CN101328426B - Composition of emulsified heavy oil - Google Patents
Composition of emulsified heavy oil Download PDFInfo
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- CN101328426B CN101328426B CN2007100696516A CN200710069651A CN101328426B CN 101328426 B CN101328426 B CN 101328426B CN 2007100696516 A CN2007100696516 A CN 2007100696516A CN 200710069651 A CN200710069651 A CN 200710069651A CN 101328426 B CN101328426 B CN 101328426B
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Abstract
The invention relates to a formula of emulsified heavy oil. The formula consists of heavy oil, water and an addition agent, wherein the percentages by weight of the compositions of the formula include: 69.9 to 89.9 percent of the heavy oil, 10 to 30 percent of the water and 0.1 percent of the addition agent; moreover, the addition agent comprises the following compositions in portion by weight: 6 to 20 portions of cobalt iso-octoate, 6 to 20 portions of manganese iso-octoate, 1 to 10 portions of nickel naphthenate, 35 to 65 portions of sorbitan monooleate, 4 to 8 portions of sorbitan polyoxyethylene monooleate, 1 to 2 portions of nonyl phenol polyoxyethylene (6) ether, 4 to 8 portions of sodium hydroxide, 2 to 4 portions of xylene, 1 to 6 portions of methanol and 1 portion of sunset red. The formula has the advantages of reasonable proportioning, advanced technological method, low price, high stability and catalytic and combustion-supporting effects.
Description
Technical field
The present invention relates to a kind of emulsification heavy oil compsn, the invention belongs to a kind of Emulsification of Fuel Oil preparation and utilisation technology in chemical industry, the energy.
Background technology
" fuel-water emulsifying " technology is exactly a fuel economy oil, reduce to consume, and the advanced power-saving technology of environment protection standard, our country researched and developed and uses its technology intermittently from the sixties, but because multiple factor does not become the effective energy-saving form.During "the 10th five-years", National Development and Reform Committee releases technology for mixing water in heavy oil, but makes slow progress, and the technology that this is energy-conservation and environmental protection is dual is not also brought economic benefit, environmental benefit, social benefit for our country at present.At present domestic still not have flameholding, storage time longer, the emulsification heavy oil report of emulsify well.
Summary of the invention
Technical problem to be solved by this invention provides a kind of reasonable ratio, and process method is advanced, and product price is low, and stability is high, and possesses the emulsification heavy oil compsn of catalysis, combustion-supporting effect.
It is this emulsification heavy oil compsn that the present invention solves the problems of the technologies described above the technical scheme that is adopted; Its prescription characteristics are: be made up of heavy oil, water and additive; Wherein, the weight percent of each component is: heavy oil 69.9%-89.9%, water 10%-30%, additive 0.1%; Additive by cobalt iso-octoate, manganese iso-octoate, nickel naphthenate, sorbitan monooleate, anhydrous sorbitol Soxylat A 25-7 monoleate, Nonyl pheno 6 ethers, sodium hydroxide, YLENE, methyl alcohol, the setting sun is red forms, wherein, the shared parts by weight of each component are: cobalt iso-octoate 6-20 part; Manganese iso-octoate 6-20 part, nickel naphthenate 1-10 part, sorbitan monooleate 35-65 part; Anhydrous sorbitol Soxylat A 25-7 monoleate 4-8 part; Nonyl pheno 6 ether 1-2 parts, sodium hydroxide 4-8 part, YLENE 2-4 part; Methyl alcohol 1-6 part, red 1 part of the setting sun.
Contain polyisobutene imide and sodium-alginate in the additive of the present invention, shared parts by weight are: polyisobutene imide 0-10 part, sodium-alginate 0-1 part.
The particle of water of the present invention is less than 2.5 microns, and distributive law is more than 95%.
