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CN103735428A - Keratin hair conditioner and preparation method thereof - Google Patents

Keratin hair conditioner and preparation method thereof Download PDF

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Publication number
CN103735428A
CN103735428A CN201310752202.7A CN201310752202A CN103735428A CN 103735428 A CN103735428 A CN 103735428A CN 201310752202 A CN201310752202 A CN 201310752202A CN 103735428 A CN103735428 A CN 103735428A
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component
keratin
hair conditioner
emulsifying pot
preparation
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CN201310752202.7A
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CN103735428B (en
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胡志标
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GUANGZHOU CITY BAIYUN DISTRICT DARONG FINE CHEMICAL Co Ltd
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GUANGZHOU CITY BAIYUN DISTRICT DARONG FINE CHEMICAL Co Ltd
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Abstract

The invention relates to a keratin hair conditioner. The keratin hair conditioner is prepared from cetostearyl alcohol, behenyl trimethyl ammonium chloride, stearin, cetyl trimethyl ammonium chloride, cyclopentasiloxane, C12-15 benzoate, dimethyl siloxane, diamino siloxane, propylene glycol, sodium pyrrolidone carboxylate, olive oil, hydrolyzed keratin, previtamin B5, methylparaben, propylparaben, 2-methyl-4-isothiazolin-3-one, essence and water. The invention further relates a method for preparing the keratin hair conditioner. The keratin hair conditioner can be used for enabling hair to be smoother and glossier, and can be used for repairing the damage of hairlines to enable the damaged hairlines to be subjected to excellent repairing care.

