CN101250339A - Ultraviolet light curing vacuum coating foundation and finish - Google Patents
Ultraviolet light curing vacuum coating foundation and finish Download PDFInfo
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- CN101250339A CN101250339A CNA2008100272496A CN200810027249A CN101250339A CN 101250339 A CN101250339 A CN 101250339A CN A2008100272496 A CNA2008100272496 A CN A2008100272496A CN 200810027249 A CN200810027249 A CN 200810027249A CN 101250339 A CN101250339 A CN 101250339A
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Abstract
The invention discloses ultraviolet light curing vacuum plating primer and finish, wherein primer is formed by random proportion of double function aliphatic polyurethane acrylic ester, epoxy acrylic ester, trifunctional acrylic ester, double function acrylic ester, adhesion promoting resin, photo initiator, diluent, and auxiliary agent, finish is formed by random proportion of high function aliphatic polyurethane acrylic ester, large molecular resin, double functional aliphatic polyurethane acrylic ester, trifunctional aliphatic polyurethane acrylic ester, adhesion promoting resin, photo initiator, diluent, and auxiliary agent. The surface of substrate material is conducted with painting treatment of primer, which increases the plainness and adhesion fastness of the vacuum plating film, and vacuum plating film is conducted with the surface painting treatment of UV vacuum plating finish, which can prevent oxidization of metal film layer and endows vacuum plating film with excellent surface abrasion resistance and extreme wonderful hand feeling.
Description
Technical field
The present invention relates to a kind of ultraviolet-curing paint, relate in particular to and the matching used coating of vacuum plating.
Background technology
Vacuum coating technology claims physical gas phase deposition technology (PVD) again, be under vacuum condition, with metal-plated on the surface of plastic rubber substrate and form a kind of novel process of laminated film, by metallization can be gold and silver, copper, zinc, chromium, aluminium etc., thereby realize the metallization of plastic cement outward appearance, in order to make coating open and flat, performances such as metalluster, brightness are arranged, then need handle in the application of plating piece upper base finish paint respectively in the plated film front and back.At the bottom of Chinese patent CN1281011 is a kind ultraviolet-curing vacuum coating, finish paint, the degree lacquer is by acrylic acid modified bisphenol A epoxide resin, polyvalent alcohol and Hydroxyethyl acrylate and toluene two different hydrogen acid ether affixtures, reactive diluent, light trigger, auxiliary agent is formed, finish paint is by polyester acrylate, the phenolic aldehyde epoxy acrylate, reactive thinner, light trigger, adhesion promoter, auxiliary agent is formed, above-mentioned composition is all by after certain weight percent proportioning, mixing and stirring, make, along with the miniaturization day by day of modern digital product, exquisitenessization, existing these coating make that the plating piece coating adhesion is poor, the plating piece surface irregularity, shortcoming such as wear no resistance.
Summary of the invention
The present invention need solve the planeness and the poor adhesive force of vacuum coating, and the problem that prevents the metallic diaphragm oxidation.
The technical solution adopted in the present invention is: at the bottom of a kind of ultraviolet light polymerization UV vacuum plating, finish paint:
Priming paint promotes resin, light trigger, thinner, any proportioning of auxiliary agent to form by two sense aliphatic urethane acrylates, epoxy acrylate, trifunctional acrylate, two functional acrylates, sticking power; Finish paint promotes resin, light trigger, thinner, any proportioning of auxiliary agent to form by high official's energy aliphatic urethane acrylate, macromolecular resin, two sense aliphatic urethane acrylates, trifunctional aliphatic urethane acrylate, sticking power.
Further: the consisting of of above-mentioned priming paint: two sense aliphatic urethane acrylates, 5～30wt%, epoxy acrylate 10～40wt%, trifunctional acrylate 5～25wt%, two functional acrylates, 5～25wt%, sticking power promote resin 5～10wt%, light trigger 1～5wt%, thinner 20～60wt%, auxiliary agent 0.01～1wt%; Finish paint consists of: high official's energy aliphatic urethane acrylate 5～20wt%, macromolecular resin 10～30wt%, two sense aliphatic urethane acrylates, 5～20wt%, trifunctional aliphatic urethane acrylate 10～20wt%, sticking power promote resin 1～5wt%, light trigger 1～5wt%, thinner 20～60wt%, auxiliary agent 0.01～1wt%.
