CN109602063A - A kind of acid modification agent and its application method in low temperature cigarette reconstituted tobacoo - Google Patents
A kind of acid modification agent and its application method in low temperature cigarette reconstituted tobacoo Download PDFInfo
- Publication number
- CN109602063A CN109602063A CN201910104544.5A CN201910104544A CN109602063A CN 109602063 A CN109602063 A CN 109602063A CN 201910104544 A CN201910104544 A CN 201910104544A CN 109602063 A CN109602063 A CN 109602063A
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- China
- Prior art keywords
- modification agent
- reconstituted tobacoo
- acid modification
- acid
- low temperature
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Classifications
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/12—Steaming, curing, or flavouring tobacco
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/14—Forming reconstituted tobacco products, e.g. wrapper materials, sheets, imitation leaves, rods, cakes; Forms of such products
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Manufacture Of Tobacco Products (AREA)
Abstract
The invention discloses a kind of acid modification agent, by weight percentage include 5~20% phosphoric acid, 30~50% citric acids, 10~20% lactic acid, 10~30% fumaric acid, 0~20% malic acid.Application method of the acid modification agent in low temperature cigarette reconstituted tobacoo is also disclosed, is included the following steps, soak extraction stage a, soak extraction stage b, coating fluid preparatory phase, thin slice chip base preparatory phase and reconstituted tobacoo preparatory phase.Acid modification agent Environmental Safety, is applied in the high-nicotine reconstituted tobacoo of low temperature cigarette, and flue gas irritation can be effectively reduced, and keeps fragrance stable, soft, preferably improves the suction quality of cigarette.Acid modification agent can add in reconstituted tobacoo production process on demand, and easy to operate, controllability is strong, it is often more important that the production technology and production equipment for not changing original reconstituted tobacoo can meet the requirement of industrialized production.
Description
Technical field
The invention belongs to low temperature cigarette novel tobacco fields, and in particular to a kind of acid modification agent and its use in low temperature cigarette
Application method in reconstituted tobacoo.
Background technique
In recent years, as people are to the growing interest of smoking and health problem, tobacco control environment is increasingly serious, novel tobacco system
Product, especially low temperature cigarette (heating the cigarette that do not burn) are because being greatly reduced harmful components and can obtain and pumping similar in traditional cigarette
It inhales satisfaction and is a dark horse.In the low temperature cigarette product of existing maturation, the cigarette core material overwhelming majority is reconstituted tobacoo.Tobacco is thin
Piece is also known as reconstituted tobacco, is the Discarded Tobaccos objects such as the offal that will be discarded during production of cigarettes, the low-grade hypo-tobacco leaf of offal and part
Matter forms that shape is close or product better than natural tobacco by working process, and then reapplies in production of cigarettes application.
Nicotine is the important material base of tobacco and tobacco product organoleptic quality.During smoking cigarette, nicotine is by people
Body absorbs " strength " sense that can generate initial " top " and throat.However, consumer is in suction by reconstituted tobacoo system at present
When standby low temperature cigarette, either periphery heating or inner core heating, reaction has that physiology satisfaction is inadequate.This is
Since low temperature cigarette tobacco segment is usually no more than 0.2 gram (about 0.7 gram of traditional cigarette), meanwhile, the flue gas machine for releasing of low temperature cigarette
Reason is different from the combustion mechanism of traditional cigarette, and nicotine and fragrance matter are to add in heating source to cigarette core material in low temperature cigarette
Meet the needs of smoker by volatilization generation flue gas when hot (500 DEG C or less are even lower), therefore, it is limited effectively at
Divide and is more difficult to be completely transferred to flue gas at the heating temperature.
In order to enhance the strength of low temperature cigarette, meeting the first demand of consumer's drawing tobacco product --- suction meets
Sense, the reconstituted tobacoo of high-nicotine content is in low temperature cigarette using universal.However, the high-nicotine reconstituted tobacoo wooden miscellaneous gas when heated
Heavier, irritation is obvious, therefore, is modified to high-nicotine content reconstituted tobacoo, develops suction satisfaction height and suction product
The good low temperature cigarette of matter has become the problem of tobacco scientific worker's urgent need to resolve.