Description

A kind of keratin hair conditioner and preparation method thereof
Technical field
The present invention relates to household chemicals field, particularly a kind of keratin hair conditioner and preparation method thereof.
Background technology
Environment in recent years pollution grows worse, in atmosphere pollution, cause the compositions such as acidity that hair decomposes to increase, uitraviolet intensity increases, and the change of consumption habit, the factors such as electricity is sent out, hair-waving, hair dyeing are more universal all cause present a big chunk crowd's a hair epidermis to be subject to very large destruction, the phenomenon such as dry hair, fracture ubiquity, hair conditioner expedites the emergence of thus.In prior art, hair conditioner is generally all comprised of cationic compound, emulsifying agent, thickening agent, esters, due to its have cation and weak acid feature, the electrostatic accumulation bringing due to washing for hair, difficult combing, without the situation such as glossy, withered, make moderate progress, if but use every day, what cation was too much is deposited on hair, makes hair send out weight, lackluster, easily dirty, also can scalp irritation occur itching, the phenomenons such as dandruff.
Summary of the invention
In order to overcome the deficiencies in the prior art, the object of the present invention is to provide a kind of can make hair more smooth, have more glossyly, and can repair hair damage, make impaired hair obtain keratin hair conditioner of splendid restoration care and preparation method thereof.
For addressing the above problem, the technical solution adopted in the present invention is as follows:
A keratin hair conditioner, is prepared from by following compositions in weight percentage:
Figure BDA0000451721320000011
Figure BDA0000451721320000021
Surplus is water.
A preparation method for keratin hair conditioner, comprises step:
A. the component A of water and propylene glycol composition is added in water pot and heated up in rear suction emulsifying pot;
B. the B component of cetearyl alcohol, mountain Yu base trimethyl ammonium chloride, tristerin, CTAB, methyl hydroxybenzoate and propylparaben composition is added in oil phase pot and in suction emulsifying pot, stirred with component A after intensification;
C. by cyclopentasiloxane, C 12-15the component C that benzoate, dimethyl siloxane, two amino silicone and olive oil form adds in the emulsifying pot containing the component A stirring and B, stirs homogenizing 5 minutes, the processing of lowering the temperature;
D. component D pyrrolidone sodium carboxylate, hydrolysis of keratin, dexpanthenol, MIT and essence being formed joins in the emulsifying pot containing component A, B, C after cooling processing and stirs, and obtains keratin hair conditioner.
Preferably, suction emulsifying pot after component A is warming up to 85 ℃ in described step a.
Preferably, in described step b, B component is warming up to 80 ℃, and is incubated to the rear suction emulsifying pot of the whole fusings of B component.
Preferably, in described step c, component A, B, C stirred homogenizing after 5 minutes, were incubated 10 minutes, and then were cooled to below 45 ℃.
Compared to existing technology, beneficial effect of the present invention is:
1, it is careful that A component forms an outward appearance, the cationic conditioning mastic of high brightness, so wherein two amino silicones because the flexibility of hair is promoted greatly with two amino, C 12-15benzoate has fabulous dispersibility, and film forming and oils and fats in this product of A can be disperseed fast, reaches to sprawl more evenly, uses after this product, dry send out more smooth, glossy;
2, B component hair nutrition supplementing, repair impaired hair quality, hydrolysis of keratin is wherein identical with hair structure with dexpanthenol, very easily fill up hair because dying, scald and the cavity of the impaired formation of hot moulding, pyrrolidone sodium carboxylate is the extremely strong film former of a kind of moisture retention, propylene glycol is as infiltration wetting agent, accelerate the infiltration of nutritional labeling, olive oil can be penetrated into sends out the oils and fats that core supplements hair loss, can not bring extra burden to hair;
So filling up of the hydrolysis of keratin that 3 these products pass through and dexpanthenol, repairs, then wraps up by the film forming of pyrrolidone sodium carboxylate and siloxanes, then moistens with olive oil, makes impaired hair quality obtain splendid restoration care.
The specific embodiment
Below in conjunction with the specific embodiment, the present invention is described in further detail.
Embodiment 1
Get respectively following materials: 81.6% water, 3.0% propylene glycol, 5.0% cetearyl alcohol, 1.2% mountain Yu base trimethyl ammonium chloride, 1.2% tristerin, 1.2% CTAB, 0.2% methyl hydroxybenzoate, 0.1% propylparaben, 1.0% cyclopentasiloxane, 0.5%C 12-15benzoate, 1.0% dimethyl siloxane, 0.5% pair of amino silicone, 1.5% olive oil, 0.5% pyrrolidone sodium carboxylate, 0.5% hydrolysis of keratin, 0.5% dexpanthenol, 0.1%2-methyl-4-isothiazoline-3-ketone and 0.4% essence.
Above-mentioned raw materials is followed these steps to add and in vacuum emulsification pot, prepares keratin hair conditioner:
A. component A water and propylene glycol being formed add in water pot, be warming up to 85 ℃ after in suction emulsifying pot;
B. B component cetearyl alcohol, mountain Yu base trimethyl ammonium chloride, tristerin, CTAB, methyl hydroxybenzoate and propylparaben being formed adds in oil phase pot and is warming up to 80 ℃, and is incubated to B component and all in suction emulsifying pot, stirs with component A after fusing;
