CN109288723A - A kind of cosmetic composition containing nanocellulose and preparation method thereof - Google Patents
A kind of cosmetic composition containing nanocellulose and preparation method thereof Download PDFInfo
- Publication number
- CN109288723A CN109288723A CN201811440214.5A CN201811440214A CN109288723A CN 109288723 A CN109288723 A CN 109288723A CN 201811440214 A CN201811440214 A CN 201811440214A CN 109288723 A CN109288723 A CN 109288723A
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- China
- Prior art keywords
- cosmetic composition
- cellulose
- total weight
- content
- nano
- Prior art date
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- 239000000203 mixture Substances 0.000 title claims abstract description 227
- 239000002537 cosmetic Substances 0.000 title claims abstract description 155
- 238000002360 preparation method Methods 0.000 title claims abstract description 55
- 229920001046 Nanocellulose Polymers 0.000 title abstract 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 60
- 239000002994 raw material Substances 0.000 claims abstract description 31
- 230000037303 wrinkles Effects 0.000 claims abstract description 26
- 230000002087 whitening effect Effects 0.000 claims abstract description 23
- 239000004615 ingredient Substances 0.000 claims abstract description 22
- 229920002678 cellulose Polymers 0.000 claims description 113
- 239000001913 cellulose Substances 0.000 claims description 113
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims description 76
- BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 claims description 76
- 238000010438 heat treatment Methods 0.000 claims description 63
- HCZKYJDFEPMADG-TXEJJXNPSA-N masoprocol Chemical compound C([C@H](C)[C@H](C)CC=1C=C(O)C(O)=CC=1)C1=CC=C(O)C(O)=C1 HCZKYJDFEPMADG-TXEJJXNPSA-N 0.000 claims description 60
- 238000003756 stirring Methods 0.000 claims description 56
- 239000000686 essence Substances 0.000 claims description 43
- 239000002253 acid Substances 0.000 claims description 41
- 150000002148 esters Chemical class 0.000 claims description 39
- 239000004006 olive oil Substances 0.000 claims description 39
- 235000008390 olive oil Nutrition 0.000 claims description 39
- 239000005977 Ethylene Substances 0.000 claims description 38
- 235000013871 bee wax Nutrition 0.000 claims description 38
- 239000012166 beeswax Substances 0.000 claims description 38
- JEIPFZHSYJVQDO-UHFFFAOYSA-N iron(III) oxide Inorganic materials O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 claims description 38
- 238000002156 mixing Methods 0.000 claims description 38
- 229910052697 platinum Inorganic materials 0.000 claims description 38
- 239000004408 titanium dioxide Substances 0.000 claims description 38
- 229920006037 cross link polymer Polymers 0.000 claims description 36
- ZDHRAACDPXUCHC-UHFFFAOYSA-N 3,4-diethyl-2-hexoxyphenol;5-methoxy-4-phenyltriazine Chemical compound COC1=CN=NN=C1C1=CC=CC=C1.CCCCCCOC1=C(O)C=CC(CC)=C1CC ZDHRAACDPXUCHC-UHFFFAOYSA-N 0.000 claims description 35
- VBICKXHEKHSIBG-UHFFFAOYSA-N 1-monostearoylglycerol Chemical compound CCCCCCCCCCCCCCCCCC(=O)OCC(O)CO VBICKXHEKHSIBG-UHFFFAOYSA-N 0.000 claims description 31
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 claims description 28
- BJRNKVDFDLYUGJ-RMPHRYRLSA-N hydroquinone O-beta-D-glucopyranoside Chemical compound O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@H]1OC1=CC=C(O)C=C1 BJRNKVDFDLYUGJ-RMPHRYRLSA-N 0.000 claims description 28
- 239000000243 solution Substances 0.000 claims description 27
- 238000009499 grossing Methods 0.000 claims description 20
- 229920000168 Microcrystalline cellulose Polymers 0.000 claims description 16
- 239000008367 deionised water Substances 0.000 claims description 16
- 229910021641 deionized water Inorganic materials 0.000 claims description 16
- 239000008108 microcrystalline cellulose Substances 0.000 claims description 16
- 229940016286 microcrystalline cellulose Drugs 0.000 claims description 16
- 235000019813 microcrystalline cellulose Nutrition 0.000 claims description 16
- 102000008186 Collagen Human genes 0.000 claims description 15
- 108010035532 Collagen Proteins 0.000 claims description 15
- 229920002385 Sodium hyaluronate Polymers 0.000 claims description 15
- 229920001436 collagen Polymers 0.000 claims description 15
- 229910052751 metal Inorganic materials 0.000 claims description 15
- 239000002184 metal Substances 0.000 claims description 15
- 239000012266 salt solution Substances 0.000 claims description 15
- 229940010747 sodium hyaluronate Drugs 0.000 claims description 15
- YWIVKILSMZOHHF-QJZPQSOGSA-N sodium;(2s,3s,4s,5r,6r)-6-[(2s,3r,4r,5s,6r)-3-acetamido-2-[(2s,3s,4r,5r,6r)-6-[(2r,3r,4r,5s,6r)-3-acetamido-2,5-dihydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-2-carboxy-4,5-dihydroxyoxan-3-yl]oxy-5-hydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-3,4,5-trihydroxyoxane-2- Chemical compound [Na+].CC(=O)N[C@H]1[C@H](O)O[C@H](CO)[C@@H](O)[C@@H]1O[C@H]1[C@H](O)[C@@H](O)[C@H](O[C@H]2[C@@H]([C@@H](O[C@H]3[C@@H]([C@@H](O)[C@H](O)[C@H](O3)C(O)=O)O)[C@H](O)[C@@H](CO)O2)NC(C)=O)[C@@H](C(O)=O)O1 YWIVKILSMZOHHF-QJZPQSOGSA-N 0.000 claims description 15
- ZZZCUOFIHGPKAK-UHFFFAOYSA-N D-erythro-ascorbic acid Natural products OCC1OC(=O)C(O)=C1O ZZZCUOFIHGPKAK-UHFFFAOYSA-N 0.000 claims description 14
- OQILCOQZDHPEAZ-UHFFFAOYSA-N Palmitinsaeure-octylester Natural products CCCCCCCCCCCCCCCC(=O)OCCCCCCCC OQILCOQZDHPEAZ-UHFFFAOYSA-N 0.000 claims description 14
- 239000002202 Polyethylene glycol Substances 0.000 claims description 14
- 229930003268 Vitamin C Natural products 0.000 claims description 14
- 229960000271 arbutin Drugs 0.000 claims description 14
- GJQLBGWSDGMZKM-UHFFFAOYSA-N ethylhexyl palmitate Chemical group CCCCCCCCCCCCCCCC(=O)OC(CC)CCCCC GJQLBGWSDGMZKM-UHFFFAOYSA-N 0.000 claims description 14
- BJRNKVDFDLYUGJ-UHFFFAOYSA-N p-hydroxyphenyl beta-D-alloside Natural products OC1C(O)C(O)C(CO)OC1OC1=CC=C(O)C=C1 BJRNKVDFDLYUGJ-UHFFFAOYSA-N 0.000 claims description 14
- 229920001223 polyethylene glycol Polymers 0.000 claims description 14
- 235000019154 vitamin C Nutrition 0.000 claims description 14
- 239000011718 vitamin C Substances 0.000 claims description 14
- 235000010980 cellulose Nutrition 0.000 claims description 13
- 230000001804 emulsifying effect Effects 0.000 claims description 12
- TWRXJAOTZQYOKJ-UHFFFAOYSA-L Magnesium chloride Chemical compound [Mg+2].[Cl-].[Cl-] TWRXJAOTZQYOKJ-UHFFFAOYSA-L 0.000 claims description 10
- 239000004909 Moisturizer Substances 0.000 claims description 10
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims description 10
- 230000001333 moisturizer Effects 0.000 claims description 10
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 9
- 239000003242 anti bacterial agent Substances 0.000 claims description 9
- 239000003963 antioxidant agent Substances 0.000 claims description 9
- 230000003078 antioxidant effect Effects 0.000 claims description 9
- 235000006708 antioxidants Nutrition 0.000 claims description 9
- 239000003974 emollient agent Substances 0.000 claims description 9
- -1 finish Substances 0.000 claims description 9
- 239000000516 sunscreening agent Substances 0.000 claims description 9
- 239000002562 thickening agent Substances 0.000 claims description 9
- 239000003995 emulsifying agent Substances 0.000 claims description 8
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims description 6
- 239000002304 perfume Substances 0.000 claims description 6
- 229910001629 magnesium chloride Inorganic materials 0.000 claims description 5
- 239000011780 sodium chloride Substances 0.000 claims description 5
- ZTHYODDOHIVTJV-UHFFFAOYSA-N Propyl gallate Chemical compound CCCOC(=O)C1=CC(O)=C(O)C(O)=C1 ZTHYODDOHIVTJV-UHFFFAOYSA-N 0.000 claims description 4
- XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical group [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 claims description 4
- OSORMYZMWHVFOZ-UHFFFAOYSA-N phenethyl benzoate Chemical compound C=1C=CC=CC=1C(=O)OCCC1=CC=CC=C1 OSORMYZMWHVFOZ-UHFFFAOYSA-N 0.000 claims description 4
- 238000004321 preservation Methods 0.000 claims description 4
- 235000013599 spices Nutrition 0.000 claims description 4
- 235000011187 glycerol Nutrition 0.000 claims description 3
- IXPNQXFRVYWDDI-UHFFFAOYSA-N 1-methyl-2,4-dioxo-1,3-diazinane-5-carboximidamide Chemical compound CN1CC(C(N)=N)C(=O)NC1=O IXPNQXFRVYWDDI-UHFFFAOYSA-N 0.000 claims description 2
