CN102958365A - Noxious arthropod control composition and noxious arthropod control method - Google Patents
Noxious arthropod control composition and noxious arthropod control method Download PDFInfo
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- CN102958365A CN102958365A CN2011800317463A CN201180031746A CN102958365A CN 102958365 A CN102958365 A CN 102958365A CN 2011800317463 A CN2011800317463 A CN 2011800317463A CN 201180031746 A CN201180031746 A CN 201180031746A CN 102958365 A CN102958365 A CN 102958365A
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N47/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid
- A01N47/02—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having no bond to a nitrogen atom
- A01N47/06—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having no bond to a nitrogen atom containing —O—CO—O— groups; Thio analogues thereof
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/34—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom
- A01N43/36—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom five-membered rings
- A01N43/38—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom five-membered rings condensed with carbocyclic rings
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
- A01N37/34—Nitriles
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/02—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms
- A01N43/04—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom
- A01N43/06—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom five-membered rings
- A01N43/12—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom five-membered rings condensed with a carbocyclic ring
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Abstract
A noxious arthropod control composition comprising spirotetramat and at least one blast disease control compound selected from the group (A): a group consisting of ferimzone, fthalide, tricyclazole, kasugamycin hydrochloride, azoxystrobin, thiophanate-methyl, diclocymet, fenoxanil, tebufloquin and pyribencarb.
Description
Technical field
The present invention relates to prevent and kill off pest with the method for control of composition and pest.
Background technology
In the past, as the active ingredient of the composition of preventing and kill off harmful arthropod, known had a large amount of compounds (for example with reference to The Pesticide Manual-15th edition (BCPC periodical); ISBN978-1-901396-18-8.)。
Summary of the invention
Problem of the present invention is, the composition of preventing and kill off harmful arthropod that has the preventive effect of the excellence of harmful arthropod is provided.
That is, the present invention is following [1]～[5] items.
[1] a kind of composition of preventing and kill off harmful arthropod, the compound of preventing and kill off rice blast more than a kind that it contains spiral shell worm ethyl ester and is selected from group (A).
Group (A) is the group that is made of ferimzone, Rabcide, tricyclazole, kasugarnycin hydrochloride, Fluoxastrobin, thiophanate-methyl, two chlorine zarilamid, zarilamid, isobutyl ethoxyquin and pyrrole bacterium benzene prestige.
[2] according to [1] described composition of preventing and kill off harmful arthropod, wherein, spiral shell worm ethyl ester is 10: 1～1: 100 with the weight ratio of preventing and kill off the compound of rice blast.
[3] a kind of the method for control of harmful arthropod, it comprises the operation that spiral shell worm ethyl ester and the effective dose that is selected from the compound of preventing and kill off rice blast more than a kind of group (A) is applied to plant or cultivation of plants ground.
Group (A) is the group that is made of ferimzone, Rabcide, tricyclazole, kasugarnycin hydrochloride, Fluoxastrobin, thiophanate-methyl, two chlorine zarilamid, zarilamid, isobutyl ethoxyquin and pyrrole bacterium benzene prestige.
[4] according to [3] described the method for control, wherein, spiral shell worm ethyl ester is 10: 1～1: 100 with the weight ratio of preventing and kill off the compound of rice blast.
[5] according to [3] or [4] described the method for control, wherein, harmful arthropod is brown planthopper, white-backed planthopper or small brown rice planthopper.
Embodiment
The composition of preventing and kill off harmful arthropod of the present invention is (the following compound of originally preventing and kill off rice blast that sometimes also is designated as of the compound of preventing and kill off rice blast more than a kind that contains spiral shell worm ethyl ester and be selected from following group (A).) composition.
Group (A) is the group that is made of ferimzone, Rabcide, tricyclazole, kasugarnycin hydrochloride, Fluoxastrobin, thiophanate-methyl, two chlorine zarilamid, zarilamid, isobutyl ethoxyquin and pyrrole bacterium benzene prestige.
The spiral shell worm ethyl ester that uses among the present invention is known compound, for example can make by the method for putting down in writing in the Japanese Unexamined Patent Application Publication 2000-516918 communique.
In addition, the ferimzone that uses among the present invention, Rabcide, tricyclazole, kasugarnycin hydrochloride, Fluoxastrobin, thiophanate-methyl, two chlorine zarilamid and zarilamid all are known compounds, for example be recorded in " The Pesticide Manual-15th edition (BCPC periodical); ISBN 978-1-901396-18-8 " 497,904,1163,685,62,1128,340 and 479 pages etc. in.These compounds can obtain or obtain by known method manufacturing by commercially available preparation.
