CN103773165B - A kind of waterproof flame-retardant coating for wooden lampshade and preparation method thereof - Google Patents
A kind of waterproof flame-retardant coating for wooden lampshade and preparation method thereof Download PDFInfo
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- RNFJDJUURJAICM-UHFFFAOYSA-N 2,2,4,4,6,6-hexaphenoxy-1,3,5-triaza-2$l^{5},4$l^{5},6$l^{5}-triphosphacyclohexa-1,3,5-triene Chemical compound N=1P(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP=1(OC=1C=CC=CC=1)OC1=CC=CC=C1 RNFJDJUURJAICM-UHFFFAOYSA-N 0.000 title claims abstract description 23
- 239000003063 flame retardant Substances 0.000 title claims abstract description 21
- 238000002360 preparation method Methods 0.000 title claims abstract description 11
- 238000000576 coating method Methods 0.000 title abstract description 20
- 239000011248 coating agent Substances 0.000 title abstract description 17
- MQIUGAXCHLFZKX-UHFFFAOYSA-N Di-n-octyl phthalate Natural products CCCCCCCCOC(=O)C1=CC=CC=C1C(=O)OCCCCCCCC MQIUGAXCHLFZKX-UHFFFAOYSA-N 0.000 claims abstract description 16
- BJQHLKABXJIVAM-UHFFFAOYSA-N bis(2-ethylhexyl) phthalate Chemical compound CCCCC(CC)COC(=O)C1=CC=CC=C1C(=O)OCC(CC)CCCC BJQHLKABXJIVAM-UHFFFAOYSA-N 0.000 claims abstract description 16
- -1 borate ester Chemical class 0.000 claims abstract description 16
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 14
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 claims abstract description 13
- 239000004202 carbamide Substances 0.000 claims abstract description 13
- FPAFDBFIGPHWGO-UHFFFAOYSA-N dioxosilane;oxomagnesium;hydrate Chemical compound O.[Mg]=O.[Mg]=O.[Mg]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O FPAFDBFIGPHWGO-UHFFFAOYSA-N 0.000 claims abstract description 13
- 239000000839 emulsion Substances 0.000 claims abstract description 13
- WXZMFSXDPGVJKK-UHFFFAOYSA-N pentaerythritol Chemical compound OCC(CO)(CO)CO WXZMFSXDPGVJKK-UHFFFAOYSA-N 0.000 claims abstract description 13
- 239000000049 pigment Substances 0.000 claims abstract description 13
- 229920002401 polyacrylamide Polymers 0.000 claims abstract description 13
- 125000000118 dimethyl group Chemical group [H]C([H])([H])* 0.000 claims abstract description 12
- 229920002545 silicone oil Polymers 0.000 claims abstract description 12
- QDOXWKRWXJOMAK-UHFFFAOYSA-N dichromium trioxide Chemical compound O=[Cr]O[Cr]=O QDOXWKRWXJOMAK-UHFFFAOYSA-N 0.000 claims abstract description 11
- 239000003973 paint Substances 0.000 claims abstract description 5
- 239000000203 mixture Substances 0.000 claims description 20
- 238000000498 ball milling Methods 0.000 claims description 10
- 239000004327 boric acid Substances 0.000 claims description 5
- 238000000034 method Methods 0.000 claims description 2
- XZMCDFZZKTWFGF-UHFFFAOYSA-N Cyanamide Chemical compound NC#N XZMCDFZZKTWFGF-UHFFFAOYSA-N 0.000 claims 3
- 229920003171 Poly (ethylene oxide) Polymers 0.000 claims 3
- YSMRWXYRXBRSND-UHFFFAOYSA-N TOTP Chemical compound CC1=CC=CC=C1OP(=O)(OC=1C(=CC=CC=1)C)OC1=CC=CC=C1C YSMRWXYRXBRSND-UHFFFAOYSA-N 0.000 claims 3
- 229940059574 pentaerithrityl Drugs 0.000 claims 3
- 238000007599 discharging Methods 0.000 claims 1
- 229920000877 Melamine resin Polymers 0.000 abstract description 10
