CN103614005A - Aqueous woodenware paint titanium white slurry and its preparation method - Google Patents
Aqueous woodenware paint titanium white slurry and its preparation method Download PDFInfo
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- CN103614005A CN103614005A CN201310537989.5A CN201310537989A CN103614005A CN 103614005 A CN103614005 A CN 103614005A CN 201310537989 A CN201310537989 A CN 201310537989A CN 103614005 A CN103614005 A CN 103614005A
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Abstract
The invention relates to a woodenware paint and a preparation method, and especially relates to aqueous woodenware paint titanium white slurry and its preparation method, which belong to the paint field for building decoration. The provided aqueous woodenware paint titanium white slurry comprises the following raw materials by weight: 13-14 parts of water, 5-6 parts of dispersant, 0.45-0.55 parts of wetting agent, 0.5-0.6 parts of antifoaming agent, 2.0-2.5 parts of cosolvent and 70-75 parts of titanium dioxide. The prepared aqueous woodenware paint titanium white slurry has good system stability, good moisture retention and difficult secondary flocculation, addition of the slurry can be carried out by simple stirring, so that the production efficiency is effectively increased.
Description
Technical field
The present invention relates to a kind of titanium dioxide slurry and preparation method thereof, particularly a kind of aqueous woodware paint titanium dioxide slurry and preparation method thereof, belongs to architectural decoration paint field.
Background technology
Along with economic progress and the deterioration of environment, people are also more and more higher to the requirement of environmental protection, healthy living in recent years, and increasing enterprise starts to have a go at aqueous woodware paint.
Yet the production problem of aqueous wooden ware white finish paint always tired jail every slip-stick artist, in order to obtain the titanium dioxide slurry of stably dispersing, in water-borne coatings formula system, conventionally first titanium dioxide is disperseed to make slurry in water, then slurry is joined and in emulsion, makes coating.
But, there is following problem in existing titanium dioxide slurry preparation technology: during due to high speed dispersion titanium dioxide, does not introduce Mierocrystalline cellulose, and the water of pulling an oar in formula system adds limited, cannot well soak titanium dioxide, quick-drying while therefore causing titanium dioxide slurry to disperse, easily forms secondary flocculation, jitter time is more of a specified duration, titanium dioxide slurry flocculation is more, and titanium dioxide cannot be well distributed in the middle of whole system, causes system stability poor; In addition, at present the pigment content of titanium dioxide slurry is generally all less than 70%, and slurry system easily layering again, causes while adding the problem of high speed dispersion again.
Summary of the invention
In order to solve the above-mentioned problems in the prior art, the invention provides a kind of aqueous woodware paint titanium dioxide slurry and preparation method thereof, the prepared aqueous woodware paint titanium dioxide slurry system stability of the present invention is good, moisture retention is good, be difficult for causing secondary flocculation, only need simple agitation to add, effectively improved production efficiency.
Technical scheme of the present invention provides a kind of aqueous woodware paint titanium dioxide slurry, mainly formulated by following weight proportion by following raw material:
In said components, water, dispersion agent, wetting agent, defoamer, solubility promoter, titanium dioxide are the necessary components of preparation aqueous woodware paint titanium dioxide slurry of the present invention;
Described water is ordinary tap water, and the carrier during as titanium dioxide making beating, regulates making beating viscosity;
Described dispersion agent adopts the block copolymer solution that contains pigment affinity groups or the acrylate copolymer Solution Dispersion agent that contains pigment affinity groups, and in help system, color stuffing is dispersed in system uniformly;
Described wetting agent adopts polyhydroxy ether class non-ionic wetting agent or oleoyl epoxy alkane segmented copolymer, the wetting agent disperseing as color stuffing, the viscosity of color stuffing dispersion pulp in reduction system;
Described defoamer adopts modified dimethyl polysiloxane solution, in system, can suppress Bubble formation, prevents from producing bubble in brushing and spraying process;
Described solubility promoter adopts propylene glycol, is used for extending the open hour of system, and the system that prevents is flocculated because quick-drying causes color stuffing secondary;
Described titanium dioxide adopts Rutile type Titanium Dioxide or anatase thpe white powder, as dispersed object in system.