The isobutyl ethoxyquin that uses among the present invention and pyrrole bacterium benzene prestige all are known compounds, for example can disclose No. 2001/092231 brochure and internationally disclose the method manufacturing of putting down in writing in No. 2001/010825 brochure by the world.
Although the spiral shell worm ethyl ester in the composition of preventing and kill off harmful arthropod of the present invention is proportional without particular determination with containing of the compound of originally preventing and kill off rice blast, but the spiral shell worm ethyl ester with respect to 1000 weight portions, originally the compound of preventing and kill off rice blast is generally 10～1000000 weight portions, be preferably 100～100000 weight portions (namely, spiral shell worm ethyl ester: originally prevent and kill off the compound of rice blast=10: 1～1: 100), 100～10000 weight portions (that is, spiral shell worm ethyl ester: originally prevent and kill off the compound of rice blast=10: 1～1: 10) more preferably.
The composition of preventing and kill off harmful arthropod of the present invention can be the composition that only spiral shell worm ethyl ester and the compound of originally preventing and kill off rice blast is formed, but usually use spiral shell worm ethyl ester and the compound of originally preventing and kill off rice blast are mixed with inert carrier, add as required surfactant or other preparation auxiliary material, thereby make the composition of finish, emulsion, suspending agent, wetting powder, water-dispersible granules, pulvis, granule etc.
In addition, the composition of preventing and kill off harmful arthropod behind the above-mentioned preparation can directly use as the harmful arthropod agent for preventing and eliminating, perhaps is re-used as the harmful arthropod agent for preventing and eliminating behind the inert fraction (water, sand, plant wet goods) that adds other and uses.
In the composition of preventing and kill off harmful arthropod behind the preparation, spiral shell worm ethyl ester and the total amount of originally preventing and kill off the compound of rice blast be generally 0.01～99 % by weight, is preferably the scope of 0.1～90 % by weight, more preferably the scope of 0.5～70 % by weight.
As inert carrier, can enumerate solid carrier and liquid-carrier.
As solid carrier, such as enumerating by mineral such as kaolin, attapulgite soil, bentonite, montmorillonite, Emathlite, pyrophyllite, talcum, diatomite, calcites, the natural organic matters such as corncob powder, walnut parting, the synthesis of organic substance such as urea, the salt such as calcium carbonate, ammonium sulfate, the micro mist that the synthesizing inorganic things such as synthetic oxidizing aqueous silicon etc. form or shot-like particle etc.As liquid-carrier, such as enumerating the aromatic hydrocarbons such as dimethylbenzene, alkylbenzene, methyl naphthalene, the alcohols such as 2-propyl alcohol, ethylene glycol, propane diols, ethylene glycol monomethyl ether, the ketones such as acetone, cyclohexanone, isophorone, soybean oil, cottonseed wet goods vegetable oil, petroleum aliphatic hydrocarbon, ester class, methyl-sulfoxide, acetonitrile and water.
As surfactant, such as enumerating the anion surfactants such as alkyl phosphate salt, alkylaryl sulfonates, dialkyl sulfosuccinates, polyoxyethylene alkylaryl ether phosphate ester salt, lignosulfonates, napsylate formaldehyde condensation products, the non-ionic surface active agents such as polyoxyethylene alkylaryl ether, polyxyethylated polyoxypropylene block copolymers, sorbitan fatty acid ester, and the cationic surfactant such as alkyl trimethyl ammonium salt.
As other preparation auxiliary material, such as enumerating the water soluble polymers such as polyvinyl alcohol, polyvinylpyrrolidone, the polysaccharoses such as gum Arabic, alginic acid and salt thereof, CMC (carboxymethyl cellulose), xanthans, the inorganic matter such as aluminium-magnesium silicate, alumina sol, preservative, the stabilizing agents such as colouring agent and PAP (acid phosphatase isopropyl ester), BHT.
The composition of preventing and kill off harmful arthropod of the present invention can be used for from by plant being ingested, inhales protective plant the injuring that harmful arthropod (for example harmful insect and harmful acarian) that juice etc. injures causes.
Have the harmful arthropod of preventive effect as the composition of preventing and kill off harmful arthropod of the present invention, for example can enumerate following arthropods.
