Nothing Special   »   [go: up one dir, main page]

CN101787864B - Water plugging method for fractured water-flooded oil well for water injection development of oil reservoir in low-permeability reservoir - Google Patents

Water plugging method for fractured water-flooded oil well for water injection development of oil reservoir in low-permeability reservoir Download PDF

Info

Publication number
CN101787864B
CN101787864B CN 201010124334 CN201010124334A CN101787864B CN 101787864 B CN101787864 B CN 101787864B CN 201010124334 CN201010124334 CN 201010124334 CN 201010124334 A CN201010124334 A CN 201010124334A CN 101787864 B CN101787864 B CN 101787864B
Authority
CN
China
Prior art keywords
ldn
blocking agent
water
injection
stratum
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
CN 201010124334
Other languages
Chinese (zh)
Other versions
CN101787864A (en
Inventor
任雁鹏
李勇
王玉功
顾菁华
葛海江
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
China National Petroleum Corp
CNPC Chuanqing Drilling Engineering Co Ltd
Original Assignee
CNPC Chuanqing Drilling Engineering Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by CNPC Chuanqing Drilling Engineering Co Ltd filed Critical CNPC Chuanqing Drilling Engineering Co Ltd
Priority to CN 201010124334 priority Critical patent/CN101787864B/en
Publication of CN101787864A publication Critical patent/CN101787864A/en
Application granted granted Critical
Publication of CN101787864B publication Critical patent/CN101787864B/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Landscapes

  • Soil Conditioners And Soil-Stabilizing Materials (AREA)

Abstract

The invention discloses a water plugging method for a fractured water-flooded oil well of a water injection development reservoir of a low-permeability reservoir, which relates to the technical field of a transformation process for controlling water, stabilizing oil and increasing yield of the oil well in the oil exploitation process, and comprises the following steps: 1) four kinds of plugging agents DQ-1, DQ-2, LDN-1 and LDN-2 with different strengths are prepared on site; 2) continuously pressing the plugging agents DQ-1 and DQ-2 prepared in the step 1) into natural microcracks of the stratum by using an alternative injection process; 3) pressing the plugging agent LDN-1 prepared in the step 1) into natural cracks and artificial cracks of a stratum; 4) pressing the plugging agent LDN-2 prepared in the step 1) into an artificial crack for sealing; the use temperature of the four plugging agents is 0-75 ℃; the concentration of the four plugging agents is 0.5-5%; the pumping pressure of the cement truck or the fracturing truck is less than 30 MPa. The invention can effectively realize the technical effects of increasing and stabilizing the yield of the low-permeability fractured reservoir and improving the oil layer recovery ratio, and can also realize the effective plugging of natural fractures and artificial fractures.

