CN109953297B - Preparation method of whole dried lemon and lemon dried orange peel - Google Patents
Preparation method of whole dried lemon and lemon dried orange peel Download PDFInfo
- Publication number
- CN109953297B CN109953297B CN201910347634.7A CN201910347634A CN109953297B CN 109953297 B CN109953297 B CN 109953297B CN 201910347634 A CN201910347634 A CN 201910347634A CN 109953297 B CN109953297 B CN 109953297B
- Authority
- CN
- China
- Prior art keywords
- lemon
- dried
- fruits
- whole
- fruit
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- 235000005979 Citrus limon Nutrition 0.000 title claims abstract description 215
- 238000002360 preparation method Methods 0.000 title claims abstract description 19
- 244000248349 Citrus limon Species 0.000 title abstract 8
- 235000013399 edible fruits Nutrition 0.000 claims abstract description 148
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 76
- 238000007605 air drying Methods 0.000 claims abstract description 53
- 238000002791 soaking Methods 0.000 claims abstract description 25
- 230000002950 deficient Effects 0.000 claims abstract description 23
- 102000004190 Enzymes Human genes 0.000 claims abstract description 21
- 108090000790 Enzymes Proteins 0.000 claims abstract description 21
- 238000001035 drying Methods 0.000 claims abstract description 19
- 230000001954 sterilising effect Effects 0.000 claims abstract description 14
- 239000002131 composite material Substances 0.000 claims abstract description 7
- 244000131522 Citrus pyriformis Species 0.000 claims description 207
- 238000000034 method Methods 0.000 claims description 25
- 235000011389 fruit/vegetable juice Nutrition 0.000 claims description 24
- 239000008223 sterile water Substances 0.000 claims description 23
- 229940088598 enzyme Drugs 0.000 claims description 19
- 108010014251 Muramidase Proteins 0.000 claims description 17
- 102000016943 Muramidase Human genes 0.000 claims description 17
- 108010062010 N-Acetylmuramoyl-L-alanine Amidase Proteins 0.000 claims description 17
- 229960000274 lysozyme Drugs 0.000 claims description 17
- 235000010335 lysozyme Nutrition 0.000 claims description 17
- 239000004325 lysozyme Substances 0.000 claims description 17
- 230000008569 process Effects 0.000 claims description 16
- 235000011869 dried fruits Nutrition 0.000 claims description 13
- 244000131360 Morinda citrifolia Species 0.000 claims description 11
- 235000017524 noni Nutrition 0.000 claims description 11
- 239000002245 particle Substances 0.000 claims description 11
- 150000001875 compounds Chemical class 0.000 claims description 10
- 238000004659 sterilization and disinfection Methods 0.000 claims description 9
- 238000002156 mixing Methods 0.000 claims description 8
- 238000003756 stirring Methods 0.000 claims description 8
- ZCYVEMRRCGMTRW-UHFFFAOYSA-N 7553-56-2 Chemical compound [I] ZCYVEMRRCGMTRW-UHFFFAOYSA-N 0.000 claims description 7
- 239000011630 iodine Substances 0.000 claims description 7
- 229910052740 iodine Inorganic materials 0.000 claims description 7
- 150000003839 salts Chemical class 0.000 claims description 7
- 241000219469 Nyctaginaceae Species 0.000 claims description 6
- 238000001816 cooling Methods 0.000 claims description 6
- 238000004080 punching Methods 0.000 claims description 6
- 229910003460 diamond Inorganic materials 0.000 claims description 2
- 239000010432 diamond Substances 0.000 claims description 2
- 230000000694 effects Effects 0.000 abstract description 15
- 239000004615 ingredient Substances 0.000 abstract description 5
- 239000000654 additive Substances 0.000 abstract description 3
- 235000016709 nutrition Nutrition 0.000 abstract description 3
- 238000011160 research Methods 0.000 abstract description 2
- 230000000052 comparative effect Effects 0.000 description 22
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 18
- 238000000855 fermentation Methods 0.000 description 14
- 239000000796 flavoring agent Substances 0.000 description 14
- 235000019634 flavors Nutrition 0.000 description 14
- 239000003205 fragrance Substances 0.000 description 14
- 241000207199 Citrus Species 0.000 description 12
- 235000020971 citrus fruits Nutrition 0.000 description 12
- 230000004151 fermentation Effects 0.000 description 12
- 241001122767 Theaceae Species 0.000 description 10
- 239000003921 oil Substances 0.000 description 10
- 230000008859 change Effects 0.000 description 9
- 239000000843 powder Substances 0.000 description 9
- 244000179886 Moringa oleifera Species 0.000 description 8
- 235000011347 Moringa oleifera Nutrition 0.000 description 8
- 235000021022 fresh fruits Nutrition 0.000 description 8
- 238000012545 processing Methods 0.000 description 8
- 210000003491 skin Anatomy 0.000 description 8
- 238000003860 storage Methods 0.000 description 8
- 241000894006 Bacteria Species 0.000 description 7
- 238000006243 chemical reaction Methods 0.000 description 7
- 238000005516 engineering process Methods 0.000 description 6
- 206010033546 Pallor Diseases 0.000 description 5
- 210000002615 epidermis Anatomy 0.000 description 5
- 239000007788 liquid Substances 0.000 description 5
- 239000002932 luster Substances 0.000 description 5
- 235000017166 Bambusa arundinacea Nutrition 0.000 description 4
- 235000017491 Bambusa tulda Nutrition 0.000 description 4
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 4
- 244000082204 Phyllostachys viridis Species 0.000 description 4
- 235000015334 Phyllostachys viridis Nutrition 0.000 description 4
- 239000011425 bamboo Substances 0.000 description 4
- 239000011449 brick Substances 0.000 description 4
- 230000006870 function Effects 0.000 description 4
- 235000015097 nutrients Nutrition 0.000 description 4
- 230000036961 partial effect Effects 0.000 description 4
- 238000007514 turning Methods 0.000 description 4
- 241000675108 Citrus tangerina Species 0.000 description 3
- 240000004808 Saccharomyces cerevisiae Species 0.000 description 3
- 230000009471 action Effects 0.000 description 3
- 239000003963 antioxidant agent Substances 0.000 description 3
- 230000003078 antioxidant effect Effects 0.000 description 3
- 230000004071 biological effect Effects 0.000 description 3
- 239000000428 dust Substances 0.000 description 3
- 238000001914 filtration Methods 0.000 description 3
- 235000015203 fruit juice Nutrition 0.000 description 3
- 238000003306 harvesting Methods 0.000 description 3
- 230000001788 irregular Effects 0.000 description 3
- 239000000575 pesticide Substances 0.000 description 3
- 230000001681 protective effect Effects 0.000 description 3
- 239000002994 raw material Substances 0.000 description 3
- 230000002829 reductive effect Effects 0.000 description 3
- 239000002689 soil Substances 0.000 description 3
- 238000009423 ventilation Methods 0.000 description 3
- 206010011732 Cyst Diseases 0.000 description 2
- 241000255925 Diptera Species 0.000 description 2
- 206010020649 Hyperkeratosis Diseases 0.000 description 2
- 206010039792 Seborrhoea Diseases 0.000 description 2
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 2
- 206010052428 Wound Diseases 0.000 description 2
- 208000027418 Wounds and injury Diseases 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- 206010000496 acne Diseases 0.000 description 2
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 2
- 230000004888 barrier function Effects 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 2
- 230000008901 benefit Effects 0.000 description 2
- 238000009835 boiling Methods 0.000 description 2
- 229940041514 candida albicans extract Drugs 0.000 description 2
- 208000031513 cyst Diseases 0.000 description 2
- 230000029087 digestion Effects 0.000 description 2
- 238000003912 environmental pollution Methods 0.000 description 2
- 239000004744 fabric Substances 0.000 description 2
- OVBPIULPVIDEAO-LBPRGKRZSA-N folic acid Chemical compound C=1N=C2NC(N)=NC(=O)C2=NC=1CNC1=CC=C(C(=O)N[C@@H](CCC(O)=O)C(O)=O)C=C1 OVBPIULPVIDEAO-LBPRGKRZSA-N 0.000 description 2
- 239000011521 glass Substances 0.000 description 2
- 229910052742 iron Inorganic materials 0.000 description 2