In addition, technique scheme of the present invention can also further be improved as follows:
A kind of aqueous woodware paint titanium dioxide slurry of the present invention, also comprises the raw material of following weight proportion:
Water 2-8 part
Anti-settling agent 0.5-0.8 part
Sanitas 0.2-0.3 part.
Described anti-settling agent adopts not containing the modified urea solution of N-Methyl pyrrolidone, and effect is to prevent that system is after storing for some time, and color stuffing is deposited to container bottom, is difficult to stir.
Described sanitas adopts isothiazolinone disinfecting agent, is used for the growth of bacterium in inhibition system, plays the effect of sterilization and anticorrosion.
The above-mentioned weight proportion of the combination of these components and each component, determines by lot of experiments, and the paint film that aforesaid combination and weight proportion form the prepared aqueous woodware paint titanium dioxide slurry of the present invention has the excellent balance of every technical feature.
The method of preparing aqueous woodware paint titanium dioxide slurry of the present invention comprises following step of sequentially carrying out:
Start dispersion machine and adjust rotating speed to 700-800 rev/min, under this speed, first slowly add successively water 13-14 part, dispersion agent 5-6 part, wetting agent 0.45-0.55 part, defoamer 0.5-0.6 part, solubility promoter 2.0-2.5 part and titanium dioxide 70-75 part, then adjust dispersing speed to 1800-2000 rev/min, disperse 15-20 minute to slurries evenly after, detect paint liquid fineness≤40 μ m.
Accordingly, all right further improvement of method of preparing aqueous woodware paint titanium dioxide slurry of the present invention is as follows, and it comprises following step of sequentially carrying out:
The preparation method of described aqueous woodware paint titanium dioxide slurry comprises following step of sequentially carrying out:
Start dispersion machine and adjust rotating speed to 700-800 rev/min, under this speed, first slowly add successively water 13-14 part, dispersion agent 5-6 part, wetting agent 0.45-0.55 part, defoamer 0.5-0.6 part, solubility promoter 2.0-2.5 part and titanium dioxide 70-75 part, then adjust dispersing speed to 1800-2000 rev/min, disperse 15-20 minute to slurries evenly after, detect paint liquid fineness≤40 μ m, adjust dispersing speed 800-1000 rev/min, under this speed, add successively water 2-8 part, anti-settling agent 0.5-0.8 part and sanitas 0.2-0.3 part, disperse 3-8 minute even to slurries.
Compared with prior art, tool has the following advantages the prepared aqueous woodware paint titanium dioxide slurry of the present invention:
1,, in the situation that processing unit is constant, well color stuffing fineness is disperseed to get off.
2, solved because water in formula is less or do not have Mierocrystalline cellulose to cause the problems such as color stuffing system quick-drying, moisture retention be poor, made system high speed dispersion well.
3, the titanium dioxide pigment content of producing is high, can reach 70-75%.
4, titanium dioxide slurry system stability is good, and 55 ℃ of heat are stored up 30 days, without layering, thick without returning without skinning and fineness.
While 5, adding, without high speed dispersion again, as long as simple agitation can be used as titanium dioxide slurry and add in aqueous woodware paint, solved the problem that does not have the scattered coating surface weak effect causing because of titanium dioxide, enhanced productivity.
Embodiment
Below by embodiment, further illustrate the present invention:
Embodiment 1-1:
An aqueous woodware paint titanium dioxide slurry, formulated by following weight proportion by following raw material:
The preparation method of this aqueous woodware paint titanium dioxide slurry comprises following step of sequentially carrying out:
Start dispersion machine and adjust rotating speed to 700 rev/min, under this speed, first slowly add successively 70 parts of 13 parts, water, 5 parts of dispersion agents, 0.5 part of wetting agent, 0.5 part of defoamer, 2.0 parts of solubility promoters and titanium dioxides, then adjust dispersing speed to 1800 rev/min, disperse 15 minutes to slurries evenly after, detect paint liquid fineness≤40 μ m.
