysis does not exceed standard, also can use.
Described anion surfactant is that polyoxyethylenated alcohol sodium sulfate, Sodium dodecylbenzene sulfonate wherein one or both are arbitrarily than mixture.
Described nonionogenic tenside is that fatty alcohol-polyoxyethylene ether, alkyl polyglucoside wherein one or both are arbitrarily than mixture.
Described wetting Agent for Printing Inks be propylene glycol, glycerol, Sorbitol Powder wherein one or more arbitrarily than mixture.
Described thickening material be Vltra tears, sodium alginate, sodium-chlor wherein one or more arbitrarily than mixture.
Described pH adjusting agent be citric acid and Trisodium Citrate arbitrarily than mixture and/or lactic acid and Sodium.alpha.-hydroxypropionate arbitrarily than mixture.
Described softener is that ester based quaternary ammonium salt, consistent lubricant essence wherein one or both are arbitrarily than mixture.
Footgear personal cleansing liquid and preparation method thereof of the present invention is as follows:
(1) deionized water of the anion surfactant of weight percent 15 ~ 20% and weight percent 35 ~ 50% is added in stirring tank, be heated to 65 ~ 85 DEG C of dissolvings, add the nonionogenic tenside of weight percent 10 ~ 15% and the antibacterial deodorant of weight percent 12 ~ 20% again, stir until it all dissolves;
(2) be cooled to the thickening material of 35 ~ 50 DEG C of postemphasis amount per-cents 1 ~ 4%, the softener of weight percent 0.5 ~ 3%, the wetting Agent for Printing Inks of weight percent 3 ~ 6% stir; Then pH adjusting agent adjust ph to 7 ~ 8 of weight percent 1 ~ 10% are added;
(3) finally add the white dyes of weight percent 0.05 ~ 1% and the essence of weight percent 0.05 ~ 0.5%, stirs after 5 ~ 10 minutes, sample examination, qualifiedly can discharging to pack; Namely the footgear personal cleansing liquid containing humic acids/salt is prepared.
Wash the evaluation method QB/T 2738-2012 of agent QB/T 1224-2012 and daily chemical products antibacterial bacteriostatic effect by liquid according to People's Republic of China's light industry industry standard-dress material, the footgear personal cleansing liquid technical indicator detected result that the inventive method obtains is as follows:
Beneficial effect of the present invention is as follows:
(1) not only soil removability is good for product of the present invention, and a large amount of bacterium can effectively killed on footgear and fungi, suppress it to regenerate, also fast and effeciently can remove the peculiar smell on footgear or stink simultaneously;
(2) after product washing of the present invention, waste water inflow water drain or urinal etc. can continue to play deodouring effect, also can be used as the natural plant fertilizer such as fruit tree, improvement soil;
(3) pleasant, the anti-hard water of product delicate fragrance of the present invention, antistatic, performance is gentle, pungency is little, protects the skin of footgear and people to greatest extent;
(4) humic acids contained by product of the present invention or humate itself have the function of Antimicrobial preservative, therefore do not need to add sanitas in addition, environmental protection;
(5) product usage quantity of the present invention can reach better effect less, easy rinsed clean, and saving water resource all has good effect in cold water and warm water;
(6) the product antibacterial and deodouring time of the present invention is long, and life-time service is to control sweaty feet and the important active effect of the smelly performance of pin, and it is joyful to make us body and mind;
(7) simple, the cost of product preparation process of the present invention compared with low, practical value is high, face of promoting is large, be applicable to suitability for industrialized production.
Embodiment
Below in conjunction with embodiment, the present invention is described in further detail, but scope is not limited to described content.
Embodiment 1: this footgear personal cleansing liquid composition and weight percent as follows:
Antibacterial deodorant 12%: xanthohumic acid accounts for 7%, ulmic acid sodium accounts for 5%;
Anion surfactant 15%: polyoxyethylenated alcohol sodium sulfate accounts for 8%, Sodium dodecylbenzene sulfonate accounts for 7%;
Nonionogenic tenside 15%: fatty alcohol-polyoxyethylene ether accounts for 8%, alkyl polyglucoside accounts for 7%;
Wetting Agent for Printing Inks 3%: propylene glycol accounts for 1%, glycerol accounts for 1%, Sorbitol Powder accounts for 1%;
Thickening material 3%: Vltra tears accounts for 1%, sodium alginate accounts for 1%, sodium-chlor accounts for 1%;
PH adjusting agent 5%: citric acid accounts for 3%, Trisodium Citrate accounts for 2%;
Softener 2%: ester based quaternary ammonium salt accounts for 1%, consistent lubricant essence accounts for 1%;
White dyes 0.2%; Essence 0.1%; Deionized water 44.7%.