The present invention compares with prior art and has the following advantages and effect: the present invention improves the vaporization rate of gob, makes the more fully more even of fuel combustion, thereby reaches the energy-conserving and environment-protective purpose.The rate of economizing gasoline that emulsification heavy oil uses can reach 10%-20%, and because incendiary has more fully more evenly reduced the content of oxynitride, oxysulfide and flue dust in the flue gas.Therefore promote emulsification heavy oil for solving energy shortage, improve environment, all have crucial meaning.The present invention's stability is high, and possesses catalysis, combustion-supporting effect.The present invention can be used in the heavy oil of the various qualities and the trade mark, and the formulation ratio of each component is reasonable, and preparation technology is reasonable in design.
Embodiment
Below in conjunction with embodiment the present invention is done further detailed description, following examples are to explanation of the present invention and the present invention is not limited to following examples.
Embodiment 1
The preparation process of additive of the present invention has been described with the lower section:
Get 15 kilograms of cobalt iso-octoates, 10 kilograms of manganese iso-octoates, 5 kilograms of nickel naphthenates, 45 kilograms of sorbitan monooleates; 4.5 kilograms of anhydrous sorbitol Soxylat A 25-7 monoleates, 1.3 kilograms in Nonyl pheno 6 ethers, 5 kilograms of polyisobutene imide, 7 kilograms in sodium hydroxide; 2.5 kilograms of YLENE, 4 kilograms of methyl alcohol, 0.4 kilogram of sodium-alginate; Red 1 kilogram of the setting sun mixes to stir and processes 100.7 kilograms additive, and is subsequent use.
The preparation process of emulsification heavy oil of the present invention has been described with the lower section:
800 kilograms of heavy oil are heated to 80 degrees centigrade, add 70 degrees centigrade 199 kilograms of hot water and 1 kilogram 30 degrees centigrade additive then, continuously stirring 10 minutes uses mulser to cut emulsification 50 minutes, prepares emulsification heavy oil.This emulsification heavy oil at normal temperatures three months stationary phases not stratified, no oily water separation phenomenon.
Embodiment 2
Get 18 kilograms of cobalt iso-octoates, 8 kilograms of manganese iso-octoates, 3 kilograms of nickel naphthenates, 48 kilograms of sorbitan monooleates; 5 kilograms of anhydrous sorbitol Soxylat A 25-7 monoleates, 1.7 kilograms in Nonyl pheno 6 ethers, 8 kilograms of polyisobutene imide, 7.5 kilograms in sodium hydroxide; 2.7 kilograms of YLENE, 4.5 kilograms of methyl alcohol, 0.7 kilogram of sodium-alginate; Red 1 kilogram of the setting sun mixes to stir and processes 108.1 kilograms additive, and is subsequent use.
The preparation process of emulsification heavy oil of the present invention has been described with the lower section:
720 kilograms of heavy oil are heated to 80 degrees centigrade, add 70 degrees centigrade 279 kilograms of hot water and 1 kilogram 30 degrees centigrade additive then, continuously stirring 10 minutes uses mulser to cut emulsification 50 minutes, prepares emulsification heavy oil.This emulsification heavy oil at normal temperatures three months stationary phases not stratified, no oily water separation phenomenon.
Embodiment 3
Get 12 kilograms of cobalt iso-octoates, 17 kilograms of manganese iso-octoates, 6 kilograms of nickel naphthenates, 63 kilograms of sorbitan monooleates; 4 kilograms of anhydrous sorbitol Soxylat A 25-7 monoleates, 1.9 kilograms in Nonyl pheno 6 ethers, 6 kilograms of polyisobutene imide, 4 kilograms in sodium hydroxide; 2 kilograms of YLENE, 6 kilograms of methyl alcohol, 0.1 kilogram of sodium-alginate; Red 1 kilogram of the setting sun mixes to stir and processes 123 kilograms additive, and is subsequent use.
The preparation process of emulsification heavy oil of the present invention has been described with the lower section:
709 kilograms of heavy oil are heated to 80 degrees centigrade, add 70 degrees centigrade 290 kilograms of hot water and 1 kilogram 30 degrees centigrade additive then, continuously stirring 10 minutes uses mulser to cut emulsification 50 minutes, prepares emulsification heavy oil.This emulsification heavy oil at normal temperatures three months stationary phases not stratified, no oily water separation phenomenon.