Summary of the invention
The present invention provides a kind of low temperature cigarette tobacco flake additive and its application methods, solve high-nicotine tobacco
The wooden miscellaneous gas is heavier when heated for thin slice, the obvious problem of irritation.
In order to solve the above-mentioned technical problem, the technical scheme adopted by the invention is that: a kind of acid modification agent, the acidity
Modifying agent includes 5~20% phosphoric acid by weight percentage, 30~50% citric acids, 10~20% lactic acid, 10~30% fumaric acid,
0~20% malic acid.
Further, the modification of reconstituted tobacoo of the acid modification agent for nicotine content greater than 1.2%.
A kind of application method based on acid modification agent of any of claims 1 or 2 in low temperature cigarette reconstituted tobacoo,
The following steps are included:
S1, soak extraction stage a: 3~5 times of tobacco material quality of water is added in weighed tobacco material and accounts for tobacco
The acid modification agent of material quality 0.05%~0.8%, by its 40 DEG C~60 DEG C of ultrasonic extracting machine at a temperature of impregnate, it is super
Sound extracts 2~4 hours, obtains solidliquid mixture, solidliquid mixture is filtered separation, obtains solid and extraction after separation of solid and liquid
Take liquid；
S2, soak extraction stage b: impregnated after the water of 2~3 times of tobacco material quality of addition in solid in step sl,
Ultrasonic extraction obtains solidliquid mixture, and solidliquid mixture is filtered separation, obtains solid and extract liquor, by extraction obtained
Liquid is taken to merge with extract liquor in step S1；
S3, coating fluid preparatory phase: it is added in combined extract liquor and accounts for tobacco material quality 0.05%~1% essence perfume
Material, after mixing, is concentrated extract liquor using Rotary Evaporators, and coating fluid is made；
S4, thin slice chip base preparatory phase: sheets of fibres chip base is made in the solid in step S2；
S5, reconstituted tobacoo preparatory phase: coating fluid and Alevaire even application is in chip base and dry, obtain low temperature volume
Cigarette reconstituted tobacoo, slice, chopping are spare.
Further, in the step S1, tobacco material includes offal, offal and pipe tobacco.
Further, in the step S4, sheets of fibres chip base is made by paper process, thick slurry method, roll-in method in solid.
Further, in the step S2, immersion, the condition of ultrasonic extraction are identical as in step S1.
Further, in the step S3, flavors and fragrances is to aoxidize isophorone, 2,6,6- cyclohexene -1 trimethyl -2-,
4- diketone, alpha, beta-lonone, 5 methyl furfural, vanillic aldehyde, benzyl alcohol, linalool, 2 methyl valeric acid, neryl acetate, dihydro
One of actinidia lactone, laurene, ethylmaltol, 3- acetylpyridine, 3-ethylpyridine and 2- methylpyrazine or two
Kind or more mixture.
Further, in the step S5, Alevaire is glycerol.
Further, the acid modification agent for accounting for tobacco material quality 0.05%~0.8% is in the step S3, described
It is added at least one step of step S4.
Further, in the step S3, the liquid volume after concentration is the 15%~25% of former extract liquor volume.
Advantageous effects of the invention: acid modification agent Environmental Safety, is applied to the high-nicotine of low temperature cigarette
In reconstituted tobacoo, flue gas irritation can be effectively reduced, keep fragrance stable, soft, preferably improve the suction quality of cigarette.Acid
Property modifying agent can add in reconstituted tobacoo production process on demand, and easy to operate, controllability is strong, it is often more important that does not change
The production technology and production equipment of original reconstituted tobacoo, can meet the requirement of industrialized production.
Specific embodiment
The invention will be further described below.Following embodiment is only used for clearly illustrating technical side of the invention
Case, and not intended to limit the protection scope of the present invention.
A kind of acid modification agent includes 5~20% phosphoric acid, 30~50% citric acids, 10~20% creams by weight percentage
Acid, 10~30% fumaric acid, 0~20% malic acid.Reconstituted tobacoo of the acid modification agent for nicotine content greater than 1.2% changes
Into.Acid modification agent Environmental Safety, is applied in the high-nicotine reconstituted tobacoo of low temperature cigarette, and flue gas stimulation can be effectively reduced
Property, keep fragrance stable, soft, preferably improves the suction quality of cigarette.