- JDSHMPZPIAZGSV-UHFFFAOYSA-N melamine Chemical compound NC1=NC(N)=NC(N)=N1 JDSHMPZPIAZGSV-UHFFFAOYSA-N 0.000 abstract description 10
- 229940051841 polyoxyethylene ether Drugs 0.000 abstract description 10
- 229920000056 polyoxyethylene ether Polymers 0.000 abstract description 10
- 230000000694 effects Effects 0.000 abstract description 3
- 150000002148 esters Chemical class 0.000 abstract description 3
- 239000007983 Tris buffer Substances 0.000 abstract description 2
- 229910019142 PO4 Inorganic materials 0.000 abstract 1
- 239000010452 phosphate Substances 0.000 abstract 1
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 abstract 1
- 230000001681 protective effect Effects 0.000 abstract 1
- JZZBTMVTLBHJHL-UHFFFAOYSA-N tris(2,3-dichloropropyl) phosphate Chemical compound ClCC(Cl)COP(=O)(OCC(Cl)CCl)OCC(Cl)CCl JZZBTMVTLBHJHL-UHFFFAOYSA-N 0.000 description 8
- 229940117975 chromium trioxide Drugs 0.000 description 4
- WGLPBDUCMAPZCE-UHFFFAOYSA-N chromium trioxide Inorganic materials O=[Cr](=O)=O WGLPBDUCMAPZCE-UHFFFAOYSA-N 0.000 description 4
- GAMDZJFZMJECOS-UHFFFAOYSA-N chromium(6+);oxygen(2-) Chemical compound [O-2].[O-2].[O-2].[Cr+6] GAMDZJFZMJECOS-UHFFFAOYSA-N 0.000 description 4
- 239000000463 material Substances 0.000 description 4
- 238000003756 stirring Methods 0.000 description 4
- BTBUEUYNUDRHOZ-UHFFFAOYSA-N Borate Chemical compound [O-]B([O-])[O-] BTBUEUYNUDRHOZ-UHFFFAOYSA-N 0.000 description 3
- 238000005034 decoration Methods 0.000 description 2
- 230000003796 beauty Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- AMTWCFIAVKBGOD-UHFFFAOYSA-N dioxosilane;methoxy-dimethyl-trimethylsilyloxysilane Chemical compound O=[Si]=O.CO[Si](C)(C)O[Si](C)(C)C AMTWCFIAVKBGOD-UHFFFAOYSA-N 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
- 230000003000 nontoxic effect Effects 0.000 description 1
- 229940083037 simethicone Drugs 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 230000009967 tasteless effect Effects 0.000 description 1
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- Paints Or Removers (AREA)
- Fireproofing Substances (AREA)
Abstract
本发明提供一种木质灯罩用防水阻燃涂料及其制备方法，该涂料以质量份计含有以下成分：季戊四醇10～22份，三聚氰胺8～20份，滑石粉15～25份，磷酸三(2,3-二氯丙基)酯6～14份，硼酸酯1～2.2份，邻苯二甲酸二辛酯5.8～13.2份，水15～25份，尿素12～20份，二甲基硅油0.06～0.14份，三氧化二铬0.2～0.5份，烷基酚聚氧乙烯醚0.05～0.15份，聚丙烯酰胺乳液90～105份，颜料0.5～1.3份。本发明提供的涂料具有优良的防水和阻燃功能，并且其耐摩擦性能显著，对木质灯罩具有很好的保护和装饰作用。The invention provides a waterproof and flame-retardant coating for wooden lampshades and a preparation method thereof. The coating contains the following components in parts by mass: 10-22 parts of pentaerythritol, 8-20 parts of melamine, 15-25 parts of talcum powder, tris(2) phosphate , 6-14 parts of 3-dichloropropyl) ester, 1-2.2 parts of borate ester, 5.8-13.2 parts of dioctyl phthalate, 15-25 parts of water, 12-20 parts of urea, dimethyl silicone oil 0.06-0.14 parts, 0.2-0.5 parts of dichromium trioxide, 0.05-0.15 parts of alkylphenol polyoxyethylene ether, 90-105 parts of polyacrylamide emulsion, 0.5-1.3 parts of pigment. The paint provided by the invention has excellent waterproof and flame-retardant functions, and has remarkable friction resistance, and has good protective and decorative effects on wooden lampshades.