Embodiment 4
Get 6 kilograms of cobalt iso-octoates, 20 kilograms of manganese iso-octoates, 4 kilograms of nickel naphthenates, 65 kilograms of sorbitan monooleates; 4.2 kilograms of anhydrous sorbitol Soxylat A 25-7 monoleates, 2 kilograms in Nonyl pheno 6 ethers, 3 kilograms of polyisobutene imide, 6.5 kilograms in sodium hydroxide; 3.5 kilograms of YLENE, 4.8 kilograms of methyl alcohol, 1 kilogram of sodium-alginate; Red 1 kilogram of the setting sun mixes to stir and processes 121 kilograms additive, and is subsequent use.
The preparation process of emulsification heavy oil of the present invention has been described with the lower section:
849 kilograms of heavy oil are heated to 80 degrees centigrade, add 70 degrees centigrade 150 kilograms of hot water and 1 kilogram 30 degrees centigrade additive then, continuously stirring 10 minutes uses mulser to cut emulsification 50 minutes, prepares emulsification heavy oil.This emulsification heavy oil at normal temperatures three months stationary phases not stratified, no oily water separation phenomenon.
Embodiment 5
Get 7 kilograms of cobalt iso-octoates, 18 kilograms of manganese iso-octoates, 2 kilograms of nickel naphthenates, 40 kilograms of sorbitan monooleates; 6 kilograms of anhydrous sorbitol Soxylat A 25-7 monoleates, 1 kilogram in Nonyl pheno 6 ethers, 7.8 kilograms in sodium hydroxide; 3.8 kilograms of YLENE, 5.5 kilograms of methyl alcohol, 0.8 kilogram of sodium-alginate; Red 1 kilogram of the setting sun mixes to stir and processes 92.9 kilograms additive, and is subsequent use.
The preparation process of emulsification heavy oil of the present invention has been described with the lower section:
870 kilograms of heavy oil are heated to 80 degrees centigrade, add 70 degrees centigrade 129 kilograms of hot water and 1 kilogram 30 degrees centigrade additive then, continuously stirring 10 minutes uses mulser to cut emulsification 50 minutes, prepares emulsification heavy oil.This emulsification heavy oil at normal temperatures three months stationary phases not stratified, no oily water separation phenomenon.
Embodiment 6
Get 9 kilograms of cobalt iso-octoates, 16 kilograms of manganese iso-octoates, 10 kilograms of nickel naphthenates, 50 kilograms of sorbitan monooleates; 4.8 kilograms of anhydrous sorbitol Soxylat A 25-7 monoleates, 1.1 kilograms in Nonyl pheno 6 ethers, 1 kilogram of polyisobutene imide, 8 kilograms in sodium hydroxide; 4 kilograms of YLENE, 1.2 kilograms of methyl alcohol, 0.2 kilogram of sodium-alginate; Red 1 kilogram of the setting sun mixes to stir and processes 106.3 kilograms additive, and is subsequent use.
The preparation process of emulsification heavy oil of the present invention has been described with the lower section:
899 kilograms of heavy oil are heated to 80 degrees centigrade, add 70 degrees centigrade 100 kilograms of hot water and 1 kilogram 30 degrees centigrade additive then, continuously stirring 10 minutes uses mulser to cut emulsification 50 minutes, prepares emulsification heavy oil.This emulsification heavy oil at normal temperatures three months stationary phases not stratified, no oily water separation phenomenon.
Embodiment 7
Get 20 kilograms of cobalt iso-octoates, 7 kilograms of manganese iso-octoates, 1 kilogram of nickel naphthenate, 61 kilograms of sorbitan monooleates; 5.5 kilograms of anhydrous sorbitol Soxylat A 25-7 monoleates, 1.5 kilograms in Nonyl pheno 6 ethers, 10 kilograms of polyisobutene imide, 4 kilograms in sodium hydroxide; 3 kilograms of YLENE, 5.8 kilograms of methyl alcohol, 0.3 kilogram of sodium-alginate; Red 1 kilogram of the setting sun mixes to stir and processes 120.1 kilograms additive, and is subsequent use.