The application method of a kind of acid modification agent in low temperature cigarette reconstituted tobacoo, comprising the following steps: S1, immersion mention
It takes stage a: accurately weighing a certain amount of offal and offal composition tobacco material, tobacco material quality 3 is added in tobacco material
~5 times of water and the acid modification agent for accounting for tobacco material quality 0.05%~0.8%, place it in ultrasonic extracting machine at 40 DEG C
It is impregnated under conditions of~60 DEG C, ultrasonic extraction 2-4 hours, obtains solidliquid mixture, solidliquid mixture is filtered separation, Gu
Solid and extract liquor are obtained after liquid separation.S2, soak extraction stage b: 2~3 times of tobacco originals are added in solid in step sl
Expect quality water after impregnate, ultrasonic extraction, obtain solidliquid mixture, solidliquid mixture be filtered separation, obtain solid with
Extract liquor merges extract liquor obtained with extract liquor in step S1.S3, coating fluid preparatory phase: in combined extract liquor
Addition accounts for 0.05%~1% flavors and fragrances of tobacco material quality, after mixing, is carried out using Rotary Evaporators to extract liquor dense
Contracting, is made coating fluid；Flavors and fragrances is oxidation isophorone, 2,6,6- trimethyl -2- cyclohexene -1,4- diketone, β-purple sieve
Blue ketone, 5 methyl furfural, vanillic aldehyde, benzyl alcohol, linalool, 2 methyl valeric acid, neryl acetate, dihydroactinidiolide, the moon
One or more mixtures of osmanthus alkene, ethylmaltol, 3- acetylpyridine, 3-ethylpyridine and 2- methylpyrazine.
S4, thin slice chip base preparatory phase: sheets of fibres chip base is made by paper process, thick slurry method, roll-in method in the solid in step S2.
S5, reconstituted tobacoo preparatory phase: coating fluid and Alevaire even application is in chip base and dry, it obtains low temperature cigarette and uses tobacco
Thin slice, slice, chopping are spare, and Alevaire is preferably glycerol.
Acid modification agent in the application method in low temperature cigarette reconstituted tobacoo, account for tobacco material quality 0.05%~
0.8% acid modification agent can also step S3, step S4 at least one step in add.Step S3 at this time are as follows: closing
And extract liquor in be added account for 0.05%~1% flavors and fragrances of tobacco material quality and account for tobacco material quality 0.05%~
0.8% acid modification agent is concentrated coating fluid is made after mixing.Tobacco material quality is accounted for when not being added in step S1
Can also be added in 0.05%~0.8% acid modification agent, step S3 or step S4 account for tobacco material quality 0.05%~
0.8% acid modification agent.Acid modification agent can add in reconstituted tobacoo production process on demand, easy to operate, controllably
Property is strong, it is often more important that does not change the production technology and production equipment of original reconstituted tobacoo, can meet the requirement of industrialized production.
Embodiment one: application method of the acid modification agent in low temperature cigarette reconstituted tobacoo
S1, soak extraction stage a: being added 3 times of tobacco material quality of water in weighed tobacco material and accounts for tobacco original
The acid modification agent for expecting quality 0.4%, place it in ultrasonic extracting machine impregnated under conditions of 50 DEG C, ultrasonic extraction 2 it is small
When, solidliquid mixture is obtained, solidliquid mixture is filtered separation, obtains solid and extract liquor after separation of solid and liquid；Acidity changes
Property agent includes 18% phosphoric acid by weight percentage, 46% citric acid, 10% lactic acid, 14% fumaric acid, 12% malic acid.
S2, soak extraction stage b: it after the water of 2 times of tobacco material quality is added in solid in step sl, places it in
In ultrasonic extracting machine under conditions of 50 DEG C impregnate, ultrasonic extraction 2 hours, obtain solidliquid mixture, by solidliquid mixture into
Row is separated by filtration, and obtains solid and extract liquor, extract liquor obtained is merged with extract liquor in step S1.