Embodiment 1-2:
An aqueous woodware paint titanium dioxide slurry, formulated by following weight proportion by following raw material:
The preparation method of this aqueous woodware paint titanium dioxide slurry comprises following step of sequentially carrying out:
Start dispersion machine and adjust rotating speed to 800 rev/min, under this speed, first slowly add successively 73 parts of 14 parts, water, 5 parts of dispersion agents, 0.5 part of wetting agent, 0.5 part of defoamer, 2.0 parts of solubility promoters and titanium dioxides, then adjust dispersing speed to 1800 rev/min, disperse 20 minutes to slurries evenly after, detect paint liquid fineness≤40 μ m.
Embodiment 1-3:
An aqueous woodware paint titanium dioxide slurry, formulated by following weight proportion by following raw material:
The preparation method of this aqueous woodware paint titanium dioxide slurry comprises following step of sequentially carrying out:
Start dispersion machine and adjust rotating speed to 750 rev/min, under this speed, first slowly add successively 75 parts of 13 parts, water, 5.5 parts of dispersion agents, 0.45 part of wetting agent, 0.6 part of defoamer, 2.5 parts of solubility promoters and titanium dioxides, then adjust dispersing speed to 1900 rev/min, disperse 18 minutes to slurries evenly after, detect paint liquid fineness≤40 μ m.
Embodiment 1-4:
An aqueous woodware paint titanium dioxide slurry, formulated by following weight proportion by following raw material:
The preparation method of this aqueous woodware paint titanium dioxide slurry comprises following step of sequentially carrying out:
Start dispersion machine and adjust rotating speed to 800 rev/min, under this speed, first slowly add successively 75 parts of 14 parts, water, 5 parts of dispersion agents, 0.5 part of wetting agent, 0.5 part of defoamer, 2.0 parts of solubility promoters and titanium dioxides, then adjust dispersing speed to 2000 rev/min, disperse 15 minutes to slurries evenly after, detect paint liquid fineness≤40 μ m.
Embodiment 1-5:
An aqueous woodware paint titanium dioxide slurry, formulated by following weight proportion by following raw material:
The preparation method of this aqueous woodware paint titanium dioxide slurry comprises following step of sequentially carrying out:
Start dispersion machine and adjust rotating speed to 800 rev/min, under this speed, first slowly add successively 73 parts of 13 parts, water, 6 parts of dispersion agents, 0.55 part of wetting agent, 0.55 part of defoamer, 2.5 parts of solubility promoters and titanium dioxides, then adjust dispersing speed to 2000 rev/min, disperse 20 minutes to slurries evenly after, detect paint liquid fineness≤40 μ m.
Embodiment 2-1:
An aqueous woodware paint titanium dioxide slurry, formulated by following weight proportion by following raw material:
The preparation method of this aqueous woodware paint titanium dioxide slurry comprises following step of sequentially carrying out:
Start dispersion machine and adjust rotating speed to 700 rev/min, under this speed, first slowly add successively 70 parts of 13 parts, water, 5 parts of dispersion agents, 0.5 part of wetting agent, 0.5 part of defoamer, 2.0 parts of solubility promoters and titanium dioxides, then adjust dispersing speed to 1800 rev/min, disperse 15 minutes to slurries evenly after, detect paint liquid fineness≤40 μ m, adjust 800 revs/min of dispersing speed, under this speed, add successively 0.2 part of 8 parts, water, 0.8 part of anti-settling agent and sanitas, disperse 3 minutes even to slurries.
Embodiment 2-2:
An aqueous woodware paint titanium dioxide slurry, formulated by following weight proportion by following raw material:
The preparation method of this aqueous woodware paint titanium dioxide slurry comprises following step of sequentially carrying out:
Start dispersion machine and adjust rotating speed to 800 rev/min, under this speed, first slowly add successively 73 parts of 14 parts, water, 5 parts of dispersion agents, 0.5 part of wetting agent, 0.5 part of defoamer, 2.0 parts of solubility promoters and titanium dioxides, then adjust dispersing speed to 1800 rev/min, disperse 15 minutes to slurries evenly after, detect paint liquid fineness≤40 μ m, adjust 800 revs/min of dispersing speed, under this speed, add successively 0.2 part of 4.2 parts, water, 0.6 part of anti-settling agent and sanitas, disperse 8 minutes even to slurries.
