CN102977412A - Finger extrusion-frangible soft capsule and its preparation method and use - Google Patents
Finger extrusion-frangible soft capsule and its preparation method and use Download PDFInfo
- Publication number
- CN102977412A CN102977412A CN2011102580811A CN201110258081A CN102977412A CN 102977412 A CN102977412 A CN 102977412A CN 2011102580811 A CN2011102580811 A CN 2011102580811A CN 201110258081 A CN201110258081 A CN 201110258081A CN 102977412 A CN102977412 A CN 102977412A
- Authority
- CN
- China
- Prior art keywords
- capsule
- soft capsule
- frangible
- pushes
- finger
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Landscapes
- Seasonings (AREA)
- Manufacturing Of Micro-Capsules (AREA)
Abstract
The invention relates to a finger extrusion-frangible soft capsule and its preparation method and use. The preparation method comprises that an outer hydrophilic liquid phase and an inner oleophilic liquid phase coated by the outer hydrophilic liquid phase are extruded simultaneously by a coextrusion method; the extruded capsules are immersed in a solidification liquid to form seamless spherical soft capsules under the action of surface tension; the seamless spherical soft capsules are dried at a temperature of 10 to 40 DEG C at humidity of 15 to 50% for 18 to 28 hours; the finger extrusion-frangible soft capsules having sizes of 2-4mm are screened out from the dried seamless spherical soft capsules; and the finger extrusion-frangible soft capsules are embedded into cigarette filter tips. In smoking, a smoker can press and break the finger extrusion-frangible soft capsule by fingers according to personal favorite and habit so that release time of essence is controlled and a cigarette local flavor is changed and thus the finger extrusion-frangible soft capsule can provide taste sense and auditory sense dual enjoyment for smokers.
Description
Technical field
What the present invention relates to is a kind of frangible soft capsule of pointing extruding, and particularly a kind of the finger the smoker can make the capsule material break under institute's applied pressure and discharge soft capsule of core and its production and use.
Background technology
Soft capsule for loading oils or to solution, suspension even solid and the semisolid small containers of glue without solvency action, is widely used in the aspects such as daily use chemicals, medicine, food, bio-science as a kind of.The capsule material of soft capsule can effectively completely cut off core and extraneous unstable environment, plays the effect of protection core, controls simultaneously the release of core, so that core slowly or immediately discharges under suitable condition.The delivery mode of soft capsule core can be divided into diffusion, rete breaks and cyst membrane is degraded 3 kinds.It is to utilize extruding and rubbing effect destruction capsule material that rete breaks, and this is a kind of the simplest and can discharge fast the mode of core.
In recent years, it is an effective means of improving the quality of products that tobacco product is carried out the perfuming processing, and it plays a part not replace for the fragrance of augmenting, modify cigarette.At present, using more widely, the flavouring cigarette method is to add essence microcapsule in pipe tobacco or filter tip.The people such as Peng Ronghuai [Preparation of Menthol Microcapsules with Phase Separation-coacervation Method, tobacco science and technology, 2003,8:27 ~ 28] prepare menthol microcapsules with complex coacervation, and microcapsule are applied in the cigarette, smoking result shows that microcapsule have strengthened the ability that cigarette keeps menthol preferably.
The release of its essence of tradition perfuming method is freely to carry out with the burning of cigarette, can't be controlled by the smoker time of releasing of essence.At present there has been bibliographical information to control the essence technology of time of releasing by the smoker.CN101203213A(frangible soft capsule of finger extruding and preparation method thereof, Ma Naifeiersa company) take the hydrocolloids such as gelatin, gellan gum, agar as raw material has prepared a kind of breakable capsule, capsule also has the characteristic that the finger extruding is broken, but complicated process of preparation and condition of cure are strict, the solidification process of capsule is divided into the low temperature gel and divalent ion solidified for two steps, needs strict regulation and control solidifying agent temperature and pH value in solidification process.