- FJKROLUGYXJWQN-UHFFFAOYSA-M 4-hydroxybenzoate Chemical compound OC1=CC=C(C([O-])=O)C=C1 FJKROLUGYXJWQN-UHFFFAOYSA-M 0.000 claims description 2
- UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 claims description 2
- 229920002134 Carboxymethyl cellulose Polymers 0.000 claims description 2
- 239000004287 Dehydroacetic acid Substances 0.000 claims description 2
- WHUUTDBJXJRKMK-UHFFFAOYSA-N Glutamic acid Natural products OC(=O)C(N)CCC(O)=O WHUUTDBJXJRKMK-UHFFFAOYSA-N 0.000 claims description 2
- 239000004354 Hydroxyethyl cellulose Substances 0.000 claims description 2
- 229920000663 Hydroxyethyl cellulose Polymers 0.000 claims description 2
- WHUUTDBJXJRKMK-VKHMYHEASA-N L-glutamic acid Chemical compound OC(=O)[C@@H](N)CCC(O)=O WHUUTDBJXJRKMK-VKHMYHEASA-N 0.000 claims description 2
- JVTAAEKCZFNVCJ-UHFFFAOYSA-M Lactate Chemical compound CC(O)C([O-])=O JVTAAEKCZFNVCJ-UHFFFAOYSA-M 0.000 claims description 2
- 239000004166 Lanolin Substances 0.000 claims description 2
- 240000007817 Olea europaea Species 0.000 claims description 2
- OFOBLEOULBTSOW-UHFFFAOYSA-N Propanedioic acid Natural products OC(=O)CC(O)=O OFOBLEOULBTSOW-UHFFFAOYSA-N 0.000 claims description 2
- BGNXCDMCOKJUMV-UHFFFAOYSA-N Tert-Butylhydroquinone Chemical group CC(C)(C)C1=CC(O)=CC=C1O BGNXCDMCOKJUMV-UHFFFAOYSA-N 0.000 claims description 2
- 239000001697 butter ester Substances 0.000 claims description 2
- 239000001768 carboxy methyl cellulose Substances 0.000 claims description 2
- 235000010948 carboxy methyl cellulose Nutrition 0.000 claims description 2
- 239000008112 carboxymethyl-cellulose Substances 0.000 claims description 2
- 229960000541 cetyl alcohol Drugs 0.000 claims description 2
- GVJHHUAWPYXKBD-UHFFFAOYSA-N d-alpha-tocopherol Natural products OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-UHFFFAOYSA-N 0.000 claims description 2
- SASYSVUEVMOWPL-NXVVXOECSA-N decyl oleate Chemical compound CCCCCCCCCCOC(=O)CCCCCCC\C=C/CCCCCCCC SASYSVUEVMOWPL-NXVVXOECSA-N 0.000 claims description 2
- JEQRBTDTEKWZBW-UHFFFAOYSA-N dehydroacetic acid Chemical compound CC(=O)C1=C(O)OC(C)=CC1=O JEQRBTDTEKWZBW-UHFFFAOYSA-N 0.000 claims description 2
- 229940061632 dehydroacetic acid Drugs 0.000 claims description 2
- PGRHXDWITVMQBC-UHFFFAOYSA-N dehydroacetic acid Natural products CC(=O)C1C(=O)OC(C)=CC1=O PGRHXDWITVMQBC-UHFFFAOYSA-N 0.000 claims description 2
- 235000019258 dehydroacetic acid Nutrition 0.000 claims description 2
- 235000013922 glutamic acid Nutrition 0.000 claims description 2
- 239000004220 glutamic acid Substances 0.000 claims description 2
- 229960002989 glutamic acid Drugs 0.000 claims description 2
- BXWNKGSJHAJOGX-UHFFFAOYSA-N hexadecan-1-ol Chemical compound CCCCCCCCCCCCCCCCO BXWNKGSJHAJOGX-UHFFFAOYSA-N 0.000 claims description 2
- 235000019447 hydroxyethyl cellulose Nutrition 0.000 claims description 2
- BEJNERDRQOWKJM-UHFFFAOYSA-N kojic acid Chemical compound OCC1=CC(=O)C(O)=CO1 BEJNERDRQOWKJM-UHFFFAOYSA-N 0.000 claims description 2
- WZNJWVWKTVETCG-UHFFFAOYSA-N kojic acid Natural products OC(=O)C(N)CN1C=CC(=O)C(O)=C1 WZNJWVWKTVETCG-UHFFFAOYSA-N 0.000 claims description 2
- 229960004705 kojic acid Drugs 0.000 claims description 2
- 235000019388 lanolin Nutrition 0.000 claims description 2
- 229940039717 lanolin Drugs 0.000 claims description 2
- VZCYOOQTPOCHFL-UPHRSURJSA-N maleic acid Chemical compound OC(=O)\C=C/C(O)=O VZCYOOQTPOCHFL-UPHRSURJSA-N 0.000 claims description 2
- 239000011976 maleic acid Substances 0.000 claims description 2
- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 claims description 2
- 229940098888 phenethyl benzoate Drugs 0.000 claims description 2
- WVDDGKGOMKODPV-ZQBYOMGUSA-N phenyl(114C)methanol Chemical compound O[14CH2]C1=CC=CC=C1 WVDDGKGOMKODPV-ZQBYOMGUSA-N 0.000 claims description 2
- 239000000473 propyl gallate Substances 0.000 claims description 2
- 235000010388 propyl gallate Nutrition 0.000 claims description 2
- 229940075579 propyl gallate Drugs 0.000 claims description 2
- 229920002545 silicone oil Polymers 0.000 claims description 2
- 239000000661 sodium alginate Substances 0.000 claims description 2
- 235000010413 sodium alginate Nutrition 0.000 claims description 2
- 229940005550 sodium alginate Drugs 0.000 claims description 2
- 239000004250 tert-Butylhydroquinone Substances 0.000 claims description 2
- 235000019281 tert-butylhydroquinone Nutrition 0.000 claims description 2
- 235000010384 tocopherol Nutrition 0.000 claims description 2
- 239000011732 tocopherol Substances 0.000 claims description 2
- 229960001295 tocopherol Drugs 0.000 claims description 2
- 229930003799 tocopherol Natural products 0.000 claims description 2
- VZCYOOQTPOCHFL-UHFFFAOYSA-N trans-butenedioic acid Natural products OC(=O)C=CC(O)=O VZCYOOQTPOCHFL-UHFFFAOYSA-N 0.000 claims description 2
- ZEMPKEQAKRGZGQ-VBJOUPRGSA-N triricinolein Chemical compound CCCCCC[C@@H](O)C\C=C/CCCCCCCC(=O)OCC(OC(=O)CCCCCCC\C=C/C[C@H](O)CCCCCC)COC(=O)CCCCCCC\C=C/C[C@H](O)CCCCCC ZEMPKEQAKRGZGQ-VBJOUPRGSA-N 0.000 claims description 2
- 229940099259 vaseline Drugs 0.000 claims description 2
- 150000003722 vitamin derivatives Chemical class 0.000 claims description 2
- 239000011787 zinc oxide Substances 0.000 claims description 2
- GVJHHUAWPYXKBD-IEOSBIPESA-N α-tocopherol Chemical compound OC1=C(C)C(C)=C2O[C@@](CCC[C@H](C)CCC[C@H](C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-IEOSBIPESA-N 0.000 claims description 2
- TYYHDKOVFSVWON-UHFFFAOYSA-N 2-butyl-2-methoxy-1,3-diphenylpropane-1,3-dione Chemical compound C=1C=CC=CC=1C(=O)C(OC)(CCCC)C(=O)C1=CC=CC=C1 TYYHDKOVFSVWON-UHFFFAOYSA-N 0.000 claims 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims 1
- 241001165494 Rhodiola Species 0.000 claims 1
- 244000042430 Rhodiola rosea Species 0.000 claims 1
- 235000003713 Rhodiola rosea Nutrition 0.000 claims 1
- 229960005193 avobenzone Drugs 0.000 claims 1
- 125000003976 glyceryl group Chemical group [H]C([*])([H])C(O[H])([H])C(O[H])([H])[H] 0.000 claims 1
- 239000002070 nanowire Substances 0.000 claims 1
- 229940049964 oleate Drugs 0.000 claims 1
- ZQPPMHVWECSIRJ-KTKRTIGZSA-N oleic acid Chemical compound CCCCCCCC\C=C/CCCCCCCC(O)=O ZQPPMHVWECSIRJ-KTKRTIGZSA-N 0.000 claims 1
- QQONPFPTGQHPMA-UHFFFAOYSA-N propylene Natural products CC=C QQONPFPTGQHPMA-UHFFFAOYSA-N 0.000 claims 1
- 125000004805 propylene group Chemical group [H]C([H])([H])C([H])([*:1])C([H])([H])[*:2] 0.000 claims 1
- 239000011734 sodium Substances 0.000 claims 1
- 229910052708 sodium Inorganic materials 0.000 claims 1
- 230000000694 effects Effects 0.000 abstract description 9
- 230000003020 moisturizing effect Effects 0.000 abstract description 6
- 230000001153 anti-wrinkle effect Effects 0.000 abstract description 3
- 208000003351 Melanosis Diseases 0.000 abstract description 2
- 125000002887 hydroxy group Chemical group [H]O* 0.000 abstract description 2
- 238000010521 absorption reaction Methods 0.000 abstract 1
- 231100000344 non-irritating Toxicity 0.000 abstract 1
- PQUXFUBNSYCQAL-UHFFFAOYSA-N 1-(2,3-difluorophenyl)ethanone Chemical compound CC(=O)C1=CC=CC(F)=C1F PQUXFUBNSYCQAL-UHFFFAOYSA-N 0.000 description 37
- 229940047670 sodium acrylate Drugs 0.000 description 37
- IIZPXYDJLKNOIY-JXPKJXOSSA-N 1-palmitoyl-2-arachidonoyl-sn-glycero-3-phosphocholine Chemical compound CCCCCCCCCCCCCCCC(=O)OC[C@H](COP([O-])(=O)OCC[N+](C)(C)C)OC(=O)CCC\C=C/C\C=C/C\C=C/C\C=C/CCCCC IIZPXYDJLKNOIY-JXPKJXOSSA-N 0.000 description 36
- 239000000787 lecithin Substances 0.000 description 36
- 235000010445 lecithin Nutrition 0.000 description 36
- 229940067606 lecithin Drugs 0.000 description 36
- HCZKYJDFEPMADG-UHFFFAOYSA-N erythro-nordihydroguaiaretic acid Natural products C=1C=C(O)C(O)=CC=1CC(C)C(C)CC1=CC=C(O)C(O)=C1 HCZKYJDFEPMADG-UHFFFAOYSA-N 0.000 description 22
- 229960003951 masoprocol Drugs 0.000 description 22
- 238000005984 hydrogenation reaction Methods 0.000 description 21
- 230000006870 function Effects 0.000 description 15
- 230000008859 change Effects 0.000 description 13
- 238000012545 processing Methods 0.000 description 12
- 238000000265 homogenisation Methods 0.000 description 9
- 230000004215 skin function Effects 0.000 description 6
- 238000011156 evaluation Methods 0.000 description 4
- JYEUMXHLPRZUAT-UHFFFAOYSA-N 1,2,3-triazine Chemical compound C1=CN=NN=C1 JYEUMXHLPRZUAT-UHFFFAOYSA-N 0.000 description 3
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 3
- 235000021355 Stearic acid Nutrition 0.000 description 3
- 235000009508 confectionery Nutrition 0.000 description 3
- 238000002242 deionisation method Methods 0.000 description 3