Description
技术领域 technical field
本发明涉及涂料领域，尤其涉及一种木质灯罩用防水阻燃涂料及其制备方法。 The invention relates to the field of coatings, in particular to a waterproof and flame-retardant coating for wooden lampshades and a preparation method thereof.
背景技术 Background technique
木质灯罩具有环保安全、古朴美观等特点，是室内装饰的一个重要组成部分。木质灯罩也存在容易吸水变潮，遇火易燃的缺点。因此，需要在木质灯罩表面涂一层涂料，使其具有防水阻燃的特性，用以延长灯罩的使用寿命，同时增加其美观度。但是，市场上现有的木质灯罩用涂料的防水和阻燃效果差，同时耐磨性能也不高，使其的适用范围受到了限制。 The wooden lampshade has the characteristics of environmental protection, safety, simplicity and beauty, and is an important part of interior decoration. Wooden lampshades also have the disadvantages of easily absorbing water and becoming damp, and being flammable in case of fire. Therefore, it is necessary to coat a layer of paint on the surface of the wooden lampshade to make it waterproof and flame-retardant, so as to prolong the service life of the lampshade and increase its aesthetics. However, the waterproof and flame-retardant effect of existing coatings for wooden lampshades on the market is poor, and the wear resistance is not high at the same time, so that its scope of application is limited.
发明内容 Contents of the invention
解决的技术问题：针对现有的木质灯罩用涂料防水、阻燃和耐磨效果差的缺点，本发明提供一种木质灯罩用防水阻燃涂料及其制备方法。 Technical problem to be solved: Aiming at the disadvantages of poor waterproof, flame-retardant and wear-resistant effects of existing coatings for wooden lampshades, the invention provides a waterproof and flame-retardant coating for wooden lampshades and a preparation method thereof.
技术方案：一种木质灯罩用防水阻燃涂料，以质量份计含有以下成分：季戊四醇10～22份，三聚氰胺8～20份，滑石粉15～25份，磷酸三(2,3-二氯丙基)酯6～14份，硼酸酯1～2.2份，邻苯二甲酸二辛酯5.8～13.2份，水15～25份，尿素12～20份，二甲基硅油0.06～0.14份，三氧化二铬0.2～0.5份，烷基酚聚氧乙烯醚0.05～0.15份，聚丙烯酰胺乳液90～105份，颜料0.5～1.3份。 Technical solution: A waterproof and flame-retardant coating for wooden lampshades, which contains the following components in parts by mass: 10-22 parts of pentaerythritol, 8-20 parts of melamine, 15-25 parts of talcum powder, tris(2,3-dichloropropane phosphate) 6-14 parts of base) ester, 1-2.2 parts of boric acid ester, 5.8-13.2 parts of dioctyl phthalate, 15-25 parts of water, 12-20 parts of urea, 0.06-0.14 parts of dimethyl silicone oil, three 0.2-0.5 parts of dichromium oxide, 0.05-0.15 parts of alkylphenol polyoxyethylene ether, 90-105 parts of polyacrylamide emulsion, and 0.5-1.3 parts of pigment.