Summary of the invention
In view of the deficiencies in the prior art, the object of the invention is to grope prescription and technique by lot of experiments, a kind of soft capsule frangible when pushing of pointing is provided, after this soft capsule is used for tobacco product, the smoker can like according to self and custom is used finger squeeze and destroy soft capsule in smoking process, the time of releasing of control essence, the local flavor of change cigarette.
The object of the present invention is achieved like this:
A kind of capsule material of pointing the frangible soft capsule of extruding, contain the component of following weight part:
| Water | 1000 parts |
| Jelling agent | 3 ~ 20 parts |
| Softening agent | 1 ~ 10 part. |
Preferably, described finger pushes the capsule material of frangible soft capsule, is comprised of the component of following weight part:
| Water | 1000 parts |
| Jelling agent | 6 ~ 18 parts |
| Weighting agent | 5 ~ 25 parts |
| Softening agent | 1.5 ~ 3.5 parts. |
Described jelling agent only comprises carrageeman, or comprises carrageeman and at least aly be selected from gelatin, agar, pectin, xanthan gum, gum arabic and treated starch, and the weight ratio of carrageeman and other glue is 70/30 to 30/70; The weight ratio of preferred carrageeman and other glue is 50/50 to 40/60.
Described weighting agent is selected from following one or more: dextrin, Star Dri 5, cyclodextrin, Vltra tears, hydroxypropylcellulose, methylcellulose gum, polyvinyl alcohol and polyvalent alcohol.
Described softening agent is selected from following one or more glycerine, sorbyl alcohol, maltose alcohol, triactin and polyoxyethylene glycol, and the amount ratio of described jelling agent and softening agent is 4 ~ 16:1.
Water in the described capsule material component is deionized water.
Described finger pushes the capsule material of frangible soft capsule, comprises tinting material, and described tinting material is edible colorant or pigment.
The present invention also provides a kind of finger to push frangible soft capsule, comprise core and the soft capsule material that is wrapped in the core outside, it is characterized in that: described core accounts for the 50 ~ 92%(preferred 80 ~ 91% of soft capsule gross weight), described soft capsule material is above-mentioned any capsule material, described core is oil loving food flavour or spices, and described essence is peppermint, Chinese cassia tree, coffee berry.
In addition, the 3rd purpose of the present invention provides a kind of preparation method who points the frangible soft capsule of extruding, comprises the steps:
(1) take by weighing a certain proportion of capsule material raw material, add successively entry, softening agent, jelling agent and weighting agent in the glue tank under 60 ~ 80 ℃ (preferred 70 ~ 75 ℃), stir until material fully dissolves, the insulation de-bubbled forms glue;
(2) adopt coetrusion to prepare seamless capsule, the glue parcel food flavour or the spices that prepare are extruded simultaneously, capsule forms seamless spheroid after extruding, and extrusion temperature is 60 ~ 90 ℃ (preferred 70 ~ 80 ℃);
(3) seamless capsule is immersed in the solidification liquid 1 ~ 3 hour, described solidification liquid is paraffin oil, methyl-silicone oil or vegetables oil;
(4) seamless capsule being placed temperature is 10 ~ 40 ℃, and humidity is under 15 ~ 50% the environment air-dry 18 ~ 28 hours, and is fully dry; The preferred air-dry temperature of capsule is 18 ~ 22 ℃, and humidity is 20 ~ 30%, and air-dry time is 20 ~ 25 hours;
(5) it is air-dry that the residual solidification liquid of usefulness oil-Absorbing Sheets wiping capsule surface is placed vent position again under room temperature environment, or air-dry with under room temperature environment, placing again vent position behind the organic solvent washing capsule, described organic solvent is acetone, ethyl acetate, ethanol fire sherwood oil.
According to embodiment of the present invention, the diameter of capsule is 2 ~ 4.5mm, preferred 2.5 ~ 4mm.Gross weight is 5 ~ 60mg, preferred 20 ~ 40mg.Core accounts for 50 ~ 92% of capsule gross weight, and preferred 80 ~ 91%.
Frangible soft capsule of the present invention refers to that but the smoker with finger squeeze and destroy capsule material, discharges core.The crushing strength of capsule is 0.9 ~ 10N, preferred 4 ~ 8N.