- YQEMORVAKMFKLG-UHFFFAOYSA-N glycerine monostearate Natural products CCCCCCCCCCCCCCCCCC(=O)OC(CO)CO YQEMORVAKMFKLG-UHFFFAOYSA-N 0.000 description 3
- SVUQHVRAGMNPLW-UHFFFAOYSA-N glycerol monostearate Natural products CCCCCCCCCCCCCCCCC(=O)OCC(O)CO SVUQHVRAGMNPLW-UHFFFAOYSA-N 0.000 description 3
- 239000004519 grease Substances 0.000 description 3
- 239000001257 hydrogen Substances 0.000 description 3
- 229910052739 hydrogen Inorganic materials 0.000 description 3
- 230000006872 improvement Effects 0.000 description 3
- 238000000034 method Methods 0.000 description 3
- OQCDKBAXFALNLD-UHFFFAOYSA-N octadecanoic acid Natural products CCCCCCCC(C)CCCCCCCCC(O)=O OQCDKBAXFALNLD-UHFFFAOYSA-N 0.000 description 3
- 239000008117 stearic acid Substances 0.000 description 3
- 241000196324 Embryophyta Species 0.000 description 2
- 230000008901 benefit Effects 0.000 description 2
- 238000001514 detection method Methods 0.000 description 2
- 241000220317 Rosa Species 0.000 description 1
- 206010040880 Skin irritation Diseases 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 239000006071 cream Substances 0.000 description 1
- 238000004132 cross linking Methods 0.000 description 1
- NZZIMKJIVMHWJC-UHFFFAOYSA-N dibenzoylmethane Chemical compound C=1C=CC=CC=1C(=O)CC(=O)C1=CC=CC=C1 NZZIMKJIVMHWJC-UHFFFAOYSA-N 0.000 description 1
- 230000002500 effect on skin Effects 0.000 description 1
- 238000004945 emulsification Methods 0.000 description 1
- 230000001815 facial effect Effects 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 239000006210 lotion Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 230000007246 mechanism Effects 0.000 description 1
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- 239000002121 nanofiber Substances 0.000 description 1
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- 238000006467 substitution reaction Methods 0.000 description 1
- MAZWDMBCPDUFDJ-UHFFFAOYSA-N trans-Traumatinsaeure Natural products OC(=O)CCCCCCCCC=CC(O)=O MAZWDMBCPDUFDJ-UHFFFAOYSA-N 0.000 description 1
- MAZWDMBCPDUFDJ-VQHVLOKHSA-N traumatic acid Chemical compound OC(=O)CCCCCCCC\C=C\C(O)=O MAZWDMBCPDUFDJ-VQHVLOKHSA-N 0.000 description 1
- 238000005303 weighing Methods 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/731—Cellulose; Quaternized cellulose derivatives
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/04—Topical preparations for affording protection against sunlight or other radiation; Topical sun tanning preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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Abstract
本发明属于化妆品的制备技术领域，具体涉及一种含有纳米纤维素的化妆品组合物及其制备方法。该化妆品组合物充分利用了纳米纤维素的纯天然植物属性，其原料价格低，资源丰富，且表面含有大量的羟基，吸水保湿性能优异。同时，纳米纤维素具有高长径比和高比表面积，直径小于100nm，远远小于紫外线的波长，能够反射日光中的紫外光，在此基础上进一步添加保湿润肤成分、美白祛斑成分或除皱抗皱成分，使化妆品兼具优良的美白祛斑功效，对皮肤无刺激性，提高了产品的舒适性和安全性。The invention belongs to the technical field of preparation of cosmetics, in particular to a cosmetic composition containing nanocellulose and a preparation method thereof. The cosmetic composition makes full use of the pure natural plant properties of nanocellulose, the raw material price is low, the resources are abundant, the surface contains a large number of hydroxyl groups, and the water absorption and moisturizing performance is excellent. At the same time, nanocellulose has a high aspect ratio and high specific surface area, and its diameter is less than 100nm, which is far less than the wavelength of ultraviolet rays. It can reflect ultraviolet light in sunlight. Wrinkle and anti-wrinkle ingredients, make cosmetics have both excellent whitening and freckle-removing effects, non-irritating to the skin, and improve the comfort and safety of the product.
Description
Technical field
The invention belongs to the preparation technical fields of cosmetics, and in particular to a kind of cosmetic combinations containing nano-cellulose
Object and preparation method thereof.
Background technique
Cosmetics are one of main skin care modes, and effect depends primarily on the effective component contained by itself.At present
Cosmetics huge number on the market, effect are not quite similar.Wherein, the principle active component of Moisturizer is sodium hyaluronate or water
The biomolecule such as collagen are solved, still not using natural plant fibre as the Moisturizer of principle active component.
Summary of the invention
The primary purpose of the present invention is that providing a kind of cosmetic composition containing nano-cellulose.
Another object of the present invention is to provide the preparation methods of the above-mentioned cosmetic composition containing nano-cellulose.
To achieve the goals above, The technical solution adopted by the invention is as follows:
A kind of cosmetic composition containing nano-cellulose, with the total weight of cosmetic composition, containing 20%~
The partial size of 50% nano-cellulose, nano-cellulose is less than 100nm.
Preferably, the partial size of the nano-cellulose is less than 80nm.
It is furthermore preferred that the partial size of the nano-cellulose is less than 60nm.
Preferably, the cosmetic composition containing nano-cellulose is lotion or cream.
Preferably, the cosmetic composition containing nano-cellulose also include thickener, emulsifier, antibacterial agent,
Finish, essence and deionized water, and include that moisturizer, emollient, sun-screening agent, antioxidant, whitening spot-removing ingredient and smoothing wrinkle are crease-resistant
One or more of ingredient.
It is furthermore preferred that the moisturizer be one or both of glycerol, propylene glycol, sorbierite and polyethylene glycol with
On.
It is further preferred that the content of the moisturizer is the 1%~5% of cosmetic composition total weight, more into one
Step preferably 2%~3%.
It is furthermore preferred that the emollient be ethylhexyl palmitate, decyl oleate, saualane, phenethyl benzoate,
One or more of cetanol lactate and maleic acid ricinolein.
It is further preferred that the content of the emollient is the 1%~5% of cosmetic composition total weight, more into one
Step preferably 2%~4%.
It is furthermore preferred that the sun-screening agent is zinc oxide, titanium dioxide, dimethyl PABA ethylhexyl, butylmethoxy
One or more of dibenzoyl methane and bis-ethylhexoxyphenol methoxyphenyl triazine.
It is further preferred that the content of the sun-screening agent be cosmetic composition total weight 0.5%~3%, more into
One step is preferably 1.7%~2.3%.
It is furthermore preferred that the antioxidant is tert-butyl hydroquinone, glutamic acid, tocopherol, propylgallate, positive dihydro are cured
Create one or more of sour (NDGA).
It is further preferred that the content of the antioxidant is the 0.01%~0.1% of cosmetic composition total weight, more
Further preferably 0.05%~0.08%.
It is furthermore preferred that the whitening spot-removing ingredient is one or both of quinhydrones, arbutin, kojic acid and vitamin C
More than.
It is further preferred that the content of the whitening spot-removing ingredient is the 2%~6% of cosmetic composition total weight,
It is still more preferably 3%~5%.
It is furthermore preferred that the crease-resistant ingredient of the smoothing wrinkle is Sodium Hyaluronate, collagen, mate leaf extract and rose
One of rare gadol extract is a variety of.
It is further preferred that the content of the crease-resistant ingredient of the smoothing wrinkle is the 2~6% of cosmetic composition total weight, more
Further preferably 3~5%.
It is furthermore preferred that the emulsifier is glycerin monostearate, hydrolecithin, lanolin and the smooth olive oil of sorb
One or more of acid esters.
It is further preferred that the content of the emulsifier is the 3%~6% of cosmetic composition total weight, more into one
Step preferably 4%~5%.
It is furthermore preferred that the antibacterial agent is Buddhist nun's platinum rouge, p-hydroxybenzoate, benzyl alcohol, one in dehydroacetic acid
Kind is two or more.
It is further preferred that the content of the antibacterial agent be cosmetic composition total weight 0.1%~2%, more into
One step is preferably 0.5%~0.8%.
It is furthermore preferred that the thickener is hydroxyethyl cellulose, carboxymethyl cellulose, sodium alginate, PEG-80 glycerol
One or more of base butter ester and sodium acrylate/ethylene isodecyl acid esters cross-linked polymer.
It is further preferred that the content of the thickener is the 2%~5% of cosmetic composition total weight, more into one
Step preferably 3%~4%.