Semiptera insect: small brown rice planthopper (Laodelphax striatellus), brown planthopper (Nilaparvatalugens), the plant hoppers such as white-backed planthopper (Sogatella furcifera), rice leafhopper (Nephotettixcincticeps), the leafhopper classes such as nephotettix bipunctatus (Nephotettix virescens), cotten aphid (Aphisgossypii), black peach aphid (Myzus persicae), cabbage aphid (Brevicoryne brassicae), root of Beijing euphorbia Macrosiphus spp (Macrosiphum euphorbiae), the thick volume aphid of eggplant (Aulacorthum solani), rhopalosiphum padi (Rhopalosiphum padi), the Phytophthiras such as tangerine aphid (Toxoptera citricidus), greenhouse whitefly (Trialeurodes vaporariorum), Bemisia tabaci (Bemisia tabaci), the aleyrodid classes such as Bemisia argentifolii (Bemisia argentifolii), California red scale (Aonidiella aurantii), san jose scale (Comstockaspis perniciosa), arrowhead scales (Unaspis citri), ceroplastes rubens (Ceroplastesrubens), the a red-spotted lizard classes such as cottonycushion scale (Icerya purchasi) etc.;
Acarina pest: the leaf tick classes such as T.urticae Koch (Tetranychus urticae), citrus red mite (crm) (Panonychuscitri), Oligonychus etc.;
In above-mentioned harmful arthropod, as preference, can enumerate the plant hoppers such as small brown rice planthopper (Laodelphaxstriaellus), brown planthopper (Nilaparvata lugens), white-backed planthopper (Sogatella furcifera).
The composition of preventing and kill off harmful arthropod of the present invention can use preventing and kill off under the purpose of plant disease, such as the rice blast that can prevent and kill off rice (Magnaporthe grisea) etc.
The composition of preventing and kill off harmful arthropod of the present invention is by being applied to plant or cultivation of plants ground, thereby can be used for preventing and kill off harmful arthropod.As plant, can enumerate the cauline leaf of plant, the flower of plant, the fruit of plant, the seed of plant etc. here.
The method of control of harmful arthropod of the present invention is by processing to carry out with the composition of preventing and kill off harmful arthropod of the present invention, particularly, can enumerate cauline leaf and processing to plant stem-leaf, the soil treatment etc. such as broadcast sowing to the processing on plant cultivation ground etc.
In the situation that with harmful arthropod compositions-treated plant of the present invention or cultivation of plants ground, its treating capacity can be because of the kind of handled plant, change as the kind of the harmful arthropod of preventing and kill off object or occurrence degree, preparation form, toeatment period, meteorological condition etc., but in spiral shell worm ethyl ester and the total amount of originally preventing and kill off the compound of rice blast, the place of this plant of cultivation of every 10000m2 is generally 1～5000g, is preferably 10～500g.
Emulsion, wetting powder, suspending agent etc. are dilute with water usually, processes by broadcasting sowing.At this moment, spiral shell worm ethyl ester is generally 0.0001～3 % by weight with the total concentration of originally preventing and kill off the compound of rice blast, is preferably the scope of 0.0005～1 % by weight.Pulvis, granule etc. usually do not dilute and directly process.
The method of control of harmful arthropod of the present invention can the crop land such as dry land, paddy field, lawn, fruit tree garden or non-agricultural cultivated land with in use.
In addition, the present invention can be below cultivation in the crop land etc. of cited " plant " etc. in order to prevent and kill off the harmful arthropod of this crop land.
Crops: corn, rice, wheat, barley, rye, oat, Chinese sorghum, cotton, soybean, pea, French beans, peanut, buckwheat, beet, rape, sunflower, sugarcane, tobacco etc.,
Vegetables: solanaceous vegetable (eggplant, tomato, green pepper, capsicum, potato etc.), cucurbitaceae vegetable (cucumber, pumpkin, custard squash, watermelon, muskmelon, pumpkin etc.), brassicaceous vegetable (radish, turnip, horseradish, root-mustard, Chinese cabbage, wild cabbage, black mustard, cabbage, cauliflower etc.), composite vegetable (burdock, crowndaisy chrysanthemum, arithoke, lettuce etc.), liliaceous vegetable (green onion, onion, garlic, asparagus), Umbelliferae vegetables (carrot, celery, celery, parsnip etc.), goosefoot vegetable (spinach, Swiss chard etc.), Labiatae vegetables (purple perilla, peppermint, sweet basil etc.), strawberry, sweet potato, Chinese yam, taro etc.
Flowers (rose, chrysanthemum etc.),
Ornamental plants,
The lawn,
Fruit tree: pomaceous fruit (apple, European pear, Japanese pear, oblonga Quinces Quince etc.), drupe class (peach, plum, nectarine, plum, cherry, apricot, plum etc.), citrus (tangerine, orange, lemon, bitter orange, grapefruit etc.), nut fruits (chestnut, English walnut, fibert, almond, pistachio, cashew nut, macadamia nut etc.), soft fruits (blueberry, Cranberry, blackberry, blueberry, raspberry etc.), grape, persimmon, olive, loquat, banana, coffee, coconut, oil palm etc.;
Tree beyond the fruit tree: tea tree, mulberry tree, flowers and trees, Jie Lushu (ash tree, birch, dogwood, eucalyptus, ginkgo, cloves, maple, Oak Tree, willow, cercis, sweet gum, plane tree, beech tree, arbor-vitae, fir, siebold hemlock, needle juniper, pine tree, dragon spruce, Japanese yew) etc.
