A kind of synchronous production device making dendrobium candidum oral liquid, decoction piece beverage
Technical field
The present invention relates to a kind of synchronous production device making dendrobium candidum oral liquid decoction piece beverage, belong to common technology scope Internet of Things bioengineering field, the synchronous production process unit of low temperature explosion plant cell.
Background technology
Dendrobium candidum rises establishing in large scale in the whole nation, the stem of noble dendrobium is the perennial herbaceous plant that grows nonparasitically upon another plant of the orchid family, there is unique medical value, be described as first of nine immortal grass and be used as medicine with stem, Chinese medicine is called the stem of noble dendrobium, belong to the yin tonics " Chinese Pharmacopoeia " in tonic, according to the fast development of current growing dendrobium, the establishing in large scale of industrialization, the plantation casual household of surging forward, and exactly lack catching up with of scale deep processing industry, rest on maple use stratagems on seek market, vegetables valency will be there is in stem of noble dendrobium price of going down for a long time, (2012 the end of the year stem of noble dendrobium price fresh goods per kilogram be 800-1500 unit, with the cost ratio of 2010, 50% has been dropped) in 2 years.
Owing at least containing more than 30% heat-sensitive substance in plant, fear high temperature, and dendrobium candidum finished product technique major part rests on tender stem is twisted into helical form or spring-like, dry, commodity are that maple bucket stores, the reprocessing of maple bucket must pass through high temperature, does not have new dendrobium candidum deep processed product, fine work to develop, and after forming stem of noble dendrobium collection, price significantly drops.
The extracting method of plant polyose is generally extracting in boiling water, cycle is long, temperature is high, liquid ratio is large, being unfavorable for suitability for industrialized production, low-temperature ultrahigh-pressure (UHP) cell blasting technique, is according to the plant cell explosion between several pressure variations and one or more circulating pressure, be 95% of content by the recovery rate of explosion cell dendrobium polysaccharide, draw the manufacturing technique method of oral liquid the best.
The extracting method of current existing Dendrobium officinale polysaccharide is: dendrobium candidum water is: 100ml/g; Extracting temperature is 100 DEG C, and extraction time is 3-5 hour, has at least the WATER AS FLOW MEDIUM of more than 60% to waste after extraction, and more advanced have electromagnetic oscillation, enzyme digestion reaction, ultrasonic wave extract, all industrialization cost and height because its energy is little, complex technical process.
Documents: the dendrobium polysaccharide extracting method of 200810162493.3,201210080911.0 response phase method dendrobium polysaccharide extraction processes, 201210291799.5 disposable dendrobium polysaccharide EN separating and extracting process, all there is defect, dendrobium polysaccharide peptide yield and low, that effects of energy saving and emission reduction the is undesirable defect of Dendrobium Plants waste.
The superelevation isostatic cool pressing continuous sterilization process of the liquid food of documents 201110148468.1 and device, it just carries out sterile test to liquid food, although this oral liquid belongs to liquid range (liquid food) and only belongs to conventional adopted name, especially its technological requirement of difference due to plant variety is also different, more specifically be that the difference of Chinese herbal medicine target plant, cell elite releasing effect are also just different, single pressure limit only plays sterilization functions, and the long power consumption of its process time is large and have lost utilization rate.
The dendrobium polysaccharide extracting method of documents 200810162493.3,201210080911.0 response phase method dendrobium polysaccharide extraction processes, all there is the defect that dendrobium candidum resource cannot utilize completely, also have that polysaccharide discharges that incomplete product yield is low, effects of energy saving and emission reduction cannot improve in technological process defect.
Dendrobium candidum contains abundant polysaccharose substance, there is the effect strengthening immunologic function, there is no the technique follow-up that can realize scale deep processing, stem of noble dendrobium raw materials market will supply exceed demand, static UHP common technology is combined with dynamic supersonic speed water jet technique, the preliminary experiment of technological process shows, low-temperature ultrahigh-pressure can impel the ripe explosion of dendrobium polysaccharide cell, under supersonic speed water jet operating mode, void effect explosion dendrobium candidum plant cell, dendrobium polysaccharide content release more than 95%, (UHP) be the abbreviation of plant cell blasting technique, through looking into domestic and foreign literature, all be difficult electronic program control (UHP) general character pressure to be combined with spiral jet jet pipe, produce supersonic jet and swash the relevant technological report that quick-fried stem of noble dendrobium plant cell extracts polysaccharide.