Sticking power described in the lacquer of above-mentioned bottom surface promotes that resin is one or both in ethylene-vinyl acetate copolymer, propylene-acetate ethylene copolymer, the phenoxy group dimethyl-silicon hydride compounds; Described light trigger is one or more in phenyl-phosphonite diethyl ester, benzophenone, α monohydroxy isopropyl benzene ketone, the α monohydroxy phenylcyclohexane ketone, and these light triggers have higher light sensitivity and thermostability; Described thinner is one or more in hexanediyl ester, neopentyl glycol diacrylate enzyme, the Viscoat 295; Auxiliary agent commonly used has auxiliary agents such as stopper, defoamer, flow agent and color stuffing, and their main effect is to improve coating property, increases the UV photosensitive perception, reduces difficulty of construction.
With at the bottom of the above-mentioned ultraviolet light polymerization UV vacuum plating, finish paint is applied to vacuum coating technology, promptly use vacuum plating PVD technology to plate before the button of digital electronic goods such as mobile phone, MP3, digital camera, form, the shell, substrate surface is done the application of above-mentioned priming paint and handled, increased the planeness and the attachment fastness of vacuum coating; After vacuum plating, vacuum coating is done the external coating of UV vacuum plating finish paint and handled, prevent the metallic diaphragm oxidation, give its excellent surface abrasion resistance and splendid feel.To have the distinctive texture of metal, gloss through the base material of above-mentioned prime treatment, and improve surface abrasion resistance and feel largely.
With at the bottom of the above-mentioned ultraviolet light polymerization UV vacuum plating, the shell of digital electronic goods such as mobile phone of handling of finish paint and vacuum plating PVD complete sets of Techniques, MP3, digital camera has the following advantages:
1, the strong adhesion between coating and the metallic diaphragm;
2, environmental testing excellent performance has passed through tests such as salt spray resistance, water boiling resistance, hot and humid, cold cycling, and coating is excellent;
3, excellent abrasive, the wear-resisting test of RCA reaches more than 500 times, and the surface does not have wearing and tearing.
Embodiment
At the bottom of the vacuum plating of following examples medium ultraviolet optical curing of UV, finish paint is preferably filled a prescription is at random; these prescriptions are the indefiniteness embodiment; it just is used to specify the present invention, and those skilled in the art can be protection scope of the present invention according to thinking of the present invention and the prescription that the proportioning of selecting materials filters out fully.
Embodiment 1
At the bottom of a kind of ultraviolet-curing vacuum coating, finish paint, wherein consisting of of priming paint: two sense aliphatic urethane acrylate 30wt%, epoxy acrylate 10wt%, trifunctional acrylate 5wt%, two functional acrylate 5wt%, sticking power promote resin 5wt%, light trigger 1～5wt%, thinner 20～60wt%, auxiliary agent 0.01～1wt%; Finish paint consists of: high official's energy aliphatic urethane acrylate 6wt%, macromolecular resin 8wt%, two sense aliphatic urethane acrylate 20wt%, trifunctional aliphatic urethane acrylate 11wt%, sticking power promote resin 4wt%, light trigger 1～5wt%, thinner 20～60wt%, auxiliary agent 0.01～1wt%, wherein sticking power promotes that resin is that ethylene-vinyl acetate copolymer, light trigger are that phenyl-phosphonite diethyl ester, thinner are hexanediyl esters, adds usual auxiliaries.
At the bottom of the ultraviolet light polymerization UV vacuum plating with above-mentioned prescription, the shell of digital electronic goods such as mobile phone of handling of finish paint and vacuum plating PVD complete sets of Techniques, MP3, digital camera has the following advantages:
1, the strong adhesion between coating and the metallic diaphragm;
2, environmental testing excellent performance has passed through tests such as salt spray resistance, water boiling resistance, hot and humid, cold cycling, and coating is excellent;
3, excellent abrasive, the wear-resisting test of RCA reaches more than 500 times, and the surface does not have wearing and tearing.
Embodiment 2
At the bottom of a kind of ultraviolet-curing vacuum coating, finish paint, wherein consisting of of priming paint: two sense aliphatic urethane acrylate 8wt%, epoxy acrylate 30wt%, trifunctional acrylate 10wt%, two functional acrylate 10wt%, sticking power promote resin 8wt%, light trigger 1～5wt%, thinner 20～60wt%, auxiliary agent 0.01～1wt%; Finish paint consists of: high official's energy aliphatic urethane acrylate 20wt%, macromolecular resin 8wt%, two sense aliphatic urethane acrylate 10wt%, trifunctional aliphatic urethane acrylate 15wt%, sticking power promote resin 4wt%, light trigger 1～5wt%, thinner 20～60wt%, auxiliary agent 0.01～1wt%, sticking power promotes that resin is propylene-acetate ethylene copolymer in the above-mentioned end, the finish paint, described light trigger is a benzophenone, described thinner is a neopentyl glycol diacrylate enzyme, adds usual auxiliaries.