After frangible soft capsule of the present invention embedded cigaratte filter, the smoker can like according to self and custom is used finger squeeze and destroy soft capsule, the time of releasing of control essence, the local flavor of change cigarette in smoking process.Therefore, the 4th purpose of the present invention is to provide described finger to push the purposes of frangible soft capsule in the preparation tobacco product.
Wherein, the capsule material that term " frangible " refers to capsule can be pointed under institute's applied pressure the smoker and destroy, and moment discharges core rapidly.Essence in the core is released when cigarette combustion, has changed the mouthfeel of cigarette, and freely controls essence time of releasing by the smoker.
Compared with prior art, the present invention has following advantage and progressive significantly: (1) the present invention with carrageeman or carrageeman and at least a hydrocolloid as the capsule material, adopt coetrusion to prepare the essence soft capsule, finish solidification process by the low temperature gel, and need not precipitation bath pH value, its technique is simple and easy to control.(2) the prepared frangible soft capsule of the present invention can be pointed in the extruding, the smoker can like according to self and custom is used finger squeeze and destroy soft capsule in smoking process, the time of releasing of control essence, change the local flavor of cigarette, in capsules break, have click sound or " bang " sound produces, and gives the dual enjoyment of smoker's sense of taste and the sense of hearing.
Embodiment
Further specify the present invention below by embodiment.The preparation method of the embodiment of the invention is only used for illustrating the present invention, rather than limitation of the present invention, and the simple modifications to preparation method of the present invention under design prerequisite of the present invention all belongs to the scope of protection of present invention.
Embodiment 1:
A kind of preparation method who points the frangible soft capsule of extruding, it comprises the steps:
(1) take by weighing 1000g water, the 10g carrageeman, the 5g cyclodextrin, the 2g sorbyl alcohol adds entry, softening agent, jelling agent and weighting agent successively in the glue tank under 70 ℃, stir until material fully dissolves the insulation de-bubbled.
(2) adopt coetrusion to prepare seamless capsule, extrusion temperature is 70 ℃.
(3) will extrude seamless capsule substantially spherical in shape and be immersed in the methyl-silicone oil 1.5 hours.
(4) soft capsule of producing in the step (3) being placed temperature is 20 ℃, and humidity is under 40% the environment air-dry 24 hours, and is fully dry.
(5) with the dried soft capsule of oil-Absorbing Sheets wiping, remove the residual solidification liquid of capsule surface.
The above-mentioned soft capsule diameter for preparing is 3.5 ± 0.1mm.
Use DPYD-A dripping pill table hardness tester to measure the crushing strength of capsule, method is as follows:
Capsule is placed in the middle of the tester tray, abuts against on the fixed dam, open the tester switch, push rod advances with the fixed speed of 1mm/s, and the extruding capsule is until push rod overlaps experiment end, push rod automatic backing substantially with fixed dam.The peak pressure that push rod applies in the each experiment of gauger record is capsule crushing hardness.Measure 3 ~ 8 samples.
The above-mentioned soft capsule crushing strength for preparing is 3.3N.
Embodiment 2:
A kind of preparation method who points the frangible soft capsule of extruding, it comprises the steps:
(1) take by weighing 1000g water, the 5g carrageeman, the 10g gelatin, 1g pectin, 1g glycerine adds entry, softening agent, jelling agent successively in the glue tank under 73 ℃, stir until material fully dissolves the insulation de-bubbled.
(2) adopt coetrusion to prepare seamless capsule, extrusion temperature is 69 ℃.
(3) will extrude seamless capsule substantially spherical in shape and be immersed in the paraffin oil 2 hours.
(4) soft capsule of producing in the step (3) being placed temperature is 17 ℃, and humidity is under 35% the environment air-dry 19 hours, and is fully dry.
(5) air-dry with under room temperature environment, placing again vent position behind the organic solvent-acetone washing capsule.
The above-mentioned soft capsule diameter for preparing is 4.0 ± 0.1mm.Crushing strength is 4.7N.