It is furthermore preferred that the finish is one or both of olive oil, stearate, beeswax, silicone oil and vaseline
More than.
It is further preferred that the content of the finish is the 2%~5% of cosmetic composition total weight, further
Preferably 3%~4%.
It is furthermore preferred that the content of the essence is the 0.5%~1% of cosmetic composition total weight, it is further excellent
It is selected as 0.6%~0.8%.
It is furthermore preferred that the cosmetic composition containing nano-cellulose is by following raw material by weight percentage
Composition:
Above-mentioned raw materials weight adds up to 100%.The formula is the cosmetic composition with moisture-keeping functions.
It is furthermore preferred that the cosmetic composition containing nano-cellulose is by following raw material by weight percentage
Composition:
Above-mentioned raw materials weight adds up to 100%.The formula is the cosmetic composition with whitening spot-removing function.
It is furthermore preferred that the cosmetic composition containing nano-cellulose is by following raw material by weight percentage
Composition:
Above-mentioned raw materials weight adds up to 100%.The formula is the cosmetic composition with crease-resistant smoothing wrinkle function.
Invention further provides the preparation method of the above-mentioned cosmetic composition containing nano-cellulose, including it is as follows
Step:
(1) preparation of nano-cellulose
Microcrystalline cellulose is soluble in water, it is high-pressure homogeneous, cellulose solution is obtained, metal salt solution bridge joint is added, from
Heart concentration, obtains nano-cellulose gel；
(2) preparation of water phase
By nano-cellulose gel, moisturizer, emollient, whitening spot-removing ingredient, the crease-resistant ingredient of smoothing wrinkle, sun-screening agent, emulsification
Agent, essence, antioxidant and deionized water mixing, dissolve by heating, stir evenly, obtain mixture A；
(3) preparation of oily phase
Thickener, vitamin derivative, antibacterial agent and finish are mixed, is dissolved by heating, is stirred evenly, obtain mixture B；
(4) preparation of cosmetic composition
Mixture A and mixture B is mixed, is stirred evenly, is dissolved by heating, heat preservation, then high pressure or emulsifying homogeneous, it is cooled to
Room temperature to get arrive the cosmetic composition containing nano-cellulose.
Preferably, when described in step (1) that microcrystalline cellulose is soluble in water, the mass ratio of microcrystalline cellulose and water is
1:20。
Preferably, pressure high-pressure homogeneous described in step (1) be 20000~30000psi, circular treatment 3~6 times.
Preferably, metal salt solution described in step (1) is in calcium chloride solution, magnesium chloride solution and sodium chloride solution
One or more.
Preferably, the quality that metal salt solution is added described in step (1) is the 3~6% of cellulose solution quality.
Preferably, the temperature of heating for dissolving described in step (2) is 60~90 DEG C.
Preferably, the temperature of heating for dissolving described in step (3) is 50~80 DEG C.
Preferably, the temperature of heating for dissolving described in step (4) is 60~80 DEG C, when a length of 30~60min of heat preservation.
Preferably, high-pressure homogeneous described in step (4) to be carried out using high pressure homogenizer, pressure is 10~30MPa, circulation
1~3 time.
Preferably, emulsifying homogeneous described in step (4) is carried out using emulsifying homogeneous machine, and temperature is 60 DEG C, circulation
30min。
Compared with the prior art, the invention has the following advantages and beneficial effects:
Nano-cellulose is added in cosmetics by the present invention, take full advantage of the pure plant of nano-cellulose at
Point, cost of material is low, and it is resourceful, and a large amount of hydroxyl is contained on surface, water suction performance of keeping humidity is excellent.Meanwhile nanofiber
Element has high length-diameter ratio and a high-specific surface area, and diameter is less than 100nm, the far smaller than wavelength of ultraviolet light, can be in reflecting sunlight
Ultraviolet light, further addition skin-moisturizing, skin ingredient, whitening spot-removing ingredient or the crease-resistant ingredient of smoothing wrinkle, make cosmetics on this basis
Excellent whitening effect is had both, to no skin irritation, improves the comfortableness and security of product.
Specific embodiment
Below with reference to embodiment, invention is further described in detail, and embodiments of the present invention are not limited thereto.It is right
In not specifically specified technological parameter, routine techniques progress can refer to.
The purchase of the microcrystalline cellulose used in the following example is in Wei Feng Biotechnology Co., Ltd of Zhengzhou City, food
Grade, partial size are 20~80 μm.
Embodiment 1
The present embodiment provides a kind of cosmetic composition and its system containing nano-cellulose with skin-moisturizing, skin function
Preparation Method.
The cosmetic composition is made of following raw material by weight percentage:
Nano-cellulose 20%, sorbierite 2%, polyethylene glycol 1.5%, ethylhexyl palmitate 2%, saualane 2.5%,
Glycerin monostearate 2.5%, hydrogenates lecithin 2.5%, Buddhist nun's platinum rouge 0.7%, and sodium acrylate/ethylene isodecyl acid esters crosslinking gathers
Close object 3.5%, olive oil 1.5%, beeswax 2.5%, bis-ethylhexoxyphenol methoxyphenyl triazine 1.5%, titanium dioxide
0.6%, nordihydroguaiaretic acid (NDGA) 0.05%, essence 0.6% and water 56.05%.
The preparation method of the above-mentioned cosmetic composition containing nano-cellulose with skin-moisturizing, skin function, including it is following
Step:
(1) microcrystalline cellulose 1:20 in mass ratio is soluble in water, the homogeneous in high pressure homogenizer, homogenization pressure
20000psi, circular treatment 6 times, (quality that metal salt solution is added is cellulose solution quality to addition calcium chloride solution bridge joint
5%), obtain nano-cellulose gel after centrifugal concentrating.
(2) nano-cellulose gel, sorbierite, polyethylene glycol, ethylhexyl palmitate, saualane, monostearate is sweet
Grease, hydrogenation lecithin, essence, nordihydroguaiaretic acid, bis-ethylhexoxyphenol methoxyphenyl triazine, titanium dioxide and go from
Sub- water mixing, dissolves by heating at 60 DEG C, stirs evenly, obtain mixture A.
(3) sodium acrylate/ethylene isodecyl acid esters cross-linked polymer, Buddhist nun's platinum rouge, olive oil and beeswax are mixed, at 50 DEG C
Lower heating for dissolving, stirs evenly, and obtains mixture B.
(4) it is stirred after mixing mixture A and mixture B, dissolves by heating, stir evenly at 60 DEG C, keep the temperature 60min,
30min is recycled in emulsifying homogeneous machine, temperature is cooled to room temperature at 60 DEG C to get the change containing nano-cellulose is arrived
Cosmetic compositions.
Embodiment 2
The present embodiment provides a kind of cosmetic composition and its system containing nano-cellulose with skin-moisturizing, skin function
Preparation Method.
The cosmetic composition is made of following raw material by weight percentage:
Nano-cellulose 30%, sorbierite 2.5%, polyethylene glycol 1%, ethylhexyl palmitate 2.5%, saualane 2%,
Glycerin monostearate 2% hydrogenates lecithin 2.5%, Buddhist nun's platinum rouge 0.5%, sodium acrylate/ethylene isodecyl acid esters cross-linked polymeric
Object 3%, olive oil 2%, beeswax 2%, bis-ethylhexoxyphenol methoxyphenyl triazine 1%, titanium dioxide 0.7%, positive dihydro are cured
Create acid (NDGA) 0.07%, essence 0.8% and water 47.43%.
The preparation method of the above-mentioned cosmetic composition containing nano-cellulose with skin-moisturizing, skin function, including it is following
Step:
(1) microcrystalline cellulose 1:20 in mass ratio is soluble in water, the homogeneous in high pressure homogenizer, homogenization pressure
30000psi, circular treatment 3 times, (quality that metal salt solution is added is cellulose solution quality to addition magnesium chloride solution bridge joint
5%), obtain nano-cellulose gel after centrifugal concentrating.
(2) nano-cellulose gel, sorbierite, polyethylene glycol, ethylhexyl palmitate, saualane, monostearate is sweet
Grease, hydrogenation lecithin, essence, nordihydroguaiaretic acid, bis-ethylhexoxyphenol methoxyphenyl triazine, titanium dioxide and go from
Sub- water mixing, dissolves by heating at 90 DEG C, stirs evenly, obtain mixture A.
(3) sodium acrylate/ethylene isodecyl acid esters cross-linked polymer, Buddhist nun's platinum rouge, olive oil and beeswax are mixed, at 80 DEG C
Lower heating for dissolving, stirs evenly, and obtains mixture B.
(4) it is stirred after mixing mixture A and mixture B, dissolves by heating, stir evenly at 80 DEG C, keep the temperature 30min,
30min is recycled in emulsifying homogeneous machine, temperature is cooled to room temperature at 60 DEG C to get the change containing nano-cellulose is arrived
Cosmetic compositions.
Embodiment 3
The present embodiment provides a kind of cosmetic composition and its system containing nano-cellulose with skin-moisturizing, skin function
Preparation Method.
The cosmetic composition is made of following raw material by weight percentage:
Nano-cellulose 50%, sorbierite 1.5%, polyethylene glycol 2%, ethylhexyl palmitate 2%, saualane 3% are single
Tristerin 3% hydrogenates lecithin 2%, Buddhist nun's platinum rouge 0.8%, sodium acrylate/ethylene isodecyl acid esters cross-linked polymer
4%, olive oil 1%, beeswax 3%, bis-ethylhexoxyphenol methoxyphenyl triazine 1.5%, titanium dioxide 0.8%, positive dihydro is cured
Create acid (NDGA) 0.08%, essence 0.8% and water 24.52%.
The preparation method of the above-mentioned cosmetic composition containing nano-cellulose with skin-moisturizing, skin function, including it is following
Step:
(1) microcrystalline cellulose 1:20 in mass ratio is soluble in water, the homogeneous in high pressure homogenizer, homogenization pressure
25000psi, circular treatment 4 times, (quality that metal salt solution is added is cellulose solution quality to addition sodium chloride solution bridge joint
5%), obtain nano-cellulose gel after centrifugal concentrating.
