CN109125215A

CN109125215A - A kind of amino acid is had no time clean face powder

Info

Publication number: CN109125215A
Application number: CN201811232242.8A
Authority: CN
Inventors: 徐宇辉
Original assignee: Shanghai Huangming Cultural Communication Co Ltd
Current assignee: Shanghai Huangming Cultural Communication Co Ltd
Priority date: 2018-10-22
Filing date: 2018-10-22
Publication date: 2019-01-04

Abstract

The present invention relates to face-cleaning articles field, a kind of amino acid is provided and is had no time clean face powder and preparation method thereof, the effect of the protection skin for improving clean face powder.A kind of amino acid provided by the invention is had no time clean face powder, including 16 ~ 20 mass parts of sodium lauroyl glutamate, 15 ~ 25 mass parts of cornstarch, 1 ~ 5 mass parts of trehalose, 0.2 ~ 3 mass parts of 3-o- ethylascorbyl, 0.1 ~ 1 mass parts of carnosine, 2 ~ 6 mass parts of Chinese medical extract.Chinese medical extract, cornstarch, sodium lauroyl glutamate, trehalose, ascorbic acid, carnosine are compounded into clean face powder obtained, there is the effect of excellent cleaning and protection skin, it is small to the irritation of skin.

Description

A kind of amino acid is had no time clean face powder

Technical field

The present invention relates to face-cleaning articles fields, and in particular to a kind of amino acid is had no time clean face powder.

Background technique

Face cleaning or clean face always are a mostly important link of skin care.The skin of people, especially skin of face, when Quarter is all in contact with external environment.Dust, the smog, microorganism to suspend in air, is all easily absorbing on our skins； The sebum of smegma is easy after retaining for a long time by air oxidation and bacterial decomposition, harmful skin；Sweat evaporation can will be consolidated Body object secretion etc. remains in skin surface, stimulates skin；The skin of dead cell meeting and secretion that cuticula metabolism falls off Together, attachment generates dirt on the skin for rouge, sweat and external dust, interferes the secretion of sebum and sweat, breeds bacterium；It is right For the people often to make up, foundation cream, kermes, eye shadow, the lipstick etc. being coated on the face are easily absorbing on the skin.If skin is cleared up Not enough thoroughly, it is easy to cause clogging of pores, the problems such as skin water oil is unbalance, sensibility skin, skin ageing.

Popular face cleaning product currently on the market is divided into soap base, table work, soap table compound system, not special according to respective skin Point, which is distinguished, to be used, and is easy to keep cuticula thinning over time, or even destroy skin barrier, is become sensitive skin.Clean face powder is mesh Relatively mild product in preceding cleaning class skin care item, while helping skin cleaning, moreover it is possible to the allergy rate for reducing skin, by wide Big women's pursues.In today that beauty market makes rapid progress, clean face powder has been increasingly becoming irreplaceable one of clean skin product. But clean face powder manufacturing technology currently on the market is uniformly mixed powder material is fine ground, there are different solid powders it Between the problem of being settled because of density difference, the disadvantages of when use easily causes powder spreading.Amino acid cleansing product be at present more Pro-skin, mild face cleaning product, not tight with rear skin, moisture-retaining capacity is strong, is the cleaning products that sensitive flesh is suitble to use.But ammonia Base acid surfaces activating agent foaminess and cleaning capacity are general.

Summary of the invention

Present invention solves the technical problem that improve the effect of the protection skin of clean face powder, provide a kind of amino acid have no time it is clean Yan Fen.

In order to solve the above technical problem, the present invention provides technical solution are as follows:

A kind of amino acid is had no time clean face powder, including 16 ~ 20 mass parts of sodium lauroyl glutamate, 15 ~ 25 mass parts of cornstarch, sea 1 ~ 5 mass parts of algae sugar, 0.2 ~ 3 mass parts of 3-o- ethylascorbyl, 0.1 ~ 1 mass parts of carnosine, 2 ~ 6 mass of Chinese medical extract Part.

Ascorbic acid can have significant whitening effect, and sodium lauroyl glutamate, trehalose have significant moistening effect, special The carnosine of " skin cleans husband " Jia Ru be referred to as, hydration moisture-keeping function is formed with natural plants acidic amino acid, make unique Tender skin technology is purified, mildly can meet different skin quality cleanliness requirements, more flesh in effective deep layer cleaning skin, deep net clear flesh bottom Skin injects the tender skin factor of moisturizing, allows the more soft and smooth delicacy of clean skin, and cornstarch has certain adhesive effect, for being granulated, at Divide day heat, it is smaller to the harm of skin.

Chinese medical extract, cornstarch, sodium lauroyl glutamate, trehalose, ascorbic acid, carnosine compounding is obtained clean Yan Fen has the effect of excellent cleaning and protection skin, small to the irritation of skin.

Preferably, including 18 ~ 20 mass parts of sodium lauroyl glutamate, 17 ~ 25 mass parts of cornstarch, 3 ~ 5 matter of trehalose Measure part, 0.8 ~ 3 mass parts of 3-o- ethylascorbyl, 0.6 ~ 1 mass parts of carnosine, 4 ~ 6 mass parts of Chinese medical extract.Herein preferably In range, the face cleaning skin effect of clean face powder has more significant effect.

Preferably, including 18 mass parts of sodium lauroyl glutamate, 17 mass parts of cornstarch, 3 mass parts of trehalose, 3-o- 0.8 mass parts of ethylascorbyl, 0.6 mass parts of carnosine, 4 mass parts of Chinese medical extract.Clean face powder obtained is matched by this Irritation is minimum, while the effect of face cleaning skin care has more significant effect.