- 238000002386 leaching Methods 0.000 description 2
- XMGQYMWWDOXHJM-UHFFFAOYSA-N limonene Chemical compound CC(=C)C1CCC(C)=CC1 XMGQYMWWDOXHJM-UHFFFAOYSA-N 0.000 description 2
- 230000014759 maintenance of location Effects 0.000 description 2
- 229910052760 oxygen Inorganic materials 0.000 description 2
- 239000001301 oxygen Substances 0.000 description 2
- 230000020477 pH reduction Effects 0.000 description 2
- 208000008742 seborrheic dermatitis Diseases 0.000 description 2
- 239000011780 sodium chloride Substances 0.000 description 2
- 229910001220 stainless steel Inorganic materials 0.000 description 2
- 239000010935 stainless steel Substances 0.000 description 2
- 239000004575 stone Substances 0.000 description 2
- 230000036561 sun exposure Effects 0.000 description 2
- 210000001519 tissue Anatomy 0.000 description 2
- 238000001291 vacuum drying Methods 0.000 description 2
- 239000000341 volatile oil Substances 0.000 description 2
- 238000005406 washing Methods 0.000 description 2
- 239000012138 yeast extract Substances 0.000 description 2
- WVXRAFOPTSTNLL-NKWVEPMBSA-N 2',3'-dideoxyadenosine Chemical compound C1=NC=2C(N)=NC=NC=2N1[C@H]1CC[C@@H](CO)O1 WVXRAFOPTSTNLL-NKWVEPMBSA-N 0.000 description 1
- 206010000234 Abortion spontaneous Diseases 0.000 description 1
- 241000167854 Bourreria succulenta Species 0.000 description 1
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
- BHPQYMZQTOCNFJ-UHFFFAOYSA-N Calcium cation Chemical compound [Ca+2] BHPQYMZQTOCNFJ-UHFFFAOYSA-N 0.000 description 1
- 208000024172 Cardiovascular disease Diseases 0.000 description 1
- 241000931705 Cicada Species 0.000 description 1
- WTEVQBCEXWBHNA-UHFFFAOYSA-N Citral Natural products CC(C)=CCCC(C)=CC=O WTEVQBCEXWBHNA-UHFFFAOYSA-N 0.000 description 1
- 235000009088 Citrus pyriformis Nutrition 0.000 description 1
- 206010011224 Cough Diseases 0.000 description 1
- 235000009917 Crataegus X brevipes Nutrition 0.000 description 1
- 235000013204 Crataegus X haemacarpa Nutrition 0.000 description 1
- 235000009685 Crataegus X maligna Nutrition 0.000 description 1
- 235000009444 Crataegus X rubrocarnea Nutrition 0.000 description 1
- 235000009486 Crataegus bullatus Nutrition 0.000 description 1
- 235000017181 Crataegus chrysocarpa Nutrition 0.000 description 1
- 235000009682 Crataegus limnophila Nutrition 0.000 description 1
- 240000000171 Crataegus monogyna Species 0.000 description 1
- 235000004423 Crataegus monogyna Nutrition 0.000 description 1
- 235000002313 Crataegus paludosa Nutrition 0.000 description 1
- 235000009840 Crataegus x incaedua Nutrition 0.000 description 1
- 206010013954 Dysphoria Diseases 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 206010019345 Heat stroke Diseases 0.000 description 1
- 244000157072 Hylocereus undatus Species 0.000 description 1
- 235000018481 Hylocereus undatus Nutrition 0.000 description 1
- 206010020772 Hypertension Diseases 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- 206010062717 Increased upper airway secretion Diseases 0.000 description 1
- 208000000913 Kidney Calculi Diseases 0.000 description 1
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 1
- 240000003394 Malpighia glabra Species 0.000 description 1
- 235000014837 Malpighia glabra Nutrition 0.000 description 1
- 240000000249 Morus alba Species 0.000 description 1
- 235000008708 Morus alba Nutrition 0.000 description 1
- OVBPIULPVIDEAO-UHFFFAOYSA-N N-Pteroyl-L-glutaminsaeure Natural products C=1N=C2NC(N)=NC(=O)C2=NC=1CNC1=CC=C(C(=O)NC(CCC(O)=O)C(O)=O)C=C1 OVBPIULPVIDEAO-UHFFFAOYSA-N 0.000 description 1
- 240000002853 Nelumbo nucifera Species 0.000 description 1
- 235000006508 Nelumbo nucifera Nutrition 0.000 description 1
- 235000006510 Nelumbo pentapetala Nutrition 0.000 description 1
- 206010028980 Neoplasm Diseases 0.000 description 1
- 206010029148 Nephrolithiasis Diseases 0.000 description 1
- 244000288157 Passiflora edulis Species 0.000 description 1
- 235000000370 Passiflora edulis Nutrition 0.000 description 1
- 201000005702 Pertussis Diseases 0.000 description 1
- 244000046052 Phaseolus vulgaris Species 0.000 description 1
- 235000010627 Phaseolus vulgaris Nutrition 0.000 description 1
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 1
- 206010034972 Photosensitivity reaction Diseases 0.000 description 1
- 108010059820 Polygalacturonase Proteins 0.000 description 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 1
- 241000220317 Rosa Species 0.000 description 1
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 1
- LEHOTFFKMJEONL-UHFFFAOYSA-N Uric Acid Chemical compound N1C(=O)NC(=O)C2=C1NC(=O)N2 LEHOTFFKMJEONL-UHFFFAOYSA-N 0.000 description 1
- TVWHNULVHGKJHS-UHFFFAOYSA-N Uric acid Natural products N1C(=O)NC(=O)C2NC(=O)NC21 TVWHNULVHGKJHS-UHFFFAOYSA-N 0.000 description 1
- TVXBFESIOXBWNM-UHFFFAOYSA-N Xylitol Natural products OCCC(O)C(O)C(O)CCO TVXBFESIOXBWNM-UHFFFAOYSA-N 0.000 description 1
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 1
- 230000006578 abscission Effects 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- 230000003213 activating effect Effects 0.000 description 1
- 239000004480 active ingredient Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 238000010564 aerobic fermentation Methods 0.000 description 1
- 230000002776 aggregation Effects 0.000 description 1
- 238000004220 aggregation Methods 0.000 description 1
- 230000003064 anti-oxidating effect Effects 0.000 description 1
- 230000036528 appetite Effects 0.000 description 1
- 235000019789 appetite Nutrition 0.000 description 1
- 239000011324 bead Substances 0.000 description 1
- 125000000499 benzofuranyl group Chemical class O1C(=CC2=C1C=CC=C2)* 0.000 description 1
- 235000013361 beverage Nutrition 0.000 description 1
- 230000000975 bioactive effect Effects 0.000 description 1
- 239000008280 blood Substances 0.000 description 1
- 210000004369 blood Anatomy 0.000 description 1
- 230000023555 blood coagulation Effects 0.000 description 1
- 210000001124 body fluid Anatomy 0.000 description 1
- 239000010839 body fluid Substances 0.000 description 1
- 206010006451 bronchitis Diseases 0.000 description 1
- 239000011575 calcium Substances 0.000 description 1
- 229910052791 calcium Inorganic materials 0.000 description 1
- 229910001424 calcium ion Inorganic materials 0.000 description 1
- 150000001720 carbohydrates Chemical class 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 239000000919 ceramic Substances 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 235000019693 cherries Nutrition 0.000 description 1
- 229940043350 citral Drugs 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 239000000571 coke Substances 0.000 description 1
- 235000009508 confectionery Nutrition 0.000 description 1
- 230000008602 contraction Effects 0.000 description 1
- 125000000332 coumarinyl group Chemical class O1C(=O)C(=CC2=CC=CC=C12)* 0.000 description 1
- 206010061428 decreased appetite Diseases 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 230000018109 developmental process Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 235000013325 dietary fiber Nutrition 0.000 description 1
- 238000007599 discharging Methods 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 230000003203 everyday effect Effects 0.000 description 1
- 108010093305 exopolygalacturonase Proteins 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 238000011049 filling Methods 0.000 description 1
- 229960000304 folic acid Drugs 0.000 description 1
- 235000019152 folic acid Nutrition 0.000 description 1
- 239000011724 folic acid Substances 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 235000013373 food additive Nutrition 0.000 description 1
- 239000002778 food additive Substances 0.000 description 1
- 235000011194 food seasoning agent Nutrition 0.000 description 1
- 230000002538 fungal effect Effects 0.000 description 1
- WTEVQBCEXWBHNA-JXMROGBWSA-N geranial Chemical compound CC(C)=CCC\C(C)=C\C=O WTEVQBCEXWBHNA-JXMROGBWSA-N 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- 235000020627 health maintaining nutrition Nutrition 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 238000009775 high-speed stirring Methods 0.000 description 1