Description

Low permeability reservoir waterflooding reservoir Fractured water logging oil well shutoff method
Technical field
The present invention relates in the oil exploitation process oil well be carried out the reforming technology technical field of water and oil control volume increase, exactly relate to a kind of low permeability reservoir waterflooding reservoir Fractured water cut oil shutoff method.
Background technology
In the low permeability fractured oilfield development process, because the impact of formation fracture (natural microcrack and artificial fracture) is developed and be subjected to long-term injecting water, the non-homogeneity on stratum is unusually serious, make injected water often ooze flow in fracture along height, and involve less permeable layer less than oil-containing, the water filling of this poor efficiency not only affects the crude oil recovery percent of reserves, and owing to the consumption of the energy, the processing of production fluid, the corrosion of pipeline etc. have increased the cost that recovers the oil.
Conventional water-plugging technology generally is to adopt single injection technology to inject from oil well single blocking agent slug, then closing well Hou Ning.
Being that the Chinese patent literature of CN101476452A discloses a kind of water-control fracturing yield increasing method for oil gas well such as publication number, is a kind of take the jelly system of meeting the automatic viscosity reduction of end water as fracturing fluid and cover sand take wax and split technology as the control hydraulic pressure of part proppant specifically.At present when the hyposmosis bottom water reservoir being carried out the fracturing construction, because inter-laminar stress difference is little or just do not have interlayer to form inter-laminar stress difference at all, effectively stop the extension expansion of crack on vertical, the crack that causes fracturing to form extends into the bottom water layer and enters pit shaft along channelling on the crack vertical, causes the sudden and violent property water logging of oil well.The present invention adopts when pressing crack construction, carries coated proppant that paraffin and quartz sand is mixed into by thickening agent and crosslinking agent and coats and stop up at the underground chemical degradation that carries out, and forms plugged zone.It has effectively solved existing manual shielding layer and can not effectively avoid the problem of waterflood and adopt the fracturing fluid that carries diversion agent or diverting agent to meet water base not viscosity reduction and the slower problem of settling rate.
Such water-plugging technology is unsuitable for the shutoff of all low permeability fractured oil reservoirs of buried depth 800m-2500m on the one hand, on the other hand, the sweep area of blocking agent shutoff is few, period of validity is short, also on the one hand, the measure of shutoff is single, and correctional effect is not good, can't realize the effective shutoff to intrinsic fracture and man-made fracture.
Summary of the invention
For solving the problems of the technologies described above, the present invention proposes a kind of shutoff method that is suitable for all low permeability fractured oil reservoirs of buried depth 800m-2500m, use the present invention and can effectively realize low permeability fractured reservoir stimulation, stable yields, improve the technique effect of reservoir recovery, and can also realize the effective shutoff to intrinsic fracture and man-made fracture.
The present invention is by adopting following technical proposals to realize:
A kind of low permeability reservoir waterflooding reservoir Fractured water logging oil well shutoff method is characterized in that step is as follows:
1) four kinds of different blocking agent DQ-1, DQ-2, LDN-1 and LDN-2 of on-the-spot preparation strength:
The preparation method of described DQ-1 blocking agent is: polyacrylonitrile, formaldehyde and water are uniformly mixed to form the aqueous solution according to 5: 2: 93 mass ratio, and this aqueous solution is DQ-1 blocking agent finished product;
Wherein, polyacrylonitrile and formaldehyde shared mass percent in the aqueous solution is respectively 5% and 2%, (for example: polyacrylonitrile 5g, formaldehyde 2g, water 93g)
The preparation method of described DQ-2 blocking agent is: with hydrophobic association polyacrylamide, formaldehyde, phenol and water according to 0.3: 2: 1: 96.7 mass ratio is uniformly mixed to form the aqueous solution, and this aqueous solution is DQ-2 blocking agent finished product;
Wherein, hydrophobic association polyacrylamide, formaldehyde and phenol shared mass percent in the aqueous solution is respectively 0.3%, 2% and 1%, (for example: hydrophobic association polyacrylamide 0.3g, formaldehyde 2g, phenol 1g, water 96.7g)
The preparation method of described LDN-1 blocking agent is: starch conversion polyacrylonitrile, polyethylene alcohol and water are uniformly mixed to form the aqueous solution according to 3: 0.2: 96.8 mass ratio, and this aqueous solution is LDN-1 blocking agent finished product;
Wherein, starch conversion is poly-is respectively 3% and 0.2% with polyvinyl alcohol shared mass percent in the aqueous solution.(for example: starch conversion polyacrylonitrile 3g, polyvinyl alcohol 0.2g, water 96.8g)
The starch conversion polyacrylonitrile is starch/modified polyacrylonitrile fiber dimension.
The concrete grammar of described LDN-2 blocking agent is: with epoxy resin, hexamethylenetetramine, polyethylene alcohol and water according to 3: 2: 0.2: 94.8 mass ratio is uniformly mixed to form the aqueous solution, and this aqueous solution is LDN-2 blocking agent finished product;
Wherein, epoxy resin, hexamethylenetetramine and polyvinyl alcohol shared mass percent 3%, 2% and 0.2% in the aqueous solution.(for example: epoxy resin 3g, hexamethylenetetramine 2g, polyvinyl alcohol 0.2g, water 94.8g)