Preferably, the Chinese medical extract includes 1 ~ 5 mass parts of aloe extract, 2 ~ 4 mass of citrus young fruit extract Part, 2 ~ 5 mass parts of hens and chickens extract, 3 ~ 6 mass parts of Magnolia binodii extract, 3 ~ 8 mass parts of Kiwi extract are more Flower 3 ~ 5 mass parts of rye grass extract, 1 ~ 10 mass parts of marine algae extract, 2 ~ 7 mass parts of Radix Platycodonis extract, perilla leaf extract 4 ~ 6 mass parts, 1 ~ 3 mass parts of PORIA ALBA extract.Several Chinese medical extracts are compounded, can significant nourishes rough skin, make Skin slip is bright, delicate have no time, is fresh and clean；Aloe extract and marine algae extract have outstanding moistening effect；It spends more Rye grass, Magnolia binodii, perilla leaf compounding have certain bactericidal effect, the quality of skin can be improved；Radix Platycodonis extract and white Fu Siberian cocklebur extract can further eliminate the bacterium of skin surface；Contain a certain amount of ascorbic acid in Kiwi berry, it can be into one Walk skin whitening；Hens and chickens can effective nourishes rough skin.

Preferably, the Chinese medical extract includes 3 mass parts of aloe extract, 3 mass parts of citrus young fruit extract, room Push up long-living 4 mass parts of flower extract, 5 mass parts of Magnolia binodii extract, 4 mass parts of Kiwi extract, Itanlian rye extraction 4 mass parts of object, 6 mass parts of marine algae extract, 4 mass parts of Radix Platycodonis extract, 5 mass parts of perilla leaf extract, PORIA ALBA extract 2 mass parts of object.Chinese medical extract obtained is matched by this, there is more significant improvement skin, the effect of nourishes rough skin.

Preferably, the Chinese medical extract is made by the following method: by aloe, citrus young fruit, hens and chickens, prestige After spring flower, Itanlian rye, campanulaceae, perilla leaf, PORIA ALBA air-dry, is mixed after being milled to powder, obtain mixed-powder；It will mixing Powder ultrasonic extraction 20 ~ 50 minutes at 25 ~ 30 DEG C take supernatant, obtain primary extract after obtained mixed liquor centrifuge separation； Primary extract is passed through in macroporous absorbent resin and carries out adsorbing separation, is 30%-80% with the concentration expressed in percentage by volume of 100 ~ 150 mass parts The first ethanol solution heating and refluxing extraction 2-3 times, 0.5-2 hours each, filtering merges each secondary ethanol extract, recycles second Alcohol continues to be concentrated under reduced pressure to give the first medicinal extract to no alcohol taste；After marine algae extract is mixed with the ethyl alcohol of 20 ~ 30 mass parts, together The mixing of first medicinal extract, after mixing evenly, is concentrated under reduced pressure to give the second medicinal extract；Macroporous absorbent resin on the second obtained medicinal extract is used The water elution of 4-8 times of column volume discards water lotion, then the second second of the concentration expressed in percentage by volume 50%-100% with 3-8 times of column volume Alcoholic solution elution, collects ethanol elution part, recycles ethyl alcohol, is concentrated under reduced pressure, dry, obtains the first powder；Kiwifruit fruit is gone Skin is cleaned, freezes 90 ~ 150min after slice at -4 DEG C ~ -20 DEG C, and the deionized water mashing of 80 ~ 100 mass parts is added, is added PH is adjusted to 3 ~ 4 by citric acid, and pectase is added and stirs evenly, in 50 ~ 55 DEG C of 6 ~ 8h of hydrolysis, then adjusts pH to 7 ~ 7.5, pancreas is added Enzyme after mixing evenly, after 35 ~ 38 DEG C of 10 ~ 12h of hydrolysis, enzymatic hydrolysis, after mixed liquor ultrafiltration, takes filtrate, obtains after dry Second powder；Chinese medical extract is obtained after first powder and the second powder are mixed.Repeatedly extracting simultaneously will be in Traditional Chinese drug mixture Effective component adequately extract, obtained powder is to the nonirritant of skin；Effective component in kiwifruit fruit can Adequately to be extracted through enzyme；The two is mixed, obtained Chinese medical extract can effectively improve skin quality.

Preferably, the Chinese medical extract is made by the following method: by aloe, citrus young fruit, hens and chickens, prestige After spring flower, Itanlian rye, campanulaceae, perilla leaf, PORIA ALBA air-dry, is mixed after being milled to powder, obtain mixed-powder；It will mixing Powder ultrasonic extraction 30 minutes at 28 DEG C take supernatant, obtain primary extract after obtained mixed liquor centrifuge separation；It will just mention Object, which is passed through in macroporous absorbent resin, carries out adsorbing separation, the first ethanol solution for being 40% with the concentration expressed in percentage by volume of 120 mass parts Heating and refluxing extraction 3 times, 1.5 hours every time, filtering merged each secondary ethanol extract, recycles ethyl alcohol to no alcohol taste, continues to depressurize It is concentrated to get the first medicinal extract；After marine algae extract is mixed with the ethyl alcohol of 25 mass parts, mixes, stir evenly with the first medicinal extract Afterwards, it is concentrated under reduced pressure to give the second medicinal extract；Macroporous absorbent resin is discarded with the water elution of 6 times of column volumes on the second obtained medicinal extract Water lotion, then eluted with the second ethanol solution of the concentration expressed in percentage by volume 80% of 7 times of column volumes, collect ethanol elution part, recycling Ethyl alcohol is concentrated under reduced pressure, dry, obtains the first powder；It will be freezed at -10 DEG C after kiwifruit fruit peeling, clean, slice 100min is added the deionized water mashing of 90 mass parts, citric acid is added, pH is adjusted to 3.5, pectase is added and stirs evenly, 54 DEG C of hydrolysis 7h, then pH to 7.2 is adjusted, pancreatin is added after mixing evenly, after 37 DEG C of hydrolysis 11h, enzymatic hydrolysis, by mixed liquor After ultrafiltration, filtrate is taken, obtains the second powder after dry；Chinese medical extract is obtained after first powder and the second powder are mixed.It presses The Chinese medical extract that this technique is produced, which can effectively improve it, improves the effect of skin quality.