- 238000007654 immersion Methods 0.000 description 1
- 230000003116 impacting effect Effects 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 230000000415 inactivating effect Effects 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 239000011229 interlayer Substances 0.000 description 1
- 230000002147 killing effect Effects 0.000 description 1
- 239000010410 layer Substances 0.000 description 1
- 230000000670 limiting effect Effects 0.000 description 1
- 229940087305 limonene Drugs 0.000 description 1
- 235000001510 limonene Nutrition 0.000 description 1
- 150000002629 limonins Chemical class 0.000 description 1
- 239000011777 magnesium Substances 0.000 description 1
- 229910052749 magnesium Inorganic materials 0.000 description 1
- 230000007721 medicinal effect Effects 0.000 description 1
- HEBKCHPVOIAQTA-UHFFFAOYSA-N meso ribitol Natural products OCC(O)C(O)C(O)CO HEBKCHPVOIAQTA-UHFFFAOYSA-N 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 208000015994 miscarriage Diseases 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 208000010125 myocardial infarction Diseases 0.000 description 1
- 210000000056 organ Anatomy 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 230000000149 penetrating effect Effects 0.000 description 1
- 208000026435 phlegm Diseases 0.000 description 1
- 239000011574 phosphorus Substances 0.000 description 1
- 229910052698 phosphorus Inorganic materials 0.000 description 1
- 239000011591 potassium Substances 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- 230000002265 prevention Effects 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 230000006798 recombination Effects 0.000 description 1
- 238000005215 recombination Methods 0.000 description 1
- 230000005070 ripening Effects 0.000 description 1
- 210000003296 saliva Anatomy 0.000 description 1
- 150000004671 saturated fatty acids Chemical class 0.000 description 1
- 230000028327 secretion Effects 0.000 description 1
- 238000007873 sieving Methods 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 208000000995 spontaneous abortion Diseases 0.000 description 1
- 230000000638 stimulation Effects 0.000 description 1
- 210000002784 stomach Anatomy 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000011593 sulfur Substances 0.000 description 1
- 229910052717 sulfur Inorganic materials 0.000 description 1
- 229920002994 synthetic fiber Polymers 0.000 description 1
- 229940116411 terpineol Drugs 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 238000000108 ultra-filtration Methods 0.000 description 1
- 229940116269 uric acid Drugs 0.000 description 1
- 238000012795 verification Methods 0.000 description 1
- 235000013343 vitamin Nutrition 0.000 description 1
- 239000011782 vitamin Substances 0.000 description 1
- 229940088594 vitamin Drugs 0.000 description 1
- 229930003231 vitamin Natural products 0.000 description 1
- 150000003722 vitamin derivatives Chemical class 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
- 239000002023 wood Substances 0.000 description 1
- 239000003357 wound healing promoting agent Substances 0.000 description 1
- 239000000811 xylitol Substances 0.000 description 1
- HEBKCHPVOIAQTA-SCDXWVJYSA-N xylitol Chemical compound OC[C@H](O)[C@@H](O)[C@H](O)CO HEBKCHPVOIAQTA-SCDXWVJYSA-N 0.000 description 1
- 229960002675 xylitol Drugs 0.000 description 1
- 235000010447 xylitol Nutrition 0.000 description 1
- 239000011701 zinc Substances 0.000 description 1
- 229910052725 zinc Inorganic materials 0.000 description 1
Images
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23B—PRESERVING, e.g. BY CANNING, MEAT, FISH, EGGS, FRUIT, VEGETABLES, EDIBLE SEEDS; CHEMICAL RIPENING OF FRUIT OR VEGETABLES; THE PRESERVED, RIPENED, OR CANNED PRODUCTS
- A23B7/00—Preservation or chemical ripening of fruit or vegetables
- A23B7/14—Preserving or ripening with chemicals not covered by groups A23B7/08 or A23B7/10
- A23B7/153—Preserving or ripening with chemicals not covered by groups A23B7/08 or A23B7/10 in the form of liquids or solids
- A23B7/154—Organic compounds; Microorganisms; Enzymes
- A23B7/155—Microorganisms; Enzymes; Antibiotics
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23B—PRESERVING, e.g. BY CANNING, MEAT, FISH, EGGS, FRUIT, VEGETABLES, EDIBLE SEEDS; CHEMICAL RIPENING OF FRUIT OR VEGETABLES; THE PRESERVED, RIPENED, OR CANNED PRODUCTS
- A23B7/00—Preservation or chemical ripening of fruit or vegetables
- A23B7/16—Coating with a protective layer; Compositions or apparatus therefor
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L19/00—Products from fruits or vegetables; Preparation or treatment thereof
- A23L19/03—Products from fruits or vegetables; Preparation or treatment thereof consisting of whole pieces or fragments without mashing the original pieces
- A23L19/05—Stuffed or cored products; Multilayered or coated products; Binding or compressing of original pieces
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L5/00—Preparation or treatment of foods or foodstuffs, in general; Food or foodstuffs obtained thereby; Materials therefor
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L5/00—Preparation or treatment of foods or foodstuffs, in general; Food or foodstuffs obtained thereby; Materials therefor
- A23L5/40—Colouring or decolouring of foods
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L5/00—Preparation or treatment of foods or foodstuffs, in general; Food or foodstuffs obtained thereby; Materials therefor
- A23L5/40—Colouring or decolouring of foods
- A23L5/41—Retaining or modifying natural colour by use of additives, e.g. optical brighteners
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L5/00—Preparation or treatment of foods or foodstuffs, in general; Food or foodstuffs obtained thereby; Materials therefor
- A23L5/57—Chemical peeling or cleaning of harvested fruits, vegetables or other foodstuffs
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/75—Rutaceae (Rue family)
- A61K36/752—Citrus, e.g. lime, orange or lemon
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/10—Preparation or pretreatment of starting material
- A61K2236/19—Preparation or pretreatment of starting material involving fermentation using yeast, bacteria or both; enzymatic treatment
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Polymers & Plastics (AREA)
- Food Science & Technology (AREA)
- Nutrition Science (AREA)
- Natural Medicines & Medicinal Plants (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Zoology (AREA)
- Wood Science & Technology (AREA)
- General Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medical Informatics (AREA)
- Biotechnology (AREA)
- Botany (AREA)
- Alternative & Traditional Medicine (AREA)
- Medicinal Chemistry (AREA)
- Pharmacology & Pharmacy (AREA)
- Epidemiology (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Preparation Of Fruits And Vegetables (AREA)
Abstract
The invention discloses a preparation method of whole dried lemon fruits and dried lemon peels, which comprises the following steps: (1) sterilizing with cold water, namely sterilizing with sterile cold water; (2) soaking the composite enzyme to fade the composite enzyme into uniform color; (3) pricking holes to fully evaporate water; (4) and (5) air drying, color protection and drying. The dried whole lemon is prepared and is utilized to prepare the dried orange peel, the research on preparing the dried orange peel from the lemon is unique, defective fruits are fully utilized, the preparation method is simple and easy to operate, the color is naturally protected without adding additives such as color protection and the like, the dried orange peel is prepared according to the characteristics of the whole lemon, the medicinal value of the dried orange peel is better exerted, the nutritional ingredients are higher, the activity of the lemon ingredients is maintained, and the color of the dried orange peel can be basically uniform and unified.
