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CN102669304B - Selenium-enriched tea oil - Google Patents

Selenium-enriched tea oil Download PDF

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CN102669304B
CN102669304B CN 201210137102 CN201210137102A CN102669304B CN 102669304 B CN102669304 B CN 102669304B CN 201210137102 CN201210137102 CN 201210137102 CN 201210137102 A CN201210137102 A CN 201210137102A CN 102669304 B CN102669304 B CN 102669304B
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subsequent use
tea oil
oil
selenium
tea
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CN102669304A (en
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邹先明
管天球
李文东
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Abstract

The invention discloses selenium-enriched tea oil, relating to the technical field of biological medicines. The selenium-enriched tea oil is made from the following raw materials in percentage by weight: 5-10 wt% of ginseng, 1-5 wt% of peanut, 1-8 wt% of purple sweet potato, 1-5 wt% of garlic, 1-10 wt% of oat and 65-80 wt% of tea seed. The preparation method of the selenium-enriched tea oil comprises the following steps of: preparing the materials, carrying out water extraction, carrying out alcohol extraction, drying, squeezing, carrying out alkaline wash, adsorbing, filtering and extracting, thereby obtaining the selenium-enriched tea oil. The product has the characteristics of selenium enrichment, multiple healthcare effects, and the like. The selenium-enriched tea oil disclosed by the invention is suitable for being eaten by people of all ages, in particular for the middle-aged and aged.