S3, coating fluid preparatory phase: being added the flavors and fragrances for accounting for tobacco material quality 1% in combined extract liquor, mixes
After closing uniformly, extract liquor is concentrated using Rotary Evaporators, the liquid volume after concentration is the 25% of former extract liquor volume,
Coating fluid is made；It includes 5% oxidation isophorone, 10%2,6,6- trimethyl -2- that flavors and fragrances forms by weight percentage
Cyclohexene -1,4- diketone, 11% vanillic aldehyde, 20% linalool, 6%2- methylvaleric acid, 20% dihydroactinidiolide, 8% month
Osmanthus alkene, 8% ethylmaltol, 7%3- acetylpyridine, 5%2- methylpyrazine.
S4, thin slice chip base preparatory phase: sheets of fibres chip base is made using paper process in the solid in step S2；
S5, reconstituted tobacoo preparatory phase: coating fluid and glycerol even application is in chip base and dry, obtain low temperature cigarette
With reconstituted tobacoo, slice, chopping are spare.
Embodiment two: application method of the acid modification agent in low temperature cigarette reconstituted tobacoo
S1, soak extraction stage a: being added 4 times of tobacco material quality of water in weighed tobacco material and accounts for tobacco original
The acid modification agent for expecting quality 0.5% places it in immersion, ultrasonic extraction 2.5 under conditions of 55 DEG C in ultrasonic extracting machine
Hour, solidliquid mixture is obtained, solidliquid mixture is filtered separation, obtains solid and extract liquor after separation of solid and liquid；It is acid
Modifying agent includes 13% phosphoric acid, 45% citric acid, 18% lactic acid, 24% fumaric acid by weight percentage.
S2, soak extraction stage b: it after the water of 2.5 times of tobacco material quality is added in solid in step sl, is set
It is impregnated under conditions of 55 DEG C in ultrasonic extracting machine, ultrasonic extraction 2.5 hours, obtains solidliquid mixture, solid-liquid is mixed
Object is filtered separation, obtains solid and extract liquor, and extract liquor obtained is merged with extract liquor in step S1.
S3, coating fluid preparatory phase: being added the flavors and fragrances for accounting for tobacco material quality 0.6% in combined extract liquor,
After mixing, extract liquor is concentrated using Rotary Evaporators, the liquid volume after concentration is former extract liquor volume
20%, coating fluid is made；It includes 22%2,6,6- trimethyl -2- cyclohexene -1,4- that flavors and fragrances forms by weight percentage
Diketone, 16% alpha, beta-lonone, 16%5- methyl furfural, benzyl alcohol, 18%2- methylvaleric acid, 13% neryl acetate, 8% month
Osmanthus alkene, 7%2- methylpyrazine.
S4, thin slice chip base preparatory phase: sheets of fibres chip base is made using thick slurry method in the solid in step S2；
S5, reconstituted tobacoo preparatory phase: coating fluid and glycerol even application is in chip base and dry, obtain low temperature cigarette
With reconstituted tobacoo, slice, chopping are spare.
Application effect appraisal: acid of the invention is not added the reconstituted tobacoo prepared using embodiment 1,2 method of embodiment and
The reconstituted tobacoo (comparative sample) of property modifying agent rolls into cigarette respectively, carries out aesthetic quality with identical low temperature cigarette smoking set and comments
Valence, evaluation results are shown in Table 1.
Check problem: sample and check table are provided to 6 experts that smoke panel test, it is desirable that member of smoking requires to refer to items according to table
Mark is smoked panel test.
1 smoking result of the embodiment of the present invention of table
As shown in Table 1, the reconstituted tobacoo after acid modification agent of the present invention is added is more suitable for low temperature cigarette, can significant effective
Low temperature cigarette flue gas irritation is reduced, keeps flue gas stable, soft, hence it is evident that improve the suction organoleptic quality of low temperature cigarette.
The above is only a preferred embodiment of the present invention, it is noted that for the ordinary skill people of the art
For member, without departing from the technical principles of the invention, several improvement and deformations can also be made, these improvement and deformations
Also it should be regarded as protection scope of the present invention.
Claims (10)
1. a kind of acid modification agent, which is characterized in that the acid modification agent includes 5~20% phosphoric acid by weight percentage, 30~
50% citric acid, 10~20% lactic acid, 10~30% fumaric acid, 0~20% malic acid.