Description
Technical Field
The invention relates to the technical field of food processing, in particular to a preparation method of whole dried lemon fruits and lemon dried orange peels.
Background
The lemon is a fruit which is recognized in the world and has extremely high healthy nutrition and medicinal value, and has the effects of reducing phlegm and relieving cough, promoting the secretion of saliva or body fluid and invigorating stomach, and is used for treating bronchitis, pertussis, inappetence, miscarriage prevention of pregnant women, qi circulation promotion due to stasis removal, and heatstroke dysphoria. With the development of science and technology, experiments of deeply researching the activities of various functional components of the lemon show that the lemon has the effects of reducing blood fat, reducing uric acid, resisting oxidation and cancers, can prevent cardiovascular diseases, can reduce the concentration of calcium ions to promote blood coagulation, prevent and treat hypertension and myocardial infarction, prevent renal calculus and the like.
In recent years, the lemon industry in China develops rapidly, farmers can especially create industry without leaving the country, but because fresh fruits are mainly concentrated on 8-12 months to come into the market, the supply is greater than the demand, the lemon begins to change color after picking within three and five days, and the stock condition and the stock cost are high, so that a plurality of fruit growers cannot bear the lemon, only can pick the lemon by a large amount, rot the lemon in fruit lands at will, and discard the lemon after being sold and rotten, so that the lemon causes environmental pollution once, the fruit growers do not harvest abundantly, the economic benefit is reduced, especially in the harvest season, even if fruits are stored, pedicel abscission can be caused to cause fungal rotting, and a plurality of inferior fruits cannot be used in the field, so that the inferior fruits are used without time, are discarded unfortunately, bring pollution and worries, do not hurt farmers at all, but need lemons in the whole market, therefore, only slices are sold in the existing lemon processing process, and high-temperature baking is mostly adopted in the process. In order to improve the appearance and color, food additives or sulfur is used for fumigating, baking and protecting color, so that potential safety hazards are brought, even if a vacuum drying technology is used, the vacuum drying technology is difficult to become a mainstream processing technology due to large one-time investment, high operation cost and small yield, and is irretrievable, and the prior art rarely focuses on researching feasible processes of whole lemons and dried orange peels.
The preparation method of the whole dried lemon and the lemon dried orange peel has the following advantages: first, the whole fruit is utilized, the original nutrient components and main functional components are kept to the maximum extent, and the functional effect is played on the edible and medicinal effects. Secondly, the operation is simple and convenient, fruit growers can automatically perform primary processing, do not worry about high yield and poor harvest in a busy season, and do not discard secondary waste fruits to cause environmental pollution. And thirdly, the lemon and dried orange peel provide raw materials of the original ecological original taste and no additive for the pharmaceutical industry, so that the use value of the lemon is improved and the use range is enlarged. And fourthly, the planting cost is reduced, the processing cost is also reduced, the enthusiasm of fruit growers for expanding seeds is stimulated, and the market competitiveness of processing enterprises is improved. Five, one industry is prosperous, and brings other industrial effects, such as bamboo industry, cloth industry, pharmaceutical industry, tea industry, seasoning industry and craftsman industry.
Disclosure of Invention
In view of the above, the present invention provides a method for preparing whole dried lemon fruits and dried lemon peels, which solves the above problems.
The technical means adopted by the invention are as follows: a preparation method of whole lemon dried fruits comprises the following steps:
(1) cold water sterilization: rinsing lemon fruits by using sterile cold water, fishing out and draining, soaking the lemon fruits in the sterile cold water added with lysozyme, and selecting good fruits and defective fruits;
(2) soaking with composite enzyme: crushing the defective fruits sterilized by cold water into particles, adding non-iodine edible salt, stirring, adding sterile water, decocting to obtain juice, and cooling to obtain lemon juice for later use;
taking the components in a weight ratio of 45-55: 35-45: 5-15, mixing the noni compound enzyme, sterile water and lemon juice for soaking the fruits;
(3) hole punching: pricking 3-5 cm of pulp from the top end of the fruit base of the lemon by using a diamond cone tool;
(4) air drying: and (3) placing the lemon fruits on an air drying frame for airing in a ventilating way, adopting a black cover to cover the air drying frame when the moisture content is 5-10%, and airing to obtain the whole lemon dried fruits.
Further, in the step (1), the temperature of the sterile cold water is 20-25 ℃.
Further, in the step (1), the weight of the lysozyme added is 0.05-0.07% of the weight of the sterile cold water, and the lysozyme is soaked for 35-45 min.
Further, in the step (2), 3-5% of non-iodine edible salt is added according to the weight ratio and stirred.
Further, in the step (2), the weight ratio of the defective fruit particles to the added sterile water is 1: 5 to 7.
Further, in the step (2), the soaking time is 15-40 d.
Further, in the step (4), the lemon fruits are turned up and down every 5-7 days.
Further, in the step (4), the time of the air drying process is 40-50 d.
Further, in the step (4), the airing is carried out by placing the aired frame under the sun for airing for 50-70 min before ten o 'clock in the morning or after four o' clock in the afternoon, and then moving the aired frame into a room with the temperature of 25-27 ℃.
The invention also discloses a preparation method of the dried lemon peel, which is characterized in that the dried whole lemon fruit prepared by the preparation method of the dried whole lemon fruit according to any one of claims 1 to 9 is subjected to full-covering stewing and baking to obtain the dried lemon peel;
wherein, the braising and baking are fully covered: and (3) completely covering the air drying rack by using a black cover, airing, and drying by using hot air until the surface color of the lemon fruit is uniform, thus obtaining the lemon dried orange peel.
Compared with the prior art, the invention has the beneficial effects that: 1. the lemon fruit is cleaned and soaked by low-temperature sterile water, and because the lemon peel contains lemon essential oil, citral, a small amount of citronellac acid-terpineol and the like, the lemon peel is dissolved in boiling water, the peel browning and the loss of functional components can be caused by adopting blanching processes such as boiling water and the like, the lemon color is blackened by sterilizing and inactivating enzymes at high temperature, and the pulp is blackened along with the browning, so that the use and edible value are lost. The functional components of the lemon can be kept and epidermal oil cells and cell tissues are not damaged by adopting cold water washing and soaking at a lower temperature, the lysozyme added can keep freshness and prevent rotting, and bacteria on the surface of the lemon can be removed and the regrowth of the bacteria can be inhibited. 2. The compound ferment is used for soaking, firstly, the color and luster can be unified, and the color skin on the surface of the lemon after soaking is faded to become light yellow; secondly, an anti-oxidation protective film can be formed, color protection and color retention measures are not required to be added, the film can be placed under common conditions, and the color cannot be changed; thirdly, the fruit wound healing agent has certain repairing effect on the calluses, the wound is prevented from being rotten, and fourthly, when the water is evaporated, the epidermis is orderly evaporated and contracted, and irregular pimples cannot appear. 3. The thick peel of lemon fruit is adhered to the pulp, the pulp sacs are tightly wrapped with the pulp juice, the moisture of the lemon fruit cannot be completely squeezed out in the subsequent air drying process, the oil content of the peel is high, oil and water are difficult to dissolve, the barrier property exists, the fruit base is originally a conveying pipeline for introducing nutrients, the nutrients wither after the fruit is picked up and the moisture of the pulp is contracted and extruded by the peel, and the pulp can be externally penetrated and evaporated from the hole. 4. The lemon mainly comprises limonene, limonin compounds, coumarin compounds, citric acid, essential oil and the like as functional components, the coumarone compounds are natural photosensitive components, cannot endure continuous sunshine exposure, generate photosensitive reaction, lose edible and medicinal functions, keep active components, and can ensure the bioactive effect, and mechanical heat drying and continuous sun exposure not only can change the color and luster, but also lose the bioactivity, and cannot achieve the edible effect and medicinal value. The air drying process is the only processing process for keeping the active biological effect and ensuring the color and luster not to generate browning. 5. The stewing ensures that hot air flow is dispersed and recovered, slowly dries the lemon fruit skin and generates color reaction, and promotes the color of the whole fruit to be basically uniform and uniform. The research of the lemon dried orange peel prepared by the invention has uniqueness, natural color protection is realized without adding additives such as color protection and the like, the lemon dried orange peel is prepared into the dried orange peel according to the characteristics of whole lemons, the first whole lemon dried orange peel is named, not only is the lemon dried orange peel harmonious and superior to the efficacy and the function of citrus dried orange peel, but also more importantly, the lemon dried orange peel has more complete and richer functional nutritional ingredients and medicinal value range than the citrus dried orange peel and the maximum reservation of active ingredients, the medicinal value of the lemon dried orange peel is better exerted, the nutritional ingredients are higher, the activity of the lemon ingredients is kept, and the color is basically uniform and unified.