(2) nano-cellulose gel, sorbierite, polyethylene glycol, ethylhexyl palmitate, saualane, monostearate is sweet
Grease, hydrogenation lecithin, essence, nordihydroguaiaretic acid, bis-ethylhexoxyphenol methoxyphenyl triazine, titanium dioxide and go from
Sub- water mixing, dissolves by heating at 75 DEG C, stirs evenly, obtain mixture A.
(3) sodium acrylate/ethylene isodecyl acid esters cross-linked polymer, Buddhist nun's platinum rouge, olive oil and beeswax are mixed, at 65 DEG C
Lower heating for dissolving, stirs evenly, and obtains mixture B.
(4) it is stirred after mixing mixture A and mixture B, dissolves by heating, stir evenly at 70 DEG C, keep the temperature 45min,
30min is recycled in emulsifying homogeneous machine, temperature is cooled to room temperature at 60 DEG C to get the change containing nano-cellulose is arrived
Cosmetic compositions.
Reference examples 1
Reference examples of the present embodiment as embodiment 1, provide a kind of cosmetic composition without containing nano-cellulose and
Preparation method.
The cosmetic composition is made of following raw material by weight percentage:
Sorbierite 2%, polyethylene glycol 1.5%, ethylhexyl palmitate 2%, saualane 2.5%, glycerin monostearate
2.5%, hydrogenate lecithin 2.5%, Buddhist nun's platinum rouge 0.7%, sodium acrylate/ethylene isodecyl acid esters cross-linked polymer 3.5%, olive
Oil 1.5%, beeswax 2.5%, bis-ethylhexoxyphenol methoxyphenyl triazine 1.5%, titanium dioxide 0.6%, nordihydroguaiaretic acid
(NDGA) 0.05%, essence 0.6% and water 76.05%.
The preparation method of the above-mentioned cosmetic composition without containing nano-cellulose, comprising the following steps:
(1) by sorbierite, polyethylene glycol, ethylhexyl palmitate, saualane, glycerin monostearate, hydrogenation lecithin,
Essence, nordihydroguaiaretic acid, bis-ethylhexoxyphenol methoxyphenyl triazine, titanium dioxide and deionized water mixing, at 60 DEG C
It dissolves by heating, stirs evenly, obtain mixture A.
(2) sodium acrylate/ethylene isodecyl acid esters cross-linked polymer, Buddhist nun's platinum rouge, olive oil and beeswax are mixed, at 50 DEG C
Lower heating for dissolving, stirs evenly, and obtains mixture B.
(3) it is stirred after mixing mixture A and mixture B, dissolves by heating, stir evenly at 60 DEG C, keep the temperature 60min,
30min is recycled in emulsifying homogeneous machine, temperature at 60 DEG C, be cooled to room temperature to get to described without containing nano-cellulose
Cosmetic composition.
Reference examples 2
Reference examples of the present embodiment as embodiment 2, provide a kind of cosmetic composition without containing nano-cellulose and
Preparation method.
The cosmetic composition is made of following raw material by weight percentage:
Sorbierite 2.5%, polyethylene glycol 1%, ethylhexyl palmitate 2.5%, saualane 2%, glycerin monostearate
2%, hydrogenate lecithin 2.5%, Buddhist nun's platinum rouge 0.5%, sodium acrylate/ethylene isodecyl acid esters cross-linked polymer 3%, olive oil
2%, beeswax 2%, bis-ethylhexoxyphenol methoxyphenyl triazine 1%, titanium dioxide 0.7%, nordihydroguaiaretic acid (NDGA)
0.07%, essence 0.8% and water 77.43%.
The preparation method of the above-mentioned cosmetic composition without containing nano-cellulose, comprising the following steps:
(1) by sorbierite, polyethylene glycol, ethylhexyl palmitate, saualane, glycerin monostearate, hydrogenation lecithin,
Essence, nordihydroguaiaretic acid, bis-ethylhexoxyphenol methoxyphenyl triazine, titanium dioxide and deionized water mixing, at 90 DEG C
It dissolves by heating, stirs evenly, obtain mixture A.
(2) sodium acrylate/ethylene isodecyl acid esters cross-linked polymer, Buddhist nun's platinum rouge, olive oil and beeswax are mixed, at 80 DEG C
Lower heating for dissolving, stirs evenly, and obtains mixture B.
(3) it is stirred after mixing mixture A and mixture B, dissolves by heating, stir evenly at 80 DEG C, keep the temperature 30min,
30min is recycled in emulsifying homogeneous machine, temperature at 60 DEG C, be cooled to room temperature to get to described without containing nano-cellulose
Cosmetic composition.
Reference examples 3
Reference examples of the present embodiment as embodiment 3, provide a kind of cosmetic composition without containing nano-cellulose and
Preparation method.
The cosmetic composition is made of following raw material by weight percentage:
Sorbierite 1.5%, polyethylene glycol 2%, ethylhexyl palmitate 2%, saualane 3%, glycerin monostearate
3%, hydrogenation lecithin 2%, Buddhist nun's platinum rouge 0.8%, sodium acrylate/ethylene isodecyl acid esters cross-linked polymer 4%, olive oil 1%,
Beeswax 3%, bis-ethylhexoxyphenol methoxyphenyl triazine 1.5%, titanium dioxide 0.8%, nordihydroguaiaretic acid (NDGA)
0.08%, essence 0.8% and water 74.52%.
The preparation method of the above-mentioned cosmetic composition without containing nano-cellulose, comprising the following steps:
(1) by sorbierite, polyethylene glycol, ethylhexyl palmitate, saualane, glycerin monostearate, hydrogenation lecithin,
Essence, nordihydroguaiaretic acid, bis-ethylhexoxyphenol methoxyphenyl triazine, titanium dioxide and deionized water mixing, at 75 DEG C
It dissolves by heating, stirs evenly, obtain mixture A.
(2) sodium acrylate/ethylene isodecyl acid esters cross-linked polymer, Buddhist nun's platinum rouge, olive oil and beeswax are mixed, at 65 DEG C
Lower heating for dissolving, stirs evenly, and obtains mixture B.
(3) it is stirred after mixing mixture A and mixture B, dissolves by heating, stir evenly at 70 DEG C, keep the temperature 45min,
30min is recycled in emulsifying homogeneous machine, temperature at 60 DEG C, be cooled to room temperature to get to described without containing nano-cellulose
Cosmetic composition.
The cosmetic composition of Examples 1 to 3 and reference examples 1~3 is used one week to 30 volunteers, with 0~10 point
Scoring mechanism give the marking of following indices, the sum of overall assessment result=indices score/index quantity, evaluation index has
Appearance, smear, moistening effect, toughness.
The measuring method of moisturizing rate: each three parts of cosmetic composition of 2g are accurately weighed, are moved in culture dish, on balance
Culture dish, is then put into drier, weighs again after 8 hours by weighing, calculates moisturizing rate.
Moisturizing rate=M2/M1× 100%
M in formula1It is the example weight before placing, M2It is the example weight after placing.
The evaluation result of 1 skin-moisturizing, skin effect of table
| Sample | Skin sense top SCORES | Moisturizing rate |
| Embodiment 1 | 7 | 64% |
| Embodiment 2 | 8 | 72% |
| Embodiment 3 | 9 | 78% |
| Reference examples 1 | 6 | 54% |
| Reference examples 2 | 7 | 50% |
| Reference examples 3 | 6 | 56% |
The experimental results showed that, in embodiments of the present invention, the cosmetic composition skin sense of nano-cellulose is added in table 1
Scoring is high, and improves the moisturizing rate of cosmetic composition, and moisture preserving time is long, and soothing effect is significant.
Embodiment 4
The present embodiment provides a kind of cosmetic composition and its system containing nano-cellulose with whitening spot-removing function
Preparation Method.
The cosmetic composition is made of following raw material by weight percentage:
Nano-cellulose 20%, quinhydrones 2%, arbutin 1.5%, vitamin C 1.5%, glycerin monostearate 2.5%,
Hydrogenate lecithin 2.5%, Buddhist nun's platinum rouge 0.7%, sodium acrylate/ethylene isodecyl acid esters cross-linked polymer 3.5%, olive oil
1.5%, beeswax 2.5%, bis-ethylhexoxyphenol methoxyphenyl triazine 1.5%, titanium dioxide 0.6%, nordihydroguaiaretic acid
(NDGA) 0.05%, essence 0.6% and water 59.05%.
The preparation method of the above-mentioned cosmetic composition containing nano-cellulose with whitening spot-removing function, including it is following
Step:
(1) microcrystalline cellulose 1:20 in mass ratio is soluble in water, the homogeneous in high pressure homogenizer, homogenization pressure
20000psi, circular treatment 6 times, (quality that metal salt solution is added is cellulose solution quality to addition calcium chloride solution bridge joint
5%), obtain nano-cellulose gel after centrifugal concentrating.
(2) by nano-cellulose gel, quinhydrones, arbutin, vitamin C, glycerin monostearate, hydrogenation lecithin, perfume (or spice)
Essence, nordihydroguaiaretic acid, bis-ethylhexoxyphenol methoxyphenyl triazine, titanium dioxide and deionized water mixing, add at 60 DEG C
Heat of solution stirs evenly, and obtains mixture A.
(3) sodium acrylate/ethylene isodecyl acid esters cross-linked polymer, Buddhist nun's platinum rouge, olive oil and beeswax are mixed, at 50 DEG C
Lower heating for dissolving, stirs evenly, and obtains mixture B.
(4) it is stirred after mixing mixture A and mixture B, dissolves by heating, stir evenly at 60 DEG C, keep the temperature 60min,
It recycles 3 times, processing pressure 10MPa, is cooled to room temperature to get the change containing nano-cellulose is arrived in high pressure homogenizer
Cosmetic compositions.
Embodiment 5
The present embodiment provides a kind of cosmetic composition and its system containing nano-cellulose with whitening spot-removing function
Preparation Method.