In above-mentioned plant, as preference, can enumerate corn, wheat, rice etc.
Above-mentioned " plant " can be the plant that is endowed tolerance by the method for breeding based on gene recombination technology or mating.
Embodiment
Below the present invention will be described in more detail by formulation example, application examples and test example, but the present invention not only is defined in following example.It should be noted that, in following example, as long as without specified otherwise, part all represents weight portion.
Formulation example 1
In the process that the diatomite with 4 parts lauryl sodium sulfate, 2 parts calcium lignosulfonate, 20 parts synthetic oxidizing aqueous silicon powder and 54 parts mixes, add 10 parts spiral shell worm ethyl ester and 10 parts ferimzone, fully mix, thereby obtain wetting powder.
Formulation example 2
In the process that the diatomite with 4 parts lauryl sodium sulfate, 2 parts calcium lignosulfonate, 20 parts synthetic oxidizing aqueous silicon powder and 54 parts mixes, add 10 parts spiral shell worm ethyl ester and 10 parts Rabcide, fully mix, thereby obtain wetting powder.
Formulation example 3
In the process that the diatomite with 4 parts lauryl sodium sulfate, 2 parts calcium lignosulfonate, 20 parts synthetic oxidizing aqueous silicon powder and 54 parts mixes, add 10 parts spiral shell worm ethyl ester and 10 parts kasugarnycin hydrochloride, fully mix, thereby obtain wetting powder.
Formulation example 4
In the process that the diatomite with 4 parts lauryl sodium sulfate, 2 parts calcium lignosulfonate, 20 parts synthetic oxidizing aqueous silicon powder and 54 parts mixes, add 10 parts spiral shell worm ethyl ester and 10 parts tricyclazole, fully mix, thereby obtain wetting powder.
Formulation example 5
In the process that the diatomite with 4 parts lauryl sodium sulfate, 2 parts calcium lignosulfonate, 20 parts synthetic oxidizing aqueous silicon powder and 54 parts mixes, add 10 parts spiral shell worm ethyl ester and 10 parts Fluoxastrobin, fully mix, thereby obtain wetting powder.
Formulation example 6
In the process that the diatomite with 4 parts lauryl sodium sulfate, 2 parts calcium lignosulfonate, 20 parts synthetic oxidizing aqueous silicon powder and 54 parts mixes, add 10 parts spiral shell worm ethyl ester and 10 parts thiophanate-methyl, fully mix, thereby obtain wetting powder.
Formulation example 7
In the process that the diatomite with 4 parts lauryl sodium sulfate, 2 parts calcium lignosulfonate, 20 parts synthetic oxidizing aqueous silicon powder and 54 parts mixes, add 10 parts spiral shell worm ethyl ester and two chlorine zarilamids of 10 parts, fully mix, thereby obtain wetting powder.
Formulation example 8
In the process that the diatomite with 4 parts lauryl sodium sulfate, 2 parts calcium lignosulfonate, 20 parts synthetic oxidizing aqueous silicon powder and 54 parts mixes, add 10 parts spiral shell worm ethyl ester and 10 parts zarilamid, fully mix, thereby obtain wetting powder.
Formulation example 9
In the process that the diatomite with 4 parts lauryl sodium sulfate, 2 parts calcium lignosulfonate, 20 parts synthetic oxidizing aqueous silicon powder and 54 parts mixes, add 10 parts spiral shell worm ethyl ester and 10 parts isobutyl ethoxyquin, fully mix, thereby obtain wetting powder.
Formulation example 10
In the process that the diatomite with 4 parts lauryl sodium sulfate, 2 parts calcium lignosulfonate, 20 parts synthetic oxidizing aqueous silicon powder and 54 parts mixes, add 10 parts spiral shell worm ethyl ester and 10 parts pyrrole bacterium benzene prestige, fully mix, thereby obtain wetting powder.
Formulation example 11
The spiral shell worm ethyl ester, 7.5 parts ferimzone and 7.5 parts the Rabcide that in the process that the diatomite with 4 parts lauryl sodium sulfate, 2 parts calcium lignosulfonate, 20 parts synthetic oxidizing aqueous silicon powder and 54 parts mixes, add 5 parts, fully mix, thereby obtain wetting powder.