Embodiment 2-3:
An aqueous woodware paint titanium dioxide slurry, formulated by following weight proportion by following raw material:
The preparation method of this aqueous woodware paint titanium dioxide slurry comprises following step of sequentially carrying out:
Start dispersion machine and adjust rotating speed to 750 rev/min, under this speed, first slowly add successively 75 parts of 13 parts, water, 5.5 parts of dispersion agents, 0.45 part of wetting agent, 0.6 part of defoamer, 2.5 parts of solubility promoters and titanium dioxides, then adjust dispersing speed to 1900 rev/min, disperse 18 minutes to slurries evenly after, detect paint liquid fineness≤40 μ m, adjust 900 revs/min of dispersing speed, under this speed, add successively 0.2 part of 2 parts, water, 0.6 part of anti-settling agent and sanitas, disperse 6 minutes even to slurries.
Embodiment 2-4(most preferred embodiment):
An aqueous woodware paint titanium dioxide slurry, formulated by following weight proportion by following raw material:
The preparation method of this aqueous woodware paint titanium dioxide slurry comprises following step of sequentially carrying out:
Start dispersion machine and adjust rotating speed to 800 rev/min, under this speed, first slowly add successively 75 parts of 14 parts, water, 5 parts of dispersion agents, 0.5 part of wetting agent, 0.5 part of defoamer, 2.0 parts of solubility promoters and titanium dioxides, then adjust dispersing speed to 2000 rev/min, disperse 15 minutes to slurries evenly after, detect paint liquid fineness≤40 μ m, adjust 1000 revs/min of dispersing speed, under this speed, add successively 0.2 part of 2.3 parts, water, 0.5 part of anti-settling agent and sanitas, disperse 3 minutes even to slurries.
Embodiment 2-5:
An aqueous woodware paint titanium dioxide slurry, formulated by following weight proportion by following raw material:
The preparation method of this aqueous woodware paint titanium dioxide slurry comprises following step of sequentially carrying out:
Start dispersion machine and adjust rotating speed to 800 rev/min, under this speed, first slowly add successively 73 parts of 13 parts, water, 6 parts of dispersion agents, 0.55 part of wetting agent, 0.55 part of defoamer, 2.5 parts of solubility promoters and titanium dioxides, then adjust dispersing speed to 2000 rev/min, disperse 20 minutes to slurries evenly after, detect paint liquid fineness≤40 μ m, adjust 1000 revs/min of dispersing speed, under this speed, add successively 0.3 part of 3.5 parts, water, 0.6 part of anti-settling agent and sanitas, disperse 8 minutes even to slurries.
In above each embodiment:
Titanium dioxide is preferably anatase thpe white powder;
Defoamer is preferably 1293 of extra large river chemical industry;
Solubility promoter is preferably propylene glycol;
Sanitas is preferably the RS of THOR;
Anti-settling agent is preferably the BYKE-420 of BYK.
In above each embodiment, the aqueous woodware paint titanium dioxide slurry of all being prepared by each embodiment carries out pigment content and stability in storage detects, and detected result is as shown in the table:
Table 1-1---the experimental data of the pigment content index of each embodiment of this aqueous woodware paint titanium dioxide slurry
| Project | Pigment content % |
| Embodiment 1-1 | 70% |
| Embodiment 1-2 | 73% |
| Embodiment 1-3 | 75% |
| Embodiment 1-4 | 75% |
| Embodiment 1-5 | 73% |
From table, 1-1 can obviously find out, all >=70%, the titanium dioxide slurry pigment content of producing is high for the pigment content of the titanium dioxide slurry of each embodiment of aqueous woodware paint titanium dioxide slurry of the present invention.
Table 1-2---the experimental data of the pigment content index of each embodiment of this aqueous woodware paint titanium dioxide slurry
| Project | Pigment content % |
| Embodiment 2-1 | 70% |
| Embodiment 2-2 | 73% |
| Embodiment 2-3 | 75% |
| Embodiment 2-4 | 75% |
| Embodiment 2-5 | 73% |
From table, 1-2 can obviously find out, all >=70%, the titanium dioxide slurry pigment content of producing is high for the pigment content of the titanium dioxide slurry of each embodiment of aqueous woodware paint titanium dioxide slurry of the present invention.