The invention discloses a kind of synchronous production device making dendrobium candidum oral liquid decoction piece beverage, belong to Chinese herbal medicine and extract innovation art field, it is the extension in industrial generic technology (UHP) innovation, tunnel type accumulator is combined down with spiral jet jet pipe process conditions, with less than 20 degree low temperature 500Mpa above ultra high pressure liquid moment explosion dendrobium candidum plant cells, peptidoglycan content and much higher finished product synchronous production process unit method, tunnel type accumulator can meet the requirement that medium-sized batches is produced.
Summary of the invention
The innovation of this device creates (UHP) process conditions, is technological deficiency before overcoming, from enzyme digestion reaction, ultrasonic wave leaching
Carry, the reform with the Technology Integration such as CO 2 supercritical, fluid extraction summary deficiency factor analysed by UF membrane, alcohol, tunnel type stores
Can maximize reduction batch production operating cost by device, play the overall economic efficiency of dendrobium candidum; Improve dendrobium polysaccharide purity (peptidoglycan).Compare ultrasonic wave that at present application is more, the greatest problem of electromagnetic oscillation crush method is: in ultrasonic vibration process, sound wave is absorbed by solution and produces large heat, in time heat can not be shifted out, the temperature of cell suspending liquid is impelled sharply to raise, cause enzyme and other bioactivator deactivation, also because of sound wave transmission and the heat radiation difficulty of large-rolume container, limit the large-scale application of industrialization, (UHP) is the abbreviation of ultra high pressure liquid technology.
This device can solve the problems of the technologies described above, with the time of plant cell circulation explosion, pressure and temp chain rate and solid-liquid ratio, these affect in the factor of dendrobium polysaccharide recovery rate, carry out process conditions innovation, during tunnel type accumulator release pressure, produce the conversion of positive negative energy, in spiral jet jet pipe, produce 2 Mach of supersonic jets, thus improve the yield of Dendrobium officinale polysaccharide, three kinds of finished products synchronous output in a technological process, reduces the consumption of the energy.
Peptidoglycan content is different by the difference of the stem of noble dendrobium place of production, kind, management, due to dendrobium candidum Jing Gan tissue tight, active ingredient releases condition needs more than 130 degree high temperature, high temperature destroys again the heat-sensitive substance in plant cell, make the poor stability of active substance of plant and cell wall structure is relatively tightr, it is low and without dendrobium candidum deep processing high-quality finished product that existing technique extracts content.
The present invention is to provide a kind of the synchronous production technique and the device that make stem of noble dendrobium oral liquid decoction piece beverage, control tunnel type accumulator with electronic program to be combined with supersonic speed water jet technique, in spiral jet jet pipe, the conversion of positive negative energy is carried out under sensor information guiding, produce void effect and swash broken dendrobium candidum plant cell, release peptidoglycan content and high synchronous production process unit.
Concrete technical scheme of the present invention is as follows:
Make a synchronous production device for dendrobium candidum oral liquid, decoction piece beverage, be jointly made up of hydraulic pressure unit 1, pressure transmitter 2, tunnel type accumulator 3, spiral jet jet pipe 4, central processing unit 5, pressure sensing valve 6, the time relay 7, signal conversion receiver 8, control valve 9, information processor 10, data acquisition unit 11, power source 12, junction sensor 13.
Central processing unit 5 connection signal conversion receiver 8, information processor 10, the time relay 7, information processor 10, data acquisition unit 11, the time relay 7 connection hydraulic pressure unit 1, power source 12, hydraulic pressure unit 1 pipe leads to and connects pressure transmitter 2, pressure transmitter 2 pipe leads to and connects tunnel type accumulator 3, the two ends of tunnel type accumulator 3 are provided with pressure sensing valve 6, tunnel type accumulator 3 one end is fixedly connected with pressure transmitter 2, one end pipe leads to and connects spiral jet jet pipe 4, control valve 9, junction sensor 13 is arranged on spiral jet jet pipe 4 with on the tube connector of tunnel type accumulator 3, it is characterized in that: described tunnel type accumulator 1 is that 3 stainless steel pressure-bearing pipes connect into door case type, and the U-shaped adapter connection in one end of multiple doorframe pipe is arranged in tunnel type, described in be arranged in tunnel the number of permutations decided by the volume=internal diameter × length of designing requirement.