C. by cyclopentasiloxane, C 12-15the component C that benzoate, dimethyl siloxane, two amino silicone and olive oil form adds in the emulsifying pot containing the component A stirring and B, stirs homogenizing 5 minutes, is incubated 10 minutes, and then is cooled to below 45 ℃;
D. component D pyrrolidone sodium carboxylate, hydrolysis of keratin, dexpanthenol, MIT and essence being formed joins in the emulsifying pot containing component A, B, C after cooling processing and stirs, and detects and obtain keratin hair conditioner A1.
Embodiment 2
Get respectively following materials: 70.5% water, 5.0% propylene glycol, 7.0% cetearyl alcohol, 2.0% mountain Yu base trimethyl ammonium chloride, 2.0% tristerin, 2.0% CTAB, 0.2% methyl hydroxybenzoate, 0.1% propylparaben, 2.0% cyclopentasiloxane, 1.0%C 12-15benzoate, 1.5% dimethyl siloxane, 1.0% pair of amino silicone, 2.0% olive oil, 1.0% pyrrolidone sodium carboxylate, 1.0% hydrolysis of keratin, 0.8% dexpanthenol, 0.1%2-methyl-4-isothiazoline-3-ketone and 0.8% essence.
Above-mentioned raw materials is followed these steps to add and in vacuum emulsification pot, prepares keratin hair conditioner:
A. component A water and propylene glycol being formed add in water pot, be warming up to 85 ℃ after in suction emulsifying pot;
B. B component cetearyl alcohol, mountain Yu base trimethyl ammonium chloride, tristerin, CTAB, methyl hydroxybenzoate and propylparaben being formed adds in oil phase pot and is warming up to 80 ℃, and is incubated to B component and all in suction emulsifying pot, stirs with component A after fusing;
C. by cyclopentasiloxane, C 12-15the component C that benzoate, dimethyl siloxane, two amino silicone and olive oil form adds in the emulsifying pot containing the component A stirring and B, stirs homogenizing 5 minutes, is incubated 10 minutes, and then is cooled to below 45 ℃;
D. component D pyrrolidone sodium carboxylate, hydrolysis of keratin, dexpanthenol, MIT and essence being formed joins in the emulsifying pot containing component A, B, C after cooling processing and stirs, and detects and obtain keratin hair conditioner A2.
Embodiment 3
Get respectively following materials: 75.2% water, 4.0% propylene glycol, 6.0% cetearyl alcohol, 1.5% mountain Yu base trimethyl ammonium chloride, 1.5% tristerin, 2.0% CTAB, 0.2% methyl hydroxybenzoate, 0.1% propylparaben, 2.0% cyclopentasiloxane, 0.8%C 12-15benzoate, 1.2% dimethyl siloxane, 0.8% pair of amino silicone, 1.8% olive oil, 0.8% pyrrolidone sodium carboxylate, 0.6% hydrolysis of keratin, 0.6% dexpanthenol, 0.1%2-methyl-4-isothiazoline-3-ketone and 0.8% essence.
Above-mentioned raw materials is followed these steps to add and in vacuum emulsification pot, prepares keratin hair conditioner:
A. component A water and propylene glycol being formed add in water pot, be warming up to 85 ℃ after in suction emulsifying pot;
B. B component cetearyl alcohol, mountain Yu base trimethyl ammonium chloride, tristerin, CTAB, methyl hydroxybenzoate and propylparaben being formed adds in oil phase pot and is warming up to 80 ℃, and is incubated to B component and all in suction emulsifying pot, stirs with component A after fusing;
C. by cyclopentasiloxane, C 12-15the component C that benzoate, dimethyl siloxane, two amino silicone and olive oil form adds in the emulsifying pot containing the component A stirring and B, stirs homogenizing 5 minutes, is incubated 10 minutes, and then is cooled to below 45 ℃;
D. component D pyrrolidone sodium carboxylate, hydrolysis of keratin, dexpanthenol, MIT and essence being formed joins in the emulsifying pot containing component A, B, C after cooling processing and stirs, and detects and obtain keratin hair conditioner A3.
Hair caring chamber testing experiment
Take China on the market well-known product B salable A1, A2, A3 in reference product and embodiment contrast respectively.Experimenter's double blinding two products on probation provide 0-10 to indices and divide, and representative in 10 minutes is own the most satisfied to this performance, and 0 part of representative is dissatisfied.Experimenter is the women of routine use hair care product.30 experimenters are divided into 3 groups at random, and each group adopts identical program and time practical B product on half hair of experimenter by professional teacher respectively, uses A1, A2 or A3 on second half hair, then with same amount enough water, rinses out.Experimenter oneself is hair dryness finalization.Application form is issued to 30 professional teachers and 30 experimenters fill in respectively corresponding project.Result is as following table 1:
Table 1, hair caring chamber testing experiment result
? B A1 A2 A3
Slipping after top 7.2 7.3 7.6 7.4
Cardability after dispersion 7 7.2 7.3 7.4
Soft and smooth property during bath 7.2 7.2 7.6 7.5
Cardability after bath 6.8 7.1 7.5 7.5
The wet feel of sending out 6.9 7.2 7.6 7.5
Wet Comb rationality 7 7.2 7.4 7.4
Antistatic 6.6 6.8 7 7
The easy degree of shaping 6.4 6.3 6.3 6.3
The dry feel of sending out 6.6 7 7.2 7.2
The dry elasticity of sending out 6.8 7.2 7.3 7.2
Total satisfaction 6.8 7.1 7.4 7.3
As can be seen from Table 1, compare existing product, the keratin hair conditioner that the present invention produces make hair more smooth, have more glossyly, and can better repair hair damage, increase the elasticity of hair, hair is had to better repairing effect.
To one skilled in the art, can make other various corresponding changes and deformation according to technical scheme described above and design, and within these all changes and deformation all should belong to the protection domain of the claims in the present invention.