上述所述的一种木质灯罩用防水阻燃涂料，以质量份计含有以下成分：季戊四醇16份，三聚氰胺14份，滑石粉20份，磷酸三(2,3-二氯丙基)酯10份，硼酸酯1.6份，邻苯二甲酸二辛酯9.5份，水20份，尿素16份，二甲基硅油0.1份，三氧化二铬0.35份，烷基酚聚氧乙烯醚0.1份，聚丙烯酰胺乳液98份，颜料0.9份。 The above-mentioned waterproof and flame-retardant coating for a wooden lampshade contains the following components in parts by mass: 16 parts of pentaerythritol, 14 parts of melamine, 20 parts of talcum powder, and 10 parts of tris(2,3-dichloropropyl) phosphate , 1.6 parts of borate ester, 9.5 parts of dioctyl phthalate, 20 parts of water, 16 parts of urea, 0.1 part of dimethyl silicone oil, 0.35 part of dichromium trioxide, 0.1 part of alkylphenol polyoxyethylene ether, poly Acrylamide emulsion 98 parts, pigment 0.9 part.
上述所述的一种木质灯罩用防水阻燃涂料的制备步骤如下：将季戊四醇、三聚氰胺、滑石粉、磷酸三(2,3-二氯丙基)酯、硼酸酯、邻苯二甲酸二辛酯和水加入搅拌器中，搅拌混合0.5h，然后加入颜料混合均匀，接着进行球磨，球磨12h后出料，再与尿素、二甲基硅油、烷基酚聚氧乙烯醚和三氧化二铬混合均匀，最后加入聚丙烯酰胺乳液，混合均匀后即得成品。 The preparation steps of the above-mentioned waterproof and flame-retardant coating for a wooden lampshade are as follows: pentaerythritol, melamine, talcum powder, tris (2,3-dichloropropyl) phosphate, boric acid ester, dioctyl phthalate Put the ester and water into the mixer, stir and mix for 0.5h, then add the pigment and mix evenly, then carry out ball milling, and discharge the material after ball milling for 12 hours, then mix with urea, dimethyl silicone oil, alkylphenol polyoxyethylene ether and chromium trioxide Mix well, and finally add polyacrylamide emulsion, mix well to get the finished product.
有益效果：本发明提供的一种木质灯罩用防水阻燃涂料及其制备方法，该涂料无毒无味，安全环保，具有优良的防水和阻燃功能，并且其耐摩擦性能显著，对木质灯罩具有很好的保护和装饰作用。 Beneficial effects: the present invention provides a waterproof and flame-retardant coating for wooden lampshades and a preparation method thereof. The coating is non-toxic, tasteless, safe and environmentally friendly, has excellent waterproof and flame-retardant functions, and has remarkable friction resistance, and has a strong impact on wooden lampshades. Good protection and decoration.
具体实施方式 detailed description
实施例1Example 1
本实施例提供一种木质灯罩用防水阻燃涂料，以质量份计含有以下成分：季戊四醇10份，三聚氰胺8份，滑石粉15份，磷酸三(2,3-二氯丙基)酯6份，硼酸酯1份，邻苯二甲酸二辛酯5.8份，水15份，尿素12份，二甲基硅油0.06份，三氧化二铬0.2份，烷基酚聚氧乙烯醚0.05份，聚丙烯酰胺乳液90份，颜料0.5份。 This embodiment provides a waterproof and flame-retardant coating for wooden lampshades, which contains the following components in parts by mass: 10 parts of pentaerythritol, 8 parts of melamine, 15 parts of talcum powder, and 6 parts of tris(2,3-dichloropropyl) phosphate , 1 part of borate ester, 5.8 parts of dioctyl phthalate, 15 parts of water, 12 parts of urea, 0.06 part of dimethyl silicone oil, 0.2 part of dichromium trioxide, 0.05 part of alkylphenol polyoxyethylene ether, poly Acrylamide emulsion 90 parts, pigment 0.5 part.