The preparation method of footgear personal cleansing liquid described in the present embodiment, concrete steps are as follows:
(1) deionized water of 80g polyoxyethylenated alcohol sodium sulfate, 70g Sodium dodecylbenzene sulfonate and 447g is added in stirring tank, be heated to 75 DEG C of dissolvings, add 80g fatty alcohol-polyoxyethylene ether, 70g alkyl polyglucoside and 70g xanthohumic acid, 50g ulmic acid sodium again, stir until it all dissolves;
(2) add 10g Vltra tears after being cooled to 40 DEG C, 10g sodium alginate, 10g sodium-chlor, 10g ester based quaternary ammonium salt, 10g consistent lubricant essence, 10g propylene glycol, 10g glycerol, 10g Sorbitol Powder stir; Then 30g citric acid, 20g Trisodium Citrate adjust ph to 7.5 is added;
(3) finally add the white dyes of 2g and the essence of 1g, stir after 8 minutes, sample examination, qualified can discharging packaging; Namely the footgear personal cleansing liquid containing humic acids/salt is prepared.
The present embodiment technical target of the product detected result is as follows:
Embodiment 2: this footgear personal cleansing liquid composition and weight percent as follows:
Antibacterial deodorant 15%: xanthohumic acid accounts for 5%, ulmic acid accounts for 5%, ulmic acid sodium accounts for 5%;
Anion surfactant 16%: polyoxyethylenated alcohol sodium sulfate accounts for 8%, Sodium dodecylbenzene sulfonate accounts for 8%;
Nonionogenic tenside 12%: fatty alcohol-polyoxyethylene ether accounts for 6%, alkyl polyglucoside accounts for 6%;
Wetting Agent for Printing Inks 6%: propylene glycol accounts for 2%, glycerol accounts for 2%, Sorbitol Powder accounts for 2%;
Thickening material 3%: Vltra tears accounts for 1%, sodium alginate accounts for 1%, sodium-chlor accounts for 1%;
PH adjusting agent 6%: lactic acid accounts for 2%, Sodium.alpha.-hydroxypropionate accounts for 4%;
Softener 3%: ester based quaternary ammonium salt accounts for 2%, consistent lubricant essence accounts for 1%;
White dyes 0.2%; Essence 0.2%; Deionized water 38.6%.
The preparation method of footgear personal cleansing liquid described in the present embodiment, concrete steps are as follows:
(1) deionized water of 80g polyoxyethylenated alcohol sodium sulfate, 80g Sodium dodecylbenzene sulfonate and 386g is added in stirring tank, be heated to 80 DEG C of dissolvings, add 60g fatty alcohol-polyoxyethylene ether, 60g alkyl polyglucoside and 50g xanthohumic acid, 50g ulmic acid, 50g ulmic acid sodium again, stir until it all dissolves;
Add 10g Vltra tears after (2) 45 DEG C, 10g sodium alginate, 10g sodium-chlor, 20g ester based quaternary ammonium salt, 10g consistent lubricant essence, 20g propylene glycol, 20g glycerol, 20g Sorbitol Powder stir; Then 20g lactic acid, 40g Sodium.alpha.-hydroxypropionate adjust ph to 7.2 is added;
(3) finally add the white dyes of 2g and the essence of 2g, stir after 6 minutes, sample examination, qualified can discharging packaging; Namely the footgear personal cleansing liquid containing humic acids/salt is prepared.
The present embodiment technical target of the product detected result is as follows:
Embodiment 3: this footgear personal cleansing liquid composition and weight percent as follows:
Antibacterial deodorant 20%: xanthohumic acid accounts for 5%, ulmic acid accounts for 2%, SODLUM FULVATE accounts for 8%, ulmic acid sodium accounts for 5%;
Anion surfactant 17%: polyoxyethylenated alcohol sodium sulfate accounts for 8%, Sodium dodecylbenzene sulfonate accounts for 9%;
Nonionogenic tenside 10%: fatty alcohol-polyoxyethylene ether accounts for 5%, alkyl polyglucoside accounts for 5%;
Wetting Agent for Printing Inks 4%: propylene glycol accounts for 2%, glycerol accounts for 2%;
Thickening material 2%: Vltra tears accounts for 1%, sodium-chlor accounts for 1%;
PH adjusting agent 5%: citric acid accounts for 3%, Trisodium Citrate accounts for 2%;
Softener 2%: ester based quaternary ammonium salt accounts for 1%, consistent lubricant essence accounts for 1%;
White dyes 0.3%; Essence 0.3%; Deionized water 39.4%.