The preparation process of emulsification heavy oil of the present invention has been described with the lower section:
789 kilograms of heavy oil are heated to 80 degrees centigrade, add 70 degrees centigrade 210 kilograms of hot water and 1 kilogram 30 degrees centigrade additive then, continuously stirring 10 minutes uses mulser to cut emulsification 50 minutes, prepares emulsification heavy oil.This emulsification heavy oil at normal temperatures three months stationary phases not stratified, no oily water separation phenomenon.
Embodiment 8
Get 16 kilograms of cobalt iso-octoates, 10 kilograms of manganese iso-octoates, 9 kilograms of nickel naphthenates, 38 kilograms of sorbitan monooleates; 8 kilograms of anhydrous sorbitol Soxylat A 25-7 monoleates, 1.8 kilograms in Nonyl pheno 6 ethers, 9 kilograms of polyisobutene imide, 4.3 kilograms in sodium hydroxide; 3.3 kilograms of YLENE, 3.8 kilograms of methyl alcohol, 0.9 kilogram of sodium-alginate; Red 1 kilogram of the setting sun mixes to stir and processes 105.1 kilograms additive, and is subsequent use.
The preparation process of emulsification heavy oil of the present invention has been described with the lower section:
760 kilograms of heavy oil are heated to 80 degrees centigrade, add 70 degrees centigrade 239 kilograms of hot water and 1 kilogram 30 degrees centigrade additive then, continuously stirring 10 minutes uses mulser to cut emulsification 50 minutes, prepares emulsification heavy oil.This emulsification heavy oil at normal temperatures three months stationary phases not stratified, no oily water separation phenomenon.
Embodiment 9
Get 13 kilograms of cobalt iso-octoates, 12 kilograms of manganese iso-octoates, 5 kilograms of nickel naphthenates, 35 kilograms of sorbitan monooleates; 7.5 kilograms of anhydrous sorbitol Soxylat A 25-7 monoleates, 1.2 kilograms in Nonyl pheno 6 ethers, 7 kilograms of polyisobutene imide, 5 kilograms in sodium hydroxide; 2.1 kilograms of YLENE, 3.2 kilograms of methyl alcohol, 0.6 kilogram of sodium-alginate; Red 1 kilogram of the setting sun mixes to stir and processes 92.6 kilograms additive, and is subsequent use.
The preparation process of emulsification heavy oil of the present invention has been described with the lower section:
730 kilograms of heavy oil are heated to 80 degrees centigrade, add 70 degrees centigrade 269 kilograms of hot water and 1 kilogram 30 degrees centigrade additive then, continuously stirring 10 minutes uses mulser to cut emulsification 50 minutes, prepares emulsification heavy oil.This emulsification heavy oil at normal temperatures three months stationary phases not stratified, no oily water separation phenomenon.
Embodiment 10
Get 8 kilograms of cobalt iso-octoates, 19 kilograms of manganese iso-octoates, 4 kilograms of nickel naphthenates, 36 kilograms of sorbitan monooleates; 7.6 kilograms of anhydrous sorbitol Soxylat A 25-7 monoleates, 1.7 kilograms in Nonyl pheno 6 ethers, 2 kilograms of polyisobutene imide, 6 kilograms in sodium hydroxide; 2.4 kilograms of YLENE, 1 kilogram of methyl alcohol, 0.5 kilogram of sodium-alginate; Red 1 kilogram of the setting sun mixes to stir and processes 89.2 kilograms additive, and is subsequent use.