Drawings
In order to more clearly illustrate the technical solutions in the embodiments of the present invention, the drawings used in the description of the embodiments will be briefly introduced below, and it is obvious that the drawings in the following description are only preferred embodiments of the present invention, and it is obvious for those skilled in the art that other drawings can be obtained according to these drawings without inventive exercise.
FIG. 1 is a process flow diagram of the present invention;
FIG. 2 is a drawing of dried whole lemon fruit and slices after air drying in accordance with the present invention;
fig. 3 shows the whole lemon dried orange peel prepared by the invention.
Detailed Description
The principles and features of this invention are described below in conjunction with the following examples, which are set forth to illustrate, but are not to be construed to limit the scope of the invention.
As shown in figures 1-3, per 100g of lemon, the lemon contains the following main nutrients:
5-6 g of citric acid; the total amount of the vitamin ABC group is 53.25 mg, wherein 53 mg of folic acid, 26 mg of calcium, 0.6 mg of iron, 8 mg of magnesium, 16 mg of phosphorus, 138 mg of potassium, 2 mg of sodium, 0.06 mg of zinc, 1.1 g of protein, 0.3 g of total fat, 2.8 g of dietary fiber, 6.25 g of carbohydrate and 0.039 g of saturated fatty acid.
The main functions of lemon are:
example 1
A preparation method of whole lemon dried fruits comprises the following steps:
(1) cold water sterilization: rinsing lemon fruits by using sterile cold water, removing dust soil and dirt on the surfaces of the lemon fruits, removing residual pesticides, fishing out and draining, and then soaking the lemon fruits in sterile cold water added with lysozyme for 35min, wherein the weight of the lysozyme is 0.05% of the weight of the sterile cold water, the lysozyme can keep the lemon fruits fresh, can kill bacteria on the surfaces of the lemons and inhibit the regrowth of the lemons, and then selecting good fruits and defective fruits; the temperature of the sterile water was 20 ℃.
(2) Soaking with composite enzyme: crushing partial defective fruits sterilized by cold water into particles, adding 3% of non-iodine edible salt according to the weight ratio, stirring, adding sterile water, decocting and taking juice, wherein the weight ratio of the defective fruit particles to the added sterile water is 1: and 5, cooling to obtain lemon juice for later use.
Taking the components in a weight ratio of 45: 35: 5, mixing the noni compound enzyme, sterile water and lemon juice, and soaking the fruits for 15 days.
(3) Hole punching: the triangular rhombus cone tool is used for pricking 3cm of pulp from the top end of the fruit base of the lemon, and the pulp cannot be pricked thoroughly.
(4) Air drying: placing lemon fruits on an air drying frame for ventilation and air drying, turning the lemon fruits up and down every 5 days, removing the problematic lemon fruits, ensuring that the drying humidity is basically consistent, covering the air drying frame by using a black cover when the moisture residue is 5%, placing the air drying frame under the sun for airing for 50min before ten minutes in the morning or after four and a half in the afternoon, then moving the air drying frame into a room with the temperature of 25 ℃, absorbing the solar heat by using the black cover to form stuffy airflow in the cover, squeezing the residual moisture in the pulp, forcing the oil seborrhea to change the color of the surface of the peel, and continuously draining the final residual moisture from the lemon fruits. The two stages are soft in sunlight, the heat energy absorbed by the air drying rack is not high, the air drying process is carried out for 40 days, the main components of the lemon fruits which are not completely dried are not decomposed, only an external action is formed, the water in the pulp is continuously squeezed to be outwards and is discharged and evaporated, the whole dried lemon fruits are obtained, the dried lemon fruits can be used for storage, the defective fruits can be sliced, and the dried lemon fruits can be ground into powder and the like.
And carrying out full-covering stewing and drying on the whole dried lemon fruits to obtain lemon dried orange peels, wherein the full-covering stewing and drying: completely covering the air drying rack by using a black cover, placing the air drying rack under the sun before ten o 'clock in the morning or after four o' clock in the afternoon for 50min, moving the air drying rack into a room with the temperature of 25 ℃, and drying by using hot air until the surface color of the lemon fruit is uniform, thus obtaining the whole-fruit lemon dried orange peel. The black cover around is easy to absorb heat and also dissipate heat, so that hot air is ensured to be dissipated, the lemon fruit peel is slowly dried and color reaction is generated, and the lemon fruit peel not only has the fragrance of the dried orange peel, but also has sour fragrance.
Example 2
A preparation method of whole lemon dried fruits comprises the following steps:
(1) cold water sterilization: rinsing lemon fruits by using sterile cold water, removing dust soil and dirt on the surfaces of the lemon fruits, removing residual pesticides, fishing out and draining, and then soaking the lemon fruits in sterile cold water added with lysozyme for 45min, wherein the weight of the added lysozyme is 0.07 percent of the weight of the sterile cold water, the added lysozyme can keep the lemon fruits fresh, can kill bacteria on the surfaces of the lemon fruits and inhibit the regrowth of the bacteria, and selects good fruits and defective fruits; the temperature of the sterile water was 25 ℃.
(2) Soaking with composite enzyme: crushing partial defective fruits sterilized by cold water into particles, adding 5% of non-iodine edible salt according to the weight ratio, stirring, adding sterile water, decocting and taking juice, wherein the weight ratio of the defective fruit particles to the added sterile water is 1: and 7, cooling to obtain lemon juice for later use.
Taking the components in a weight ratio of 55: 45: 15, mixing the noni compound enzyme, sterile water and lemon juice, and soaking the fruits for 40 days.
(3) Hole punching: the triangular rhombus cone tool is used for pricking 5cm of pulp from the top end of the fruit base of the lemon, so that the pulp cannot be pricked thoroughly.
(4) Air drying: placing lemon fruits on an air drying frame for ventilation and air drying, turning the lemon fruits up and down every 7 days, removing the problem lemon fruits, ensuring the drying humidity to be basically consistent, when the water content is 10%, covering the air drying frame by using a black cover, placing the air drying frame under the sun for airing for 70min before ten o 'clock in the morning or after four o' clock in the afternoon, then moving the air drying frame into a room with the temperature of 27 ℃, absorbing the solar heat by using the black cover to form stuffy airflow on the inner surface of the cover, squeezing the residual water in the pulp, forcing the oil to flow on the surface of the peel to change color, and continuously discharging the final residual water from the lemon fruits. The two stages are soft in sunlight, the heat energy absorbed by the air drying frame is not high, the time of the air drying process is 50 days, the main components of the lemon fruits which are not completely dried are not affected, only an external action is formed, the water in the pulp is continuously squeezed to be outwards and is discharged and evaporated, the whole dried lemon fruits are obtained, the dried lemon fruits can be used for storage, the defective fruits can be sliced, and the dried lemon fruits can be ground into powder and the like.