Embodiment 3:
A kind of preparation method who points the frangible soft capsule of extruding, it comprises the steps:
(1) take by weighing 1000g water, the 5g carrageeman, the 9g gelatin, 2g agar, the 5g polyvinyl alcohol, 1g glycerine, the 1g sorbyl alcohol adds entry, softening agent, jelling agent and weighting agent successively in the glue tank under 78 ℃, stir until material fully dissolves the insulation de-bubbled.
(2) adopt coetrusion to prepare seamless capsule, extrusion temperature is 71 ℃.
(3) will extrude seamless capsule substantially spherical in shape and be immersed in the paraffin oil 2 hours.
(4) soft capsule of producing in the step (3) being placed temperature is 18 ℃, and humidity is under 41% the environment air-dry 20 hours, and is fully dry.
(5) air-dry with under room temperature environment, placing again vent position behind the organic solvent-acetone washing capsule.
The above-mentioned soft capsule diameter for preparing is 2.5 ± 0.1mm.Crushing strength is 2.0N.
Embodiment 4:
A kind of preparation method who points the frangible soft capsule of extruding, it comprises the steps:
(1) take by weighing 1000g water, the 6g carrageeman, the 6g treated starch, the 7g hydroxypropylcellulose, the 2g triactin, the 1g sorbyl alcohol adds entry, softening agent, jelling agent and weighting agent successively in the glue tank under 76 ℃, stir until material fully dissolves the insulation de-bubbled.
(2) adopt coetrusion to prepare seamless capsule, extrusion temperature is 70 ℃.
(3) will extrude seamless capsule substantially spherical in shape and be immersed in the paraffin oil 2.5 hours.
(4) soft capsule of producing in the step (3) being placed temperature is 16 ℃, and humidity is under 39% the environment air-dry 18 hours, and is fully dry.
(5) air-dry with under room temperature environment, placing again vent position behind the organic solvent-acetone washing capsule.
The above-mentioned soft capsule diameter for preparing is 3.5 ± 0.1mm.Crushing strength is 3.5N.
Quantity value of the present invention is not restricted to the described embodiments, in claims in the listed scope, and continuous value.
Claims (10)
1. point the capsule material that pushes frangible soft capsule for one kind, it is characterized in that: the component that contains following weight part:
。
2. finger according to claim 1 pushes the capsule material of frangible soft capsule, it is characterized in that: the component by following weight part forms:
。
3. finger according to claim 1 and 2 pushes the capsule material of frangible soft capsule, it is characterized in that: described jelling agent only comprises carrageeman, or comprise carrageeman and at least aly be selected from gelatin, agar, pectin, xanthan gum, gum arabic and treated starch, and the weight ratio of carrageeman and other glue is 70/30 to 30/70.
4. finger according to claim 1 and 2 pushes the capsule material of frangible soft capsule, it is characterized in that: described weighting agent is selected from following one or more: dextrin, Star Dri 5, cyclodextrin, Vltra tears, hydroxypropylcellulose, methylcellulose gum, polyvinyl alcohol and polyvalent alcohol.
5. finger according to claim 1 and 2 pushes the capsule material of frangible soft capsule, it is characterized in that: described softening agent is selected from following one or more glycerine, sorbyl alcohol, maltose alcohol, triactin and polyoxyethylene glycol, and the amount ratio of described jelling agent and softening agent is 4 ~ 16:1.
6. finger according to claim 1 and 2 pushes the capsule material of frangible soft capsule, it is characterized in that: the water in the described capsule material component is deionized water.
7. finger according to claim 1 pushes the capsule material of frangible soft capsule, it is characterized in that: comprise tinting material, described tinting material is edible colorant or pigment.
8. a finger pushes frangible soft capsule, comprise core and the soft capsule material that is wrapped in the core outside, it is characterized in that: described core accounts for 50 ~ 92% of soft capsule gross weight, described soft capsule material is claim 1 or 2 described capsule materials, described core is oil loving food flavour or spices, and described essence is peppermint, Chinese cassia tree, coffee berry.