The preparation process of emulsification heavy oil of the present invention has been described with the lower section:
699 kilograms of heavy oil are heated to 80 degrees centigrade, add 70 degrees centigrade 300 kilograms of hot water and 1 kilogram 30 degrees centigrade additive then, continuously stirring 10 minutes uses mulser to cut emulsification 50 minutes, prepares emulsification heavy oil.This emulsification heavy oil at normal temperatures three months stationary phases not stratified, no oily water separation phenomenon.
Embodiment 11
Get 17 kilograms of cobalt iso-octoates, 13 kilograms of manganese iso-octoates, 3 kilograms of nickel naphthenates, 43 kilograms of sorbitan monooleates; 5.9 kilograms of anhydrous sorbitol Soxylat A 25-7 monoleates, 1.4 kilograms in Nonyl pheno 6 ethers, 5 kilograms of polyisobutene imide, 5.5 kilograms in sodium hydroxide; 3.1 kilograms of YLENE, 1.7 kilograms of methyl alcohol, 0.4 kilogram of sodium-alginate; Red 1 kilogram of the setting sun mixes to stir and processes 100 kilograms additive, and is subsequent use.
The preparation process of emulsification heavy oil of the present invention has been described with the lower section:
889 kilograms of heavy oil are heated to 80 degrees centigrade, add 70 degrees centigrade 110 kilograms of hot water and 1 kilogram 30 degrees centigrade additive then, continuously stirring 10 minutes uses mulser to cut emulsification 50 minutes, prepares emulsification heavy oil.This emulsification heavy oil at normal temperatures three months stationary phases not stratified, no oily water separation phenomenon.
Embodiment 12
Get 19 kilograms of cobalt iso-octoates, 6 kilograms of manganese iso-octoates, 7 kilograms of nickel naphthenates, 54 kilograms of sorbitan monooleates; 6.5 kilograms of anhydrous sorbitol Soxylat A 25-7 monoleates, 1.6 kilograms in Nonyl pheno 6 ethers, 4 kilograms of polyisobutene imide, 6.8 kilograms in sodium hydroxide; 3.6 kilograms of YLENE, 2 kilograms of methyl alcohol, 0.7 kilogram of sodium-alginate; Red 1 kilogram of the setting sun mixes to stir and processes 112.2 kilograms additive, and is subsequent use.
The preparation process of emulsification heavy oil of the present invention has been described with the lower section:
829 kilograms of heavy oil are heated to 80 degrees centigrade, add 70 degrees centigrade 170 kilograms of hot water and 1 kilogram 30 degrees centigrade additive then, continuously stirring 10 minutes uses mulser to cut emulsification 50 minutes, prepares emulsification heavy oil.This emulsification heavy oil at normal temperatures three months stationary phases not stratified, no oily water separation phenomenon.
Embodiment 13
Get 10 kilograms of cobalt iso-octoates, 11 kilograms of manganese iso-octoates, 8 kilograms of nickel naphthenates, 57 kilograms of sorbitan monooleates; 7 kilograms of anhydrous sorbitol Soxylat A 25-7 monoleates, 1.9 kilograms in Nonyl pheno 6 ethers, 6 kilograms of polyisobutene imide; 5.2 kilograms in sodium hydroxide, 2.8 kilograms of YLENE, 2.5 kilograms of methyl alcohol; Red 1 kilogram of the setting sun mixes to stir and processes 112.4 kilograms additive, and is subsequent use.
The preparation process of emulsification heavy oil of the present invention has been described with the lower section:
719 kilograms of heavy oil are heated to 80 degrees centigrade, add 70 degrees centigrade 180 kilograms of hot water and 1 kilogram 30 degrees centigrade additive then, continuously stirring 10 minutes uses mulser to cut emulsification 50 minutes, prepares emulsification heavy oil.This emulsification heavy oil at normal temperatures three months stationary phases not stratified, no oily water separation phenomenon.
In above embodiment, be suitable for the heavy oil of the various qualities and the trade mark.