Description

A kind of rich selenium tea oil
Technical field
The present invention relates to the biological medicine technology field, particularly a kind of rich selenium tea oil.
Background technology
Oil tea is the distinctive woody oleiferous plants of China, also is the oil crops that China greatly develops.The comprehensive utilization value of oil tea is very high, contains a lot of high bioactivators, such as the active material to the human body beneficial such as vitamin E, Tea Polyphenols, squalene.Selenium is respectfully called " kindling material of life " by domestic and international the world of medicine and nutrition educational circles, enjoys " long-lived element ", " anticancer king ", " heart patron saint " and good reputations such as " natural antidotes "; Selenium is 1/10000000th at the tissue intensive amount, but it has determined the existence of life, is that other materials are irreplaceable to the great function of human health; Scarce selenium can directly cause the human immunological competence to descend, and clinical medicine proves, threatens 40 various diseases of human health and life all relevant with the scarce selenium of human body, such as cancer, cardiovascular disease, hepatopathy, cataract, pancreas disease, diabetes, genital system diseases etc.In the last few years, some occur and contained the edible oil of selenium element, such as Chinese patent (number of patent application is 201010163757.4) " complex intensifying medicine-food two-purpose edible oil and manufacture method thereof ", its batching comprises vitamin A, vitamin D, vitamin E, leukotrienes, linoleic acid and selenium, the mass percent of each batching is: vitamin A is 0.3%-0.8%, vitamin D is 0.000003%-0.000016%, vitamin E is 0.006%-0.04%, leukotrienes is 6%-26%, linoleic acid is 12%-80%, and selenium is 0.0000001%-0.000006%; This product has nutritional oil concurrently and health-care oil is integrated, hypertension, high fat of blood, hyperglycaemia, high cholesterol, cardiovascular and cerebrovascular disease, fatty liver, obesity and senile dementia can be effectively prevented and treated to a certain extent, memory can be strengthened to a certain extent simultaneously.Chinese patent (number of patent application is 200910066402.0) " selenizing 3/6 balance edible oil " and for example, its proportioning is: a-leukotrienes and linoleic ratio are 1: 1~10, and vitamin E is 0~1%, and Organic Selenium is 0.5~2500 μ g/kg; The aforementioned proportion of this invention has different proportion requirement according to actual needs, such as popular 3/6 balance edible oil, a-leukotrienes: linoleic acid=1: 5~10, calculate according to taking in for each person every day 25 gram edible oils, should satisfy human body and take in the above linoleic acid of 10 grams and the above a-leukotrienes standard of 2 grams every day; Selenizing 3/6 balance edible oil of this invention mainly refers to various all kinds of plant meal oil, comprises that the proportionings such as safflower seed oil, siritch, linseed oil, perilla oil, walnut oil, sunflower oil, peanut oil, soya-bean oil, corn oil, cottonseed oil, peanut oil, rapeseed oil, sesame oil, tea oil form; Selenizing 3/6 balance edible oil that this invention is stated can add in vitamin E, fat-soluble tea polyphenol, butylated hydroxy anisole (BHA), 2,6 BHTs (BHT) one or more as protective agent; Selenizing 3/6 balance edible oil of this invention is to add micro-Organic Selenium in 3/6 balance edible oil of different proportion, and Organic Selenium derives from selenide of carragheen, and the selenide of carragheen selenium content is 125mg/g; Selenizing 3/6 balance edible oil of this invention not only provides people's balanced nutrients, mends selenium, and selenium has the effect that keeps Oil stability, can overcome many carbon unrighted acid chemical property stable not, meet light and the easy failure of high temperature, be difficult for the shortcoming of long preservation.
Summary of the invention
Technical problem to be solved by this invention provides and a kind ofly contains the more edible oil of selenium element, and its preparation method is provided.
The technical solution used in the present invention is a kind of rich selenium tea oil of invention, is to be prepared from by following raw material by weight percentage:
The purple potato 1-8 of ginseng 5-10 peanut 1-5
Garlic 1-5 oat 1-10 tea seed 65-80.
The technical scheme of its optimization is to be prepared from by following raw material by weight percentage:
Ginseng 8 peanuts 3 purple potatos 5
Garlic 3 oats 6 tea seeds 75.
Meanwhile, also provide a kind of preparation method of rich selenium tea oil, its technical process is as follows:
A, get the raw materials ready: get by weight percentage ginseng, peanut, purple potato, garlic, oat, tea seed, for subsequent use respectively;
B, water extraction: ginseng for subsequent use, purple potato, garlic, oat are dropped in the pot for solvent extraction, added used ginseng, purple potato, garlic, oat gross weight 4-6 purified water doubly, boil extraction, the time is 1.0-2.0h, filters, and collects recrement, and is for subsequent use;
C, alcohol extracting: recrement for subsequent use is mixed with peanut, add recrement and peanut gross weight 4-8 50-95%(volumetric concentration doubly) edible ethanol, 30-70 ℃ of lower the immersion, the time is 1.0-2.5h, filtration; Add in the recrement again with the 50-95%(volumetric concentration of amount doubly) edible ethanol extract, the time is 1.0-1.5h, filters, and collects the material slag after extracting, and is for subsequent use;
D, oven dry: material slag for subsequent use 40-60 ℃ of lower oven dry, is become the dry material slag, for subsequent use;
E, squeezing: dry material slag for subsequent use is mixed with the tea seed, press through colding pressing and process (usually below 60 ℃, best temperature is 4-10 ℃), collect the coarse tea oil that squeezes out, for subsequent use;
F, alkali cleaning: with coarse tea oil for subsequent use, putting into concentration is in the aqueous alkali of 0.5-1.2%, coarse tea oil 2-4 times weight, stirs, and leaves standstill (time is at 0.5-2.5h), separates, and collects the upper strata oil solution, becomes alkali cleaning tea oil, for subsequent use;
G, absorption: alkali cleaning tea oil for subsequent use is put into pot for solvent extraction, add the neutral active carbon that accounts for alkali cleaning tea oil weight 10-15%, fully stir, filter, 3 times repeatedly, collect fluid, become absorption tea oil, for subsequent use;
