CN102578711A - Sodium alginate microparticles for cigarette filter and filtered cigarette - Google Patents
Sodium alginate microparticles for cigarette filter and filtered cigarette Download PDFInfo
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- CN102578711A CN102578711A CN201210017865XA CN201210017865A CN102578711A CN 102578711 A CN102578711 A CN 102578711A CN 201210017865X A CN201210017865X A CN 201210017865XA CN 201210017865 A CN201210017865 A CN 201210017865A CN 102578711 A CN102578711 A CN 102578711A
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- sodium alginate
- particulate
- cigarette
- mass percent
- cigarette filter
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- 239000000661 sodium alginate Substances 0.000 title claims abstract description 98
- 229940005550 sodium alginate Drugs 0.000 title claims abstract description 98
- IXPNQXFRVYWDDI-UHFFFAOYSA-N 1-methyl-2,4-dioxo-1,3-diazinane-5-carboximidamide Chemical compound CN1CC(C(N)=N)C(=O)NC1=O IXPNQXFRVYWDDI-UHFFFAOYSA-N 0.000 title claims abstract description 97
- 235000010413 sodium alginate Nutrition 0.000 title claims abstract description 97
- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 41
- 239000011859 microparticle Substances 0.000 title abstract 5
- 238000000034 method Methods 0.000 claims abstract description 17
- 239000002245 particle Substances 0.000 claims abstract description 16
- 235000013599 spices Nutrition 0.000 claims abstract description 15
- 238000001035 drying Methods 0.000 claims abstract description 9
- 238000002360 preparation method Methods 0.000 claims description 32
- 239000000796 flavoring agent Substances 0.000 claims description 20
- 235000013355 food flavoring agent Nutrition 0.000 claims description 19
- 239000003795 chemical substances by application Substances 0.000 claims description 16
- 239000000463 material Substances 0.000 claims description 13
- UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 claims description 10
- 238000004043 dyeing Methods 0.000 claims description 8
- 229920001817 Agar Polymers 0.000 claims description 6
- 239000004375 Dextrin Substances 0.000 claims description 6
- 229920001353 Dextrin Polymers 0.000 claims description 6
- 229920002472 Starch Polymers 0.000 claims description 6
- 239000008272 agar Substances 0.000 claims description 6
- 235000010419 agar Nutrition 0.000 claims description 6
- 230000007797 corrosion Effects 0.000 claims description 6
- 238000005260 corrosion Methods 0.000 claims description 6
- 235000019425 dextrin Nutrition 0.000 claims description 6
- 239000008107 starch Substances 0.000 claims description 6
- 235000019698 starch Nutrition 0.000 claims description 6
- 239000008187 granular material Substances 0.000 claims description 5
- 239000000203 mixture Substances 0.000 claims description 5
- 239000000049 pigment Substances 0.000 claims description 4
- 244000215068 Acacia senegal Species 0.000 claims description 3
- 241000206575 Chondrus crispus Species 0.000 claims description 3
- 108010010803 Gelatin Proteins 0.000 claims description 3
- 229920000084 Gum arabic Polymers 0.000 claims description 3
- 235000010489 acacia gum Nutrition 0.000 claims description 3
- 239000000205 acacia gum Substances 0.000 claims description 3
- 239000008273 gelatin Substances 0.000 claims description 3
- 229920000159 gelatin Polymers 0.000 claims description 3
- 235000019322 gelatine Nutrition 0.000 claims description 3
- 235000011852 gelatine desserts Nutrition 0.000 claims description 3
- 229920002907 Guar gum Polymers 0.000 claims description 2
- 239000000665 guar gum Substances 0.000 claims description 2
- 235000010417 guar gum Nutrition 0.000 claims description 2
- 229960002154 guar gum Drugs 0.000 claims description 2
- 239000003205 fragrance Substances 0.000 abstract description 5
- 230000000391 smoking effect Effects 0.000 abstract description 3
- 239000000383 hazardous chemical Substances 0.000 abstract description 2
- 238000000197 pyrolysis Methods 0.000 abstract 1
- 241000208125 Nicotiana Species 0.000 description 7
- 235000002637 Nicotiana tabacum Nutrition 0.000 description 7
- 239000000975 dye Substances 0.000 description 4
- 230000000694 effects Effects 0.000 description 4
- 238000002485 combustion reaction Methods 0.000 description 3
- 230000006378 damage Effects 0.000 description 3
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 2
- 241000628997 Flos Species 0.000 description 2
- 239000003546 flue gas Substances 0.000 description 2