9. one kind prepares the method that finger claimed in claim 8 pushes frangible soft capsule, comprises the steps:
(1) take by weighing a certain proportion of capsule material raw material, add successively entry, softening agent, jelling agent and weighting agent in the glue tank under 60 ~ 80 ℃, stir until material fully dissolves, the insulation de-bubbled forms glue;
(2) adopt coetrusion to prepare seamless capsule, the glue parcel food flavour or the spices that prepare are extruded simultaneously, capsule forms seamless spheroid after extruding, and extrusion temperature is 60 ~ 90 ℃;
(3) seamless capsule is immersed in the solidification liquid 1 ~ 3 hour, described solidification liquid is paraffin oil, methyl-silicone oil or vegetables oil;
(4) seamless capsule being placed temperature is 10 ~ 40 ℃, and humidity is under 15 ~ 50% the environment air-dry 18 ~ 28 hours, and is fully dry;
(5) it is air-dry that the residual solidification liquid of usefulness oil-Absorbing Sheets wiping capsule surface is placed vent position again under room temperature environment, or air-dry with under room temperature environment, placing again vent position behind the organic solvent washing capsule, described organic solvent is acetone, ethyl acetate, ethanol fire sherwood oil.
10. finger claimed in claim 8 pushes the purposes of frangible soft capsule in the preparation tobacco product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201110258081.1A CN102977412B (en) | 2011-09-02 | 2011-09-02 | Finger extrusion-frangible soft capsule and its preparation method and use |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201110258081.1A CN102977412B (en) | 2011-09-02 | 2011-09-02 | Finger extrusion-frangible soft capsule and its preparation method and use |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN102977412A true CN102977412A (en) | 2013-03-20 |
| CN102977412B CN102977412B (en) | 2015-05-20 |
Family
ID=47851778
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201110258081.1A Expired - Fee Related CN102977412B (en) | 2011-09-02 | 2011-09-02 | Finger extrusion-frangible soft capsule and its preparation method and use |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN102977412B (en) |
Cited By (22)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103190702A (en) * | 2013-04-27 | 2013-07-10 | 红塔辽宁烟草有限责任公司 | Soft capsule with capability of enhancing sensory humidity-keeping performance of cigarette, as well as preparation method and application of soft capsule |
| CN103361173A (en) * | 2013-07-26 | 2013-10-23 | 上海华宝生物科技有限公司 | Preparation method of controllable-releasing and warm-wet-environment-resistance vegetable glue compound cigarette capsule, product obtained and applications thereof |
| CN103653230A (en) * | 2013-08-30 | 2014-03-26 | 湖北中烟工业有限责任公司 | Fragile soft capsule and preparation method thereof |
| CN104479871A (en) * | 2014-12-15 | 2015-04-01 | 湖北中烟工业有限责任公司 | Crumbable carbon dioxide solid flavor ball and application of flavor ball in cigarette filter rod |
| CN104560392A (en) * | 2014-12-15 | 2015-04-29 | 湖北中烟工业有限责任公司 | Inflatable solid flavor ball as well as preparation method and application of inflatable solid flavor ball in cigarette filter sticks |
| CN104886765A (en) * | 2015-06-18 | 2015-09-09 | 湖北中烟工业有限责任公司 | Tobacco double-layer solid flavor ball preparation method and application thereof |
| CN104886554A (en) * | 2015-04-30 | 2015-09-09 | 山东圣健生物科技有限公司 | Pomander soft capsule and preparation method thereof |
| CN105105328A (en) * | 2015-08-05 | 2015-12-02 | 湖北中烟工业有限责任公司 | Brittle solid spice bead for cigarette filter stick and preparation method thereof |