H, filtration: absorption tea oil for subsequent use is filtered (crossing the 100-200 mesh filter screen), remove active carbon and other impurity particle, collect the fluid after filtering, become filtration tea oil, for subsequent use;
I, extraction: filtration tea oil for subsequent use through supercritical fluid extraction (spe medium is carbon dioxide), is collected the fluid of extraction, namely get rich selenium tea oil, in the rich selenium tea oil of per 100 grams, selenium content 〉=100 μ g.
Aqueous alkali described in the f step is a kind of in sodium hydrate aqueous solution or aqueous sodium carbonate or the sodium bicarbonate aqueous solution, or two kinds or three kinds of mixed solutions, and when adopting two kinds or three kinds of mixed solutions, the consumption of each component can be single-candidate or other ratio.
Rich selenium tea oil of the present invention, adopt tea seed (Camellia oleifera Abel), ginseng (Panax ginseng C. A. Mey.), peanut (Arachis hypogaea), purple potato (Solanum tuberosum), garlic (Allium sativum L.) and oat (Bromus japonicus Thunb.) as raw material, contain a large amount of monounsaturated fatty acids, unrighted acid in the tea seed, be rich in vitamin E, also contain squalene and Flavonoid substances, anticancer, anti-inflammatory are had splendid effect.Contain multiple panaxoside and vitamin (Vitamine) B in the ginseng 1, Cobastab 2, Cobastab 12, vitamin C; 20 various trace elements such as nicotinic acid (Nicotinic acid), folic acid (Folic acid), pantothenic acid, biotin (Biotin) and nicotinic acid amide and copper, zinc, iron, manganese.Peanut contains protein 25%~36%, and fat content can reach 40%, also contains abundant Cobastab in the peanut 2.PP, A, D, E, calcium and iron etc.Purple potato is rich in selenium element and anthocyanidin.Garlic contains calcium, phosphorus, iron and vitamin C 3, also contain the trace elements such as thiamine, riboflavin, niacin, allicin, citral and selenium and germanium.Oat contains the mineral matters such as vitamin E, leukotrienes and copper, calcium, phosphorus, iron, zinc, selenium and magnesium.By the preliminary treatment to various raw materials, make its contained Organic Selenium be easy to liposoluble, and then process the tea oil that obtains with the tea seed, be rich in Organic Selenium, in the rich selenium tea oil of per 100 grams, selenium content 〉=100 μ g; Simultaneously, owing to adopt cold pressing, kept the most of active bio matter in the tea oil, thereby the rich selenium tea oil that adopts the present invention to prepare contains more selenium element.
In addition, the rich selenium tea oil of the present invention's preparation also contains multiple high-activity biological active material and the various trace elements such as a large amount of monounsaturated fatty acids, unrighted acid and vitamin E, Tea Polyphenols, flavonoids, so, have plurality of health care functions.
Following table is that the composition of rich selenium tea oil of the present invention detects data:
(content is the nutrient content of 100 gram edible parts)
Figure GDA0000266827461
Can find out from upper table data, rich selenium tea oil of the present invention, not only the content of its unrighted acid and monounsaturated fatty acids is very high, and, also contain abundant selenium element and many trace elements to the human body beneficial.
The specific embodiment
Below in conjunction with embodiment, the present invention is described further.Following explanation is the mode that exemplifies, but protection scope of the present invention is not limited to this.
The preparation technology of rich selenium tea oil of the present invention is as follows:
A, get the raw materials ready: get by weight 8 parts of ginsengs, 3 parts of peanuts, 5 parts of purple potatos, 3 parts in garlic, 6 parts of oats, 75 parts of tea seeds, add up to 100 parts, for subsequent use respectively;
B, water extraction: ginseng for subsequent use, purple potato, garlic, oat are dropped in the pot for solvent extraction, add the purified water of 5 times of used ginsengs, purple potato, garlic, oat gross weight, boil extraction, the time is 1.5h, filters, and collects recrement, and is for subsequent use;
C, alcohol extracting: recrement for subsequent use is mixed with peanut, add the edible ethanol of recrement and 6 times of peanut gross weights, volumetric concentration 75%, 50 ℃ of lower immersions, the time is 2.0h, filters; Add with the doubly edible ethanol extraction of amount, volumetric concentration 75% in recrement, the time is 1.2h, filters, and collects the material slag after extracting, and is for subsequent use again;
D, oven dry: material slag for subsequent use 50 ℃ of lower oven dry, is become the dry material slag, for subsequent use;
E, squeezing: dry material slag for subsequent use is mixed with the tea seed, press through colding pressing and process (this example adopts 10 ℃), collect the coarse tea oil that squeezes out, for subsequent use;
F, alkali cleaning: with coarse tea oil for subsequent use, put in the sodium hydrate aqueous solution of concentration 1.0%, three times of coarse tea oil weight, stir, leave standstill (time 1.5h), separate, collect the upper strata oil solution, become alkali cleaning tea oil, for subsequent use;
G, absorption: alkali cleaning tea oil for subsequent use is put into pot for solvent extraction, add the neutral active carbon that accounts for alkali cleaning tea oil weight 12%, fully stir, filter, 3 times repeatedly, collect fluid, become absorption tea oil, for subsequent use;
H, filtration: absorption tea oil for subsequent use is filtered (crossing the 100-200 mesh filter screen), remove active carbon and other impurity particle, collect the fluid after filtering, become filtration tea oil, for subsequent use;
I, extraction: with filtration tea oil for subsequent use through supercritical fluid extraction (spe medium adopts carbon dioxide, t=374.3 ℃, p=22.05 MPa), collect the fluid of extraction, namely get rich selenium tea oil of the present invention, at this moment, in the rich selenium tea oil of per 100 grams, selenium content 〉=100 μ g.
Rich selenium tea oil of the present invention, the people that are fit to each ages are edible, and it is edible especially to be fit to the elderly.