The pressure-bearing body important technological parameters=design internal diameter of tube body d≤50mm of described tunnel type accumulator 3; External diameter D≤135mm; Length 3000mm; Footpath is than K=2.7, and operating pressure pW=620Mpa, burst pressure pb=46.39pW=3246.3Mpa, design pressure pd=1.7pW=1200Mpa, design temperature are room temperature; From strengthen pressure pA=0.89pW=640Mpa, pressure ratio 16: safe-working pressure pA=0.81pW=568.25Mpa, mechanical property of materials σ s=980MPa; σ b=1310Mpa, Performance Ratio >=0.6, is characterized in that U-shaped interface adopts the seal of particular design, guarantees the capacity requirement of suitability for industrialized production.
Tunnel type accumulator 3 operating pressure of the design reaches 620Mpa, bearing capacity 800MPa, but considers that pressure is more than after 600MPa, and simple aqueous medium will freeze, and therefore, the pressure that food liquid machining adopts is no more than 600MPa usually.
Described hydraulic pressure unit 1 is the Hydraulic Station of 40-50Mpa, the time relay connected by central processing unit 5
(7) according to the dwell time periodic duty of designing requirement.
What described power source 12 adopted is novel harmonic motor, and when pressure transmitter 2 enhances pressure, motor power consumption is constant, and than conventional motor economize on electricity more than 30%, volume I is attached on Hydraulic Station bedframe.
Described pressure transmitter 2 consists of double cylinder double acting by high pressure cylinder and low pressure (LP) cylinder and electro-hydraulic reversal valve, and two ends are provided with sub-chamber and normal pressure through hole, and sub-chamber can dismantle with the main body of pressure transmitter 2, cleaning different medium, changes sealing ring.
Compared with prior art, the beneficial effect of this device is: process unit can synchronous production in making dendrobium candidum oral liquid, decoction piece beverage, with the section of being broken into first after the cleaning of fresh goods dendrobium candidum, dilution is required with clean water according to the slurries ratio of dendrobium candidum after entering high speed beater, pressurize 5-15 minute release pressure under the pressure of 450 ~ 550Mpa, pressurization, decompression cycles operate 3 partial nodes and are controlled by junction sensor, and technique overall process is 0.65 hour 50L; Dendrobium candidum slurries after release pressure adopt 3 groups of apertures to be respectively 1.2 μm, 0.8 μm, 0.6 μm ceramic membrane filter, remove slag to obtain Dendrobium officinale polysaccharide extract (oral liquid), quantitatively record the purity super existing technique far away of polyoses content through alcohol precipitation, slag is pressed into medicine materical crude slice by pharmaceutical tabletting machine.
A kind of synchronous production technique making dendrobium candidum oral liquid, decoction piece beverage that the present invention also provides, following 3 variablees can be set: the liquid ratio of dendrobium candidum dry product (maple bucket) and fresh goods and water, extract pressure and dwell time, corresponding according to eucaryotic cell structure demolition effect, utilize circulation 3 pressurizations, reduce pressure into spiral jet jet pipe, precipitation, concentrated, be separated and obtain dendrobium polysaccharide peptide, the raffinate after separation is beverage.
Contrast drew with the process time; (UHP) change of temperature and feed liquid chain rate, pressurized circulation number of times and pressure, is optimized the influence factor of dendrobium polysaccharide recovery rate, and conclusion is the temperature of optimum optimizing condition is 18.5 DEG C; The pressure that circulation pressurization is 3 times is respectively: 450Mpa10 minute, 500Mpa10 minute, 550Mpa10 minute, the process time is 0.65 hour 5L, and when chain rate is 1.25, the yield of polysaccharide can reach more than 95% of stem of noble dendrobium content.
This application of installation step for: (one) is by the section be broken at the beginning of dry product dendrobium candidum (maple bucket), soak at normal temperatures by the liquid ratio of clean water according to dendrobium candidum again, consider except remaining water enters high speed beater with clean water according to dendrobium candidum liquid material ratio again, pressurize 5-15 minute release pressure under the pressure of 450 ~ 550Mpa, pressurization, decompression cycles operate 3 times.