It preferably, further include 0.5 ~ 1 mass parts of modified active powdered carbon, the modified active in the Chinese medical extract Powdered carbon the preparation method comprises the following steps: by 3 ~ 5 mass parts of 1- methyl -3- butyl imidazole ionotropic glutamate liquid and 4 ~ 8 mass parts of glucose Mixing, uniform stirring 40min~60min, effect 30min~50min under 600W~800W microwave, addition deionized water 100 ~ 120 mass parts, obtain mixed solution；50 ~ 60 mass parts of active carbon powder are added in mixed solution, stir evenly, impregnate 40min~60min, 800W~1000W ultrasonic wave disperse 30min~40min, under 500W~800W microwave act on 30min~ 40min, filter, take filter residue, at a temperature of 80 DEG C~100 DEG C be dried in vacuo 12 ~ for 24 hours, obtain modified active powdered carbon.Active carbon can It is small to the irritation of skin to improve the cleaning effect of clean face powder, while by modified.

It preferably, further include 0.6 mass parts of modified active powdered carbon, the modified activated carbon in the Chinese medical extract Powder the preparation method comprises the following steps: 4 mass parts of 1- methyl -3- butyl imidazole ionotropic glutamate liquid and 6 mass parts of glucose are mixed, Even stirring 50min acts on 40min under 700W microwave, and 110 mass parts of deionized water are added, obtain mixed solution；It is molten mixing 55 mass parts of active carbon powder are added in liquid, stir evenly, impregnate 50min, 900W ultrasonic wave disperses 35min, in 600W microwave Lower effect 35min is filtered, is taken filter residue, be dried in vacuo 18h at a temperature of 90 DEG C, obtain modified active powdered carbon.It is made by this technique Modified activated carbon can be further improved its clean clean effect.

A kind of amino acid is had no time clean face powder, preparation method thereof, comprising the following steps: cornstarch is dissolved in 800 ~ 1000 mass In the deionized water of part；By sodium lauroyl glutamate, trehalose, 3-o- ethylascorbyl, carnosine, Chinese medical extract powder After mixing, 20 ~ 30min of fluidization dispersions at room temperature；Corn starch solution is sprayed on the powder of fluidization dispersions, is controlled Temperature is at 50 ~ 70 DEG C, and air mass flow is 800 ~ 1200m during controlling fluidization dispersions³/h；After having sprayed, continue at 50 ~ 70 DEG C 30 ~ 60min of fluidization dispersions, dried material；Material after drying is that amino acid is had no time clean face powder.Fluidization dispersions are generally fluidizing It is carried out in bed, the clean face powder as made from fluidization dispersions, uniformly, granular size is more consistent, can adequately guarantee product matter Amount.

Compared with prior art, the device have the advantages that are as follows: by Chinese medical extract, cornstarch, lauroyl paddy Propylhomoserin sodium, trehalose, ascorbic acid, carnosine compound clean face powder obtained, there is the effect of excellent cleaning and protection skin, right The irritation of skin is small.

Specific embodiment

Following implementation column is to further explanation of the invention, is not limitation of the present invention.