Claims (2)

1. rich selenium tea oil it is characterized in that being prepared from by following raw material by weight percentage:
The purple potato 1-8 of ginseng 5-10 peanut 1-5
Garlic 1-5 oat 1-10 tea seed 65-80;
Its preparation process is as follows:
A, get the raw materials ready: get by weight percentage ginseng, peanut, purple potato, garlic, oat, tea seed, for subsequent use respectively;
B, water extraction: ginseng for subsequent use, purple potato, garlic, oat are dropped in the pot for solvent extraction, added used ginseng, purple potato, garlic, oat gross weight 4-6 purified water doubly, boil extraction, the time is 1.0-2.0h, filters, and collects recrement, and is for subsequent use;
C, alcohol extracting: recrement for subsequent use is mixed with peanut, add the edible ethanol of recrement and peanut gross weight 4-8 50-95% doubly, 30-70 ℃ of lower the immersion, the time is 1.0-2.5h, filters; Add with the doubly edible ethanol extraction of the 50-95% of amount in recrement, the time is 1.0-1.5h, filters, and collects the material slag after extracting, and is for subsequent use again;
D, oven dry: material slag for subsequent use 40-60 ℃ of lower oven dry, is become the dry material slag, for subsequent use;
E, squeezing: dry material slag for subsequent use is mixed with the tea seed, press through colding pressing and process, collect the coarse tea oil that squeezes out, for subsequent use;
F, alkali cleaning: with coarse tea oil for subsequent use, putting into concentration is in the aqueous alkali of 0.5-1.2%, coarse tea oil 2-4 times weight, stirs, and leaves standstill, separates, and collects the upper strata oil solution, becomes alkali cleaning tea oil, for subsequent use;
G, absorption: alkali cleaning tea oil for subsequent use is put into pot for solvent extraction, add the neutral active carbon that accounts for alkali cleaning tea oil weight 10-15%, fully stir, filter, 3 times repeatedly, collect fluid, become absorption tea oil, for subsequent use;
H, filtration: absorption tea oil for subsequent use is filtered, remove active carbon and other impurity particle, collect the fluid after filtering, become filtration tea oil, for subsequent use;
I, extraction: filtration tea oil for subsequent use through supercritical extract, is collected the fluid of extraction, namely get rich selenium tea oil.
Aqueous alkali described in the f step is a kind of in sodium hydrate aqueous solution or aqueous sodium carbonate or the sodium bicarbonate aqueous solution, or two kinds or three kinds of mixed solutions.
2. rich selenium tea oil according to claim 1 it is characterized in that being prepared from by following raw material by weight percentage:
Ginseng 8 peanuts 3 purple potatos 5
Garlic 3 oats 6 tea seeds 75.
CN 201210137102 2012-05-05 2012-05-05 Selenium-enriched tea oil Expired - Fee Related CN102669304B (en)

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CN103060080B (en) * 2013-01-06 2013-11-20 湖南金浩茶油股份有限公司 Preparation method of blood-fat-reducing camellia oil
CN103283870B (en) * 2013-06-27 2014-03-26 管天球 Tea oil for preventing and treating constipation
CN103636815A (en) * 2013-11-21 2014-03-19 青岛佰众化工技术有限公司 High-grade health care edible oil with characteristic of long term storage
CN103636816B (en) * 2013-12-06 2015-12-09 太和县庄老汉杂粮有限公司 A kind of sesame oil with antihypertensive healthcare effect
CN104839720A (en) * 2015-05-31 2015-08-19 安庆市孝柱食品科技有限公司 Tea oil oral liquid
CN105767232B (en) * 2016-04-05 2019-11-08 长沙理工大学 A kind of selenium-enriched health care grease and preparation method thereof
CN106035756A (en) * 2016-08-16 2016-10-26 安徽康生源生态农业有限公司 Selenium-enriched tea oil and preparation technology thereof
CN106509159A (en) * 2016-10-12 2017-03-22 贵州省黎平县黔香园油脂有限公司 Preparation method of camellia oil for middle-aged and elderly people
CN107279319A (en) * 2017-07-19 2017-10-24 贵州黔香园油脂有限公司 A kind of selenium-rich tea oil
CN107227200A (en) * 2017-07-20 2017-10-03 贵州黔香园油脂有限公司 A kind of selenium-rich tea oil of suitable mid-aged population
CN113171419A (en) * 2021-05-13 2021-07-27 湖南省康多利油脂有限公司 Selenium-rich tea oil emulsion eczema patch for external application

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Non-Patent Citations (2)

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