Formulation example 12
The spiral shell worm ethyl ester, 7.5 parts kasugarnycin hydrochloride and 7.5 parts the Rabcide that in the process that the diatomite with 4 parts lauryl sodium sulfate, 2 parts calcium lignosulfonate, 20 parts synthetic oxidizing aqueous silicon powder and 54 parts mixes, add 5 parts, fully mix, thereby obtain wetting powder.
Formulation example 13
By 1 part spiral shell worm ethyl ester, 2 parts Rabcide, 87 parts kaolin and 10 parts talcum fully are pulverized and mixed, thereby obtain pulvis.
Formulation example 14
By 2 parts spiral shell worm ethyl ester, 1 part tricyclazole, 87 parts kaolin and 10 parts talcum fully are pulverized and mixed, thereby obtain pulvis.
Formulation example 15
By 2 parts spiral shell worm ethyl ester, 1 part kasugarnycin hydrochloride, 87 parts kaolin and 10 parts talcum fully are pulverized and mixed, thereby obtain pulvis.
Formulation example 16
By 2 parts spiral shell worm ethyl ester, 1 part Fluoxastrobin, 87 parts kaolin and 10 parts talcum fully are pulverized and mixed, thereby obtain pulvis.
Formulation example 17
By 2 parts spiral shell worm ethyl ester, 1 part thiophanate-methyl, 87 parts kaolin and 10 parts talcum fully are pulverized and mixed, thereby obtain pulvis.
Formulation example 18
By 2 parts spiral shell worm ethyl ester, two chlorine zarilamids of 1 part, 87 parts kaolin and 10 parts talcum fully are pulverized and mixed, thereby obtain pulvis.
Formulation example 19
By 2 parts spiral shell worm ethyl ester, 1 part zarilamid, 87 parts kaolin and 10 parts talcum fully are pulverized and mixed, thereby obtain pulvis.
Formulation example 20
By 2 parts spiral shell worm ethyl ester, 1 part isobutyl ethoxyquin, 87 parts kaolin and 10 parts talcum fully are pulverized and mixed, thereby obtain pulvis.
Formulation example 21
By 2 parts spiral shell worm ethyl ester, 1 part pyrrole bacterium benzene prestige, 87 parts kaolin and 10 parts talcum fully are pulverized and mixed, thereby obtain pulvis.
Formulation example 22
By 1 part spiral shell worm ethyl ester, 1 part ferimzone, 1 part Rabcide, 87 parts kaolin and 10 parts talcum fully are pulverized and mixed, thereby obtain pulvis.
Production Example 23
10 parts spiral shell worm ethyl esters, 5 parts Rabcide, 30 parts the white carbon that contains 50 parts of polyoxyethylene alkyl ether sulfuric ester ammonium salts and 55 parts water are mixed, carry out Crushing of Ultrafine by adopting the case of wet attrition method, thereby obtain suspending agent.
Production Example 24
5 parts spiral shell worm ethyl esters, 10 parts Fluoxastrobin, 30 parts the white carbon that contains 50 parts of polyoxyethylene alkyl ether sulfuric ester ammonium salts and 55 parts water are mixed, carry out Crushing of Ultrafine by adopting the case of wet attrition method, thereby obtain suspending agent.
Production Example 25
5 parts spiral shell worm ethyl esters, 10 parts thiophanate-methyl, 30 parts the white carbon that contains 50 parts of polyoxyethylene alkyl ether sulfuric ester ammonium salts and 55 parts water are mixed, carry out Crushing of Ultrafine by adopting the case of wet attrition method, thereby obtain suspending agent.
Production Example 26
5 parts spiral shell worm ethyl esters, two chlorine zarilamids of 10 parts, 30 parts the white carbon that contains 50 parts of polyoxyethylene alkyl ether sulfuric ester ammonium salts and 55 parts water are mixed, carry out Crushing of Ultrafine by adopting the case of wet attrition method, thereby obtain suspending agent.
Production Example 27
5 parts spiral shell worm ethyl esters, 10 parts zarilamid, 30 parts the white carbon that contains 50 parts of polyoxyethylene alkyl ether sulfuric ester ammonium salts and 55 parts water are mixed, carry out Crushing of Ultrafine by adopting the case of wet attrition method, thereby obtain suspending agent.
Production Example 28
5 parts spiral shell worm ethyl esters, 10 parts isobutyl ethoxyquin, 30 parts the white carbon that contains 50 parts of polyoxyethylene alkyl ether sulfuric ester ammonium salts and 55 parts water are mixed, carry out Crushing of Ultrafine by adopting the case of wet attrition method, thereby obtain suspending agent.