The cosmetic composition is made of following raw material by weight percentage:
Nano-cellulose 30%, quinhydrones 2.5%, arbutin 1%, vitamin C 1%, glycerin monostearate 3%, hydrogenation
Lecithin 2%, Buddhist nun's platinum rouge 0.8%, sodium acrylate/ethylene isodecyl acid esters cross-linked polymer 4%, olive oil 1%, beeswax 3%,
Bis-ethylhexoxyphenol methoxyphenyl triazine 1.5%, titanium dioxide 0.8%, nordihydroguaiaretic acid (NDGA) 0.08%, essence
0.8% and water 48.52%.
The preparation method of the above-mentioned cosmetic composition containing nano-cellulose with whitening spot-removing function, including it is following
Step:
(1) microcrystalline cellulose 1:20 in mass ratio is soluble in water, the homogeneous in high pressure homogenizer, homogenization pressure
30000psi, circular treatment 3 times, (quality that metal salt solution is added is cellulose solution quality to addition magnesium chloride solution bridge joint
5%), obtain nano-cellulose gel after centrifugal concentrating.
(2) by nano-cellulose gel, quinhydrones, arbutin, vitamin C, glycerin monostearate, hydrogenation lecithin, perfume (or spice)
Essence, nordihydroguaiaretic acid, bis-ethylhexoxyphenol methoxyphenyl triazine, titanium dioxide and deionized water mixing, add at 90 DEG C
Heat of solution stirs evenly, and obtains mixture A.
(3) sodium acrylate/ethylene isodecyl acid esters cross-linked polymer, Buddhist nun's platinum rouge, olive oil and beeswax are mixed, at 80 DEG C
Lower heating for dissolving, stirs evenly, and obtains mixture B.
(4) it is stirred after mixing mixture A and mixture B, dissolves by heating, stir evenly at 80 DEG C, keep the temperature 30min,
It recycles 1 time, processing pressure 30MPa, is cooled to room temperature to get the change containing nano-cellulose is arrived in high pressure homogenizer
Cosmetic compositions.
Embodiment 6
The present embodiment provides a kind of cosmetic composition and its system containing nano-cellulose with whitening spot-removing function
Preparation Method.
The cosmetic composition is made of following raw material by weight percentage:
Nano-cellulose 50%, quinhydrones 2%, arbutin 1.5%, vitamin C 1.3%, glycerin monostearate 2%, hydrogen
Change lecithin 2.5%, Buddhist nun's platinum rouge 0.5%, sodium acrylate/ethylene isodecyl acid esters cross-linked polymer 3%, olive oil 2%, beeswax
2%, bis-ethylhexoxyphenol methoxyphenyl triazine 1%, titanium dioxide 0.7%, nordihydroguaiaretic acid (NDGA) 0.07%, perfume
Essence 0.8% and water 30.63%.
The preparation method of the above-mentioned cosmetic composition containing nano-cellulose with whitening spot-removing function, including it is following
Step:
(1) microcrystalline cellulose 1:20 in mass ratio is soluble in water, the homogeneous in high pressure homogenizer, homogenization pressure
25000psi, circular treatment 4 times, (quality that metal salt solution is added is cellulose solution quality to addition sodium chloride solution bridge joint
5%), obtain nano-cellulose gel after centrifugal concentrating.
(2) by nano-cellulose gel, quinhydrones, arbutin, vitamin C, glycerin monostearate, hydrogenation lecithin, perfume (or spice)
Essence, nordihydroguaiaretic acid, bis-ethylhexoxyphenol methoxyphenyl triazine, titanium dioxide and deionized water mixing, add at 75 DEG C
Heat of solution stirs evenly, and obtains mixture A.
(3) sodium acrylate/ethylene isodecyl acid esters cross-linked polymer, Buddhist nun's platinum rouge, olive oil and beeswax are mixed, at 65 DEG C
Lower heating for dissolving, stirs evenly, and obtains mixture B.
(4) it is stirred after mixing mixture A and mixture B, dissolves by heating, stir evenly at 70 DEG C, keep the temperature 45min,
It recycles 2 times, processing pressure 20MPa, is cooled to room temperature to get the change containing nano-cellulose is arrived in high pressure homogenizer
Cosmetic compositions.
Reference examples 4
Reference examples of the present embodiment as embodiment 4, provide a kind of cosmetic composition without containing nano-cellulose and
Preparation method.
The cosmetic composition is made of following raw material by weight percentage:
Quinhydrones 2%, arbutin 1.5%, vitamin C 1.5%, glycerin monostearate 2.5% hydrogenate lecithin 2.5%,
Buddhist nun's platinum rouge 0.7%, sodium acrylate/ethylene isodecyl acid esters cross-linked polymer 3.5%, olive oil 1.5%, beeswax 2.5%, double-
Ethyl hexyl oxy phenol anisyl triazine 1.5%, titanium dioxide 0.6%, nordihydroguaiaretic acid (NDGA) 0.05%, essence
0.6% and water 79.05%.
The preparation method of the above-mentioned cosmetic composition without containing nano-cellulose, comprising the following steps:
(1) by quinhydrones, arbutin, vitamin C, glycerin monostearate, hydrogenation lecithin, essence, nordihydroguaiaretic acid,
Bis-ethylhexoxyphenol methoxyphenyl triazine, titanium dioxide and deionized water mixing, dissolve by heating at 60 DEG C, stir evenly,
Obtain mixture A.
(2) sodium acrylate/ethylene isodecyl acid esters cross-linked polymer, Buddhist nun's platinum rouge, olive oil and beeswax are mixed, at 50 DEG C
Lower heating for dissolving, stirs evenly, and obtains mixture B.
(3) it is stirred after mixing mixture A and mixture B, dissolves by heating, stir evenly at 60 DEG C, keep the temperature 60min,
Recycled 3 times, processing pressure 10MPa in high pressure homogenizer, be cooled to room temperature to get to described without containing nano-cellulose
Cosmetic composition.
Reference examples 5
Reference examples of the present embodiment as embodiment 5, provide a kind of cosmetic composition without containing nano-cellulose and
Preparation method.
The cosmetic composition is made of following raw material by weight percentage:
Quinhydrones 2.5%, arbutin 1%, vitamin C 1%, glycerin monostearate 3% hydrogenate lecithin 2%, Buddhist nun's platinum
Rouge 0.8%, sodium acrylate/ethylene isodecyl acid esters cross-linked polymer 4%, olive oil 1%, beeswax 3%, double-ethyl hexyl oxy phenol
Anisyl triazine 1.5%, titanium dioxide 0.8%, nordihydroguaiaretic acid (NDGA) 0.08%, essence 0.8% and water
78.52%.
The preparation method of the above-mentioned cosmetic composition without containing nano-cellulose, comprising the following steps:
(1) by quinhydrones, arbutin, vitamin C, glycerin monostearate, hydrogenation lecithin, essence, nordihydroguaiaretic acid,
Bis-ethylhexoxyphenol methoxyphenyl triazine, titanium dioxide and deionized water mixing, dissolve by heating at 90 DEG C, stir evenly,
Obtain mixture A.
(2) sodium acrylate/ethylene isodecyl acid esters cross-linked polymer, Buddhist nun's platinum rouge, olive oil and beeswax are mixed, at 80 DEG C
Lower heating for dissolving, stirs evenly, and obtains mixture B.
(3) it is stirred after mixing mixture A and mixture B, dissolves by heating, stir evenly at 80 DEG C, keep the temperature 30min,
Recycled 1 time, processing pressure 30MPa in high pressure homogenizer, be cooled to room temperature to get to described without containing nano-cellulose
Cosmetic composition.
Reference examples 6
Reference examples of the present embodiment as embodiment 6, provide a kind of cosmetic composition without containing nano-cellulose and
Preparation method.
The cosmetic composition is made of following raw material by weight percentage:
Quinhydrones 2%, arbutin 1.5%, vitamin C 1.3%, glycerin monostearate 2% hydrogenate lecithin 2.5%, Buddhist nun
Platinum rouge 0.5%, sodium acrylate/ethylene isodecyl acid esters cross-linked polymer 3%, olive oil 2%, beeswax 2%, double-ethyl hexyl oxygen
Phenol anisyl triazine 1%, titanium dioxide 0.7%, nordihydroguaiaretic acid (NDGA) 0.07%, essence 0.8% and water
80.63%.
The preparation method of the above-mentioned cosmetic composition without containing nano-cellulose, comprising the following steps:
(1) by quinhydrones, arbutin, vitamin C, glycerin monostearate, hydrogenation lecithin, essence, nordihydroguaiaretic acid,
Bis-ethylhexoxyphenol methoxyphenyl triazine, titanium dioxide and deionized water mixing, dissolve by heating at 75 DEG C, stir evenly,
Obtain mixture A.
(2) sodium acrylate/ethylene isodecyl acid esters cross-linked polymer, Buddhist nun's platinum rouge, olive oil and beeswax are mixed, at 65 DEG C
Lower heating for dissolving, stirs evenly, and obtains mixture B.
(3) it is stirred after mixing mixture A and mixture B, dissolves by heating, stir evenly at 70 DEG C, keep the temperature 45min,
Recycled 2 times, processing pressure 20MPa in high pressure homogenizer, be cooled to room temperature to get to described without containing nano-cellulose
Cosmetic composition.
The detection method of whitening spot-removing effect: selection volunteer 40 uses embodiment 4~6 and reference examples 4~6 respectively
In cosmetics, using at face's color spot as trial zone, every morning to face's color spot smear, persistently use one month, observe face
Portion's Colour patterns situation.
The evaluation result of 2 whitening spot-removing effect of table
The experimental results showed that, in embodiments of the present invention, the cosmetic composition whitening of nano-cellulose is added in table 2
Freckle effect is better than being not added with the cosmetic composition of nano-cellulose, and it is obvious to promote effect to the cosmetics of whitening spot-removing.
Embodiment 7
The present embodiment provides a kind of cosmetic compositions and its system containing nano-cellulose with the crease-resistant function of smoothing wrinkle
Preparation Method.