Embodiment 1

A kind of amino acid is had no time clean face powder, including 18 mass parts of sodium lauroyl glutamate, 17 mass parts of cornstarch, trehalose 3 Mass parts, 0.8 mass parts of 3-o- ethylascorbyl, 0.6 mass parts of carnosine, 4 mass parts of Chinese medical extract.The Chinese medicine mentions Taking object includes 3 mass parts of aloe extract, 3 mass parts of citrus young fruit extract, 4 mass parts of hens and chickens extract, prestige spring 5 mass parts of flower extract, 4 mass parts of Kiwi extract, 4 mass parts of Itanlian rye extract, 6 mass of marine algae extract Part, 4 mass parts of Radix Platycodonis extract, 5 mass parts of perilla leaf extract, 2 mass parts of PORIA ALBA extract.The Chinese medical extract It is made by the following method: by aloe, citrus young fruit, hens and chickens, Magnolia binodii, Itanlian rye, campanulaceae, perilla leaf, white After Poria cocos air-dries, is mixed after being milled to powder, obtain mixed-powder；By mixed-powder at 28 DEG C ultrasonic extraction 30 minutes, obtain After the mixed liquor centrifuge separation arrived, supernatant is taken, primary extract is obtained；Primary extract is passed through in macroporous absorbent resin and carries out absorption point From, with the first ethanol solution heating and refluxing extraction 3 times that the concentration expressed in percentage by volumes of 120 mass parts is 40%, 1.5 hours every time, mistake Filter merges each secondary ethanol extract, recycles ethyl alcohol to no alcohol taste, continues to be concentrated under reduced pressure to give the first medicinal extract；By marine algae extract After the ethyl alcohol mixing of 25 mass parts, is mixed with the first medicinal extract, after mixing evenly, be concentrated under reduced pressure to give the second medicinal extract；It obtains Macroporous absorbent resin on second medicinal extract discards water lotion, then the volume basis with 7 times of column volumes with the water elution of 6 times of column volumes Second ethanol solution of concentration 80% elutes, and collects ethanol elution part, recycles ethyl alcohol, is concentrated under reduced pressure, dry, obtains the first powder； 100min will be freezed at -10 DEG C after kiwifruit fruit peeling, clean, slice, the deionized water mashing of 90 mass parts is added, adds Enter citric acid, pH is adjusted to 3.5, pectase is added and stirs evenly, in 54 DEG C of hydrolysis 7h, then adjusts pH to 7.2, pancreatin stirring is added After uniformly, after 37 DEG C of hydrolysis 11h, enzymatic hydrolysis, after mixed liquor ultrafiltration, filtrate is taken, obtains the second powder after dry；By One powder and the second powder obtain Chinese medical extract after mixing.It further include modified active powdered carbon 0.6 in the Chinese medical extract Mass parts, the modified active powdered carbon the preparation method comprises the following steps: by 4 mass of 1- methyl -3- butyl imidazole ionotropic glutamate liquid Part and the mixing of 6 mass parts of glucose, uniform stirring 50min act on 40min under 700W microwave, and 110 mass of deionized water is added Part, obtain mixed solution；55 mass parts of active carbon powder are added in mixed solution, stir evenly, impregnate 50min, 900W is super Sound wave disperses 35min, and 35min is acted under 600W microwave, filters, takes filter residue, be dried in vacuo 18h at a temperature of 90 DEG C, obtain Modified active powdered carbon.

Chinese medical extract, cornstarch, sodium lauroyl glutamate, trehalose, ascorbic acid, carnosine compounding is obtained clean Yan Fen has the effect of excellent cleaning and protection skin, small to the irritation of skin.Several Chinese medical extracts are answered Match, can significant nourishes rough skin, make that skin slip is bright, delicate have no time, is fresh and clean；Aloe extract and marine algae extract have Outstanding moistening effect；Itanlian rye, Magnolia binodii, perilla leaf compounding have certain bactericidal effect, skin can be improved Quality；Radix Platycodonis extract and PORIA ALBA extract can further eliminate the bacterium of skin surface；Containing certain in Kiwi berry The ascorbic acid of amount, can further skin whitening；Hens and chickens can effective nourishes rough skin.Repeatedly extract simultaneously will in Effective component in medicine mixture adequately extracts, and obtained powder is to the nonirritant of skin；In kiwifruit fruit Effective component can adequately be extracted through enzyme；The two is mixed, obtained Chinese medical extract can effectively improve skin quality.It is living Property charcoal the cleaning effect of clean face powder can be improved, it is small to the irritation of skin while by modified.

A kind of amino acid is had no time face cleaning powder, preparation method thereof, comprising the following steps: cornstarch is dissolved in 1000 mass parts In deionized water；The powder of sodium lauroyl glutamate, trehalose, 3-o- ethylascorbyl, carnosine, Chinese medical extract is mixed After uniformly, fluidization dispersions 30min at room temperature；Corn starch solution is sprayed on the powder of fluidization dispersions, control temperature exists 70 DEG C, air mass flow is 1200m during controlling fluidization dispersions³/h；After having sprayed, continue to do in 70 DEG C of fluidization dispersion 60min Dry material；Material after drying is that amino acid is had no time clean face powder.

Fluidization dispersions generally carry out in a fluidized bed, and the clean face powder as made from fluidization dispersions, uniformly, granular size is more Unanimously, it can adequately guarantee product quality.