(2) enter high speed beater after the first section of being broken into after the cleaning of the fresh goods stem of noble dendrobium, then dilute with the slurries ratio of clean water according to dendrobium candidum, pressurize 15 minutes release pressures under the pressure of 450 ~ 550Mpa, pressurization, decompression cycles operate 3 times; It is characterized in that: control pressure with electronic program and generate the general character function with release, again in conjunction with spiral jet jet pipe technique, positive negative energy is changed under sensor information guiding, make stem of noble dendrobium liquid material produce void effect in spiral spray pipe chamber, nozzle exit supersonic jet swashs quick-fried dendrobium candidum plant cell.
Circulating pressure and dwell time can be set; Be pressurised into successively according to eucaryotic cell structure demolition effect: 450,500.550Mpa, the dwell time is: within 15 minutes, 10 minutes, 5 minutes, carry out decompression cycles and controlled by junction sensor, product precipitation concentration is optimized for dendrobium polysaccharide peptide, and parting liquid is beverage.
Because stainless steel can meet foodstuff sanitation-stage requirement, the dendrobium candidum slurries after release of pressure adopt 3 groups of apertures to be respectively 1.2 μm, 0.8 μm, 0.6 μm ceramic membrane filter and remove slag, and by conventional manner tablet press machine, slag are pressed into medicine materical crude slice.
Accompanying drawing explanation
Fig. 1 is pressure-bearing device tunnel type accumulator,
Fig. 2 is system and device schematic diagram.
Detailed description of the invention
This device 2 is further described by reference to the accompanying drawings below:
Described hydraulic pressure unit 1 is the conventional hydraulic station of 40-50Mpa, the time relay 7 in being connected by central processing unit 5 is according to the dwell time periodic duty of designing requirement, when power source 12 makes hydraulic pressure unit 1 start working, due to power source 12 employing is harmonic motor, enhance pressure time-harmonic wave motor power consumption at pressure transmitter 2 constant, volume is little of conventional motor economize on electricity more than 30%.
The pressure source of Hydraulic Station enters pressure transmitter 2 by pipeline, pressurization pressure is become to tunnel type accumulator 3 in the mode of multi-stage booster, tunnel type accumulator 3 is connected by three stainless steel tube gate-types, in gate-type stainless steel tube one end, U-shaped another gate-type stainless steel tube of adapter connection is arranged in series into a tunnel, required gate-type arrangement is according to the calculation of capacity of designing requirement, the number of permutations decides how many stainless steel tubes by the volume=internal diameter × length required and contacts, there is an end socket tunnel type accumulator 3 one end, end socket has a connecting hole, the import of spiral jet jet pipe 4 has a connecting hole in face first, lead on the end socket connecting hole of tunnel type accumulator 3 by pipe, the little intermediate drum circle in inner chamber two of described spiral jet jet pipe 4, apart from spout 50mm place, the target block being greater than spout aperture is installed, target bulk matter is hard ceramic.
When process design consideration is tunnel type accumulator 3 one end release pressure of 500L, the time value that central processing unit 5 is set by information processor 10, data acquisition unit 11, the time relay 7 is sent instructions to by signal conversion receiver 8, message handler 10, on the time relay 7 connection hydraulic pressure unit 1, the work of power source 12, stopping power source 12 meets the circulation of dwell time, and junction sensor 13 determines the different dwell times.
The pressure sensing valve 6 that tunnel type accumulator 3 two ends are installed, by the pressure information of pressure transmitter 2, security alarm information is by signal conversion receiver 8, message handler 10 is sent to central processing unit 5, the control valve 9 opening tunnel type accumulator 3 one end is communicated with spiral jet jet pipe 4, hydraulic fluid in tunnel type accumulator 3 enters in spiral jet jet pipe 4, the conversion of positive negative energy is produced in spiral jet jet pipe 4, release of pressure sprays 2 Mach of supersonic jets and impacts hard ceramic target block, swash the yield that quick-fried stem of noble dendrobium plant cell improves Dendrobium officinale polysaccharide further, three kinds of finished products synchronous output in a technological process, reduce the consumption of the energy.