And carrying out full-covering stewing and drying on the whole dried lemon fruits to obtain lemon dried orange peels, wherein the full-covering stewing and drying: completely covering the air drying rack by using a black cover, placing the air drying rack under the sun before ten o 'clock in the morning or after four o' clock in the afternoon for 70min, then moving the air drying rack into a room with the temperature of 27 ℃, and drying by using hot air until the surface color of the lemon fruit is uniform, thus obtaining the whole-fruit lemon dried orange peel. The black cover around is easy to absorb heat and also dissipate heat, so that hot air is ensured to be dissipated, the lemon fruit peel is slowly dried and color reaction is generated, and the lemon fruit peel not only has the fragrance of the dried orange peel, but also has sour fragrance.
Example 3
A preparation method of whole lemon dried fruits comprises the following steps:
(1) cold water sterilization: rinsing lemon fruits by using sterile cold water, removing dust soil and dirt on the surfaces of the lemon fruits, removing residual pesticides, fishing out and draining, and then soaking the lemon fruits in sterile cold water added with lysozyme for 40min, wherein the weight of the lysozyme is 0.06% of the weight of the sterile cold water, the lysozyme can keep the lemon fruits fresh, can kill bacteria on the surfaces of the lemons and inhibit the regrowth of the lemons, and then selecting good fruits and defective fruits; the temperature of the sterile water was 22 ℃.
(2) Soaking with composite enzyme: crushing partial defective fruits sterilized by cold water into particles, adding 4% of non-iodine edible salt according to the weight ratio, stirring, adding sterile water, decocting and taking juice, wherein the weight ratio of the defective fruit particles to the added sterile water is 1: and 6, cooling to obtain lemon juice for later use.
Taking the weight ratio of 50: 40: 10, mixing the noni compound enzyme, sterile water and lemon juice, and soaking the fruits for 30 days.
(3) Hole punching: the triangular rhombus cone tool is used for pricking 4cm of pulp from the top end of the fruit base of the lemon, so that the pulp cannot be pricked thoroughly.
(4) Air drying: placing lemon fruits on an air drying frame for ventilation and air drying, turning the lemon fruits up and down every 6 days, removing the problem lemon fruits, ensuring that the drying humidity is basically consistent, covering the air drying frame by using a black cover when the moisture residue is 7%, placing the air drying frame under the sun for airing for 60min before ten minutes in the morning or after four and a half in the afternoon, then moving the air drying frame into a room with the temperature of 26 ℃, absorbing the solar heat by using the black cover to form stuffy airflow in the cover, squeezing the residual moisture in the pulp, forcing the oil seborrhea to change the color of the surface of the peel, and continuously draining the final residual moisture from the lemon fruits. The two stages are soft in sunlight, the heat energy absorbed by the air drying rack is not high, the air drying process is carried out for 45 days, the main components of the lemon fruits which are not completely dried are not decomposed, only an external action is formed, the water in the pulp is continuously squeezed to be outwards and is discharged and evaporated, the whole dried lemon fruits are obtained, the dried lemon fruits can be used for storage, the defective fruits can be sliced, and the dried lemon fruits can be ground into powder and the like.
And carrying out full-covering stewing and drying on the whole dried lemon fruits to obtain lemon dried orange peels, wherein the full-covering stewing and drying: the method comprises the steps of completely covering an air drying frame by using a black cover, airing the air drying frame under the sun for 60min before ten o 'clock in the morning or after four o' clock in the afternoon, then moving the air drying frame into a room with the temperature of 26 ℃, and drying by using hot air until the surface color of lemon fruits is uniform, so that the whole-fruit lemon dried orange peel is prepared, and can be used for storage, slicing defective fruits, powdering and the like. The black cover around is easy to absorb heat and dissipate heat, the black cover is a black cloth bag, hot air is ensured to be dissipated, the lemon fruit skin is dried slowly and color reaction is generated, and the lemon fruit has the fragrance of pericarpium citri reticulatae and also has sour fragrance.
In addition, in the above embodiment, the noni complex enzyme in step (2) is produced by the patent application No. 201810036996, which specifically includes: the preparation method of the noni compound enzyme comprises the following steps:
1. pretreatment of fresh fruit
(1) Preparing fresh fruit
Preparing fermented fresh fruits according to the proportion of 62 parts of noni fruits, 5 parts of passion fruits, 2 parts of acerola cherries, 4 parts of dragon fruits and 14 parts of mulberry fruits.
(2) Sterilization of saline
The fresh fruits were washed in 7 baume sterile saline.
(3) Hot water blanching
Placing the washed fresh fruit in 100 deg.C boiled water for blanching for 5min, and rapidly blanching with binaural stainless steel strainer.
(4) Low-temperature wall-breaking juicing
Adding 1% pectinase into fresh fruit for enzymolysis for 3h, breaking wall by impact at 33 deg.C, i.e. adding high-speed stirrer (2800 rpm) into fermentation tank to break fresh fruit to make fruit grain less than 1mm, breaking wall of plant cell to make the ripening speed faster, extracting activity of various enzymes to be stronger and stronger, filtering to separate fruit juice and fruit residue, adding 0.1% lysozyme for sterilization, and using citric acid regulator pH4.2.
(5) Fermentation of
Adding an air inlet which can not be discharged, fermenting for 60 days by intermittent wall breaking and impacting while adding oxygen, wherein the fermentation temperature is 33 ℃, the fermentation time is 9 months, stirring for 30min at high speed each time for 2 times a day, adding Moringa oleifera tea yeast extract liquid of 4-5 times of the weight of fruit juice, and standing for anaerobic fermentation for 120 days.
2. Dry fruit processing
(1) Preparing 1 part of dried lotus leaves, 1 part of dried tangerine peels, 2 parts of sweet beans, 3 parts of hawthorn fruits, 11 parts of moringa tea leaves and 1 part of rose with multiple petals according to the weight of raw materials.
(2) Sterilizing the dried fruits at 136 deg.C, baking for 0.5min, and killing various bacteria in the dried fruits; using WFJ-15 type ultramicro powder to break the wall and grind the powder into ultramicro powder, and sieving the ultramicro powder with a 320-mesh sieve.
(3) Mixing the sieved dried fruit superfine powder and fruit residues obtained after fruit juice squeezing, and simultaneously adding moringa tea yeast extract with the weight 4 times that of the solid raw material.
Preparing a yeast moringa tea extracting solution:
the moringa oleifera tea comprises the following components in a weight ratio of 1: 2: the proportion of mineral water, decocting the juice for 15h by using an electrothermal ceramic earthen jar with slow fire, extracting the moringa tea liquid, adding 15 wt% of yeast liquid of the moringa tea liquid, carrying out high-speed stirring impact wall breaking treatment for 3h, adding 8 wt% of xylitol, filtering the autolyzed yeast moringa tea liquid by using a centrifugal machine, and standing for aerobic fermentation for 2 h at 25 ℃.
(4) Anaerobic digestion fermentation
Using a stainless steel leaching tank with a sight glass and an air hole which can not be discharged and entered, carrying out anaerobic leaching for 90 days, carrying out ultrafiltration to remove residues, then continuing anaerobic fermentation for 90 days (three months), stirring once at the speed limit of 1200 rpm every 6 days for 30min each time, and aiming at continuously activating the recombination, aggregation and flavor unification of various enzymes, wherein the fermentation liquor is adjusted to be 4.2 at the moment.
3. Mixed fermentation
Mixing the fermentation liquor obtained in the step of oxygen addition fermentation and the fermentation liquor obtained in the step of anaerobic digestion fermentation, putting the mixture in a large fermentation tank with a temperature control port, an air outlet port and a speed-limiting stirrer, fermenting at the rotating speed of 240 r/min for 120 days at 33 ℃, stirring for 1 time and 30min once every day, then standing and fermenting at the temperature of 28 ℃ for 60 days, stopping acidification and enzymolysis, and transferring to a storage tank for after-ripening storage.