一种木质灯罩用防水阻燃涂料的制备步骤如下：将季戊四醇、三聚氰胺、滑石粉、磷酸三(2,3-二氯丙基)酯、硼酸酯、邻苯二甲酸二辛酯和水加入搅拌器中，搅拌混合0.5h，然后加入颜料混合均匀，接着进行球磨，球磨12h后出料，再与尿素、二甲基硅油、烷基酚聚氧乙烯醚和三氧化二铬混合均匀，最后加入聚丙烯酰胺乳液，混合均匀后即得成品。 The preparation steps of a waterproof flame-retardant coating for a wooden lampshade are as follows: add pentaerythritol, melamine, talcum powder, tris(2,3-dichloropropyl) phosphate, borate, dioctyl phthalate and water In the mixer, stir and mix for 0.5h, then add the pigment and mix evenly, then carry out ball milling, discharge the material after ball milling for 12h, then mix evenly with urea, dimethyl silicone oil, alkylphenol polyoxyethylene ether and chromium trioxide, and finally Add polyacrylamide emulsion and mix well to get the finished product.
实施例2Example 2
本实施例提供一种木质灯罩用防水阻燃涂料，以质量份计含有以下成分：季戊四醇22份，三聚氰胺20份，滑石粉25份，磷酸三(2,3-二氯丙基)酯14份，硼酸酯2.2份，邻苯二甲酸二辛酯13.2份，水25份，尿素20份，二甲基硅油0.14份，三氧化二铬0.5份，烷基酚聚氧乙烯醚0.15份，聚丙烯酰胺乳液105份，颜料1.3份。 This embodiment provides a waterproof and flame-retardant coating for wooden lampshades, which contains the following components in parts by mass: 22 parts of pentaerythritol, 20 parts of melamine, 25 parts of talcum powder, and 14 parts of tris(2,3-dichloropropyl) phosphate , 2.2 parts of borate ester, 13.2 parts of dioctyl phthalate, 25 parts of water, 20 parts of urea, 0.14 part of simethicone, 0.5 part of dichromium trioxide, 0.15 part of alkylphenol polyoxyethylene ether, poly Acrylamide emulsion 105 parts, pigment 1.3 parts.
一种木质灯罩用防水阻燃涂料的制备步骤如下：将季戊四醇、三聚氰胺、滑石粉、磷酸三(2,3-二氯丙基)酯、硼酸酯、邻苯二甲酸二辛酯和水加入搅拌器中，搅拌混合0.5h，然后加入颜料混合均匀，接着进行球磨，球磨12h后出料，再与尿素、二甲基硅油、烷基酚聚氧乙烯醚和三氧化二铬混合均匀，最后加入聚丙烯酰胺乳液，混合均匀后即得成品。 The preparation steps of a waterproof flame-retardant coating for a wooden lampshade are as follows: add pentaerythritol, melamine, talcum powder, tris(2,3-dichloropropyl) phosphate, borate, dioctyl phthalate and water In the mixer, stir and mix for 0.5h, then add the pigment and mix evenly, then carry out ball milling, discharge the material after ball milling for 12h, then mix evenly with urea, dimethyl silicone oil, alkylphenol polyoxyethylene ether and chromium trioxide, and finally Add polyacrylamide emulsion and mix well to get the finished product.
实施例3Example 3
本实施例提供一种木质灯罩用防水阻燃涂料，以质量份计含有以下成分：季戊四醇16份，三聚氰胺14份，滑石粉20份，磷酸三(2,3-二氯丙基)酯10份，硼酸酯1.6份，邻苯二甲酸二辛酯9.5份，水20份，尿素16份，二甲基硅油0.1份，三氧化二铬0.35份，烷基酚聚氧乙烯醚0.1份，聚丙烯酰胺乳液98份，颜料0.9份。 This embodiment provides a waterproof and flame-retardant coating for wooden lampshades, which contains the following components in parts by mass: 16 parts of pentaerythritol, 14 parts of melamine, 20 parts of talcum powder, and 10 parts of tris(2,3-dichloropropyl) phosphate , 1.6 parts of borate ester, 9.5 parts of dioctyl phthalate, 20 parts of water, 16 parts of urea, 0.1 part of dimethyl silicone oil, 0.35 part of dichromium trioxide, 0.1 part of alkylphenol polyoxyethylene ether, poly Acrylamide emulsion 98 parts, pigment 0.9 part.