Production Example 29
5 parts spiral shell worm ethyl esters, 10 parts pyrrole bacterium benzene prestige, 30 parts the white carbon that contains 50 parts of polyoxyethylene alkyl ether sulfuric ester ammonium salts and 55 parts water are mixed, carry out Crushing of Ultrafine by adopting the case of wet attrition method, thereby obtain suspending agent.
Production Example 30
2.5 parts spiral shell worm ethyl esters, 5 parts ferimzone, 2.5 parts Rabcide, 35 parts the white carbon that contains 50 parts of polyoxyethylene alkyl ether sulfuric ester ammonium salts and 55 parts water are mixed, carry out Crushing of Ultrafine by adopting the case of wet attrition method, thereby obtain suspending agent.
Production Example 31
3 parts spiral shell worm ethyl esters, 2 parts kasugarnycin hydrochloride, 5 parts Rabcide, 35 parts the white carbon that contains 50 parts of polyoxyethylene alkyl ether sulfuric ester ammonium salts and 55 parts water are mixed, carry out Crushing of Ultrafine by employing case of wet attrition method, thereby obtain suspending agent.
Then, show effect of the present invention by test example.
Test example 1 (to the insecticidal activity test of brown planthopper)
Behind the acetone (pure pharmaceutical worker already makes with light) that contains SORGEN TW-20 (the first industrial pharmacy system) that spiral shell worm ethyl ester active component and tricyclazole active component with each 10mg are dissolved in respectively 1ml, with the spreader-sticker that contains 0.02 capacity % (trade name: DAIN (registration mark), Sumika-Takeda Garden Products Co., Ltd. system) water is diluted to normal concentration.Use the water of the spreader-sticker (DAIN) that contains 0.02 capacity % to be diluted to normal concentration the kasugarnycin hydrochloride monohydrate.With the water diluent of spiral shell worm ethyl ester, mix preparation test liquid with the water diluent of tricyclazole or kasugarnycin.
The paper pot of 2.5 leaf phases is cultivated rice, and (Oryza sativa, kind: Hoshinoyume) the above-mentioned test liquid of 20ml is broadcasted sowing in per 2 strains of seedling.After this rice seedling is air-dry, put into the glass test tube processed (diameter 30mm, height 200mm) of the water that 4.8ml is housed.In this test tube, respectively put 3 instar larvaes of 10 brown planthoppers in a suitable place to breed, place indoor (25 ℃, humidity 60%).Observed afterwards the life and death of the larva that supplies examination on 5th.According to this observed result, passing type 1) calculate dead worm rate, passing type 2) calculate the dead worm rate of proofreading and correct.It should be noted that, test is carried out 2 times repeatedly.Its mean value is as shown in table 1.
Formula 1); The dead borer population of dead worm rate (%)=treatment region/confession examination borer population * 100
Formula 2); Proofread and correct dead worm rate (%)={ (the dead worm rate of the treatment region-dead worm rate of non-treatment region)/(the dead worm rate of the non-treatment region of 100-) } * 100
Table 1
Test example 2 (to the insecticidal activity test of brown planthopper)
Be dissolved in respectively the acetone (pure pharmaceutical worker already makes with light) that contains SORGEN TW-20 (the first industrial pharmacy system) of 1ml at spiral shell worm ethyl ester active component, Fluoxastrobin active component, thiophanate-methyl active component and zarilamid active component with each 10mg after, with the spreader-sticker that contains 0.02 capacity % (trade name: DAIN (registration mark), Sumika-Takeda Garden Products Co., Ltd. system) water is diluted to normal concentration.The water diluent of spiral shell worm ethyl ester is mixed preparation test liquid with the water diluent of Fluoxastrobin, thiophanate-methyl or zarilamid.
The paper pot of 2.5 leaf phases is cultivated rice, and (Oryza sativa, kind: Hoshinoyume) the above-mentioned test liquid of 20ml is broadcasted sowing in per 2 strains of seedling.After this rice seedling is air-dry, put into the glass test tube processed (diameter 30mm, height 200mm) of the water that 4.8ml is housed.In this test tube, respectively put 3 instar larvaes of 10 brown planthoppers in a suitable place to breed, place indoor (25 ℃, humidity 60%).Observed afterwards the life and death of the larva that supplies examination on 4th.According to this observed result, with test example 1 passing type 1 similarly) calculate dead worm rate, passing type 2) calculate the dead worm rate of proofreading and correct.It should be noted that, test is carried out 2 times repeatedly, and its mean value is as shown in table 2.