The cosmetic composition is made of following raw material by weight percentage:
Nano-cellulose 20%, Sodium Hyaluronate 2%, collagen 1.5%, mate leaf extract 2% are single stearic
Acid glyceride 2.5% hydrogenates lecithin 2.5%, Buddhist nun's platinum rouge 0.7%, sodium acrylate/ethylene isodecyl acid esters cross-linked polymer
3.5%, olive oil 1.5%, beeswax 2.5%, bis-ethylhexoxyphenol methoxyphenyl triazine 1.5%, titanium dioxide 0.6%, just
Dihydro traumatic acid (NDGA) 0.05%, essence 0.6% and water 58.55%.
The preparation method of the above-mentioned cosmetic composition containing nano-cellulose with the crease-resistant function of smoothing wrinkle, including it is following
Step:
(1) microcrystalline cellulose 1:20 in mass ratio is soluble in water, the homogeneous in high pressure homogenizer, homogenization pressure
20000psi, circular treatment 6 times, (quality that metal salt solution is added is cellulose solution quality to addition calcium chloride solution bridge joint
5%), obtain nano-cellulose gel after centrifugal concentrating.
(2) by nano-cellulose gel, Sodium Hyaluronate, collagen, mate leaf extract, glycerol monostearate
Ester, hydrogenation lecithin, essence, nordihydroguaiaretic acid, bis-ethylhexoxyphenol methoxyphenyl triazine, titanium dioxide and deionization
Water mixing, dissolves by heating at 60 DEG C, stirs evenly, obtain mixture A.
(3) sodium acrylate/ethylene isodecyl acid esters cross-linked polymer, Buddhist nun's platinum rouge, olive oil and beeswax are mixed, at 50 DEG C
Lower heating for dissolving, stirs evenly, and obtains mixture B.
(4) it is stirred after mixing mixture A and mixture B, dissolves by heating, stir evenly at 60 DEG C, keep the temperature 60min,
It recycles 3 times, processing pressure 10MPa, is cooled to room temperature to get the change containing nano-cellulose is arrived in high pressure homogenizer
Cosmetic compositions.
Embodiment 8
The present embodiment provides a kind of cosmetic compositions and its system containing nano-cellulose with the crease-resistant function of smoothing wrinkle
Preparation Method.
The cosmetic composition is made of following raw material by weight percentage:
Nano-cellulose 30%, Sodium Hyaluronate 1%, collagen 2%, mate leaf extract 2.5% are single stearic
Acid glyceride 2%, hydrogenation lecithin 2.5%, Buddhist nun's platinum rouge 0.5%, sodium acrylate/ethylene isodecyl acid esters cross-linked polymer 3%,
Olive oil 2%, beeswax 2%, bis-ethylhexoxyphenol methoxyphenyl triazine 1%, titanium dioxide 0.7%, nordihydroguaiaretic acid
(NDGA) 0.07%, essence 0.8% and water 49.93%.
The preparation method of the above-mentioned cosmetic composition containing nano-cellulose with the crease-resistant function of smoothing wrinkle, including it is following
Step:
(1) microcrystalline cellulose 1:20 in mass ratio is soluble in water, the homogeneous in high pressure homogenizer, homogenization pressure
30000psi, circular treatment 3 times, (quality that metal salt solution is added is cellulose solution quality to addition magnesium chloride solution bridge joint
5%), obtain nano-cellulose gel after centrifugal concentrating.
(2) by nano-cellulose gel, Sodium Hyaluronate, collagen, mate leaf extract, glycerol monostearate
Ester, hydrogenation lecithin, essence, nordihydroguaiaretic acid, bis-ethylhexoxyphenol methoxyphenyl triazine, titanium dioxide and deionization
Water mixing, dissolves by heating at 90 DEG C, stirs evenly, obtain mixture A.
(3) sodium acrylate/ethylene isodecyl acid esters cross-linked polymer, Buddhist nun's platinum rouge, olive oil and beeswax are mixed, at 80 DEG C
Lower heating for dissolving, stirs evenly, and obtains mixture B.
(4) it is stirred after mixing mixture A and mixture B, dissolves by heating, stir evenly at 80 DEG C, keep the temperature 30min,
It recycles 1 time, processing pressure 30MPa, is cooled to room temperature to get the change containing nano-cellulose is arrived in high pressure homogenizer
Cosmetic compositions.
Embodiment 9
The present embodiment provides a kind of cosmetic compositions and its system containing nano-cellulose with the crease-resistant function of smoothing wrinkle
Preparation Method.
The cosmetic composition is made of following raw material by weight percentage:
Nano-cellulose 50%, Sodium Hyaluronate 2%, collagen 2.5%, mate leaf extract 3% are single stearic
Acid glyceride 3% hydrogenates lecithin 2%, Buddhist nun's platinum rouge 0.8%, sodium acrylate/ethylene isodecyl acid esters cross-linked polymer 4%, olive
Olive oil 1%, beeswax 3%, bis-ethylhexoxyphenol methoxyphenyl triazine 1.5%, titanium dioxide 0.8%, nordihydroguaiaretic acid
(NDGA) 0.08%, essence 0.8% and water 28.52%.
The preparation method of the above-mentioned cosmetic composition containing nano-cellulose with the crease-resistant function of smoothing wrinkle, including it is following
Step:
(1) microcrystalline cellulose 1:20 in mass ratio is soluble in water, the homogeneous in high pressure homogenizer, homogenization pressure
25000psi, circular treatment 4 times, (quality that metal salt solution is added is cellulose solution quality to addition sodium chloride solution bridge joint
5%), obtain nano-cellulose gel after centrifugal concentrating.
(2) by nano-cellulose gel, Sodium Hyaluronate, collagen, mate leaf extract, glycerol monostearate
Ester, hydrogenation lecithin, essence, nordihydroguaiaretic acid, bis-ethylhexoxyphenol methoxyphenyl triazine, titanium dioxide and deionization
Water mixing, dissolves by heating at 75 DEG C, stirs evenly, obtain mixture A.
(3) sodium acrylate/ethylene isodecyl acid esters cross-linked polymer, Buddhist nun's platinum rouge, olive oil and beeswax are mixed, at 65 DEG C
Lower heating for dissolving, stirs evenly, and obtains mixture B.
(4) it is stirred after mixing mixture A and mixture B, dissolves by heating, stir evenly at 70 DEG C, keep the temperature 45min,
It recycles 2 times, processing pressure 20MPa, is cooled to room temperature to get the change containing nano-cellulose is arrived in high pressure homogenizer
Cosmetic compositions.
Reference examples 7
Reference examples of the present embodiment as embodiment 7, provide a kind of cosmetic composition without containing nano-cellulose and
Preparation method.
The cosmetic composition is made of following raw material by weight percentage:
Sodium Hyaluronate 2%, collagen 1.5%, mate leaf extract 2%, glycerin monostearate 2.5%,
Hydrogenate lecithin 2.5%, Buddhist nun's platinum rouge 0.7%, sodium acrylate/ethylene isodecyl acid esters cross-linked polymer 3.5%, olive oil
1.5%, beeswax 2.5%, bis-ethylhexoxyphenol methoxyphenyl triazine 1.5%, titanium dioxide 0.6%, nordihydroguaiaretic acid
(NDGA) 0.05%, essence 0.6% and water 78.55%.
The preparation method of the above-mentioned cosmetic composition without containing nano-cellulose, comprising the following steps:
(1) by Sodium Hyaluronate, collagen, mate leaf extract, glycerin monostearate, hydrogenation lecithin,
Essence, nordihydroguaiaretic acid, bis-ethylhexoxyphenol methoxyphenyl triazine, titanium dioxide and deionized water mixing, at 60 DEG C
It dissolves by heating, stirs evenly, obtain mixture A.
(2) sodium acrylate/ethylene isodecyl acid esters cross-linked polymer, Buddhist nun's platinum rouge, olive oil and beeswax are mixed, at 50 DEG C
Lower heating for dissolving, stirs evenly, and obtains mixture B.
(3) it is stirred after mixing mixture A and mixture B, dissolves by heating, stir evenly at 60 DEG C, keep the temperature 60min,
Recycled 3 times, processing pressure 10MPa in high pressure homogenizer, be cooled to room temperature to get to described without containing nano-cellulose
Cosmetic composition.
Reference examples 8
Reference examples of the present embodiment as embodiment 8, provide a kind of cosmetic composition without containing nano-cellulose and
Preparation method.
The cosmetic composition is made of following raw material by weight percentage:
Sodium Hyaluronate 1%, collagen 2%, mate leaf extract 2.5%, glycerin monostearate 2%, hydrogen
Change lecithin 2.5%, Buddhist nun's platinum rouge 0.5%, sodium acrylate/ethylene isodecyl acid esters cross-linked polymer 3%, olive oil 2%, beeswax
2%, bis-ethylhexoxyphenol methoxyphenyl triazine 1%, titanium dioxide 0.7%, nordihydroguaiaretic acid (NDGA) 0.07%, perfume
Essence 0.8% and water 79.93%.
The preparation method of the above-mentioned cosmetic composition without containing nano-cellulose, comprising the following steps:
(1) by Sodium Hyaluronate, collagen, mate leaf extract, glycerin monostearate, hydrogenation lecithin,
Essence, nordihydroguaiaretic acid, bis-ethylhexoxyphenol methoxyphenyl triazine, titanium dioxide and deionized water mixing, at 90 DEG C
It dissolves by heating, stirs evenly, obtain mixture A.
(2) sodium acrylate/ethylene isodecyl acid esters cross-linked polymer, Buddhist nun's platinum rouge, olive oil and beeswax are mixed, at 80 DEG C
Lower heating for dissolving, stirs evenly, and obtains mixture B.
(3) it is stirred after mixing mixture A and mixture B, dissolves by heating, stir evenly at 80 DEG C, keep the temperature 30min,
Recycled 1 time, processing pressure 30MPa in high pressure homogenizer, be cooled to room temperature to get to described without containing nano-cellulose
Cosmetic composition.