Described tunnel type accumulator 3 is that 3 stainless steel pressure-bearing pipes connect into door case type, and the U-shaped adapter connection in one end of multiple doorframe pipe is arranged in tunnel type, described in be arranged in tunnel the number of permutations decided by the volume=internal diameter × length of designing requirement.
Described pressure transmitter 2 is made up of high pressure cylinder and low pressure (LP) cylinder and electro-hydraulic reversal valve, for double cylinder double acting, (separately having special designs) two ends are provided with sub-chamber and normal pressure through hole, sub-chamber can dismantle with the main body of pressure transmitter 2, cleaning different medium, replacing sealing ring, from the oil pressure of Hydraulic Station, oil gas in isolated pressure transmitter 2.
Pressure-bearing body important technological parameters
Design internal diameter of tube body d≤50mm; External diameter D≤135mm; Length 3000mm; Footpath is than K=2.7, and working media is water.Operating pressure pW=620Mpa, burst pressure pb=46.39pW=3246.3Mpa, design pressure pd=1.7pW=1200Mpa, design temperature are room temperature; From strengthen pressure pA=0.89pW=640Mpa, pressure ratio 16: safe-working pressure pA=0.81pW=568.25Mpa, mechanical property of materials σ s >=980MPa; σ b >=1300Mpa, Performance Ratio >=0.6.
The extra-high tension unit operating pressure of the design reaches 620Mpa, bearing capacity 800MPa, but considers that pressure is more than after 600MPa, and simple aqueous medium will freeze, and therefore, the pressure that food liquid machining adopts is no more than 600MPa usually.
Embodiment: dendrobium candidum oral liquid is produced
One, dry product processing
1, dry product soaks the dendrobium candidum dry product section of breaking is 0.5-20mm, be dipped to moisture content and be greater than 60% (weight content, general 24 hours), while soaking, there is cleaning action, mix according to the liquid ratio of 65 to 1 dendrobium candidums with clean water after considering the water more than de-soak, with the making beating of high speed beater, enter storage tank and do pressurization preparation.
2, the slurries of dendrobium candidum suck 500L extra high voltage system device with vavuum pump, pressure generator classification cycle is pressurised into 450,500,550Mpa respectively once, successively the dwell time be 15,10,5min, the 3rd release pressure rear slurry is at spiral
Produce 2 Mach of supersonic jets in jet nozzle and swash quick-fried stem of noble dendrobium plant cell, then membrane filtration removes slag, and aseptically cannedly namely becomes a kind of dendrobium candidum special efficacy oral liquid.
Two, fresh goods processing
1, iron-sheet dendrobe fresh product cleaning, shearing section are 0.5-20mm by cleaning making beating, directly pull an oar according to the liquid ratio high speed beater of 50 to 1 dendrobium candidums with clean water, enter the pressurization of storage tank do and prepare.
2, the slurries vavuum pump of fresh dendrobium candidum sucks 500L extra high voltage system device, pressure generator classification cycle is pressurised into 450,500,550Mpa respectively once, each dwell time is 10min, 3rd time release pressure rear slurry swashs quick-fried stem of noble dendrobium plant cell with 2 Mach of supersonic jets in spiral jet jet pipe, then membrane filtration removes slag, and aseptically cannedly namely becomes a kind of dendrobium candidum special efficacy oral liquid.
Three, micro-polysaccharide drink
1, concentration extraction: iron-sheet dendrobe fresh product is cleaned, is cut into 0.5-20mm section, with clean water according to 50 to 1 iron sheet stones
The solid-liquid ratio of dry measure used in former times, directly with the making beating of high speed beater, enters storage tank and does pressurization preparation.
Slurries vavuum pump sucks 500L extra high voltage system device, each once with pressure generator classification cycle pressurization 450.500.550Mpa, each dwell time 10min, 3rd time release pressure rear slurry swashs quick-fried dendrobium candidum plant cell with 2 Mach of supersonic jets, then filter and remove residue in spiral jet jet pipe.
Filtered fluid removes supernatant liquor with the drift of the alcohol precipitation method, then is respectively with 3 groups of apertures that the dehydration of 1.2 μm, 0.8 μm, 0.6 μm nano ceramics film is concentrated to obtain polysaccharide underflow, and the yield of the phend-sulphuric acid quantitative assay polysaccharide through improveing is more than 95% of stem of noble dendrobium content.