- 239000002304 perfume Substances 0.000 description 2
- 239000000779 smoke Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 240000005250 Chrysanthemum indicum Species 0.000 description 1
- 235000018959 Chrysanthemum indicum Nutrition 0.000 description 1
- 244000241257 Cucumis melo Species 0.000 description 1
- 235000015510 Cucumis melo subsp melo Nutrition 0.000 description 1
- 208000027418 Wounds and injury Diseases 0.000 description 1
- FJJCIZWZNKZHII-UHFFFAOYSA-N [4,6-bis(cyanoamino)-1,3,5-triazin-2-yl]cyanamide Chemical compound N#CNC1=NC(NC#N)=NC(NC#N)=N1 FJJCIZWZNKZHII-UHFFFAOYSA-N 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 239000003989 dielectric material Substances 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- 239000003292 glue Substances 0.000 description 1
- 208000014674 injury Diseases 0.000 description 1
- 238000000465 moulding Methods 0.000 description 1
- 231100000614 poison Toxicity 0.000 description 1
- 230000007096 poisonous effect Effects 0.000 description 1
- 230000000630 rising effect Effects 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
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Abstract
The invention provides sodium alginate microparticles for a cigarette filter and a filtered cigarette. The sodium alginate microparticles are prepared by the following steps: preparing a sodium alginate solution from sodium alginate with a viscosity smaller than 200mpa.s, then adding essence and spice, preparing sodium alginate particles by a dripping method, and finally drying to obtain the sodium alginate microparticles. By adopting the sodium alginate microparticles, the essence and spice can be added to a filter tip, the generation of hazardous materials due to pyrolysis of the essence and spice is avoided, and the fragrance of the cigarette during smoking is simultaneously increased.
Description
Technical field
The present invention relates to a kind of dielectric material that is used for cigarette filter, specifically be meant a kind of sodium alginate particulate and cigarette with filter tip that is used for cigarette filter.
Background technology
Essence spice for cigarette generally is added in the pipe tobacco, thereby discharges the effect that fragrance plays increases smoke perfume through the combustion process of pipe tobacco.But pipe tobacco can be along with the burning of pipe tobacco in combustion process, the essence and flavoring agent Pintsch process, and then produce some poisonous and hazardous materials, the smoker is caused certain harm.Essence and flavoring agent is added in the filter tip, can avoids the Pintsch process of essence and flavoring agent in the aspiration procedure.The technical issues that need to address are to find a kind of suitable medium at present; Through this medium essence and flavoring agent is added in the filter tip, make essence and flavoring agent in the process that cigarette is sucked, along with smoking constantly discharges; Promptly can increase fragrance in the flue gas, also can reduce harm the smoker.
Summary of the invention
The objective of the invention is provides a kind of sodium alginate particulate and cigarette with filter tip that is used for cigarette filter according to above-mentioned deficiency; Can essence and flavoring agent be added in the filter tip through this sodium alginate particulate; Avoid the Pintsch process of essence and flavoring agent to produce harmful substance, can increase the fragrance in the cigarette sucking process simultaneously.
The present invention realizes through following technical scheme: a kind of sodium alginate particulate that is used for cigarette filter; It prepares through following method: viscosity is mixed with the sodium alginate soln that mass percent is 1-10% less than the sodium alginate of 200mpa.s; Add the essence and flavoring agent that mass percent is 0.01-5% then; Prepare the sodium alginate particle through dropping preparation method again; Final drying promptly obtains the sodium alginate particulate, uses the curing agent cured granulate in the said dropping preparation method, and curing agent is that mass percent is the calcium chloride solution of 5-25%.
Preferably, the viscosity of said sodium alginate is 5-150mpa.s.Because sodium alginate has the different viscosities specification, the viscosity specification is big more, and solid content is lower under identical temperature and viscosity, and problems such as shrivelled appear in particulate easily that prepare.