| CN105400215A (en) * | 2015-12-14 | 2016-03-16 | 贵州中烟工业有限责任公司 | Heatproof and moisture-proof cigarette capsule material and applications thereof |
| CN105419349A (en) * | 2015-12-14 | 2016-03-23 | 贵州中烟工业有限责任公司 | Cigarette capsule wall material with humidity resistance and application thereof |
| CN105495686A (en) * | 2016-01-27 | 2016-04-20 | 云南芯韵科技开发有限公司 | Moisture-proof and embrittling treatment method of cigarette capsules and product obtained by treatment method |
| CN105540073A (en) * | 2015-12-14 | 2016-05-04 | 贵州中烟工业有限责任公司 | Brittle capsule for cigarettes and preparation method thereof |
| CN106036998A (en) * | 2016-07-18 | 2016-10-26 | 江苏浩丰生物科技有限公司 | Blast bead capable of making up for deficiencies in cigarette fragrance and moist sense and preparation method of blast bead |
| CN106174694A (en) * | 2016-08-30 | 2016-12-07 | 云南芯韵科技开发有限公司 | A kind of pluralgel fragrance slow-release granule and preparation method thereof and its purposes |
| CN106551424A (en) * | 2016-11-29 | 2017-04-05 | 湖北中烟工业有限责任公司 | A kind of preparation method and applications of the Green tea essence for cigarette drop pill |
| CN109393555A (en) * | 2018-12-07 | 2019-03-01 | 云南巴菰生物科技有限公司 | A kind of preparation method of the cigarette capsule with degrading resistance property |
| CN109549249A (en) * | 2018-12-11 | 2019-04-02 | 云南巴菰生物科技有限公司 | A kind of preparation method of cigarette preservation antioxidation capsule |
| CN110396225A (en) * | 2019-08-06 | 2019-11-01 | 河南金瑞香精香料有限公司 | A kind of quick-fried pearl wall material and preparation method thereof and dripping pill method |
| CN110754688A (en) * | 2019-11-11 | 2020-02-07 | 云南恩典科技产业发展有限公司 | Fragrant bead capable of pinching and breaking hollow large-particle filter stick and preparation method thereof |
| EP3735842A4 (en) * | 2018-01-03 | 2021-10-06 | KT&G Corporation | Aerosol-generating article and apparatus |
| CN114206139A (en) * | 2019-08-02 | 2022-03-18 | 博奥股份公司 | Smoking device comprising at least one breakable flavour capsule |
| CN116268562A (en) * | 2023-03-17 | 2023-06-23 | 江西省华宝芯荟科技有限公司 | Gelatin-free capsule for cigarettes, and preparation method and application thereof |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110859320A (en) * | 2019-10-11 | 2020-03-06 | 国药控股星鲨制药（厦门）有限公司 | Plant brittle capsule for cigarettes and preparation method thereof |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1255297A (en) * | 1999-11-08 | 2000-06-07 | 孙成建 | Method for producing instant food with konjak taste |
| US20040180083A1 (en) * | 2001-07-05 | 2004-09-16 | Sumihiro Shiraishi | Soft capsules |
| CN101168648A (en) * | 2006-10-27 | 2008-04-30 | 保能科技股份有限公司 | Composition of hygroscopic coating with surface grain and manufacturing method for the coating |
| CN101203148A (en) * | 2005-06-21 | 2008-06-18 | 玛奈·菲尔萨公司 | Smoking device incorporating a breakable capsule, breakable capsule and process for manufacturing said capsule |
-
2011
- 2011-09-02 CN CN201110258081.1A patent/CN102977412B/en not_active Expired - Fee Related
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1255297A (en) * | 1999-11-08 | 2000-06-07 | 孙成建 | Method for producing instant food with konjak taste |
| US20040180083A1 (en) * | 2001-07-05 | 2004-09-16 | Sumihiro Shiraishi | Soft capsules |
| CN101203148A (en) * | 2005-06-21 | 2008-06-18 | 玛奈·菲尔萨公司 | Smoking device incorporating a breakable capsule, breakable capsule and process for manufacturing said capsule |
| CN101168648A (en) * | 2006-10-27 | 2008-04-30 | 保能科技股份有限公司 | Composition of hygroscopic coating with surface grain and manufacturing method for the coating |
Cited By (30)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103190702A (en) * | 2013-04-27 | 2013-07-10 | 红塔辽宁烟草有限责任公司 | Soft capsule with capability of enhancing sensory humidity-keeping performance of cigarette, as well as preparation method and application of soft capsule |