At the bottom of the ultraviolet light polymerization UV vacuum plating with above-mentioned prescription, the shell of digital electronic goods such as mobile phone of handling of finish paint and vacuum plating PVD complete sets of Techniques, MP3, digital camera has the following advantages:
1, the strong adhesion between coating and the metallic diaphragm;
2, environmental testing excellent performance has passed through tests such as salt spray resistance, water boiling resistance, hot and humid, cold cycling, and coating is excellent;
3, excellent abrasive, the wear-resisting test of RCA reaches more than 500 times, and the surface does not have wearing and tearing.
Embodiment 3
At the bottom of a kind of ultraviolet-curing vacuum coating, finish paint, wherein consisting of of priming paint: two sense aliphatic urethane acrylate 8wt%, epoxy acrylate 12wt%, trifunctional acrylate 18wt%, two functional acrylate 24wt%, sticking power promote resin 7wt%, light trigger 1～5wt%, thinner 20～60wt%, auxiliary agent 0.01～1wt%; Finish paint consists of: high official's energy aliphatic urethane acrylate 15wt%, macromolecular resin 25wt%, two sense aliphatic urethane acrylate 15wt%, trifunctional aliphatic urethane acrylate 12wt%, sticking power promote resin 4wt%, light trigger 1～5wt%, thinner 20～60wt%, auxiliary agent 0.01～1wt%, and the sticking power described in the above-mentioned end, the finish paint promotes that resin is in the phenoxy group dimethyl-silicon hydride compounds; Described light trigger is a α monohydroxy isopropyl benzene ketone; Described thinner is a Viscoat 295, adds usual auxiliaries.
At the bottom of the ultraviolet light polymerization UV vacuum plating with above-mentioned prescription, the shell of digital electronic goods such as mobile phone of handling of finish paint and vacuum plating PVD complete sets of Techniques, MP3, digital camera has the following advantages:
1, the strong adhesion between coating and the metallic diaphragm;
2, environmental testing excellent performance has passed through tests such as salt spray resistance, water boiling resistance, hot and humid, cold cycling, and coating is excellent;
3, excellent abrasive, the wear-resisting test of RCA reaches more than 500 times, and the surface does not have wearing and tearing.
Embodiment 4
At the bottom of a kind of ultraviolet-curing vacuum coating, finish paint, wherein consisting of of priming paint: two sense aliphatic urethane acrylate 18wt%, epoxy acrylate 20wt%, trifunctional acrylate 15wt%, two functional acrylate 10wt%, sticking power promote resin 8wt%, light trigger 1～5wt%, thinner 20～60wt%, auxiliary agent 0.01～1wt%; Finish paint consists of: high official's energy aliphatic urethane acrylate 8wt%, macromolecular resin 20wt%, two sense aliphatic urethane acrylate 18wt%, trifunctional aliphatic urethane acrylate 11wt%, sticking power promote resin 3wt%, light trigger 1～5wt%, thinner 20～60wt%, auxiliary agent 0.01～1wt%, wherein sticking power promotes that resin is that ethylene-vinyl acetate copolymer, light trigger are that phenyl-phosphonite diethyl ester, thinner are hexanediyl esters, adds usual auxiliaries.
At the bottom of the ultraviolet light polymerization UV vacuum plating with above-mentioned prescription, the shell of digital electronic goods such as mobile phone of handling of finish paint and vacuum plating PVD complete sets of Techniques, MP3, digital camera has the following advantages:
1, the strong adhesion between coating and the metallic diaphragm;
2, environmental testing excellent performance has passed through tests such as salt spray resistance, water boiling resistance, hot and humid, cold cycling, and coating is excellent;
3, excellent abrasive, the wear-resisting test of RCA reaches more than 500 times, and the surface does not have wearing and tearing.
Embodiment 5
At the bottom of a kind of ultraviolet-curing vacuum coating, finish paint, wherein consisting of of priming paint: two sense aliphatic urethane acrylate 28wt%, epoxy acrylate 12wt%, trifunctional acrylate 8wt%, two functional acrylate 20wt%, sticking power promote resin 8wt%, light trigger 1～5wt%, thinner 20～60wt%, auxiliary agent 0.01～1wt%; Finish paint consists of: high official's energy aliphatic urethane acrylate 18wt%, macromolecular resin 25wt%, two sense aliphatic urethane acrylate 15wt%, trifunctional aliphatic urethane acrylate 11wt%, sticking power promote resin 2wt%, light trigger 1～5wt%, thinner 20～60wt%, auxiliary agent 0.01～1wt%, sticking power promotes that resin is propylene-acetate ethylene copolymer in the above-mentioned end, the finish paint, described light trigger is a benzophenone, described thinner is a neopentyl glycol diacrylate enzyme, adds usual auxiliaries.