2. acid modification agent according to claim 1, which is characterized in that the acid modification agent is greater than for nicotine content
The modification of 1.2% reconstituted tobacoo.
3. a kind of application method based on acid modification agent of any of claims 1 or 2 in low temperature cigarette reconstituted tobacoo,
It is characterized in that, comprising the following steps:
S1, soak extraction stage a: 3 ~ 5 times of tobacco material quality of water is added in weighed tobacco material and accounts for tobacco material
The acid modification agent of quality 0.05%~0.8%, by its at a temperature of immersion, ultrasound extraction at 40 DEG C ~ 60 DEG C of ultrasonic extracting machine
It takes 2 ~ 4 hours, obtains solidliquid mixture, solidliquid mixture is filtered separation, obtains solid and extract liquor after separation of solid and liquid；
S2, soak extraction stage b: immersion, ultrasound extraction after the water of 2 ~ 3 times of tobacco material quality are added in solid in step sl
Take, obtain solidliquid mixture, solidliquid mixture is filtered separation, obtains solid and extract liquor, by extract liquor obtained with
Extract liquor merges in step S1；
S3, coating fluid preparatory phase: being added in combined extract liquor and account for 0.05% ~ 1% flavors and fragrances of tobacco material quality, mixes
After uniformly, extract liquor is concentrated using Rotary Evaporators, coating fluid is made；
S4, thin slice chip base preparatory phase: sheets of fibres chip base is made in the solid in step S2；
S5, reconstituted tobacoo preparatory phase: coating fluid and Alevaire even application is in chip base and dry, obtain low temperature cigarette use
Reconstituted tobacoo, slice, chopping are spare.
4. application method of the acid modification agent according to claim 3 in low temperature cigarette reconstituted tobacoo, feature exist
In in the step S1, tobacco material includes offal, offal and pipe tobacco.
5. application method of the acid modification agent according to claim 3 in low temperature cigarette reconstituted tobacoo, feature exist
In in the step S4, sheets of fibres chip base is made by paper process, thick slurry method, roll-in method in solid.
6. application method of the acid modification agent according to claim 3 in low temperature cigarette reconstituted tobacoo, feature exist
In in the step S2, immersion, the condition of ultrasonic extraction are identical as in step S1.
7. application method of the acid modification agent according to claim 3 in low temperature cigarette reconstituted tobacoo, feature exist
In in the step S3, flavors and fragrances is oxidation isophorone, 2,6,6- trimethyl -2- cyclohexene-Isosorbide-5-Nitrae-diketone, β-purple sieve
Blue ketone, 5 methyl furfural, vanillic aldehyde, benzyl alcohol, linalool, 2 methyl valeric acid, neryl acetate, dihydroactinidiolide, the moon
One or more mixtures of osmanthus alkene, ethylmaltol, 3- acetylpyridine, 3-ethylpyridine and 2- methylpyrazine.
8. application method of the acid modification agent according to claim 3 in low temperature cigarette reconstituted tobacoo, feature exist
In in the step S5, Alevaire is glycerol.
9. application method of the acid modification agent according to claim 3 in low temperature cigarette reconstituted tobacoo, feature exist
In, the acid modification agent for accounting for tobacco material quality 0.05%~0.8% the step S3, the step S4 at least one
It is added in a step.
10. application method of the acid modification agent according to claim 3 in low temperature cigarette reconstituted tobacoo, feature exist
In in the step S3, the liquid volume after concentration is the 15% ~ 25% of former extract liquor volume.
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| CN201910104544.5A CN109602063A (en) | 2019-02-01 | 2019-02-01 | A kind of acid modification agent and its application method in low temperature cigarette reconstituted tobacoo |
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| CN201910104544.5A CN109602063A (en) | 2019-02-01 | 2019-02-01 | A kind of acid modification agent and its application method in low temperature cigarette reconstituted tobacoo |
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Cited By (1)
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| CN111772226A (en) * | 2020-08-05 | 2020-10-16 | 四川三联新材料有限公司 | Method for improving comfort of heated cigarettes |
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Application publication date: 20190412 |
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