Epoxy resin is the organic high molecular compound that contains two or more epoxide groups in the general reference molecule.
2) with step 1) in the blocking agent DQ-1 of preparation and DQ-2 adopt alternately injection technology to compress into continuously the natural microcrack on stratum with cementing truck or fracturing unit truck, finish the first slug that three grades of slugs inject; Specifically DQ-1 and DQ-2 are clamp-oned in the natural microcrack in stratum with the discharge capacity of 50-500L/min with cementing truck or fracturing unit truck, two kinds of blocking agent injection rates are aggregated in 30-200m 3Scope;
3) with step 1) in the blocking agent LDN-1 of preparation compress into intrinsic fracture and the man-made fracture on stratum with cementing truck or fracturing unit truck, finish the second slug that three grades of slugs inject; Specifically LDN-1 is clamp-oned in stratum intrinsic fracture and the man-made fracture with the discharge capacity of 50-500L/min with cementing truck or fracturing unit truck, injection rate is at 10-30m 3Scope;
4) with step 1) in the blocking agent LDN-2 of preparation compress into man-made fracture with cementing truck or fracturing unit truck and seal, finish the 3rd slug that three grades of slugs inject; Specifically LDN-2 is clamp-oned in the man-made fracture with the discharge capacity of 50-500L/min with cementing truck or fracturing unit truck, injection rate is at 8-15m 3Scope;
The serviceability temperature of four kinds of blocking agents is 0 ℃-75 ℃; The concentration of four kinds of blocking agents is 0.5-5%; The infusion pressure of cementing truck or fracturing unit truck is less than 30MPa, and four kinds of blocking agents are injected continuously, the infusion time continuously every.
The meaning of the first slug recited above, the second slug, the 3rd slug refers to: the liquid plugging agent that whole plug water construction injects the stratum is divided into three parts, the first slug refers to step 2 exactly) inject DQ-1 and the DQ-2 on stratum, two kinds of blocking agent injection rates are aggregated in 30-200m 3Scope; The second slug refers to step 3 exactly) inject the LDN-1 on stratum, injection rate is at 10-30m 3Scope; The 3rd slug just refers to step 4) inject the LDN-2 on stratum, injection rate is at 8-15m 3Scope.
In step 3) with 4) in add the initator that makes LDN-1 become glue with LDN-2, addition manner adopts artificial mode of slowly appending, addition with respect to LDN-1 blocking agent and LDN-2 blocking agent all in the scope of 0.2%-0.4% mass percent.
Described initator is that concentration is 0.03% oxalic acid solution.Come the mode of titration to measure its concentration with potassium permanganate, compound method is as follows: claim 0.3g oxalic acid crystal, be fed in the aqueous solution of 1000ml, namely get concentration and be 0.03% oxalic acid solution.
Described alternately injection technology specifically refers to: with cementing truck or fracturing unit truck selective different with the viscosity two kinds of gel rubber system DQ-1 of profit and DQ-2 are alternately clamp-oned the stratum continuously, described continuously alternately for injecting first DQ-1, DQ-2 reinjects, and then injection DQ-1, until two kinds of blocking agents are all injected, injection period improves constantly the blocking agent injection pressure, and maximum pressure is no more than 30MPa and gets final product.
Step 1) the required polyacrylonitrile of preparation DQ-1 blocking agent is that molecular weight is 3,000,000-5,000,000 polyacrylonitrile in, and the LDN-1 blocking agent viscosity for preparing is 30-100mPas.
Step 1) the required hydrophobic association polyacrylamide of preparation DQ-2 blocking agent is that molecular weight is 5,000,000-1,000 ten thousand hydrophobic association polyacrylamide in, and the viscosity of the DQ-2 blocking agent for preparing is 50-100mPas.
Step 1) the required polyacrylonitrile of preparation LDN-1 blocking agent is that molecular weight is 5,000,000-1,000 ten thousand polyacrylonitrile in, and required polyvinyl alcohol is that molecular weight is 3,000,000-5,000,000 polyvinyl alcohol, and the viscosity of the LDN-1 blocking agent for preparing is 30-50mPas.
Step 1) the required polyvinyl alcohol of preparation LDN-2 blocking agent is that molecular weight is 3,000,000-5,000,000 polyvinyl alcohol in, and the viscosity of the LDN-2 blocking agent for preparing is 30-50mPas.
Be that the CN101476452A patent documentation is that the prior art of representative is compared with publication number, the technique effect that the present invention reaches shows:
One, on the one hand, adopt alternately injection technology to compress into the microcrack on stratum with cementing truck or fracturing unit truck DQ-1 and DQ-2 because the present invention adopts, rely on the selective and viscosity differences of these two kinds of blocking agents, effectively improved the shutoff sweep area of blocking agent.On the other hand, the present invention adopts four kinds of blocking agent synergies to carry out the oilwell water shutoff construction, be particularly suited for the water blockoff of all low permeability fractured oil reservoirs of buried depth 800m-2500m, use the method and can effectively realize low permeability fractured reservoir stimulation, stable yields, improve the technique effect of reservoir recovery.Again on the one hand, the present invention is by three grades of slug injection technologies, and dependence viscosity, four kinds of blocking agent slugs that intensity is different can carry out effective shutoff to Fracture with low permeability reservoir matrix microcrack, intrinsic fracture and man-made fracture, have improved to be constructed into power.