At the bottom of the ultraviolet light polymerization UV vacuum plating with above-mentioned prescription, the shell of digital electronic goods such as mobile phone of handling of finish paint and vacuum plating PVD complete sets of Techniques, MP3, digital camera has the following advantages:
1, the strong adhesion between coating and the metallic diaphragm;
2, environmental testing excellent performance has passed through tests such as salt spray resistance, water boiling resistance, hot and humid, cold cycling, and coating is excellent;
3, excellent abrasive, the wear-resisting test of RCA reaches more than 500 times, and the surface does not have wearing and tearing.
Embodiment 6
At the bottom of a kind of ultraviolet-curing vacuum coating, finish paint, wherein consisting of of priming paint: two sense aliphatic urethane acrylate 18wt%, epoxy acrylate 28wt%, trifunctional acrylate 10wt%, two functional acrylate 6wt%, sticking power promote resin 8wt%, light trigger 1～5wt%, thinner 20～60wt%, auxiliary agent 0.01～1wt%; Finish paint consists of: high official's energy aliphatic urethane acrylate 8wt%, macromolecular resin 20wt%, two sense aliphatic urethane acrylate 18wt%, trifunctional aliphatic urethane acrylate 11wt%, sticking power promote resin 3wt%, light trigger 1～5wt%, thinner 20～60wt%, auxiliary agent 0.01～1wt%, wherein sticking power promotes that resin is that ethylene-vinyl acetate copolymer, light trigger are that phenyl-phosphonite diethyl ester, thinner are hexanediyl esters, adds usual auxiliaries.
At the bottom of the ultraviolet light polymerization UV vacuum plating with above-mentioned prescription, the shell of digital electronic goods such as mobile phone of handling of finish paint and vacuum plating PVD complete sets of Techniques, MP3, digital camera has the following advantages:
1, the strong adhesion between coating and the metallic diaphragm;
2, environmental testing excellent performance has passed through tests such as salt spray resistance, water boiling resistance, hot and humid, cold cycling, and coating is excellent;
3, excellent abrasive, the wear-resisting test of RCA reaches more than 500 times, and the surface does not have wearing and tearing.
Embodiment 7
At the bottom of a kind of ultraviolet-curing vacuum coating, finish paint, wherein consisting of of priming paint: two sense aliphatic urethane acrylate 18wt%, epoxy acrylate 20wt%, trifunctional acrylate 15wt%, two functional acrylate 10wt%, sticking power promote resin 8wt%, light trigger 1～5wt%, thinner 20～60wt%, auxiliary agent 0.01～1wt%; Finish paint consists of: high official's energy aliphatic urethane acrylate 15wt%, macromolecular resin 25wt%, two sense aliphatic urethane acrylate 15wt%, trifunctional aliphatic urethane acrylate 11wt%, sticking power promote resin 1wt%, light trigger 1～5wt%, thinner 20～60wt%, auxiliary agent 0.01～1wt%, and the sticking power described in the above-mentioned end, the finish paint promotes that resin is in the phenoxy group dimethyl-silicon hydride compounds; Described light trigger is a α monohydroxy isopropyl benzene ketone; Described thinner is a Viscoat 295, adds usual auxiliaries.
At the bottom of the ultraviolet light polymerization UV vacuum plating with above-mentioned prescription, the shell of digital electronic goods such as mobile phone of handling of finish paint and vacuum plating PVD complete sets of Techniques, MP3, digital camera has the following advantages:
1, the strong adhesion between coating and the metallic diaphragm;
2, environmental testing excellent performance has passed through tests such as salt spray resistance, water boiling resistance, hot and humid, cold cycling, and coating is excellent;
3, excellent abrasive, the wear-resisting test of RCA reaches more than 500 times, and the surface does not have wearing and tearing.
Embodiment 8
At the bottom of a kind of ultraviolet-curing vacuum coating, finish paint, wherein consisting of of priming paint: two sense aliphatic urethane acrylate 8wt%, epoxy acrylate 30wt%, trifunctional acrylate 10wt%, two functional acrylate 10wt%, sticking power promote resin 8wt%, light trigger 1～5wt%, thinner 20～60wt%, auxiliary agent 0.01～1wt%; Finish paint consists of: high official's energy aliphatic urethane acrylate 18wt%, macromolecular resin 28wt%, two sense aliphatic urethane acrylate 10wt%, trifunctional aliphatic urethane acrylate 11wt%, sticking power promote resin 4wt%, light trigger 1～5wt%, thinner 20～60wt%, auxiliary agent 0.01～1wt%, wherein sticking power promotes that resin is that ethylene-vinyl acetate copolymer, light trigger are that phenyl-phosphonite diethyl ester, thinner are hexanediyl esters, adds usual auxiliaries.