一种木质灯罩用防水阻燃涂料的制备步骤如下：将季戊四醇、三聚氰胺、滑石粉、磷酸三(2,3-二氯丙基)酯、硼酸酯、邻苯二甲酸二辛酯和水加入搅拌器中，搅拌混合0.5h，然后加入颜料混合均匀，接着进行球磨，球磨12h后出料，再与尿素、二甲基硅油、烷基酚聚氧乙烯醚和三氧化二铬混合均匀，最后加入聚丙烯酰胺乳液，混合均匀后即得成品。 The preparation steps of a waterproof flame-retardant coating for a wooden lampshade are as follows: add pentaerythritol, melamine, talcum powder, tris(2,3-dichloropropyl) phosphate, borate, dioctyl phthalate and water In the mixer, stir and mix for 0.5h, then add the pigment and mix evenly, then carry out ball milling, discharge the material after ball milling for 12h, then mix evenly with urea, dimethyl silicone oil, alkylphenol polyoxyethylene ether and chromium trioxide, and finally Add polyacrylamide emulsion and mix well to get the finished product.
上述述实施例1～实施例3的一种木质灯罩用防水阻燃涂料的技术性能指标，其检测结果如下： The technical performance index of a kind of wooden lampshade waterproof flame-retardant coating of above-mentioned embodiment 1～embodiment 3, its detection result is as follows:
检测结果 Test results
以上对本发明实施例进行了详细介绍，对于本领域的一般技术人员，依据本发明实施例的思想，在具体实施方式及应用范围上均会有改变之处，综上所述，本说明书内容不应理解为对本发明的限制。 The embodiments of the present invention have been described in detail above. For those skilled in the art, according to the ideas of the embodiments of the present invention, there will be changes in the specific implementation and application scope. In summary, the contents of this specification are not It should be understood as a limitation of the present invention.
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101654579A (en) * | 2008-12-23 | 2010-02-24 | 海龙艾默生（镇江）能源科技有限公司 | Environment-friendly cable fireproof paint and manufacturing method thereof |
| JP4557637B2 (en) * | 2004-08-25 | 2010-10-06 | 大王製紙株式会社 | Flame retardant mulching material |
| CN102061116A (en) * | 2009-11-13 | 2011-05-18 | 淄博高新技术产业开发区金霞建材厂 | Flame-retardant waterproof coating |
| CN102153937A (en) * | 2011-05-13 | 2011-08-17 | 惠东美新塑木型材制品有限公司 | Surface fireproof coating of wood plastic composite material and preparation method of surface fireproof coating |
| CN102850890A (en) * | 2012-09-05 | 2013-01-02 | 江苏正泰医药化工有限公司 | Waterproof coating material |
-
2014
- 2014-01-20 CN CN201410024303.7A patent/CN103773165B/en not_active Expired - Fee Related
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP4557637B2 (en) * | 2004-08-25 | 2010-10-06 | 大王製紙株式会社 | Flame retardant mulching material |
| CN101654579A (en) * | 2008-12-23 | 2010-02-24 | 海龙艾默生（镇江）能源科技有限公司 | Environment-friendly cable fireproof paint and manufacturing method thereof |
| CN102061116A (en) * | 2009-11-13 | 2011-05-18 | 淄博高新技术产业开发区金霞建材厂 | Flame-retardant waterproof coating |
| CN102153937A (en) * | 2011-05-13 | 2011-08-17 | 惠东美新塑木型材制品有限公司 | Surface fireproof coating of wood plastic composite material and preparation method of surface fireproof coating |
| CN102850890A (en) * | 2012-09-05 | 2013-01-02 | 江苏正泰医药化工有限公司 | Waterproof coating material |
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| CN103773165A (en) | 2014-05-07 |
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