Table 2-1---the experimental data (storing 30 days at 55 ℃) of the stability in storage of each embodiment of this aqueous woodware paint titanium dioxide slurry
| Project | Outward appearance before storing | Outward appearance after storing | Fineness before storing | Fineness after storing |
| Embodiment 1-1 | White thick slurry | Unchanged | ≤40μm | ≤40μm |
| Embodiment 1-2 | White thick slurry | Unchanged | ≤40μm | ≤40μm |
| Embodiment 1-3 | White thick slurry | Unchanged | ≤40μm | ≤40μm |
| Embodiment 1-4 | White thick slurry | Unchanged | ≤40μm | ≤40μm |
| Embodiment 1-5 | White thick slurry | Unchanged | ≤40μm | ≤40μm |
From table, 2-1 can obviously find out, the system stability in storage of each embodiment of aqueous woodware paint titanium dioxide slurry of the present invention is good, and 55 ℃ of heat are stored up 30 days, without layering, thick without returning without skinning and fineness.
Table 2-2---the experimental data (storing 30 days at 55 ℃) of the stability in storage of each embodiment of this aqueous woodware paint titanium dioxide slurry
| Project | Outward appearance before storing | Outward appearance after storing | Fineness before storing | Fineness after storing |
| Embodiment 2-1 | White thick slurry | Unchanged | ≤40μm | ≤40μm |
| Embodiment 2-2 | White thick slurry | Unchanged | ≤40μm | ≤40μm |
| Embodiment 2-3 | White thick slurry | Unchanged | ≤40μm | ≤40μm |
| Embodiment 2-4 | White thick slurry | Unchanged | ≤40μm | ≤40μm |
| Embodiment 2-5 | White thick slurry | Unchanged | ≤40μm | ≤40μm |
From table, 2-2 can obviously find out, the system stability in storage of each embodiment of aqueous woodware paint titanium dioxide slurry of the present invention is good, and 55 ℃ of heat are stored up 30 days, without layering, thick without returning without skinning and fineness.
Above-mentioned embodiment is just explained in detail technical scheme of the present invention; the present invention has more than and is only confined to above-described embodiment; those skilled in the art should be understood that; the above-mentioned principle of every foundation and the improvement of spirit on basis of the present invention, substitute, all should be within protection scope of the present invention.
Claims (6)
1. an aqueous woodware paint titanium dioxide slurry, is characterized in that: it is mainly formulated by following weight proportion by following raw material:
2. aqueous woodware paint titanium dioxide slurry according to claim 1, is characterized in that:
Described dispersion agent adopts the block copolymer solution that contains pigment affinity groups or the acrylate copolymer Solution Dispersion agent that contains pigment affinity groups;
Described wetting agent adopts polyhydroxy ether class non-ionic wetting agent or oleoyl epoxy alkane segmented copolymer;
Described defoamer adopts modified dimethyl polysiloxane solution;
Described solubility promoter adopts propylene glycol;
Described titanium dioxide adopts Rutile type Titanium Dioxide or anatase thpe white powder.
3. aqueous woodware paint titanium dioxide slurry according to claim 1 and 2, is characterized in that: it also comprises the raw material of following weight proportion:
Water 2-8 part
Anti-settling agent 0.5-0.8 part
Sanitas 0.2-0.3 part.
4. aqueous woodware paint titanium dioxide slurry according to claim 3, is characterized in that:
Described anti-settling agent adopts the modified urea solution that does not contain N-Methyl pyrrolidone;
Described sanitas adopts isothiazolinone disinfecting agent.
5. for the preparation of a preparation method for the aqueous woodware paint titanium dioxide slurry described in claim, it is characterized in that: it comprises following step of sequentially carrying out:
Start dispersion machine and adjust rotating speed to 700-800 rev/min, under this speed, first slowly add successively water 13-14 part, dispersion agent 5-6 part, wetting agent 0.45-0.55 part, defoamer 0.5-0.6 part, solubility promoter 2.0-2.5 part and titanium dioxide 70-75 part, then adjust dispersing speed to 1800-2000 rev/min, disperse 15-20 minute to slurries evenly after, detect paint liquid fineness≤40 μ m.