Embodiment 2

Embodiment 2 with embodiment 1 the difference is that, including 16 mass parts of sodium lauroyl glutamate, 15 mass parts of cornstarch, 1 mass parts of trehalose, 0.2 mass parts of 3-o- ethylascorbyl, 0.1 mass parts of carnosine, 2 mass parts of Chinese medical extract.It is described Chinese medical extract include 1 mass parts of aloe extract, 2 mass parts of citrus young fruit extract, 2 mass of hens and chickens extract Part, 3 mass parts of Magnolia binodii extract, 3 mass parts of Kiwi extract, 3 mass parts of Itanlian rye extract, seaweed extraction 1 mass parts of object, 2 mass parts of Radix Platycodonis extract, 4 mass parts of perilla leaf extract, 1 mass parts of PORIA ALBA extract.In described Medicament extract is made by the following method: by aloe, citrus young fruit, hens and chickens, Magnolia binodii, Itanlian rye, campanulaceae, purple After perilla leaf, PORIA ALBA air-dry, is mixed after being milled to powder, obtain mixed-powder；By mixed-powder at 25 DEG C ultrasonic extraction 20 Minute, after obtained mixed liquor centrifuge separation, supernatant is taken, primary extract is obtained；By primary extract be passed through in macroporous absorbent resin into Row adsorbing separation, with the first ethanol solution heating and refluxing extraction 2 times that the concentration expressed in percentage by volumes of 100 mass parts is 30%, every time 0.5 hour, filtering merged each secondary ethanol extract, recycles ethyl alcohol to no alcohol taste, continues to be concentrated under reduced pressure to give the first medicinal extract；It will After marine algae extract is with the ethyl alcohol mixing of 20 mass parts, is mixed with the first medicinal extract, after mixing evenly, be concentrated under reduced pressure to give the second leaching Cream；Macroporous absorbent resin on the second obtained medicinal extract discards water lotion with the water elution of 4 times of column volumes, then with 3 times of column volumes Concentration expressed in percentage by volume 50% the elution of the second ethanol solution, collect ethanol elution part, recycle ethyl alcohol, be concentrated under reduced pressure, it is dry, Obtain the first powder；90min will be freezed at -4 DEG C after kiwifruit fruit peeling, clean, slice, the deionization of 80 mass parts is added Water mashing, is added citric acid, and pH is adjusted to 3, and pectase is added and stirs evenly, in 50 DEG C of hydrolysis 6h, then adjusts pH to 7, pancreas is added Enzyme after mixing evenly, after 35 DEG C of hydrolysis 10h, enzymatic hydrolysis, after mixed liquor ultrafiltration, takes filtrate, obtains the second powder after dry End；Chinese medical extract is obtained after first powder and the second powder are mixed.It further include modified active in the Chinese medical extract 0.5 mass parts of powdered carbon, the modified active powdered carbon the preparation method comprises the following steps: by 1- methyl -3- butyl imidazole ionotropic glutamate liquid 3 mass parts of body and the mixing of 4 mass parts of glucose, uniform stirring 40min act on 30min under 600W microwave, and deionized water is added 100 mass parts, obtain mixed solution；50 mass parts of active carbon powder are added in mixed solution, stir evenly, impregnate 40min, 800W ultrasonic wave disperses 30min, and 30min is acted under 500W microwave, filters, takes filter residue, be dried in vacuo at a temperature of 80 DEG C 12h obtains modified active powdered carbon.

Embodiment 3

Embodiment 3 with embodiment 1 the difference is that, including 20 mass parts of sodium lauroyl glutamate, 25 mass parts of cornstarch, 5 mass parts of trehalose, 3 mass parts of 3-o- ethylascorbyl, 1 mass parts of carnosine, 6 mass parts of Chinese medical extract.In described Medicament extract includes 5 mass parts of aloe extract, 4 mass parts of citrus young fruit extract, 5 mass parts of hens and chickens extract, 6 mass parts of Magnolia binodii extract, 8 mass parts of Kiwi extract, 5 mass parts of Itanlian rye extract, marine algae extract 10 Mass parts, 7 mass parts of Radix Platycodonis extract, 6 mass parts of perilla leaf extract, 3 mass parts of PORIA ALBA extract.The Chinese medicine mentions Object is taken to be made by the following method: by aloe, citrus young fruit, hens and chickens, Magnolia binodii, Itanlian rye, campanulaceae, purple perilla After leaf, PORIA ALBA air-dry, is mixed after being milled to powder, obtain mixed-powder；By mixed-powder, ultrasonic extraction 50 is divided at 30 DEG C Clock takes supernatant, obtains primary extract after obtained mixed liquor centrifuge separation；Primary extract is passed through in macroporous absorbent resin and is carried out Adsorbing separation, with the first ethanol solution heating and refluxing extraction 3 times that the concentration expressed in percentage by volume of 150 mass parts is 80%, 2 is small every time When, filtering merges each secondary ethanol extract, recycles ethyl alcohol to no alcohol taste, continues to be concentrated under reduced pressure to give the first medicinal extract；Seaweed is mentioned After taking object to mix with the ethyl alcohol of 30 mass parts, is mixed with the first medicinal extract, after mixing evenly, be concentrated under reduced pressure to give the second medicinal extract；? To the second medicinal extract on macroporous absorbent resin with the water elution of 8 times of column volumes discard water lotion, then the volume with 8 times of column volumes Second ethanol solution of percentage concentration 100% elutes, and collects ethanol elution part, recycles ethyl alcohol, is concentrated under reduced pressure, dry, obtains first Powder；150min will be freezed at 20 DEG C after kiwifruit fruit peeling, clean, slice, the deionized water that 100 mass parts are added is beaten Citric acid is added in slurry, and pH is adjusted to 4, and pectase is added and stirs evenly, in 55 DEG C of hydrolysis 8h, then adjusts pH to 7.5, pancreatin is added After mixing evenly, after 38 DEG C of hydrolysis 12h, enzymatic hydrolysis, after mixed liquor ultrafiltration, filtrate is taken, obtains the second powder after dry； Chinese medical extract is obtained after first powder and the second powder are mixed.It further include modified active powdered carbon in the Chinese medical extract 1 mass parts, the modified active powdered carbon the preparation method comprises the following steps: by 5 mass of 1- methyl -3- butyl imidazole ionotropic glutamate liquid Part and the mixing of 8 mass parts of glucose, uniform stirring 60min act on 50min under 800W microwave, and 120 mass of deionized water is added Part, obtain mixed solution；60 mass parts of active carbon powder are added in mixed solution, stir evenly, impregnate 60min, 1000W is super Sound wave disperses 40min, and 40min is acted under 800W microwave, filters, takes filter residue, be dried in vacuo for 24 hours, obtain at a temperature of 100 DEG C Modified active powdered carbon.