Table 2
Test example 3 (to the insecticidal activity test of brown planthopper)
After spiral shell worm ethyl ester active component, isobutyl ethoxyquin active component and pyrrole bacterium benzene prestige active component with each 10mg are dissolved in respectively the acetone (pure pharmaceutical worker already makes with light) that contains SORGEN TW-20 (the first industrial pharmacy system) of 1ml, with the spreader-sticker that contains 0.02 capacity % (trade name: DAIN (registration mark), Sumika-Takeda Garden Products Co., Ltd. system) water is diluted to normal concentration.With the water diluent of spiral shell worm ethyl ester, mix preparation test liquid with the water diluent of isobutyl ethoxyquin or pyrrole bacterium benzene prestige.
The paper pot of 2.5 leaf phases is cultivated rice, and (Oryza sativa, kind: Hoshinoyume) the above-mentioned test liquid of 20ml is broadcasted sowing in per 2 strains of seedling.After this rice seedling is air-dry, put into the glass test tube processed (diameter 30mm, height 200mm) of the water that 4.8ml is housed.In this test tube, respectively put 3 instar larvaes of 10 brown planthoppers in a suitable place to breed, place indoor (25 ℃, humidity 60%).Observed afterwards the life and death of the larva that supplies examination on 4th.According to this observed result, with test example 1 passing type 1 similarly) calculate dead worm rate, passing type 2) calculate the dead worm rate of proofreading and correct.It should be noted that, test is carried out 2 times repeatedly, and its mean value is as shown in table 3.
Table 3
Test example 4 (to the insecticidal activity test of brown planthopper)
Behind the acetone (pure pharmaceutical worker already makes with light) that contains SORGEN TW-20 (the first industrial pharmacy system) that spiral shell worm ethyl ester active component and ferimzone active component with each 10mg are dissolved in respectively 1ml, with the spreader-sticker that contains 0.02 capacity % (trade name: DAIN (registration mark), Sumika-Takeda Garden Products Co., Ltd. system) water is diluted to normal concentration.The water diluent of spiral shell worm ethyl ester is mixed preparation test liquid with the water diluent of ferimzone.
The paper pot of 2.5 leaf phases is cultivated rice, and (Oryza sativa, kind: Hoshinoyume) the above-mentioned test liquid of 20ml is broadcasted sowing in per 2 strains of seedling.After this rice seedling is air-dry, put into the glass test tube processed (diameter 30mm, height 200mm) of the water that 4.8ml is housed.In this test tube, respectively put 3 instar larvaes of 10 brown planthoppers in a suitable place to breed, place indoor (25 ℃, humidity 60%).Observed afterwards the life and death of the larva that supplies examination on 6th.According to this observed result, with test example 1 passing type 1 similarly) calculate dead worm rate, passing type 2) calculate the dead worm rate of proofreading and correct.It should be noted that, test is carried out 2 times repeatedly, and its mean value is as shown in table 4.
Table 4
Utilizability on the industry
Can prevent and kill off harmful arthropod by the present invention.
Claims (5)
1. composition of preventing and kill off harmful arthropod, it contains spiral shell worm ethyl ester and is selected from the compound of preventing and kill off rice blast more than a kind of group A,
Wherein, group A is the group that is made of ferimzone, Rabcide, tricyclazole, kasugarnycin hydrochloride, Fluoxastrobin, thiophanate-methyl, two chlorine zarilamid, zarilamid, isobutyl ethoxyquin and pyrrole bacterium benzene prestige.
2. the composition of preventing and kill off harmful arthropod according to claim 1, wherein, spiral shell worm ethyl ester is 10: 1～1: 100 with the weight ratio of preventing and kill off the compound of rice blast.
3. the method for control of a harmful arthropod, it comprises the operation that spiral shell worm ethyl ester and the effective dose of the compound of preventing and kill off rice blast more than a kind that is selected from group A is applied to plant or cultivation of plants ground, wherein, group A is the group that is made of ferimzone, Rabcide, tricyclazole, kasugarnycin hydrochloride, Fluoxastrobin, thiophanate-methyl, two chlorine zarilamid, zarilamid, isobutyl ethoxyquin and pyrrole bacterium benzene prestige.
4. the method for control according to claim 3, wherein, spiral shell worm ethyl ester is 10: 1～1: 100 with the weight ratio of preventing and kill off the compound of rice blast.
5. according to claim 3 or 4 described the method for control, wherein, harmful arthropod is brown planthopper, white-backed planthopper or small brown rice planthopper.