Two, the present invention is at more than 40 mouthfuls of wells of long celebrating field use, and is efficient greater than 70%, and the individual well moisture content 100% is reduced to 67.2% before by water blockoff, and the 0.17t/d of oil output per well before by water blockoff increases to 0.60t/d.This invention is transformed for the low permeability fractured oil field brings in a well and old well repeats to transform and started a new water-plugging technique, to the low permeability fractured oil field development improve recovery ratio, increasing economic efficiency provides sound assurance.
The specific embodiment
The present invention is described in further detail below in conjunction with the specific embodiment
Embodiment 1
The invention discloses a kind of low permeability reservoir waterflooding reservoir Fractured water logging oil well shutoff method, its step is as follows:
1) four kinds of different blocking agent DQ-1, DQ-2, LDN-1 and LDN-2 of on-the-spot preparation strength:
The preparation method of described DQ-1 blocking agent is: polyacrylonitrile, formaldehyde and water are uniformly mixed to form the aqueous solution according to 5: 2: 93 mass ratio, and this aqueous solution is DQ-1 blocking agent finished product; Wherein, polyacrylonitrile and formaldehyde shared mass percent in the aqueous solution is respectively 5% and 2%, (for example: polyacrylonitrile 5g, formaldehyde 2g, water 93g)
The preparation method of described DQ-2 blocking agent is: with hydrophobic association polyacrylamide, formaldehyde, phenol and water according to 0.3: 2: 1: 96.7 mass ratio is uniformly mixed to form the aqueous solution, and this aqueous solution is DQ-2 blocking agent finished product; Wherein, hydrophobic association polyacrylamide, formaldehyde and phenol shared mass percent in the aqueous solution is respectively 0.3%, 2% and 1%, (for example: hydrophobic association polyacrylamide 0.3g, formaldehyde 2g, phenol 1g, water 96.7g)
The preparation method of described LDN-1 blocking agent is: starch conversion polyacrylonitrile, polyethylene alcohol and water are uniformly mixed to form the aqueous solution according to 3: 0.2: 96.8 mass ratio, and this aqueous solution is LDN-1 blocking agent finished product; Wherein, starch conversion is poly-is respectively 3% and 0.2% with polyvinyl alcohol shared mass percent in the aqueous solution.(for example: starch conversion polyacrylonitrile 3g, polyvinyl alcohol 0.2g, water 96.8g) starch conversion polyacrylonitrile is starch/modified polyacrylonitrile fiber dimension.
The concrete grammar of described LDN-2 blocking agent is: with epoxy resin, hexamethylenetetramine, polyethylene alcohol and water according to 3: 2: 0.2: 94.8 mass ratio is uniformly mixed to form the aqueous solution, and this aqueous solution is LDN-2 blocking agent finished product; Wherein, epoxy resin, hexamethylenetetramine and polyvinyl alcohol shared mass percent 3%, 2% and 0.2% in the aqueous solution.(for example: epoxy resin 3g, hexamethylenetetramine 2g, polyvinyl alcohol 0.2g, water 94.8g) epoxy resin is the organic high molecular compound that contains two or more epoxide groups in the general reference molecule.
2) with step 1) in the blocking agent DQ-1 of preparation and DQ-2 adopt alternately injection technology to compress into continuously the natural microcrack on stratum with cementing truck or fracturing unit truck, finish the first slug that three grades of slugs inject; Specifically DQ-1 and DQ-2 are clamp-oned in the natural microcrack in stratum with the discharge capacity of 50-500L/min with cementing truck or fracturing unit truck, two kinds of blocking agent injection rates are aggregated in 30-200m 3Scope;
3) with step 1) in the blocking agent LDN-1 of preparation compress into intrinsic fracture and the man-made fracture on stratum with cementing truck or fracturing unit truck, finish the second slug that three grades of slugs inject; Specifically LDN-1 is clamp-oned in stratum intrinsic fracture and the man-made fracture with the discharge capacity of 50-500L/min with cementing truck or fracturing unit truck, injection rate is at 10-30m 3Scope;
4) with step 1) in the blocking agent LDN-2 of preparation compress into man-made fracture with cementing truck or fracturing unit truck and seal, finish the 3rd slug that three grades of slugs inject; Specifically LDN-2 is clamp-oned in the man-made fracture with the discharge capacity of 50-500L/min with cementing truck or fracturing unit truck, injection rate is at 8-15m 3Scope;
The serviceability temperature of four kinds of blocking agents is 0 ℃-75 ℃; The concentration of four kinds of blocking agents is 0.5-5%; The infusion pressure of cementing truck or fracturing unit truck is less than 30MPa, and four kinds of blocking agents are injected continuously, the infusion time continuously every.
The meaning of the first slug recited above, the second slug, the 3rd slug refers to: the liquid plugging agent that whole plug water construction injects the stratum is divided into three parts, the first slug refers to step 2 exactly) inject DQ-1 and the DQ-2 on stratum, two kinds of blocking agent injection rates are aggregated in 30-200m 3Scope; The second slug refers to step 3 exactly) inject the LDN-1 on stratum, injection rate is at 10-30m 3Scope; The 3rd slug just refers to step 4) inject the LDN-2 on stratum, injection rate is at 8-15m 3Scope.In step 3) with 4) in add the initator that makes LDN-1 become glue with LDN-2, addition manner adopts artificial mode of slowly appending, addition with respect to LDN-1 blocking agent and LDN-2 blocking agent all in the scope of 0.2%-0.4% mass percent.Described initator is that concentration is 0.03% oxalic acid solution.Come the mode of titration to measure its concentration with potassium permanganate, compound method is as follows: claim 0.3g oxalic acid crystal, be fed in the aqueous solution of 1000ml, namely get concentration and be 0.03% oxalic acid solution.Described alternately injection technology specifically