4. Filtering, filling in glass, and sterilizing at 100 deg.C for 30 min.
In the above embodiments 1 to 3, in the step (1), the soaking container is a wooden container, such as a wooden barrel or a bamboo barrel, which prevents the citric acid from chemically reacting with the synthetic materials such as the iron container, and the water immersion surface is generally about 20cm higher than the lemon, and the bamboo product is pressed on the lemon surface to sink, so that the stone brick and the fire brick are not used, and the stone brick and the fire brick can be rotten with the fruit citric acid. In the step (2), the color and luster change can occur after soaking: the dark green lemon is faded completely to yellow lemon, the light green lemon is changed to light yellow lemon, and the yellow lemon is changed to lemon with egg yellow color. In the step (4), the air drying frame is made of bamboo or wood, is 3.5m high and 1m wide, is 8-10 cm apart from top to bottom, and comprises a bottom plate and a plurality of flat plates, wherein the bottom plate is provided with pulleys and can move, a fruit hole is dug in the flat plates according to the average size of the lemon, the lemon fruit is vertically placed, the upper part and the lower part are ventilated and drip beads, if the flat plates are designed to be placed horizontally, the single side of the lemon fruit is large in pressed area, the pulp moisture can be poured out while the pulp moisture is poured, the peel is moist and softened, the peel is easy to enter by mosquitoes while being weak, mildew and rot are caused, and 2cm gaps are reserved between the fruits on the flat plates. The defective lemon fruits can be made into tangerine peel powder, the round lemon fruits can be used as tea fruits, the irregular lemon fruits are cut into pieces to be made into preserves, and the applicability is particularly wide. In the preparation method of the lemon dried orange peel, because the lemon is afraid of exposure to heat and light, a full-covering braising and semi-hot air semi-drying process is adopted, so that hot air is ensured to be dispersed and repeated, the lemon fruit peel is slowly dried and color reaction is generated, and uniform color and fragrance are ensured. The obtained whole-fruit lemon pericarpium Citri Tangerinae can be used for medicine.
Comparative example 1
This comparative example differs from example 3 in that the temperature of the sterile cold water in step (1) was 40 ℃.
Comparative example 2
The difference between this comparative example and example 3 is that, in step (2), the complex ferment is soaked: crushing partial defective fruits after cold water sterilization into particles, adding sterile water, decocting and taking juice, wherein the weight ratio of the defective fruit particles to the added sterile water is 1: and 6, cooling to obtain lemon juice for later use.
Taking the weight ratio of 50: 50: 20, mixing the noni compound enzyme, sterile water and lemon juice, and soaking the fruits for 50 days.
Comparative example 3
The difference between the comparative example and the example 3 is that in the step (3), the soaked lemon fruit is directly air-dried without punching, namely: and (3) placing the lemon fruits on an air drying frame for airing in a ventilating way, turning the lemon fruits up and down every 6 days, airing until the residual moisture content is 10-20%, and airing for 45 days to obtain the whole lemon dried fruits.
Comparative example 4
The difference between this comparative example and example 3 is that in the method of preparing dried citrus citri reticulata, the dried citrus limon fruits after air drying are moved to a room with a temperature of 26 ℃ for storage.
Comparative example 5
Selected from citrus peel aged for 2 years on the market.
In order to verify the beneficial effects of the present invention, the following verification tests were performed:
first, identification of appearance quality of lemon dried orange peel
The citrus citri reticulata peels prepared in the examples 1 to 3 and the comparative examples 1 to 5 are taken, observed for appearance quality, and recorded with data as shown in the following table 1:
TABLE 1 identification of lemon appearance quality
Colour(s) | Fragrance | Taste of the product | |
Example 1 | Dark orange-red yellow | Pericarpium Citri Tangerinae flavor and sour flavor | Slightly pungent and bitter |
Example 2 | Brown orange red yellow | Pericarpium Citri Tangerinae flavor and sour flavor | Slightly pungent and bitter |
Example 3 | Brown orange red yellow | Pericarpium Citri Tangerinae flavor and sour flavor | Slightly pungent and bitter |
Comparative example 1 | Dark brown color | The dried orange peel has a weak fragrance | Slightly pungent and bitter |
Comparative example 2 | Dark brown color | The dried orange peel has a weak fragrance | Pungent and bitter |
Comparative example 3 | Dark black color of coke | Pericarpium Citri Tangerinae with weak flavor, scorched flavor, and sour flavor | Pungent and bitter |
Comparative example 4 | Dark brown red | Pericarpium Citri Tangerinae flavor, scorched flavor, and sour flavor | Pungent and bitter |
Comparative example 5 | Brown orange red yellow | Fragrance of dried orange peel | Slightly pungent and bitter |
As can be seen from table 1 above, the appearance quality of the whole-fruit citrus citri reticulata peel prepared by the present invention is better than that of the comparative example. Compared with the comparative example 1, the lemon washing agent is rinsed by using sterile cold water at the temperature of 20-25 ℃ without using high-temperature hot rinsing, because the lemon has functional components and strong biological activity, the functional components are dissolved and lost by heat treatment, further fragrance is lost, the color and luster also become black, the edible and medicinal values are lost, the lemon is provided with a plurality of oil cells and sunken, the oil cells are damaged by hot water blanching, the epidermis is damaged, is bitten by mosquitoes, is rotted, and the functional components can be kept in the cleaning process only by using cold water at the temperature of below 25 ℃ and using lysozyme, so that the epidermis oil cells and cell tissues are not damaged, continuous acidification is prevented, and the sterilization effect is achieved.
Compared with the comparative example 2, the invention utilizes the defective fruit to prepare the lemon juice, the lemon juice is mixed with the noni compound enzyme and sterile water according to a certain weight ratio to soak the lemon good fruit, the layer on the epidermis after the enzyme soaking is as thin as the color skin of the cicada's wing, no matter the color skin is dark green, light green or lemon yellow, the color is uniformly faded, the lemon juice becomes uniform light yellow or yellow, an antioxidant protective film can be formed, color protection and color retention measures are not added, the lemon juice can be placed under general conditions, the color can not change, the callus has certain repairing function, the wound is prevented from being corrupted, the epidermis forms orderly evaporation and contraction when the moisture evaporates, irregular pimples can not appear, the important reason is that the compound noni enzyme with strong antioxidant degree has the penetrating effect on the fruit peel and pulp, the preorder cold treatment sterilizes and retains the original functional components, form a protective barrier between each other.
Compared with the comparative example 3, the puncturing makes the water content of the pulp to be squeezed by the skin to be evaporated from the opening, and the air drying also belongs to a cold treatment, creates an environment for protecting the potential exertion of functional components, squeezes the residual water content in the pulp, forces the oil to flow to the surface of the skin to change the color, and the mechanical heat drying and the continuous sun exposure not only can change the color, but also can lose the biological activity, and can not achieve the edible effect and the medicinal value. Different from orange peel, orange peel is thin and has few tangerine pith, lemon peel is thick and has many cyst pith, a connected interlayer is arranged between peel and cyst, the orange is completely sunned to press water by heat energy, orange peel can be prepared in one step, and the process for twisting the orange is different.
Compared with the comparative example 4, the process of the invention uses the black cover to absorb heat but also dissipate heat, ensures that hot air flow is dissipated again, and semi-hot air semi-drying slowly dries the lemon fruit skin and generates color reaction. This comparative example did not undergo the step of braising, and was inferior in color and flavor to the present invention.
Compared with the comparative example 5, the orange peel prepared by the citrus on the market has similar appearance color, taste and aroma to the invention, and the whole-fruit lemon orange peel prepared by the invention has good effect.
Dried orange peel is a concept, dried fruits are called orange peel after more than one year, and the appearance is red or brownish red and dark red. The lemon dried orange peel prepared by the technology has similar appearance to citrus dried orange peel, the fragrance is more acid fragrance than citrus dried orange peel, the lemon dried orange peel has more stimulation to organs and appetite, the citric acid is alkaline acid, and the storage and conversion effects of antioxidant substances on the peel are enhanced more than acidic citrus. Therefore, the effect and the efficacy of the citrus peel beverage are higher in edible and medicinal values than those of citrus peel, and especially, the whole-fruit lemon peel prepared by the technology keeps the main functional components of the whole-fruit lemon peel completely.