| CN103361173A (en) * | 2013-07-26 | 2013-10-23 | 上海华宝生物科技有限公司 | Preparation method of controllable-releasing and warm-wet-environment-resistance vegetable glue compound cigarette capsule, product obtained and applications thereof |
| CN103361173B (en) * | 2013-07-26 | 2014-11-26 | 上海华宝生物科技有限公司 | Preparation method of controllable-releasing and warm-wet-environment-resistance vegetable glue compound cigarette capsule, product obtained and applications thereof |
| CN103653230A (en) * | 2013-08-30 | 2014-03-26 | 湖北中烟工业有限责任公司 | Fragile soft capsule and preparation method thereof |
| CN104479871A (en) * | 2014-12-15 | 2015-04-01 | 湖北中烟工业有限责任公司 | Crumbable carbon dioxide solid flavor ball and application of flavor ball in cigarette filter rod |
| CN104560392A (en) * | 2014-12-15 | 2015-04-29 | 湖北中烟工业有限责任公司 | Inflatable solid flavor ball as well as preparation method and application of inflatable solid flavor ball in cigarette filter sticks |
| CN104560392B (en) * | 2014-12-15 | 2018-02-16 | 湖北中烟工业有限责任公司 | A kind of inflatable solid spice ball and preparation method thereof and the application in cigarette filter rod |
| CN104886554A (en) * | 2015-04-30 | 2015-09-09 | 山东圣健生物科技有限公司 | Pomander soft capsule and preparation method thereof |
| CN104886554B (en) * | 2015-04-30 | 2017-07-14 | 山东圣海保健品有限公司 | Quick-fried pearl soft capsule and preparation method thereof |
| CN104886765B (en) * | 2015-06-18 | 2016-09-28 | 湖北中烟工业有限责任公司 | The cigarette preparation method and applications of bilayer solid Flavouring ball |
| CN104886765A (en) * | 2015-06-18 | 2015-09-09 | 湖北中烟工业有限责任公司 | Tobacco double-layer solid flavor ball preparation method and application thereof |
| CN105105328A (en) * | 2015-08-05 | 2015-12-02 | 湖北中烟工业有限责任公司 | Brittle solid spice bead for cigarette filter stick and preparation method thereof |
| CN105105328B (en) * | 2015-08-05 | 2018-07-17 | 湖北中烟工业有限责任公司 | A kind of loud and clear solid spice pearl and preparation method thereof for cigarette filter rod |
| CN105540073A (en) * | 2015-12-14 | 2016-05-04 | 贵州中烟工业有限责任公司 | Brittle capsule for cigarettes and preparation method thereof |
| CN105419349A (en) * | 2015-12-14 | 2016-03-23 | 贵州中烟工业有限责任公司 | Cigarette capsule wall material with humidity resistance and application thereof |
| CN105400215A (en) * | 2015-12-14 | 2016-03-16 | 贵州中烟工业有限责任公司 | Heatproof and moisture-proof cigarette capsule material and applications thereof |
| CN105495686A (en) * | 2016-01-27 | 2016-04-20 | 云南芯韵科技开发有限公司 | Moisture-proof and embrittling treatment method of cigarette capsules and product obtained by treatment method |
| CN106036998A (en) * | 2016-07-18 | 2016-10-26 | 江苏浩丰生物科技有限公司 | Blast bead capable of making up for deficiencies in cigarette fragrance and moist sense and preparation method of blast bead |
| CN106174694A (en) * | 2016-08-30 | 2016-12-07 | 云南芯韵科技开发有限公司 | A kind of pluralgel fragrance slow-release granule and preparation method thereof and its purposes |
| CN106551424A (en) * | 2016-11-29 | 2017-04-05 | 湖北中烟工业有限责任公司 | A kind of preparation method and applications of the Green tea essence for cigarette drop pill |
| CN106551424B (en) * | 2016-11-29 | 2019-07-09 | 湖北中烟工业有限责任公司 | A kind of preparation method and applications of the Green tea essence for cigarette dripping pill |
| EP3735842A4 (en) * | 2018-01-03 | 2021-10-06 | KT&G Corporation | Aerosol-generating article and apparatus |
| CN109393555A (en) * | 2018-12-07 | 2019-03-01 | 云南巴菰生物科技有限公司 | A kind of preparation method of the cigarette capsule with degrading resistance property |