2, rinsing liquid also contains polysaccharide and other element of 0.5-1.2% after measured, and rinsing liquid is aseptically canned can become a kind of drinking water containing micro-polysaccharide, and added value is considerably beyond the beverage of class mineral water.
Four, Dendrobium officinale polysaccharide medicine materical crude slice includes other element multiple such as Dendrobium officinale polysaccharide, alkaloid, EN of at least more than 0.5-1.2% due to the recrement after filtering, drying to moisture content mixes with the solid tablet 5% of (medicinal regulation permission to use) edible when being less than 20%, with pharmaceutical tabletting machine film-making, the healthcare decoction pieces being a kind of low content polysaccharide, finished product packing.
Tool of the present invention has the following advantages and efficiency
Apply a kind of synchronous production technique making dendrobium candidum oral liquid, decoction piece beverage, what adopt due to power source 12 is a kind of harmonic motor of novelty, pressure time-harmonic wave motor power consumption is enhanced constant at pressure transmitter 2, volume is little of conventional motor economize on electricity more than 30%, controls each safety alarm device and control valve guarantees technical process handling safety by electronic program.
When extra high voltage system device and spiral jet jet pipe that process conditions are below 500L, adopt pressure-bearing device tunnel type accumulator and the jet pipe inner chamber of stainless steel, reach foodstuff sanitation-stage requirement completely, maximum pressure is 6150Mpa, temperature is lower than 20 DEG C, classification is pressurised into 450.500.550Mpa and circulates after 3 times, produces void effect, swash quick-fried stem of noble dendrobium plant cell, polysaccharide release more than 95% with 2 Mach of supersonic jets under the conversion of slurries positive negative energy in by spiral jet jet pipe cavity.
Because pressure transmitter is double cylinder double acting, the large discharge of industrialization production requirements can be met, two ends are provided with sub-chamber and normal pressure through hole, sub-chamber can dismantle with the main body of pressure transmitter 2, cleaning different medium, replacing sealing ring, can from the oil pressure oil gas of Hydraulic Station in isolated pressure transmitter, oil gas can be avoided to pass pollution oral liquid by sub-chamber, be the necessary condition guaranteeing stem of noble dendrobium oral liquid, beverage medicine materical crude slice production sanitary standard.
The output being M hour 500L in the process time can reach the above industrialization of middle rank, 95% of the rate of the releasing >=stem of noble dendrobium content of polysaccharide, and shorten the production time, production process temperature is low, low saving of consuming energy production operating cost; Improve product efficiency; Chain rate reduces energy loss when being 1:25, and water resource is without waste, and production technology overall process, without zero emission, meets the production standard of national environmental protection cleaned industry, can also be applied to the low temperature sterilization of food liquid in enormous quantities, such as milk, wine, beverage.
In sum, it is the innovation of oral liquid production method that (UHP) super-pressure circulation pressurization that the present invention adopts designs a model, belong to a kind of extension of common technology, with existing technique electromagnetic oscillation, enzyme digestion reaction, supercritical ultrasonics technology is compared, its industrialization production scale and polysaccharide yield maximize (different by the polyoses content of the different cultivars stem of noble dendrobium), and the optimum condition obtained is not the value of setting, but within the scope imposed a condition, tunnel type accumulator adopts (UHP) super-pressure circulation pressurization to be combined with spiral jet jet pipe, what obtain is best quantification process conditions.
Application of installation technique is simple, and electronic program control operation is convenient, safety, and operating cost is cheap, is suitable for automatic industrial and produces; Product color is good, and dissolubility is good, and active component is high, and the active ingredient in oral liquid is absorbed by the body completely.
Finally; it is also to be noted that; a kind of synchronous production process unit making dendrobium candidum oral liquid, medicine materical crude slice, beverage; because its low temperature liquid super-pressure technique is that common technology can range of application and wide; what more than enumerate is only several specific embodiments of the present invention; obviously; the invention is not restricted to above embodiment; many retrofits, products innovation, patent family application can also be had; all distortion that those of ordinary skill in the art can directly derive or associate from content disclosed by the invention, all should think protection scope of the present invention.