6. the preparation method of aqueous woodware paint titanium dioxide slurry according to claim 5, is characterized in that: after detecting paint liquid fineness≤40 μ m, then carry out following steps:
Adjust dispersing speed 800-1000 rev/min, under this speed, add successively water 2-8 part, anti-settling agent 0.5-0.8 part and sanitas 0.2-0.3 part, disperse 3-8 minute even to slurries.
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| CN103881500A (en) * | 2014-03-27 | 2014-06-25 | 中华制漆（深圳）有限公司 | High-weather-resistance high-stain-resistance white paint for outdoor woodware and preparation method of paint |
| CN104371465A (en) * | 2014-10-29 | 2015-02-25 | 广东巴德士化工有限公司 | Single-component-based water-based pollution-resistant white finish paint |
| CN104725962A (en) * | 2015-03-20 | 2015-06-24 | 广州市佐丹士涂料有限公司 | Super-weather-proof water-based metallic paint and preparation method thereof |
| CN106349822A (en) * | 2016-09-22 | 2017-01-25 | 珠海格力电器股份有限公司 | Water-based color paste, preparation method thereof and robot |
| CN107057470A (en) * | 2017-06-14 | 2017-08-18 | 安徽康瑞高科新材料技术工程有限公司 | A kind of nitrate paint stock white and preparation method thereof |
| CN108727906A (en) * | 2018-05-22 | 2018-11-02 | 上海大学 | Aqueous Titanium dioxide slurry and the method for preparing aqueous titanium white mill base material using good pressure distribution technique |
| CN108753046A (en) * | 2018-05-28 | 2018-11-06 | 河北晨阳工贸集团有限公司 | A kind of aqueous titanium white mill base and preparation method thereof |
| IT202100022913A1 (en) * | 2021-09-06 | 2023-03-06 | S I R I Spa | PROCEDURE FOR THE PREPARATION OF A CHEMICAL FORMULATION. |
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| CN103881500A (en) * | 2014-03-27 | 2014-06-25 | 中华制漆（深圳）有限公司 | High-weather-resistance high-stain-resistance white paint for outdoor woodware and preparation method of paint |
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| CN104725962A (en) * | 2015-03-20 | 2015-06-24 | 广州市佐丹士涂料有限公司 | Super-weather-proof water-based metallic paint and preparation method thereof |
| CN106349822A (en) * | 2016-09-22 | 2017-01-25 | 珠海格力电器股份有限公司 | Water-based color paste, preparation method thereof and robot |
| CN107057470A (en) * | 2017-06-14 | 2017-08-18 | 安徽康瑞高科新材料技术工程有限公司 | A kind of nitrate paint stock white and preparation method thereof |
| CN108727906A (en) * | 2018-05-22 | 2018-11-02 | 上海大学 | Aqueous Titanium dioxide slurry and the method for preparing aqueous titanium white mill base material using good pressure distribution technique |
| CN108753046A (en) * | 2018-05-28 | 2018-11-06 | 河北晨阳工贸集团有限公司 | A kind of aqueous titanium white mill base and preparation method thereof |
| IT202100022913A1 (en) * | 2021-09-06 | 2023-03-06 | S I R I Spa | PROCEDURE FOR THE PREPARATION OF A CHEMICAL FORMULATION. |
| WO2023031248A1 (en) * | 2021-09-06 | 2023-03-09 | S.I.R.I. Spa | Process for preparation a chemical formulation |
| CN115960498A (en) * | 2022-09-21 | 2023-04-14 | 上海君子兰新材料股份有限公司 | Aqueous two-component solid-color finishing paint for woodware and preparation method thereof |
| CN115960498B (en) * | 2022-09-21 | 2024-03-15 | 上海君子兰新材料股份有限公司 | Aqueous two-component solid color finishing paint for woodware and preparation method thereof |
| CN117924972A (en) * | 2024-03-06 | 2024-04-26 | 佛山建发瑞通科技有限公司 | High-gloss general aqueous nuclear titanium white slurry and preparation method thereof |
| CN117924972B (en) * | 2024-03-06 | 2024-10-18 | 佛山建发瑞通科技有限公司 | High-gloss general aqueous nuclear titanium white slurry and preparation method thereof |
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