refers to; With cementing truck or fracturing unit truck selective different with the viscosity two kinds of gel rubber system DQ-1 of profit and DQ-2 are alternately clamp-oned the stratum continuously, described continuously alternately for injecting first DQ-1, DQ-2 reinjects, and then injection DQ-1, until two kinds of blocking agents are all injected, injection period improves constantly the blocking agent injection pressure, and maximum pressure is no more than 30MPa and gets final product.Step 1) the required polyacrylonitrile of preparation DQ-1 blocking agent is that molecular weight is 3,000,000-5,000,000 polyacrylonitrile in, and the LDN-1 blocking agent viscosity for preparing is 30-100mPas.Step 1) the required hydrophobic association polyacrylamide of preparation DQ-2 blocking agent is that molecular weight is 5,000,000-1,000 ten thousand hydrophobic association polyacrylamide in, and the viscosity of the DQ-2 blocking agent for preparing is 50-100mPas.Step 1) the required polyacrylonitrile of preparation LDN-1 blocking agent is that molecular weight is 5,000,000-1,000 ten thousand polyacrylonitrile in, and required polyvinyl alcohol is that molecular weight is 3,000,000-5,000,000 polyvinyl alcohol, and the viscosity of the LDN-1 blocking agent for preparing is 30-50mPas.Step 1) the required polyvinyl alcohol of preparation LDN-2 blocking agent is that molecular weight is 3,000,000-5,000,000 polyvinyl alcohol in, and the viscosity of the LDN-2 blocking agent for preparing is 30-50mPas.
Embodiment 2
The present invention has carried out the innovation aspect two on the basis of conventional water blockoff.
Replace injection technique
By the alternately injection technology of DQ-1 and DQ-2, rely on the shutoff sweep area of the selective and viscosity differences Effective Raise blocking agent of two kinds of blocking agents.
The technique contrast
Technology Conventional water-plugging technique Replace injection technique
Operation Adopt single blocking agent single injection technology to inject oil well, closing well Hou Ning during construction. Adopt the alternately injection technology of composite plugging agent, continual raising blocking agent injection pressure.
Advantage Routine techniques is used ripe. The shutoff sweep area of Effective Raise blocking agent is extended the expiration date.
Shortcoming The sweep area of blocking agent shutoff is few, and period of validity is short Belong to new technology, use immature.
Three grades of slug injection techniques
By three grades of slug injection technologies, four kinds of different proprietary blocking agent slugs of dependence intensity can carry out effective shutoff to Fracture with low permeability reservoir matrix microcrack and artificial fracturing crack, have improved to be constructed into power.
The technique contrast
Technology Conventional water-plugging technique Three grades of injection techniques
Operation Adopt single blocking agent single injection technology to inject oil well, closing well Hou Ning during construction. In conjunction with alternately injecting and three grades of injection technologies, adopt the realization of composite plugging agent slug to effective shutoff in matrix microcrack and artificial fracturing crack.
Advantage Belong to conventional art, use ripe, workable. The performance advantage that integrates multiple blocking agent, Effective Raise the measure success rate.
Shortcoming The measure blocking agent is single, and correctional effect is limited. Belong to new technology, use immature.
The field exemplifies:
2008-2009, different well sites are adopted and are alternately injected and three grades of injection combined process construction 3 mouthfuls of wells (X-1, X-2, X-3) in certain oil field, be Fractured water logging oil well before the measure, on average after the measure moisturely be down to 63.3% by 98.8%, on average producing crude oil daily increases 1.5m 3, measure is efficient to reach 100%, has shown stronger technical advantage.
The measure effect statistical form
Block Order Pound sign The condition of production before the measure The present condition of production Level change Oil increases day by day Tired at present
Figure GSA00000057716200071
By three grades of slug injection process techniques, inject four kinds of different proprietary blocking agent slugs of intensity, realize by as far as closely low permeability reservoir matrix microcrack and artificial fracturing crack being carried out selective shut-off; Replace injection technology by changing blocking agent viscosity, in blocking agent shutoff crack, continual raising blocking agent injection pressure improves the sweep area in blocking agent shutoff crack, improves plugging effect; Replace the man-made fracture that technique is reserved certain-length by crossing, be used for recovering the oil after the measure.
The different proprietary selective water shutoff agent of four kinds of intensity that construction is adopted is formulated as liquid state before these four kinds of water shutoff agent constructions, forms respectively gel, frozen glue and high strong solid behind the closing well certain hour of injection stratum.
During the construction of low permeability fractured Water in Water Shutoff in Oil Field, adopt the blocking agent of the different indexs of viscosity to replace injection technology, in blocking agent shutoff crack, continual raising blocking agent injection pressure improves the sweep area in blocking agent shutoff crack.
During the construction of low permeability fractured Water in Water Shutoff in Oil Field, adopt three grades of slug injection technologies, can realize the effective shutoff to matrix microcrack and artificial fracture.Design locations laid respectively at after these three grades of slugs injected: (by as far as near) microcrack-microcrack and man-made fracture top-and away from the part man-made fracture of pit shaft.