Claims (5)

1. a keratin hair conditioner, is characterized in that, by following compositions in weight percentage, is prepared from:
Figure FDA0000451721310000011
Surplus is water.
2. the preparation method of keratin hair conditioner described in claim 1, is characterized in that, comprises step:
A. the component A of water and propylene glycol composition is added in water pot and heated up in rear suction emulsifying pot;
B. the B component of cetearyl alcohol, mountain Yu base trimethyl ammonium chloride, tristerin, CTAB, methyl hydroxybenzoate and propylparaben composition is added in oil phase pot and in suction emulsifying pot, stirred with component A after intensification;
C. by cyclopentasiloxane, C 12-15the component C that benzoate, dimethyl siloxane, two amino silicone and olive oil form adds in the emulsifying pot containing the component A stirring and B, stirs homogenizing 5 minutes, the processing of lowering the temperature;
D. component D pyrrolidone sodium carboxylate, hydrolysis of keratin, dexpanthenol, MIT and essence being formed joins in the emulsifying pot containing component A, B, C after cooling processing and stirs, and obtains keratin hair conditioner.
3. the preparation method of keratin hair conditioner as claimed in claim 2, is characterized in that, suction emulsifying pot after component A is warming up to 85 ℃ in described step a.
4. the preparation method of keratin hair conditioner as claimed in claim 2, is characterized in that, in described step b, B component is warming up to 80 ℃, and is incubated to the rear suction emulsifying pot of the whole fusings of B component.
5. the preparation method of keratin hair conditioner as claimed in claim 2, is characterized in that, in described step c, component A, B, C stirred homogenizing after 5 minutes, were incubated 10 minutes, and then were cooled to below 45 ℃.
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CN105534794A (en) * 2015-12-31 2016-05-04 胡鹏 Cleaning salt
CN106726980A (en) * 2016-12-28 2017-05-31 安徽紫檀科技有限公司 Hair conditioner for preventing alopecia and preparation method thereof
CN107569423A (en) * 2017-09-25 2018-01-12 吉安市御美丽健康产业股份有限公司 A kind of ginseng hair protective element for repairing damaged hair and preparation method thereof
CN108026692A (en) * 2015-08-31 2018-05-11 株式会社岛精机制作所 Process the manufacture method of fiber and the processing method of the processing fiber, the method for suppression animal origin damage and animal origin
WO2018213652A1 (en) 2017-05-19 2018-11-22 The Procter & Gamble Company Hair care composition comprising non-volatile hydrocarbon oils and fatty esters of benzoic acid
WO2018213651A1 (en) 2017-05-19 2018-11-22 The Procter & Gamble Company Hair care composition comprising triester compounds and fatty esters of benzoic acid
CN109044936A (en) * 2018-10-26 2018-12-21 广州市白云区大荣精细化工有限公司 A kind of hair nursing cream and preparation method thereof
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US11944696B2 (en) 2010-07-02 2024-04-02 The Procter & Gamble Company Detergent product and method for making same
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US11951194B2 (en) 2017-01-27 2024-04-09 The Procter & Gamble Company Compositions in the form of dissolvable solid structures comprising effervescent agglomerated particles
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US12029799B2 (en) 2017-05-16 2024-07-09 The Procter & Gamble Company Conditioning hair care compositions in the form of dissolvable solid structures
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