Reference examples 9
Reference examples of the present embodiment as embodiment 9, provide a kind of cosmetic composition without containing nano-cellulose and
Preparation method.
The cosmetic composition is made of following raw material by weight percentage:
Sodium Hyaluronate 2%, collagen 2.5%, mate leaf extract 3%, glycerin monostearate 3%, hydrogen
Change lecithin 2%, Buddhist nun's platinum rouge 0.8%, sodium acrylate/ethylene isodecyl acid esters cross-linked polymer 4%, olive oil 1%, beeswax
3%, bis-ethylhexoxyphenol methoxyphenyl triazine 1.5%, titanium dioxide 0.8%, nordihydroguaiaretic acid (NDGA) 0.08%,
Essence 0.8% and water 75.52%.
The preparation method of the above-mentioned cosmetic composition without containing nano-cellulose, comprising the following steps:
(1) by Sodium Hyaluronate, collagen, mate leaf extract, glycerin monostearate, hydrogenation lecithin,
Essence, nordihydroguaiaretic acid, bis-ethylhexoxyphenol methoxyphenyl triazine, titanium dioxide and deionized water mixing, at 75 DEG C
It dissolves by heating, stirs evenly, obtain mixture A.
(2) sodium acrylate/ethylene isodecyl acid esters cross-linked polymer, Buddhist nun's platinum rouge, olive oil and beeswax are mixed, at 65 DEG C
Lower heating for dissolving, stirs evenly, and obtains mixture B.
(3) it is stirred after mixing mixture A and mixture B, dissolves by heating, stir evenly at 70 DEG C, keep the temperature 45min,
Recycled 2 times, processing pressure 20MPa in high pressure homogenizer, be cooled to room temperature to get to described without containing nano-cellulose
Cosmetic composition.
The detection method of smoothing wrinkle anti-wrinkle effect: selection volunteer 40 uses embodiment 7~9 and reference examples 7~9 respectively
In cosmetics, using at face wrinkles as trial zone, every morning to face wrinkles smear, persistently use one month, observe face
Portion's wrinkle situation of change.
The crease-resistant evaluation result of 3 smoothing wrinkle of table
The experimental results showed that, each product is to the improvement degree of facial wrinkles than respectively producing in reference examples in embodiment in table 3
The improvement degree of product will be high, illustrates that the cosmetic composition for being added to nano-cellulose is able to ascend smoothing wrinkle anti-wrinkle effect, right
The improvement of wrinkle is significant.
The above embodiment is a preferred embodiment of the present invention, but embodiments of the present invention are not by above-described embodiment
Limitation, other any changes, modifications, substitutions, combinations, simplifications made without departing from the spirit and principles of the present invention,
It should be equivalent substitute mode, be included within the scope of the present invention.
Claims (10)
1. a kind of cosmetic composition containing nano-cellulose, it is characterised in that: with the total weight of cosmetic composition, contain
There is 20%~50% nano-cellulose, the partial size of nano-cellulose is less than 100nm.
2. the cosmetic composition according to claim 1 containing nano-cellulose, it is characterised in that: the Nanowire
The partial size of dimension element is less than 60nm.
3. the cosmetic composition according to claim 1 or 2 containing nano-cellulose, it is characterised in that: described contains
The cosmetic composition for having nano-cellulose also includes thickener, emulsifier, antibacterial agent, finish, essence and deionized water, and is wrapped
Containing one or more of moisturizer, emollient, sun-screening agent, antioxidant, whitening spot-removing ingredient and the crease-resistant ingredient of smoothing wrinkle.
4. the cosmetic composition according to claim 3 containing nano-cellulose, it is characterised in that:
The moisturizer is one or more of glycerol, propylene glycol, sorbierite and polyethylene glycol；
The emollient is ethylhexyl palmitate, decyl oleate, saualane, phenethyl benzoate, cetanol lactate
One or more of with maleic acid ricinolein；
The sun-screening agent is zinc oxide, titanium dioxide, dimethyl PABA ethylhexyl, butylmethoxydibenzoylmethane
One or more of with bis-ethylhexoxyphenol methoxyphenyl triazine；
The antioxidant is tert-butyl hydroquinone, in glutamic acid, tocopherol, propylgallate, nordihydroguaiaretic acid (NDGA)
One or more；
The whitening spot-removing ingredient is one or more of quinhydrones, arbutin, kojic acid and vitamin C；
The crease-resistant ingredient of the smoothing wrinkle is that Sodium Hyaluronate, collagen, mate leaf extract and rose root of kirilow rhodiola extract
One of object is a variety of；
The emulsifier is one of glycerin monostearate, hydrolecithin, lanolin and the smooth olive oleate of sorb
Or it is two or more；
The antibacterial agent is one or more of Buddhist nun's platinum rouge, p-hydroxybenzoate, benzyl alcohol, dehydroacetic acid；
The thickener is hydroxyethyl cellulose, carboxymethyl cellulose, sodium alginate, PEG-80 glyceryl butter ester and propylene
One or more of sour sodium/ethylene isodecyl acid esters cross-linked polymer；
The finish is one or more of olive oil, stearate, beeswax, silicone oil and vaseline.
5. the cosmetic composition according to claim 4 containing nano-cellulose, it is characterised in that:
The content of the moisturizer is the 1%~5% of cosmetic composition total weight；
The content of the emollient is the 1%~5% of cosmetic composition total weight；
The content of the sun-screening agent is the 0.5%~3% of cosmetic composition total weight；
The content of the antioxidant is the 0.01%~0.1% of cosmetic composition total weight；
The content of the whitening spot-removing ingredient is the 2%~6% of cosmetic composition total weight；
The content of the crease-resistant ingredient of the smoothing wrinkle is the 2~6% of cosmetic composition total weight；
The content of the emulsifier is the 3%~6% of cosmetic composition total weight；
The content of the antibacterial agent is the 0.1%~2% of cosmetic composition total weight；
The content of the thickener is the 2%~5% of cosmetic composition total weight；
The content of the finish is the 2%~5% of cosmetic composition total weight；
The content of the essence is the 0.5%~1% of cosmetic composition total weight.
6. the cosmetic composition according to claim 5 containing nano-cellulose, it is characterised in that:
The content of the emollient is the 2%~4% of cosmetic composition total weight；
The content of the sun-screening agent is the 1.7%~2.3% of cosmetic composition total weight；
The content of the antioxidant is the 0.05%~0.08% of cosmetic composition total weight；
The content of the whitening spot-removing ingredient is the 3%~5% of cosmetic composition total weight；
The content of the crease-resistant ingredient of the smoothing wrinkle is the 3~5% of cosmetic composition total weight；
The content of the emulsifier is the 4%~5% of cosmetic composition total weight；
The content of the antibacterial agent is the 0.5%~0.8% of cosmetic composition total weight；
The content of the thickener is the 3%~4% of cosmetic composition total weight；
The content of the finish is the 3%~4% of cosmetic composition total weight；
The content of the essence is the 0.6%~0.8% of cosmetic composition total weight.
7. the cosmetic composition according to claim 4 containing nano-cellulose, it is characterised in that；By it is following by weight
The raw material of percentages forms:
Above-mentioned raw materials weight adds up to 100%；
Or it is made of following raw material by weight percentage:
Above-mentioned raw materials weight adds up to 100%；
Or it is made of following raw material by weight percentage:
Above-mentioned raw materials weight adds up to 100%.
8. the preparation method of the cosmetic composition described in claim 3~7 Arbitrary Term containing nano-cellulose, feature exist
In including the following steps:
(1) preparation of nano-cellulose
Microcrystalline cellulose is soluble in water, it is high-pressure homogeneous, cellulose solution is obtained, metal salt solution bridge joint is added, is centrifuged dense
Contracting, obtains nano-cellulose gel；
(2) preparation of water phase
By nano-cellulose gel, moisturizer, emollient, whitening spot-removing ingredient, the crease-resistant ingredient of smoothing wrinkle, sun-screening agent, emulsifier, perfume (or spice)
Essence, antioxidant and deionized water mixing, dissolve by heating, stir evenly, obtain mixture A；
(3) preparation of oily phase
Thickener, vitamin derivative, antibacterial agent and finish are mixed, is dissolved by heating, is stirred evenly, obtain mixture B；
(4) preparation of cosmetic composition
Mixture A and mixture B is mixed, is stirred evenly, is dissolved by heating, heat preservation, then high pressure or emulsifying homogeneous, it is cooled to room
Temperature to get arrive the cosmetic composition containing nano-cellulose.
9. the preparation method of the cosmetic composition according to claim 8 containing nano-cellulose, it is characterised in that:
When described in step (1) that microcrystalline cellulose is soluble in water, the mass ratio of microcrystalline cellulose and water is 1:20；
High-pressure homogeneous pressure described in step (1) be 20000~30000psi, circular treatment 3~6 times；
Metal salt solution described in step (1) is one of calcium chloride solution, magnesium chloride solution and sodium chloride solution or two
Kind or more；
The quality that metal salt solution is added described in step (1) is the 3~6% of cellulose solution quality.
10. the preparation method of the cosmetic composition according to claim 8 containing nano-cellulose, it is characterised in that:
The temperature of heating for dissolving described in step (2) is 60~90 DEG C；
The temperature of heating for dissolving described in step (3) is 50~80 DEG C；
The temperature of heating for dissolving described in step (4) is 60~80 DEG C, when a length of 30~60min of heat preservation；
High-pressure homogeneous described in step (4) to be carried out using high pressure homogenizer, pressure is 10~30MPa, is recycled 1~3 time；
Emulsifying homogeneous described in step (4) is carried out using emulsifying homogeneous machine, and temperature is 60 DEG C, recycles 30min.
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| CN112169008A (en) * | 2020-09-29 | 2021-01-05 | 代晓娟 | Preparation method of medical dressing based on human collagen |
| CN112641704A (en) * | 2020-12-31 | 2021-04-13 | 重庆知翔科技有限公司 | Moisturizing composition and preparation method thereof |
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