The invention provides a preparation method of whole lemon dried fruit and lemon dried orange peel, which changes the whole lemon into treasure, comprehensively utilizes the whole lemon, and keeps the whole fruit shape.
The above description is only for the purpose of illustrating the preferred embodiments of the present invention and is not to be construed as limiting the invention, and any modifications, equivalents, improvements and the like made within the spirit and principle of the present invention should be included in the scope of the present invention.
Claims (9)
1. A preparation method of whole lemon dried fruits is characterized by comprising the following steps:
(1) cold water sterilization: rinsing lemon fruits by using sterile cold water, fishing out and draining, soaking the lemon fruits in the sterile cold water added with lysozyme, and selecting good fruits and defective fruits; the temperature of the sterile cold water is 20-25 ℃;
(2) soaking with composite enzyme: crushing the defective fruits sterilized by cold water into particles, adding non-iodine edible salt, stirring, adding sterile water, decocting to obtain juice, and cooling to obtain lemon juice for later use;
taking the components in a weight ratio of 45-55: 35-45: 5-15, mixing the noni compound enzyme, sterile water and lemon juice for soaking the fruits;
(3) hole punching: pricking 3-5 cm of pulp from the top end of the fruit base of the lemon by using a diamond cone tool;
(4) air drying: and (3) placing the lemon fruits on an air drying frame for airing in a ventilating way, adopting a black cover to cover the air drying frame when the moisture content is 5-10%, and airing to obtain the whole lemon dried fruits.
2. The method for preparing the dried whole lemon according to claim 1, wherein the weight of the lysozyme added in the step (1) is 0.05-0.07% of the weight of the sterile cold water, and the dried whole lemon is soaked for 35-45 min.
3. The preparation method of the dried whole lemon according to claim 1, wherein in the step (2), 3-5% by weight of non-iodine edible salt is added and stirred.
4. The method for preparing the dried whole lemons according to the claim 1, wherein in the step (2), the weight ratio of the broken inferior lemons to the added sterile water is 1: 5 to 7.
5. The method for preparing the dried whole lemons according to claim 1, wherein the soaking time in the step (2) is 15-40 days.
6. The method for preparing the dried whole lemons according to claim 1, wherein in the step (4), the lemons are turned up and down every 5-7 days.
7. The method for preparing the dried whole lemons according to claim 1, wherein the air drying process is carried out for 40-50 days in the step (4).
8. The method for preparing the dried whole lemon according to claim 1, wherein the air-drying in the step (4) is carried out by placing the dried lemon under the sun for air-drying for 50-70 min before ten o 'clock in the morning or after four o' clock in the afternoon, and then moving the dried whole lemon into a room with a temperature of 25-27 ℃.
9. A preparation method of dried lemon peels is characterized in that the dried whole lemon fruits prepared by the preparation method of the dried whole lemon fruits according to any one of claims 1 to 8 are subjected to full-covering stewing and baking to obtain the dried lemon peels;
wherein, the braising and baking are fully covered: and (3) completely covering the air drying rack by using a black cover, airing, and drying by using hot air until the surface color of the lemon fruit is uniform, thus obtaining the lemon dried orange peel.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201910347634.7A CN109953297B (en) | 2019-04-28 | 2019-04-28 | Preparation method of whole dried lemon and lemon dried orange peel |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201910347634.7A CN109953297B (en) | 2019-04-28 | 2019-04-28 | Preparation method of whole dried lemon and lemon dried orange peel |
Publications (2)
Publication Number | Publication Date |
---|---|
CN109953297A CN109953297A (en) | 2019-07-02 |
CN109953297B true CN109953297B (en) | 2022-03-29 |
Family
ID=67026669
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201910347634.7A Active CN109953297B (en) | 2019-04-28 | 2019-04-28 | Preparation method of whole dried lemon and lemon dried orange peel |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN109953297B (en) |
Families Citing this family (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
TWI782829B (en) * | 2021-12-20 | 2022-11-01 | 國立屏東科技大學 | Method for manufacturing citri reticulatae pericarpium using lemon peel |
Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2002355004A (en) * | 2001-05-31 | 2002-12-10 | Pokka Corp | Lemon-fermented product and method for producing the same |
KR20180047542A (en) * | 2016-10-31 | 2018-05-10 | 지니홈메이드 주식회사 | Method for manufacturing lemon jelly |
Family Cites Families (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104489058A (en) * | 2014-12-18 | 2015-04-08 | 广东省农业科学院蚕业与农产品加工研究所 | Processing method for preventing dry lemon slices from browning |
CN107951016A (en) * | 2018-01-15 | 2018-04-24 | 海南百晋兴生物科技有限公司 | A kind of beautiful composite enzyme of promise and preparation method thereof |
CN108703286A (en) * | 2018-05-25 | 2018-10-26 | 重庆汇达柠檬科技集团有限公司 | A kind of compound fruit enzyme nutrient solution of lemon and its preparation method and application |
CN109619172A (en) * | 2019-01-07 | 2019-04-16 | 广西壮族自治区农业科学院园艺研究所 | Organic citrus preservation method |
-
2019
- 2019-04-28 CN CN201910347634.7A patent/CN109953297B/en active Active
Patent Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2002355004A (en) * | 2001-05-31 | 2002-12-10 | Pokka Corp | Lemon-fermented product and method for producing the same |
KR20180047542A (en) * | 2016-10-31 | 2018-05-10 | 지니홈메이드 주식회사 | Method for manufacturing lemon jelly |
Also Published As
Publication number | Publication date |
---|---|
CN109953297A (en) | 2019-07-02 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
CN109757683B (en) | Preparation method of whole-fruit citrus peel | |
CN104286159B (en) | A kind of juicy peach fresh-keeping method | |
CN104286158B (en) | A kind of honey peach gather before preservative specially | |
KR101826907B1 (en) | Dried laver using deep sea water and method thereof | |
CN103931829A (en) | Prinsepia utilis Royle tea preparation method | |
CN107668702A (en) | A kind of production technology of trifoliate orange Dulcis ferment | |
CN109953297B (en) | Preparation method of whole dried lemon and lemon dried orange peel | |
CN103589558B (en) | A kind of brewing method of Compound fruit wine | |
CN101543305B (en) | Method for preparing sow thistle drink | |
KR101074159B1 (en) | method for manufacturing dried persimmon using pine needle and Japanese apricot | |
CN105248643A (en) | Chestnut liver-nourishing and spleen-tonifying garlic juice drink and preparation method thereof | |
CN107319071A (en) | A kind of preparation method of Mulberry-leaf Tea | |
CN107242526A (en) | A kind of edible preparation method for mixing sauce of dendrobium candidum | |
CN107836675A (en) | A kind of jerusalem artichoke can and preparation method thereof | |
CN109007198B (en) | Fermented sugar-free preserved papaya and processing method thereof | |
KR101332028B1 (en) | The fermentation composition contained gombo-baechu and its manufacturing method | |
KR101254864B1 (en) | Method for manufacturing a radish tea and the products thereof | |
CN111557436A (en) | Sechium edule enzyme and preparation method thereof | |
CN111772025A (en) | Pure natural roxburgh rose preserved fruit and preparation method thereof | |
KR102679134B1 (en) | Manufacturing method for noni juice | |
CN109170656A (en) | A kind of tinned fruit processing technology | |
CN104286741B (en) | The preparation method of preserved vegetable | |
CN111205953B (en) | Myrtle fermented fruit wine and preparation method thereof | |
KR20120040616A (en) | Beverage composition using a radish | |
CN109287838B (en) | Rosa roxburghii and gastrodia elata fermented preserved fruit can |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
PB01 | Publication | ||
PB01 | Publication | ||
SE01 | Entry into force of request for substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
GR01 | Patent grant | ||
GR01 | Patent grant |