Embodiment 4

Embodiment 4 with embodiment 1 the difference is that, comprising the following steps: cornstarch is dissolved in the deionization of 800 mass parts In water；The powder of sodium lauroyl glutamate, trehalose, 3-o- ethylascorbyl, carnosine, Chinese medical extract is uniformly mixed Afterwards, fluidization dispersions 20min at room temperature；Corn starch solution is sprayed on the powder of fluidization dispersions, control temperature at 50 DEG C, Air mass flow is 800m during controlling fluidization dispersions³/h；After having sprayed, continue in 50 DEG C of fluidization dispersion 30min, dried object Material；Material after drying is that amino acid is had no time clean face powder.

Embodiment 5

Embodiment 5 with embodiment 1 the difference is that, the Chinese medical extract is that commercially available aloe extract and seaweed are extracted Object.

Embodiment 6

Embodiment 6 with embodiment 1 the difference is that, the Kiwi extract in the Chinese medical extract is by the following method It is made: by aloe, citrus young fruit, hens and chickens, Kiwi berry, Magnolia binodii, Itanlian rye, campanulaceae, perilla leaf, PORIA ALBA wind After dry, mixed after being milled to powder, obtain mixed-powder；By mixed-powder at 28 DEG C ultrasonic extraction 30 minutes, what is obtained is mixed After closing liquid centrifuge separation, supernatant is taken, primary extract is obtained；Primary extract is passed through in macroporous absorbent resin and carries out adsorbing separation, is used The concentration expressed in percentage by volume of 120 mass parts is the first ethanol solution heating and refluxing extraction 3 times of 40%, 1.5 hours every time, filters, closes And each secondary ethanol extract, ethyl alcohol is recycled to no alcohol taste, continues to be concentrated under reduced pressure to give the first medicinal extract；By marine algae extract with 25 matter After the ethyl alcohol mixing for measuring part, is mixed with the first medicinal extract, after mixing evenly, be concentrated under reduced pressure to give the second medicinal extract；The second obtained leaching Macroporous absorbent resin on cream discards water lotion, then the concentration expressed in percentage by volume with 7 times of column volumes with the water elution of 6 times of column volumes 80% the second ethanol solution elution, collects ethanol elution part, recycles ethyl alcohol, be concentrated under reduced pressure, dry, obtains Chinese medical extract.

Embodiment 7

Embodiment 7 with embodiment 1 the difference is that, the Chinese medical extract be the first powder.

Embodiment 8

Embodiment 8 with embodiment 1 the difference is that, in the Chinese medical extract be free of modified activated carbon.

Embodiment 9

Embodiment 9 with embodiment 1 the difference is that, the active carbon in the Chinese medical extract is unmodified.

Embodiment 10

Embodiment 10 with embodiment 1 the difference is that, the clean face powder the preparation method comprises the following steps: by powdered various substances It is uniformly mixed, obtains clean face powder.

Comparative example 1

Comparative example 1 with embodiment 1 the difference is that, in the clean face powder be free of carnosine.

Comparative example 2

Comparative example 2 with embodiment 1 the difference is that, in the clean face powder be free of Chinese medical extract.

Experimental example 1

30 18 ~ 50 years old Healthy Peoples are randomly selected as volunteer, the clean face powder of embodiment 1 ~ 10 is provided, it is clear by stipulated number Wash one's face portion, and whether point 5 grades of evaluation noses are not easy to feel pain, cleaning force and skin moisture increase ratio, and then record counts each will The usage experience of hope person, is averaged, and following table is experimental result.

1 user's evaluation result of table

	Nose is not easy shouting pain	Cleaning force	Overall merit
				Embodiment 1	4.92	4.94	4.93
Embodiment 2	4.62	4.75	4.69
				Embodiment 3	4.75	4.82	4.79
Embodiment 4	4.91	4.90	4.91
				Embodiment 5	3.58	3.27	3.43
Embodiment 6	4.62	4.65	4.64
				Embodiment 7	4.66	4.69	4.68
Embodiment 8	4.65	4.11	4.38
				Embodiment 9	2.78	2.99	2.89
Embodiment 10	3.16	3.28	3.22
				Comparative example 1	2.82	3.01	2.92
Comparative example 2	2.21	2.34	2.28

As it can be seen from table 1 embodiment 1 ~ 10 all has certain cleaning and bland effect, compared with comparative example 2, to skin The irritation of skin is small, show it is used in the examples there is better cleaning function containing traditional Chinese medicinal components, there is significant cleaning Soothing effect.

Embodiment 1 is preferably embodiment with embodiment 4, and overall merit is higher (average of two evaluation indexes), But the used time produced in embodiment 4 is larger, higher cost, therefore embodiment 1 is that more preferably embodiment, embodiment 2 add Measure less, cleaning effect still has significant effect compared with comparative example, shows the clean face powder comprising Chinese medicinal component in terms of decontamination Effect be more important；The grape extract that comparative example 1 uses is free of carnosine, and user's reflection is poor, shows carnosine clear Play the role of in terms of clean decontamination particularly important；Chinese medical extract is free of in comparative example 2, cleaning effect is significantly lower than embodiment With comparative example 1, show that important extraction also has important role in terms of cleaning decontamination.

The Chinese medical extract of embodiment 5 is traditional aloe and marine algae extract, and effect is poor；Wherein in embodiment 6 The addition manner of Kiwi extract in medicament extract is different, and cleaning effect is declined slightly；Traditional Chinese medicine extraction in embodiment 7 Object is free of Kiwi extract, and cleaning effect is little with 6 difference of embodiment, the acquisition modes of Kiwi extract or addition side Formula has a certain impact to cleaning effect.