Temperature is 40-85 ℃ in the process of said preparation sodium alginate soln, is preferably 45-80 ℃, more preferably 50-75 ℃.The temperature of preparation process also has bigger influence to viscosity, and viscosity is reduction trend along with the rising of temperature.
Preferably, the mass percent of said preparation sodium alginate soln is 2-8%, more preferably 2.5-6%.Preparation has bigger influence to concentration to the sodium alginate particulate, excessive concentration, even temperature is higher, viscosity is big too, and moulding is had bigger influence.
Preferably, the essence and flavoring agent mass percent of adding is 0.05-4%, is more preferably 0.1-3%.
Comprise also in the said sodium alginate soln that mass percent is the auxiliary material of sodium alginate 0.01-30%, said auxiliary material is one or more of gum arabic, gelatin, carragheen, guar gum, dextrin, soluble starch, agar, spices corrosion inhibiter.The target that adds auxiliary material improves the hardness of sodium alginate particulate and the release time that prolongs fragrance.
Preferably, said auxiliary material is dextrin, soluble starch, agar, spices corrosion inhibiter by mass ratio 1: 1: 1: 1 mixture.Can make the hardness of sodium alginate particulate strong when adding according to the above ratio, and aroma release time is also the longest.
The system speed of dripping of said dropping preparation method is 50-300/minute.Preferably, the system speed of dripping of said dropping preparation method is 70-250/minute, more preferably 80-200/minute.The sodium alginate particle diameter that can too slowly dropping preparation method obtained too soon is unbalanced.
The sodium alginate particle diameter that said dropping preparation method obtains is 1-6mm, is preferably 2-5mm, more preferably 2.5-4.5mm.
The mass percent of curing agent is 7-22%, more preferably 9-20% in the preferred said dropping preparation method.
The sodium alginate particle that dropping preparation method is obtained put into concentration be the pigment solution dyeing of 0.001-2% after 0.5-6 hour again 50 ℃ dry 1 hour down.The volatilization of the inhomogeneous and essence and flavoring agent of the dry granularity that too acutely can cause the sodium alginate particulate.
The concentration of pigment solution is preferably 0.01-1.5%, more preferably 0.1-1%.
Dyeing time is preferably 1-5 hour, more preferably 2-4 hour.
Optimized technical scheme of the present invention is: a kind of sodium alginate particulate that is used for cigarette filter; It prepares through following method: with viscosity is that the sodium alginate of 5-150mpa.s is mixed with the sodium alginate soln that mass percent is 2-8%; The temperature of preparation sodium alginate soln is 40-85 ℃; Adding auxiliary material and the mass percent that mass percent is 0.01-30% then is the essence and flavoring agent of 0.01-5%, and said auxiliary material is dextrin, soluble starch, agar, spices corrosion inhibiter by mass ratio 1: 1: 1: 1 mixture.Prepare the sodium alginate particle through dropping preparation method again, the pigment solution dyeing of putting into concentration and be 0.001-2% promptly obtained the sodium alginate particulate down in dry 1 hour at 50 ℃ after 0.5-6 hour again.Dripping system speed is 70-250/minute, and the sodium alginate particle diameter that dropping preparation method obtains is 1-6mm.Use the curing agent cured granulate in the said dropping preparation method, curing agent is that mass percent is the calcium chloride solution of 5-25%.
A kind of cigarette with filter tip that contains above-mentioned sodium alginate particulate; Contain said sodium alginate particulate in the filter tip of said cigarette with filter tip; Said sodium alginate particulate prepares through following method: viscosity is mixed with the sodium alginate soln that mass percent is 1-10% less than the sodium alginate of 200mpa.s; Add the essence and flavoring agent that mass percent is 0.01-5% then, prepare the sodium alginate particle through dropping preparation method again, final drying promptly obtains the sodium alginate particulate; Use the curing agent cured granulate in the said dropping preparation method, curing agent is that mass percent is the calcium chloride solution of 5-25%.
The present invention is a medium through the sodium alginate particulate, and essence and flavoring agent is added in the cigarette filter.The essence and flavoring agent that comprises of sodium alginate is in the process that cigarette is sucked like this; Along with smoking process constantly discharges; Can play the effect that increases smoke perfume, also can not cause the too high generation of essence and flavoring agent temperature that human body is had the material of injury, have very strong practicality.