The preparation method of footgear personal cleansing liquid described in the present embodiment, concrete steps are as follows:
(1) deionized water of 80g polyoxyethylenated alcohol sodium sulfate, 90g Sodium dodecylbenzene sulfonate and 394g is added in stirring tank, be heated to 65 DEG C of dissolvings, add 50g fatty alcohol-polyoxyethylene ether, 50g alkyl polyglucoside and 50g xanthohumic acid, 20g ulmic acid, 80g SODLUM FULVATE, 50g ulmic acid sodium again, stir until it all dissolves;
(2) add 10g Vltra tears after being cooled to 35 DEG C, 10g sodium-chlor, 10g ester based quaternary ammonium salt, 10g consistent lubricant essence, 20g propylene glycol, 20g glycerol stir; Then 30g citric acid, 20g Trisodium Citrate adjust ph to 7.8 is added;
(3) finally add the white dyes of 3g and the essence of 3g, stir after 9 minutes, sample examination, qualified can discharging packaging; Namely the footgear personal cleansing liquid containing humic acids/salt is prepared.
The present embodiment technical target of the product detected result is as follows:
Embodiment 4: this footgear personal cleansing liquid composition and weight percent as follows:
Antibacterial deodorant 15%: xanthohumic acid accounts for 8%, ulmic acid potassium accounts for 7%;
Anion surfactant 15%: polyoxyethylenated alcohol sodium sulfate accounts for 15%;
Nonionogenic tenside 15%: fatty alcohol-polyoxyethylene ether accounts for 15%;
Wetting Agent for Printing Inks 4%: glycerol accounts for 4%;
Thickening material 3%: sodium-chlor accounts for 3%;
PH adjusting agent 5%: citric acid accounts for 3%, Trisodium Citrate accounts for 2%;
Softener 2%: ester based quaternary ammonium salt accounts for 2%;
White dyes 0.4%; Essence 0.2%; Deionized water 40.4%.
The preparation method of footgear personal cleansing liquid described in the present embodiment, concrete steps are as follows:
(1) deionized water of 150g polyoxyethylenated alcohol sodium sulfate and 404g is added in stirring tank, be heated to 85 DEG C of dissolvings, then add 150g fatty alcohol-polyoxyethylene ether and 80g xanthohumic acid, 70g ulmic acid potassium, stir until it all dissolves;
Add 30g sodium-chlor after (2) 50 DEG C, 20g ester based quaternary ammonium salt, 40g glycerol stir; Then 30g citric acid, 20g Trisodium Citrate adjust ph to 7.0 is added;
(3) finally add the white dyes of 4g and the essence of 2g, stir after 10 minutes, sample examination, qualified can discharging packaging; Namely the footgear personal cleansing liquid containing humic acids/salt is prepared.
The present embodiment technical target of the product detected result is as follows:
Embodiment 5: this footgear personal cleansing liquid composition and weight percent as follows:
Antibacterial deodorant 14%: ulmic acid accounts for 14%;
Anion surfactant 20%: Sodium dodecylbenzene sulfonate accounts for 20%;
Nonionogenic tenside 13%: alkyl polyglucoside accounts for 13%;
Wetting Agent for Printing Inks 5%: Sorbitol Powder accounts for 5%;
Thickening material 4%: sodium alginate accounts for 4%;
PH adjusting agent 7%: lactic acid accounts for 3%, Sodium.alpha.-hydroxypropionate accounts for 4%;
Softener 0.5%: consistent lubricant essence accounts for 0.5%;
White dyes 1%; Essence 0.5%; Deionized water 35%.