Claims (10)

1. low permeability reservoir waterflooding reservoir Fractured water logging oil well shutoff method is characterized in that step is as follows:
1) four kinds of different blocking agent DQ-1, DQ-2, LDN-1 and LDN-2 of on-the-spot preparation strength:
The preparation method of described DQ-1 blocking agent is: polyacrylonitrile, formaldehyde and water are uniformly mixed to form the aqueous solution according to the mass ratio of 5:2:93, and this aqueous solution is DQ-1 blocking agent finished product;
The preparation method of described DQ-2 blocking agent is: hydrophobic association polyacrylamide, formaldehyde, phenol and water are uniformly mixed to form the aqueous solution according to the mass ratio of 0.3:2:1:96.7, and this aqueous solution is DQ-2 blocking agent finished product;
The preparation method of described LDN-1 blocking agent is: starch conversion polyacrylonitrile, polyethylene alcohol and water are uniformly mixed to form the aqueous solution according to the mass ratio of 3:0.2:96.8, and this aqueous solution is LDN-1 blocking agent finished product;
The concrete grammar of described LDN-2 blocking agent is: epoxy resin, hexamethylenetetramine, polyethylene alcohol and water are uniformly mixed to form the aqueous solution according to the mass ratio of 3:2:0.2:94.8, and this aqueous solution is LDN-2 blocking agent finished product;
2) adopt alternately injection technology to compress into continuously the natural microcrack on stratum with cementing truck or fracturing unit truck the blocking agent DQ-1 for preparing in the step 1) and DQ-2, finish the first slug that three grades of slugs inject; Specifically DQ-1 and DQ-2 are clamp-oned in the natural microcrack in stratum with the discharge capacity of 50-500L/min with cementing truck or fracturing unit truck, two kinds of blocking agent injection rates are aggregated in 30-200m 3Scope;
3) the blocking agent LDN-1 for preparing in the step 1) is compressed into intrinsic fracture and the man-made fracture on stratum with cementing truck or fracturing unit truck, finish the second slug that three grades of slugs inject; Specifically LDN-1 is clamp-oned in stratum intrinsic fracture and the man-made fracture with the discharge capacity of 50-500L/min with cementing truck or fracturing unit truck, injection rate is at 10-30m 3Scope;
4) the blocking agent LDN-2 for preparing in the step 1) is compressed into man-made fracture with cementing truck or fracturing unit truck and seal, finish the 3rd slug that three grades of slugs inject; Specifically LDN-2 is clamp-oned in the man-made fracture with the discharge capacity of 50-500L/min with cementing truck or fracturing unit truck, injection rate is at 8-15m 3Scope;
The serviceability temperature of four kinds of blocking agents is 0 ℃-75 ℃; The infusion pressure of cementing truck or fracturing unit truck is less than 30MPa, and four kinds of blocking agents are injected continuously, the infusion time continuously every.
2. low permeability reservoir waterflooding reservoir Fractured water logging oil well shutoff method according to claim 1, it is characterized in that: described alternately injection technology specifically refers to: with cementing truck or fracturing unit truck selective different with the viscosity two kinds of gel rubber system DQ-1 of profit and DQ-2 are alternately clamp-oned the stratum continuously, described continuously alternately for injecting first DQ-1, DQ-2 reinjects, and then injection DQ-1, until two kinds of blocking agents are all injected, injection period, improve constantly the blocking agent injection pressure, maximum pressure is no more than 30MPa and gets final product.
3. low permeability reservoir waterflooding reservoir Fractured water logging oil well shutoff method according to claim 1 and 2, it is characterized in that: in step 3) and 4) in add and to make LDN-1 become the initator of glue with LDN-2, addition manner adopts the mode of manually slowly appending, addition with respect to LDN-1 blocking agent and LDN-2 blocking agent all in the scope of 0.2%-0.4% mass percent.
4. low permeability reservoir waterflooding reservoir Fractured water logging oil well shutoff method according to claim 3, it is characterized in that: described initator is that concentration is 0.03% oxalic acid solution, come the mode of titration to measure its concentration with potassium permanganate, compound method is as follows: claim 0.3g oxalic acid crystal, be fed in the aqueous solution of 1000ml, namely get concentration and be 0.03% oxalic acid solution.
5. low permeability reservoir waterflooding reservoir Fractured water logging oil well shutoff method according to claim 1 and 2, it is characterized in that: the meaning of described the first slug, the second slug, the 3rd slug refers to: the liquid plugging agent that whole plug water construction injects the stratum is divided into three parts, the first slug refers to step 2 exactly) inject DQ-1 and the DQ-2 on stratum, two kinds of blocking agent injection rates are aggregated in 30-200m 3Scope; The second slug is exactly the LDN-1 that refers to step 3) injection stratum, and injection rate is at 10-30m 3Scope; The 3rd slug just refers to the LDN-2 on step 4) injection stratum, and injection rate is at 8-15m 3Scope.
6. low permeability reservoir waterflooding reservoir Fractured water logging oil well shutoff method according to claim 1 and 2, it is characterized in that: the required polyacrylonitrile of preparation DQ-1 blocking agent is that molecular weight is 3,000,000-5,000,000 polyacrylonitrile in the step 1), and the LDN-1 blocking agent viscosity for preparing is 30-100mPa s.
7. low permeability reservoir waterflooding reservoir Fractured water logging oil well shutoff method according to claim 1 and 2, it is characterized in that: the required hydrophobic association polyacrylamide of preparation DQ-2 blocking agent is that molecular weight is 5,000,000-1,000 ten thousand hydrophobic association polyacrylamide in the step 1), and the viscosity of the DQ-2 blocking agent for preparing is 50-100mPa s.
8. low permeability reservoir waterflooding reservoir Fractured water logging oil well shutoff method according to claim 1 and 2, it is characterized in that: the required starch conversion polyacrylonitrile of preparation LDN-1 blocking agent is that molecular weight is 5,000,000-1,000 ten thousand polyacrylonitrile in the step 1), required polyvinyl alcohol is that molecular weight is 3,000,000-5,000,000 polyvinyl alcohol, and the viscosity of the LDN-1 blocking agent for preparing is 30-50mPa s.
9. low permeability reservoir waterflooding reservoir Fractured water logging oil well shutoff method according to claim 1 and 2, it is characterized in that: the required polyvinyl alcohol of preparation LDN-2 blocking agent is that molecular weight is 3,000,000-5,000,000 polyvinyl alcohol in the step 1), and the viscosity of the LDN-2 blocking agent for preparing is 30-50mPa s.
10. low permeability reservoir waterflooding reservoir Fractured water logging oil well shutoff method according to claim 1 and 2, it is characterized in that: the starch conversion polyacrylonitrile is starch/modified polyacrylonitrile fiber dimension, and epoxy resin is the organic high molecular compound that contains two or more epoxide groups in the general reference molecule.
CN 201010124334 2010-03-15 2010-03-15 Water plugging method for fractured water-flooded oil well for water injection development of oil reservoir in low-permeability reservoir Active CN101787864B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN 201010124334 CN101787864B (en) 2010-03-15 2010-03-15 Water plugging method for fractured water-flooded oil well for water injection development of oil reservoir in low-permeability reservoir