Description of drawings
Fig. 1 is a cigarette with filter tip sketch map of the present invention;
1-filter tip, 2-sodium alginate particulate, 3-pipe tobacco.
The specific embodiment
Below further specify the present invention through specific embodiment:
Getting viscosity is the sodium alginate 10g of 5mpa.s, the sodium alginate 20g that viscosity is 20mpa.s, under 75 ℃ water-bath, is configured to the sodium alginate soln of 1000ml, adds the Dendranthema indicum extract of 3g and the essence spice for cigarette of 3g.Dropping preparation method prepares the sodium alginate particulate, drips the system speed controlling at 120/minute.Curing agent employing concentration is 15% calcium chloride solution.With the mosanom particle that the is cured 3h that in 0.5% light blue solution, dyes, dyeing is accomplished the back and is taken out and be placed in the rotary dryer, and dry 1h under 50 ℃ of conditions promptly obtains the sodium alginate particulate 1 that diameter is 2mm after the drying completion.
Getting viscosity is the sodium alginate 30g of 10mpa.s, the sodium alginate 50g that viscosity is 21mpa.s; Under 85 ℃ water-bath, be configured to the sodium alginate soln of 1000ml; Add auxiliary material gum arabic 0.1g, add the Flos Osmanthi Fragrantis extract of 5g and the essence spice for cigarette of 5g again.Prepare the sodium alginate particulate with dropping preparation method, drip the system speed controlling at 250/minute.Curing agent adopts concentration to be controlled to be 5% calcium chloride solution.With the mosanom particle that the is cured 6h that in 0.001% light blue solution, dyes, dyeing is accomplished the back and is taken out and be placed in the rotary dryer, and dry 1h under 50 ℃ of conditions promptly obtains the sodium alginate particulate 2 that diameter is 1mm after the drying completion.
Getting viscosity is the sodium alginate 20g of 150mpa.s, under 40 ℃ water-bath, is configured to the sodium alginate soln of 1000ml, and interpolation auxiliary material gelatin, carragheen, melon glue are pressed 1: 1: 1 mixture 9g of mass ratio, add the essence spice for cigarette of 0.1g again.Prepare the sodium alginate particulate with dropping preparation method, drip the system speed controlling at 50/minute.Curing agent adopts concentration to be controlled to be 25% calcium chloride solution.With the mosanom particle that the is cured 0.5h that in 2% light blue solution, dyes, dyeing is accomplished the back and is taken out and be placed in the rotary dryer, and dry 1h under 50 ℃ of conditions promptly obtains the sodium alginate particulate 3 that diameter is 6mm after the drying completion.
Embodiment 4
Getting viscosity is the sodium alginate 10g of 100mpa.s; Under 70 ℃ water-bath, be configured to the sodium alginate soln of 1000ml; Add auxiliary material dextrin, soluble starch, agar, spices corrosion inhibiter and pressed mass ratio 1: 1: 1: 1 mixture 300g, add the essence spice for cigarette of 1g again.Prepare the sodium alginate particulate with dropping preparation method, drip the system speed controlling at 300/minute.Curing agent adopts concentration to be controlled to be 15% calcium chloride solution.With the mosanom particle that the is cured 3h that in 0.5% light blue solution, dyes, dyeing is accomplished the back and is taken out and be placed in the rotary dryer, and dry 1h under 50 ℃ of conditions promptly obtains the sodium alginate particulate 4 that diameter is 1mm after the drying completion.
Embodiment 5
Getting viscosity is the sodium alginate 100g of 10mpa.s, under 65 ℃ water-bath, is configured to the sodium alginate soln of 1000ml, adds the Flos Osmanthi Fragrantis extract of 25g and the essence spice for cigarette of 25g.Prepare the sodium alginate particulate with dropping preparation method, drip the system speed controlling at 70/minute.Curing agent adopts concentration to be controlled to be 15% calcium chloride solution.The taking-up of sodium alginate particulate is placed in the rotary dryer, and dry 1h under 50 ℃ of conditions promptly obtains the sodium alginate particulate 5 that diameter is 2mm after dry the completion.
As shown in Figure 1, sodium alginate particulate 2 according to the invention is added in the filter tip 1 of cigarette, thereby avoided essence and flavoring agent is added in the pipe tobacco 3, make cigarette essence and flavoring agent in sucking process produce harmful substance with the pipe tobacco high-temp combustion.