Modified activated carbon is not contained in embodiment 8, cleaning effect has apparent decline relative to embodiment 1；Implement Active carbon in example 9 is unmodified, and cleaning effect is significantly weaker than embodiment 1 and 8, shows that active carbon is only added, without modification, The cleaning effect of clean face powder can't be improved.

The manufacturing process of clean face powder in embodiment 10 has apparent difference with embodiment 1, and cleaning effect is significantly low In embodiment 1, shows that manufacturing process is affected to clean face powder cleaning effect, may have with the dispersion effect of various composition It closes.

Experimental example 2

30 18 ~ 50 years old Healthy Peoples are randomly selected as volunteer, paper handkerchief in embodiment 1 ~ 8 is provided, use one every 30min Secondary wiping face, continuous 5 hours, measurement 5 as a child in user's face skin collagen content.

2 collagen of table and moisture content relative amount

	Opposite collagen content	Skin moisture content increase ratio (%)
			Embodiment 1	2.1	40.1
Embodiment 2	1.6	28.2
			Embodiment 3	1.7	27.1
Embodiment 4	1.8	39.3
			Embodiment 5	1	16.3
Embodiment 6	1.2	22.5
			Embodiment 7	1.1	25.1
Embodiment 8	1.8	23.1
			Embodiment 9	1.9	9.8
Embodiment 10	0.9	20.1
			Comparative example 1	1.1	21.2
Comparative example 2	0.7	10.1

As shown in table 2, Chinese medical extract can promote the synthesis of collagen to a certain extent, real on the basis of embodiment 5 It applies collagen content of the collagen content of example 1 ~ 4 compared with embodiment 5 to be significantly increased, shows to be added to Chinese medical extract Clean face powder can significantly improve skin collagen content.

The collagen production of embodiment 1 is most, is preferably embodiment, the additive amount of various raw materials in embodiment 2 It is less than embodiment 1, the yield of collagen shows that the addition of various raw materials is unsuitable very few again smaller than embodiment 1；Embodiment The additive amount of 3 various raw materials is above embodiment 1, but collagen production does not increase, therefore raw material addition is also unsuitable Excessively.

Embodiment 4 is the influence to collagen production in skin of different parameters in Traditional Chinese medicine extraction method, from embodiment 4 As can be seen that the yield of its collagen is below embodiment 1 ~ 3, show in embodiment 1 that extracting method is preferably embodiment party Case.

The acquisition methods of the Kiwi extract in Chinese medical extract in embodiment 6 are the same as the other compositions in the first powder Acquisition methods it is consistent, the content of collagen has marked difference with embodiment 1；Chinese medical extract in embodiment 7 is not Containing Kiwi extract, the content of collagen also has more apparent difference with embodiment, shows Kiwi extract pair Keeping the content of collagen has obvious action.

Above-listed detailed description is illustrating for possible embodiments of the present invention, and above embodiments are not to limit this The scope of the patents of invention, all equivalence enforcements or change without departing from carried out by the present invention, is intended to be limited solely by the scope of the patents of this case.