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN 201010124334 CN101787864B (en) 2010-03-15 2010-03-15 Water plugging method for fractured water-flooded oil well for water injection development of oil reservoir in low-permeability reservoir

Publications (2)

Publication Number Publication Date
CN101787864A CN101787864A (en) 2010-07-28
CN101787864B true CN101787864B (en) 2013-10-30

Family

ID=42531224

Family Applications (1)

Application Number Title Priority Date Filing Date
CN 201010124334 Active CN101787864B (en) 2010-03-15 2010-03-15 Water plugging method for fractured water-flooded oil well for water injection development of oil reservoir in low-permeability reservoir

Country Status (1)

Country Link
CN (1) CN101787864B (en)

Families Citing this family (19)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101435317B (en) * 2008-12-12 2012-05-23 中国石油集团川庆钻探工程有限公司 Lost-return leakage cross-linked gel plugging process
CN102344788B (en) * 2010-11-18 2013-07-31 中国石油天然气股份有限公司 Temporary plugging agent for horizontal well staged fracturing with controllable gel breaking and preparation method thereof
CN102604608A (en) * 2011-10-19 2012-07-25 中国石油化工股份有限公司 Water shutoff agent for extra-low permeability oil reservoir
CN102678098B (en) * 2012-06-01 2014-08-06 中国石油天然气股份有限公司 Lamellar flooding exhausted oil well plugging and dredging combined excavation and yield increasing method
AU2013277122B2 (en) 2012-06-21 2015-12-17 Shell Internationale Research Maatschappij B.V. Treating a subterranean formation with a mortar slurry
CN102851013A (en) * 2012-09-30 2013-01-02 中国石油集团西部钻探工程有限公司 Composite super gel plugging agent for drilling
CN104100224B (en) * 2013-04-03 2016-12-28 中国石油天然气股份有限公司 Oil well water plugging method
CN103741466B (en) * 2013-12-18 2015-10-28 四川省博仁达石油科技有限公司 A kind of pressure break modified fibre and preparation technology
CN103923626B (en) * 2014-04-11 2016-08-17 长江大学 A kind of chemical plugging agent for oilwell water shutoff and using method thereof
CN108625836B (en) * 2018-05-22 2021-01-29 中国石油天然气集团有限公司 Water control and yield increase method for low-permeability bottom water reservoir high-water-content oil well
CN110396399A (en) * 2019-06-18 2019-11-01 中国石油天然气股份有限公司 Plugging material and plugging method for large-leakage casing damage section of oil-water well
CN111350474B (en) * 2020-03-09 2021-11-09 长安大学 Plugging method of secondary cross-linked interpenetrating network gel capable of realizing deep profile control and flooding
CN111561300A (en) * 2020-05-26 2020-08-21 中国石油天然气股份有限公司 Method for improving water drive effect of water injection well of ultra-low permeability fractured reservoir
CN114427376B (en) * 2020-09-22 2024-04-26 中国石油化工股份有限公司 Method for enhancing lateral drive between wells of large-bottom water reservoir
CN115898322A (en) * 2021-09-22 2023-04-04 中国石油天然气股份有限公司 Water control process method, system and application for oil reservoir seepage field reconstruction
CN116066041B (en) * 2021-11-03 2024-07-30 中国石油天然气股份有限公司 Water injection profile adjusting method based on degradable particles
CN114183095B (en) * 2021-12-03 2023-05-02 西安石油大学 Plugging method for large-scale cracks of fractured reservoir
CN114151048B (en) * 2021-12-07 2023-04-04 西南石油大学 Gas channeling prevention and oil displacement method for compact reservoir horizontal well
CN114991729A (en) * 2022-03-22 2022-09-02 中国石油大学(北京) Subdivision water injection limit quantitative characterization method based on buried depth span and processor