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2010-146037 | 2010-06-28 | ||
| JP2010146037A JP5614125B2 (en) | 2010-06-28 | 2010-06-28 | Harmful arthropod control composition and harmful arthropod control method |
| PCT/JP2011/064602 WO2012002293A1 (en) | 2010-06-28 | 2011-06-20 | Noxious arthropod control composition and noxious arthropod control method |
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| CN201410558176.9A Division CN104396977A (en) | 2010-06-28 | 2011-06-20 | Noxious arthropod control composition and noxious arthropod control method |
| CN201410558163.1A Division CN104396976A (en) | 2010-06-28 | 2011-06-20 | Noxious arthropod control composition and noxious arthropod control method |
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| CN102958365A true CN102958365A (en) | 2013-03-06 |
| CN102958365B CN102958365B (en) | 2014-11-19 |
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| CN201410558176.9A Pending CN104396977A (en) | 2010-06-28 | 2011-06-20 | Noxious arthropod control composition and noxious arthropod control method |
| CN201180031746.3A Expired - Fee Related CN102958365B (en) | 2010-06-28 | 2011-06-20 | Noxious arthropod control composition and noxious arthropod control method |
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| CN201410558176.9A Pending CN104396977A (en) | 2010-06-28 | 2011-06-20 | Noxious arthropod control composition and noxious arthropod control method |
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| JP (1) | JP5614125B2 (en) |
| KR (1) | KR20130038899A (en) |
| CN (3) | CN104396976A (en) |
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| WO (1) | WO2012002293A1 (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104621152A (en) * | 2015-01-30 | 2015-05-20 | 北农（海利）涿州种衣剂有限公司 | Seed coating agent containing spirotetramat |
| CN106070269A (en) * | 2016-06-08 | 2016-11-09 | 北京明德立达农业科技有限公司 | A kind of composition pesticide and application thereof |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
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| JP5714416B2 (en) * | 2011-06-01 | 2015-05-07 | クミアイ化学工業株式会社 | Pest control composition and pest control method |
| CN107484767A (en) * | 2017-08-14 | 2017-12-19 | 江苏龙灯化学有限公司 | A kind of oil-based suspension and its production and use |
| US11189733B2 (en) | 2018-01-10 | 2021-11-30 | Intel Corporation | Thin-film transistors with low contact resistance |
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| CL2007003745A1 (en) * | 2006-12-22 | 2008-07-11 | Bayer Cropscience Ag | PESTICIDE COMPOSITION INCLUDING FOSETIL-AL, PROPAMOCARB-HCL AND AN ACTIVE INSECTED SUBSTANCE; AND METHOD FOR CONTROLLING FITOPATOGEN FUNDS OR DANIN INSECTICIDES OF THE PLANTS, CROPS OR SEEDS THAT INCLUDE APPLYING SUCH COMPOSITION. |
| CN101305732A (en) * | 2007-12-27 | 2008-11-19 | 天津市兴光农药厂 | Pesticide combination containing thiacloprid |
| JP2010138142A (en) * | 2008-12-15 | 2010-06-24 | Sumitomo Chemical Co Ltd | Pyridazine-n-oxide compound and controller for plant disease damage containing the same as active ingredient |
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- 2010-06-28 JP JP2010146037A patent/JP5614125B2/en not_active Expired - Fee Related
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- 2011-06-20 KR KR1020137001021A patent/KR20130038899A/en not_active Application Discontinuation
- 2011-06-20 CN CN201410558163.1A patent/CN104396976A/en active Pending
- 2011-06-20 WO PCT/JP2011/064602 patent/WO2012002293A1/en active Application Filing
- 2011-06-20 CN CN201410558176.9A patent/CN104396977A/en active Pending
- 2011-06-20 CN CN201180031746.3A patent/CN102958365B/en not_active Expired - Fee Related
- 2011-06-24 TW TW100122167A patent/TW201204251A/en unknown
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| CN101541173A (en) * | 2006-12-22 | 2009-09-23 | 拜尔农作物科学股份公司 | Pesticidal composition comprising fenamidone and an insecticide compound |
| CN101541175A (en) * | 2006-12-22 | 2009-09-23 | 拜尔农作物科学股份公司 | Pesticide composition comprising propamocarb-hydrochloride and an insecticide active substance |
| CN101553124A (en) * | 2006-12-22 | 2009-10-07 | 拜尔农作物科学股份公司 | Pesticide composition comprising fosetyl-aluminium and an insecticide active substance |
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| CN106070269A (en) * | 2016-06-08 | 2016-11-09 | 北京明德立达农业科技有限公司 | A kind of composition pesticide and application thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| WO2012002293A1 (en) | 2012-01-05 |
| CN104396976A (en) | 2015-03-11 |
| TW201204251A (en) | 2012-02-01 |
| CN102958365B (en) | 2014-11-19 |
| CN104396977A (en) | 2015-03-11 |
| JP2012006886A (en) | 2012-01-12 |
| JP5614125B2 (en) | 2014-10-29 |
| KR20130038899A (en) | 2013-04-18 |
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