| CN109393555B (en) * | 2018-12-07 | 2021-03-26 | 云南巴菰生物科技有限公司 | Preparation method of cigarette capsule with processing resistance |
| CN109549249A (en) * | 2018-12-11 | 2019-04-02 | 云南巴菰生物科技有限公司 | A kind of preparation method of cigarette preservation antioxidation capsule |
| CN114206139A (en) * | 2019-08-02 | 2022-03-18 | 博奥股份公司 | Smoking device comprising at least one breakable flavour capsule |
| CN110396225A (en) * | 2019-08-06 | 2019-11-01 | 河南金瑞香精香料有限公司 | A kind of quick-fried pearl wall material and preparation method thereof and dripping pill method |
| CN110754688A (en) * | 2019-11-11 | 2020-02-07 | 云南恩典科技产业发展有限公司 | Fragrant bead capable of pinching and breaking hollow large-particle filter stick and preparation method thereof |
| CN110754688B (en) * | 2019-11-11 | 2021-06-25 | 云南恩典科技产业发展有限公司 | Fragrant bead capable of pinching and breaking hollow large-particle filter stick and preparation method thereof |
| CN116268562A (en) * | 2023-03-17 | 2023-06-23 | 江西省华宝芯荟科技有限公司 | Gelatin-free capsule for cigarettes, and preparation method and application thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN102977412B (en) | 2015-05-20 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN102977412B (en) | Finger extrusion-frangible soft capsule and its preparation method and use | |
| CN101203148B (en) | Smoking device incorporating a breakable capsule, breakable capsule and process for manufacturing said capsule | |
| JP6852058B2 (en) | Aerosol-generating articles with dispersed flavors | |
| EP3334294B1 (en) | Flavor capsules for smoking articles | |
| RU2668327C2 (en) | Collapsible capsule, method of its manufacture and smoking device containing collapsible capsule | |
| AU2013343220B2 (en) | Products including capsules, uses and preparation thereof | |
| CN105813486B (en) | Smoking product with liquid release component | |
| CN105400215B (en) | Temperature-resistant and moisture-resistant capsule material for cigarettes and application thereof | |
| WO2014005614A1 (en) | A method of flavouring a smoking product | |
| CN106723341B (en) | Fragrance sustained-release material composition, sustained-release perfume colloid and application thereof | |
| CN109043644B (en) | Three-layer structure cigarette capsule simultaneously coated with lipid solution and water and preparation method thereof | |
| RU2670522C2 (en) | Smoking article with tactile liquid release component | |
| CN105979803A (en) | Smoking article with liquid release component having frangible shell | |
| CN105105334A (en) | Spice slow-release filter tip additive with polymer covering film as well as preparation method and application thereof | |
| TW201402025A (en) | Cigarette | |
| WO2006136199A1 (en) | Smoking device incorporating a breakable capsule, breakable capsule and process for manufacturing said capsule | |
| CN202774109U (en) | Filter stick containing aroma slow release capsule for cigarette | |
| CN208480600U (en) | A kind of discoloration Three-element composite filter core | |
| WO2018060737A1 (en) | A tobacco industry product component | |
| CN111165874B (en) | Solid aromatic bead with core-shell structure and application thereof in cigarette filter stick | |
| CN110403236B (en) | Cigarette dry bead filter rod with function of improving smoke permeation | |
| Wang et al. | Study on the Preparation of Water-storage Capsules and its Effect on the Quality of Cigarettes | |
| RU50768U1 (en) | FRAGRANCE FILTER FOR CIGARETTE (OPTIONS) | |
| CN117693297A (en) | Polyvinylidene chloride film coated flavor core-shell capsules | |
| CN115088866A (en) | Cigarette flavor-locking particles and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20150520 Termination date: 20190902 |