The preparation method of footgear personal cleansing liquid described in the present embodiment, concrete steps are as follows:
(1) deionized water of 200g Sodium dodecylbenzene sulfonate and 350g adds in stirring tank, is heated to 85 DEG C of dissolvings, then adds 130g alkyl polyglucoside and 140g ulmic acid, stirs until it all dissolves;
Add 40g sodium alginate, 5g consistent lubricant essence after (2) 35 DEG C, 50g Sorbitol Powder stirs; Then 30g lactic acid, 40g Sodium.alpha.-hydroxypropionate adjust ph to 7.0 is added;
(3) finally add the white dyes of 10g and the essence of 5g, stir after 5 minutes, sample examination, qualified can discharging packaging; Namely the footgear personal cleansing liquid containing humic acids/salt is prepared.
The present embodiment technical target of the product detected result is as follows:
Claims (2)
1. a footgear personal cleansing liquid, is characterized in that its constituent and weight percent are: antibacterial deodorant 12 ~ 20%, anion surfactant 15 ~ 20%, nonionogenic tenside 10 ~ 15%, wetting Agent for Printing Inks 3 ~ 6%, thickening material 1 ~ 4%, pH adjusting agent 1 ~ 10%, softener 0.5 ~ 3%, white dyes 0.05 ~ 1%, essence 0.05 ~ 0.5%, deionized water 35 ~ 50%;
Described antibacterial deodorant is humic acids and/or humate;
Described humic acids is xanthohumic acid and/or ulmic acid; Humate is that SODLUM FULVATE, potassium fulvate, ulmic acid sodium, ulmic acid potassium wherein one or more are arbitrarily than mixture;
Described anion surfactant is that one or both in polyoxyethylenated alcohol sodium sulfate, Sodium dodecylbenzene sulfonate are arbitrarily than mixture;
Described nonionogenic tenside is that one or both in fatty alcohol-polyoxyethylene ether, alkyl polyglucoside are arbitrarily than mixture;
Described wetting Agent for Printing Inks be propylene glycol, glycerol, Sorbitol Powder wherein one or more arbitrarily than mixture;
Described thickening material be Vltra tears, sodium alginate, sodium-chlor wherein one or more arbitrarily than mixture;
Described pH adjusting agent be citric acid and Trisodium Citrate arbitrarily than mixture and/or lactic acid and Sodium.alpha.-hydroxypropionate arbitrarily than mixture;
Described softener is that ester based quaternary ammonium salt, consistent lubricant essence wherein one or both are arbitrarily than mixture.
2. the preparation method of footgear personal cleansing liquid described in claim 1, is characterized in that following steps are carried out:
(1) deionized water of the anion surfactant of weight percent 15 ~ 20% and weight percent 35 ~ 50% is added in stirring tank, be heated to 65 ~ 85 DEG C of dissolvings, add the nonionogenic tenside of weight percent 10 ~ 15% and the antibacterial deodorant of 12 ~ 20% again, stir until it all dissolves; (2) be cooled to the thickening material of weight percent 35 ~ 50 DEG C of postemphasis amount per-cents 1 ~ 4%, the softener of weight percent 0.5 ~ 3%, the wetting Agent for Printing Inks of weight percent 3 ~ 6% stir, then add pH adjusting agent adjust ph to 7 ~ 8 of weight percent 1 ~ 10%; (3) finally add the white dyes of weight percent 0.05 ~ 1% and the essence of weight percent 0.05 ~ 0.5%, stirs after 5 ~ 10 minutes, sample examination, qualifiedly can discharging to pack; Namely footgear personal cleansing liquid is prepared.
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| CN106753829A (en) * | 2016-11-22 | 2017-05-31 | 闫博文 | A kind of preparation method of antibacterial corrosion-free type air conditioner cleaning agent |
| CN107474989A (en) * | 2017-08-29 | 2017-12-15 | 许昌市建安区第二高级中学 | A kind of shoe washing liquid |
| CN110982640A (en) * | 2019-12-19 | 2020-04-10 | 陕西科技大学 | Humic acid type static electricity removing detergent and preparation method thereof |
| CN114292710A (en) * | 2020-02-12 | 2022-04-08 | 陕西科技大学 | Feather cleaning agent and preparation method thereof |
| CN115340683B (en) * | 2022-08-10 | 2023-08-29 | 深圳市富贵花实业有限公司 | Surfactant for cleaning PCB and preparation method thereof |
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| CN1119672A (en) * | 1995-08-24 | 1996-04-03 | 邓蜀生 | High-efficiency builder for detergent |
| CN102226135A (en) * | 2011-05-12 | 2011-10-26 | 荆立民 | Sterilizing/decontaminatimg/deodorizing shoe cleaning liquid and preparation method thereof |
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