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1079484C (en) * 1999-08-19 2002-02-20 白云渡 Section regulation process for interrupted water-injection depth of water injection well
WO2007107015A1 (en) * 2006-03-30 2007-09-27 Canadian Energy Services L.P. Drilling fluid and method for reducing lost circulation
CN101158280A (en) * 2007-01-29 2008-04-09 邹积鹏 Oil well high water-bearing layer pressure blocking method
CN101476452A (en) * 2009-01-16 2009-07-08 庆阳长庆井下油田助剂有限责任公司 Water-control fracturing yield increasing method for oil gas well

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1079484C (en) * 1999-08-19 2002-02-20 白云渡 Section regulation process for interrupted water-injection depth of water injection well
WO2007107015A1 (en) * 2006-03-30 2007-09-27 Canadian Energy Services L.P. Drilling fluid and method for reducing lost circulation
CN101158280A (en) * 2007-01-29 2008-04-09 邹积鹏 Oil well high water-bearing layer pressure blocking method
CN101476452A (en) * 2009-01-16 2009-07-08 庆阳长庆井下油田助剂有限责任公司 Water-control fracturing yield increasing method for oil gas well

Non-Patent Citations (4)

* Cited by examiner, † Cited by third party
Title
.2007,第30卷(第2期),57-61. *
天然气勘探与开发&gt *
穆丽娜等.裂缝性储层油井冻胶堵水技术.&lt *
穆丽娜等.裂缝性储层油井冻胶堵水技术.<天然气勘探与开发>.2007,第30卷(第2期),57-61.

Also Published As

Publication number Publication date
CN101787864A (en) 2010-07-28

Similar Documents

Publication Publication Date Title
CN101787864B (en) Water plugging method for fractured water-flooded oil well for water injection development of oil reservoir in low-permeability reservoir
CN105089596B (en) Hydraulic fracturing transformation method for unconventional reservoir oil and gas well
CN105089603B (en) Reservoir transformation method for forming fracture network by temporary plugging and steering in fracture
CN102913221B (en) Volume transformation process of low permeability reservoir
CN101747886B (en) Fracturing fluid stock solution, full-filling preposition-free sand adding fracturing method and fracturing fluid cross-linking solution thereof
CN106567702A (en) Method for improving complexity index of deep shale gas fracture
CN107255027A (en) A kind of carbonate reservoir is combined remodeling method
CN101333922A (en) Fracturing process for removing breakdown fluid contamination
CN109209331B (en) Full-support fracturing method for fractured reservoir
CN107387053A (en) A kind of method that big passage major fracture cooperates with pressure break with complicated seam net
CN105952430A (en) Compact oil reservoir low-yield horizontal well volume fracturing energy supplementing method
CN106837274B (en) Method for injecting oil displacement agent into oil layer by fracturing to improve recovery ratio
CN101353958A (en) Oil-gas well exploitation temperature control variable mucic acid fracturing method
CN105041289A (en) Method for forming multiple seams by temporarily blocking seam and forcibly turning plane
CN101280678A (en) Oil well chemical gorge and disgorge yield increasing and inverse direction regulating block connection working process
CN101158280A (en) Oil well high water-bearing layer pressure blocking method
CN113738335B (en) Fracture control integrated volume fracturing method suitable for massive pure shale oil reservoir
CN104963672A (en) Reservoir stratum transformation method for forming seam net by temporarily blocking blast holes with clean steering materials
CN109653721A (en) A kind of saturating oil reservoir pressure break energization displacement of reservoir oil integrated technique of shallow-layer low pressure and low permeability
CN102926701B (en) Continuous mixed type water plugging process method
CN110593806B (en) Large-dose multi-slug water plugging method
CN109915093A (en) A kind of method that &#34; stifled/tune/drive &#34; integration improves oil recovery
CN101915079A (en) Integrated de-plugging yield increasing process
CN106958438B (en) A kind of method for removing blockage of polymer flooding blocking well
CN1995267A (en) Macropore plugging gelatin

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C14 Grant of patent or utility model
GR01 Patent grant
TR01 Transfer of patent right

Effective date of registration: 20201029

Address after: 100007 Dongcheng District, Dongzhimen, China, North Street, No. 9 Oil Mansion, No.

Patentee after: CHINA NATIONAL PETROLEUM Corp.

Patentee after: CNPC Chuanqing Drilling Engineering Co.,Ltd.

Address before: The 1 section of No. 3 company Chuanqing Drilling Technology Information Office Chenghua District Green Road 610051 Chengdu City, Sichuan Province

Patentee before: CNPC Chuanqing Drilling Engineering Co.,Ltd.

TR01 Transfer of patent right