At the bottom of the ultraviolet light polymerization UV vacuum plating with above-mentioned prescription, the shell of digital electronic goods such as mobile phone of handling of finish paint and vacuum plating PVD complete sets of Techniques, MP3, digital camera has the following advantages:
1, the strong adhesion between coating and the metallic diaphragm;
2, environmental testing excellent performance has passed through tests such as salt spray resistance, water boiling resistance, hot and humid, cold cycling, and coating is excellent;
3, excellent abrasive, the wear-resisting test of RCA reaches more than 500 times, and the surface does not have wearing and tearing.
Claims (4)
1, at the bottom of a kind of ultraviolet-curing vacuum coating, finish paint:
Priming paint promotes resin, light trigger, thinner, any proportioning of auxiliary agent to form by two sense aliphatic urethane acrylates, epoxy acrylate, trifunctional acrylate, two functional acrylates, sticking power;
Finish paint promotes resin, light trigger, thinner, any proportioning of auxiliary agent to form by high official's energy aliphatic urethane acrylate, macromolecular resin, two sense aliphatic urethane acrylates, trifunctional aliphatic urethane acrylate, sticking power.
2, at the bottom of the ultraviolet-curing vacuum coating as claimed in claim 1, finish paint, it is characterized in that consisting of of priming paint: two sense aliphatic urethane acrylates, 5～30wt%, epoxy acrylate 10～40wt%, trifunctional acrylate 5～25wt%, two functional acrylates, 5～25wt%, sticking power promote resin 5～10wt%, light trigger 1～5wt%, thinner 20～60wt%, auxiliary agent 0.01～1wt%.
3, at the bottom of the ultraviolet-curing vacuum coating as claimed in claim 2, finish paint, it is characterized in that finish paint consists of: high official can aliphatic urethane acrylate 5～20wt%, macromolecular resin 10～30wt%, two sense aliphatic urethane acrylates, 5～20wt%, trifunctional aliphatic urethane acrylate 10～20wt%, sticking power promote resin 1～5wt%, light trigger 1～5wt%, thinner 20～60wt%, auxiliary agent 0.01～1wt%.
4, at the bottom of the ultraviolet-curing vacuum coating as claimed in claim 3, finish paint, it is characterized in that described sticking power promotes that resin is one or both in ethylene-vinyl acetate copolymer, propylene-acetate ethylene copolymer, the phenoxy group dimethyl-silicon hydride compounds;
Described light trigger is one or more in phenyl-phosphonite diethyl ester, benzophenone, α monohydroxy isopropyl benzene ketone, the α monohydroxy phenylcyclohexane ketone;
Described thinner is one or more in hexanediyl ester, neopentyl glycol diacrylate enzyme, the Viscoat 295.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 200810027249 CN101250339B (en) | 2008-04-03 | 2008-04-03 | Ultraviolet light curing vacuum coating foundation and finish |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 200810027249 CN101250339B (en) | 2008-04-03 | 2008-04-03 | Ultraviolet light curing vacuum coating foundation and finish |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN101250339A true CN101250339A (en) | 2008-08-27 |
| CN101250339B CN101250339B (en) | 2010-09-08 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 200810027249 Expired - Fee Related CN101250339B (en) | 2008-04-03 | 2008-04-03 | Ultraviolet light curing vacuum coating foundation and finish |
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| CN (1) | CN101250339B (en) |
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| CN102086317A (en) * | 2011-01-18 | 2011-06-08 | 惠州市长润发涂料有限公司 | Vacuum plating and ultraviolet curing coating for mobile phone |
| CN102140307A (en) * | 2011-05-11 | 2011-08-03 | 湖南松井新材料有限公司 | Ultraviolet-cured paint |
| CN102206463A (en) * | 2010-03-31 | 2011-10-05 | 东莞市佩琦涂料有限公司 | Vacuum plating UV cured primer |
| CN102863893A (en) * | 2012-09-10 | 2013-01-09 | 湖南松井新材料有限公司 | Ultraviolet curing paint |
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Address after: 516221 No. 30, Petrochemical Road, Huizhou, Dayawan, Guangdong Patentee after: Huizhou Changrunfa Coating Co., Ltd. Address before: 516221 Xintang Industrial Zone, Huizhou Town, Huiyang District, Guangdong, China Patentee before: Huizhou Changrunfa Coating Co., Ltd. |
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