During burning, the emulsification heavy oil that the present invention makes can improve the vaporization rate of gob, makes the more fully more even of fuel combustion, thereby reaches the energy-conserving and environment-protective purpose.The rate of economizing gasoline that emulsification heavy oil uses can reach 10%-20%, and because incendiary has more fully more evenly reduced the content of oxynitride, oxysulfide and flue dust in the flue gas.Therefore promote emulsification heavy oil for solving energy shortage, improve environment, all have crucial meaning.
Instance:
Through the monitoring of local environmental administration, its smoke content descended 55% than former combusting heavy oil after continent architectural pottery two factories this emulsification heavy oil of use was dissolved in Foshan, and oxysulfide descends 25%, and CO descends 40%.And, make the product percent of pass of this factory rise 10% because incendiary is more abundant.
Claims (2)
1. emulsification heavy oil compsn, the prescription characteristic is: be made up of heavy oil, water and additive, wherein, the weight percent of each component is: heavy oil 69.9%-89.9%, water 10%-30%, additive 0.1%; Additive is red by cobalt iso-octoate, manganese iso-octoate, nickel naphthenate, sorbitan monooleate, anhydrous sorbitol Soxylat A 25-7 monoleate, Nonyl pheno 6 ethers, sodium hydroxide, YLENE, methyl alcohol, the setting sun, polyisobutene imide and sodium-alginate are formed; Wherein, the shared parts by weight of each component are: cobalt iso-octoate 6-20 part, manganese iso-octoate 6-20 part; Nickel naphthenate 1-10 part; Sorbitan monooleate 35-65 part, anhydrous sorbitol Soxylat A 25-7 monoleate 4-8 part, Nonyl pheno 6 ether 1-2 parts; Sodium hydroxide 4-8 part; YLENE 2-4 part, methyl alcohol 1-6 part, red 1 part of the setting sun, polyisobutene imide 1-10 part, sodium-alginate 0.1-1 part.
2. emulsification heavy oil compsn according to claim 1 is characterized in that: the particle of described water is less than 2.5 microns, and distributive law is more than 95%.
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| CN2007100696516A CN101328426B (en) | 2007-06-22 | 2007-06-22 | Composition of emulsified heavy oil |
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| CN2007100696516A CN101328426B (en) | 2007-06-22 | 2007-06-22 | Composition of emulsified heavy oil |
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| CN101328426B true CN101328426B (en) | 2012-06-20 |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN101462914B (en) * | 2009-01-12 | 2011-12-07 | 山西建烨工贸有限公司 | Environment protective emulsive explosive composite emulsifying agent |
| CN102504896B (en) * | 2011-11-09 | 2014-02-12 | 南开大学 | Method for preparing emulsified heavy oil by using microbial agent |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1357605A (en) * | 2001-08-31 | 2002-07-10 | 石生玉 | Additive for synthetic water-diesel oil fuel and its prepn and application |
| CN1401745A (en) * | 2002-09-26 | 2003-03-12 | 武汉理工大学 | Multifunctional heavy oil and fuel oil additive, preparation and use thereof in preparing emulsified oil |
| CN1542099A (en) * | 2003-11-07 | 2004-11-03 | 陆翼德 | additive for emulsified diesel oil and preparation method thereof |
| CN1566279A (en) * | 2003-06-13 | 2005-01-19 | 洪星南 | Environmental protection water-based diesel oil emulsifier |
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2007
- 2007-06-22 CN CN2007100696516A patent/CN101328426B/en not_active Expired - Fee Related
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1357605A (en) * | 2001-08-31 | 2002-07-10 | 石生玉 | Additive for synthetic water-diesel oil fuel and its prepn and application |
| CN1401745A (en) * | 2002-09-26 | 2003-03-12 | 武汉理工大学 | Multifunctional heavy oil and fuel oil additive, preparation and use thereof in preparing emulsified oil |
| CN1566279A (en) * | 2003-06-13 | 2005-01-19 | 洪星南 | Environmental protection water-based diesel oil emulsifier |
| CN1542099A (en) * | 2003-11-07 | 2004-11-03 | 陆翼德 | additive for emulsified diesel oil and preparation method thereof |
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