Cigarette with filter tip of the present invention is evaluated through suction effect, and the suction of flue gas is distinguished the flavor of has tangible flavouring effect.
Claims (10)
1. sodium alginate particulate that is used for cigarette filter; It is characterized in that it prepares through following method: viscosity is mixed with the sodium alginate soln that mass percent is 1-10% less than the sodium alginate of 200mpa.s; Add the essence and flavoring agent that mass percent is 0.01-5% then; Prepare the sodium alginate particle through dropping preparation method again; Final drying promptly obtains the sodium alginate particulate, uses the curing agent cured granulate in the said dropping preparation method, and curing agent is that mass percent is the calcium chloride solution of 5-25%.
2. according to the said sodium alginate particulate that is used for cigarette filter of claim 1, it is characterized in that: the viscosity of said sodium alginate is 5-150mpa.s.
3. according to the said sodium alginate particulate that is used for cigarette filter of claim 1, it is characterized in that: temperature is 40-85 ℃ in the process of said preparation sodium alginate soln.
4. according to the said sodium alginate particulate that is used for cigarette filter of claim 1, it is characterized in that: the mass percent of said preparation sodium alginate soln is 2-8%.
5. according to the said sodium alginate particulate that is used for cigarette filter of claim 1; It is characterized in that: comprise also in the said sodium alginate soln that mass percent is the auxiliary material of sodium alginate 0.01-30%, said auxiliary material is one or more of gum arabic, gelatin, carragheen, guar gum, dextrin, soluble starch, agar, spices corrosion inhibiter.
6. according to the said sodium alginate particulate that is used for cigarette filter of claim 5, it is characterized in that: said auxiliary material is dextrin, soluble starch, agar, spices corrosion inhibiter by mass ratio 1: 1: 1: 1 mixture.
7. according to the said sodium alginate particulate that is used for cigarette filter of claim 1, it is characterized in that: the system speed of dripping of said dropping preparation method is 70-250/minute.
8. according to the said sodium alginate particulate that is used for cigarette filter of claim 1, it is characterized in that: the sodium alginate particle diameter that said dropping preparation method obtains is 1-6mm.
9. according to the said sodium alginate particulate that is used for cigarette filter of claim 1, it is characterized in that: the sodium alginate particle that dropping preparation method is obtained put into concentration be the pigment solution dyeing of 0.001-2% after 0.5-6 hour again 50 ℃ dry 1 hour down.
10. cigarette with filter tip that contains the said sodium alginate particulate of claim 1; It is characterized in that: contain said sodium alginate particulate in the filter tip of said cigarette with filter tip; Said sodium alginate particulate prepares through following method: viscosity is mixed with the sodium alginate soln that mass percent is 1-10% less than the sodium alginate of 200mpa.s; Add the essence and flavoring agent that mass percent is 0.01-5% then, prepare the sodium alginate particle through dropping preparation method again, final drying promptly obtains the sodium alginate particulate; Use the curing agent cured granulate in the said dropping preparation method, curing agent is that mass percent is the calcium chloride solution of 5-25%.
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CN103060093A (en) * | 2012-12-28 | 2013-04-24 | 华宝食用香精香料(上海)有限公司 | Fragrance-invigorating and moisture-retention particles in cigarette and their preparation method and use |
CN103074801A (en) * | 2013-01-30 | 2013-05-01 | 湖北中烟工业有限责任公司 | Forming paper paint for reducing hazardous substances in cigarette smoke |
CN103071459A (en) * | 2013-01-30 | 2013-05-01 | 福建中烟工业有限责任公司 | Ammonia complex composite capable of selectively reducing ammonia in smoke |
CN104099179A (en) * | 2014-07-23 | 2014-10-15 | 湖北中烟工业有限责任公司 | Method for preparation of cigarette filter stick perfume beads through solid-phase Maillard reaction |
WO2014173130A1 (en) * | 2013-04-24 | 2014-10-30 | 湖北中烟工业有限责任公司 | Method for preparing carbonaceous heat source materials |
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WO2014173130A1 (en) * | 2013-04-24 | 2014-10-30 | 湖北中烟工业有限责任公司 | Method for preparing carbonaceous heat source materials |
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