Claims

The clean face powder 1. a kind of amino acid is had no time, which is characterized in that including 16 ~ 20 mass parts of sodium lauroyl glutamate, cornstarch 15 ~ 25 mass parts, 1 ~ 5 mass parts of trehalose, 0.2 ~ 3 mass parts of 3-o- ethylascorbyl, 0.1 ~ 1 mass parts of carnosine, Chinese medicine 2 ~ 6 mass parts of extract.
The clean face powder 2. a kind of amino acid according to claim 1 is had no time, which is characterized in that including sodium lauroyl glutamate 18 ~ 20 mass parts, 17 ~ 25 mass parts of cornstarch, 3 ~ 5 mass parts of trehalose, 0.8 ~ 3 mass parts of 3-o- ethylascorbyl, flesh 0.6 ~ 1 mass parts of peptide, 4 ~ 6 mass parts of Chinese medical extract.
The clean face powder 3. a kind of amino acid according to claim 2 is had no time, which is characterized in that including sodium lauroyl glutamate 18 Mass parts, 17 mass parts of cornstarch, 3 mass parts of trehalose, 0.8 mass parts of 3-o- ethylascorbyl, 0.6 mass of carnosine Part, 4 mass parts of Chinese medical extract.
The clean face powder 4. a kind of amino acid according to claim 1 is had no time, which is characterized in that the Chinese medical extract includes 1 ~ 5 mass parts of aloe extract, 2 ~ 4 mass parts of citrus young fruit extract, 2 ~ 5 mass parts of hens and chickens extract, Magnolia binodii 3 ~ 6 mass parts of extract, 3 ~ 8 mass parts of Kiwi extract, 3 ~ 5 mass parts of Itanlian rye extract, marine algae extract 1 ~ 10 mass parts, 2 ~ 7 mass parts of Radix Platycodonis extract, 4 ~ 6 mass parts of perilla leaf extract, 1 ~ 3 mass parts of PORIA ALBA extract.
The clean face powder 5. a kind of amino acid according to claim 1 is had no time, which is characterized in that the Chinese medical extract includes 3 mass parts of aloe extract, 3 mass parts of citrus young fruit extract, 4 mass parts of hens and chickens extract, Magnolia binodii extract 5 Mass parts, 4 mass parts of Kiwi extract, 4 mass parts of Itanlian rye extract, 6 mass parts of marine algae extract, campanulaceae extract 4 mass parts of object, 5 mass parts of perilla leaf extract, 2 mass parts of PORIA ALBA extract.
The clean face powder 6. a kind of amino acid according to claim 1 is had no time, which is characterized in that the Chinese medical extract passes through Following methods are made: by aloe, citrus young fruit, hens and chickens, Magnolia binodii, Itanlian rye, campanulaceae, perilla leaf, PORIA ALBA After air-drying, is mixed after being milled to powder, obtain mixed-powder；By mixed-powder at 25 ~ 30 DEG C ultrasonic extraction 20 ~ 50 minutes, After obtained mixed liquor centrifuge separation, supernatant is taken, primary extract is obtained；Primary extract is passed through in macroporous absorbent resin and is adsorbed Separation is the first ethanol solution heating and refluxing extraction 2-3 times of 30%-80% with the concentration expressed in percentage by volume of 100 ~ 150 mass parts, often 0.5-2 hours secondary, filtering merges each secondary ethanol extract, recycles ethyl alcohol to no alcohol taste, continues to be concentrated under reduced pressure to give the first leaching Cream；After marine algae extract is mixed with the ethyl alcohol of 20 ~ 30 mass parts, mixes with the first medicinal extract, after mixing evenly, be concentrated under reduced pressure To the second medicinal extract；Macroporous absorbent resin discards water lotion with the water elution of 4-8 times of column volume on the second obtained medicinal extract, then uses The second ethanol solution of the concentration expressed in percentage by volume 50%-100% of 3-8 times of column volume elutes, and collects ethanol elution part, recycles second Alcohol is concentrated under reduced pressure, dry, obtains the first powder；Will kiwifruit fruit peeling, clean, slice after at -4 DEG C ~ -20 DEG C freezing 90 ~ 150min is added the deionized water mashing of 80 ~ 100 mass parts, citric acid is added, pH is adjusted to 3 ~ 4, pectase is added and stirs It is even, in 50 ~ 55 DEG C of 6 ~ 8h of hydrolysis, then pH to 7 ~ 7.5 is adjusted, pancreatin is added after mixing evenly, in 35 ~ 38 DEG C of 10 ~ 12h of hydrolysis, After enzymatic hydrolysis, after mixed liquor ultrafiltration, filtrate is taken, obtains the second powder after dry；First powder and the second powder are mixed After obtain Chinese medical extract.
The clean face powder 7. a kind of amino acid according to claim 6 is had no time, which is characterized in that the Chinese medical extract passes through Following methods are made: by aloe, citrus young fruit, hens and chickens, Magnolia binodii, Itanlian rye, campanulaceae, perilla leaf, PORIA ALBA After air-drying, is mixed after being milled to powder, obtain mixed-powder；By mixed-powder at 28 DEG C ultrasonic extraction 30 minutes, obtain After mixed liquor centrifuge separation, supernatant is taken, primary extract is obtained；Primary extract is passed through in macroporous absorbent resin and carries out adsorbing separation, With the first ethanol solution heating and refluxing extraction 3 times that the concentration expressed in percentage by volume of 120 mass parts is 40%, 1.5 hours every time, filter, Merge each secondary ethanol extract, recycles ethyl alcohol to no alcohol taste, continue to be concentrated under reduced pressure to give the first medicinal extract；By marine algae extract with 25 After the ethyl alcohol mixing of mass parts, is mixed with the first medicinal extract, after mixing evenly, be concentrated under reduced pressure to give the second medicinal extract；Second obtained Macroporous absorbent resin on medicinal extract discards water lotion, then the concentration expressed in percentage by volume with 7 times of column volumes with the water elution of 6 times of column volumes 80% the second ethanol solution elution, collects ethanol elution part, recycles ethyl alcohol, be concentrated under reduced pressure, dry, obtains the first powder；By Mi The peeling of monkey Peach fruits is cleaned, freezes 100min after slice at -10 DEG C, and the deionized water mashing of 90 mass parts is added, lemon is added PH is adjusted to 3.5 by lemon acid, and pectase is added and stirs evenly, in 54 DEG C of hydrolysis 7h, then adjusts pH to 7.2, and pancreatin is added and stirs evenly Afterwards, after 37 DEG C of hydrolysis 11h, enzymatic hydrolysis, after mixed liquor ultrafiltration, filtrate is taken, obtains the second powder after dry；By the first powder End and the second powder obtain Chinese medical extract after mixing.
The clean face powder 8. a kind of amino acid according to claim 4 is had no time, which is characterized in that in the Chinese medical extract also Including 0.5 ~ 1 mass parts of modified active powdered carbon, the modified active powdered carbon the preparation method comprises the following steps: by 1- methyl -3- butyl miaow 3 ~ 5 mass parts of azoles ionotropic glutamate liquid and 4 ~ 8 mass parts of glucose mixing, uniform stirring 40min~60min, 600W~ 30min~50min is acted under 800W microwave, and 100 ~ 120 mass parts of deionized water are added, obtain mixed solution；In mixed solution Middle 50 ~ 60 mass parts of addition active carbon powder, stir evenly, and impregnate 40min~60min, the dispersion of 800W~1000W ultrasonic wave 30min~40min acts on 30min~40min under 500W~800W microwave, filters, filter residue is taken, in 80 DEG C~100 DEG C temperature It is lower vacuum drying 12 ~ for 24 hours, obtain modified active powdered carbon.
The clean face powder 9. a kind of amino acid according to claim 8 is had no time, which is characterized in that in the Chinese medical extract also Including 0.6 mass parts of modified active powdered carbon, the modified active powdered carbon the preparation method comprises the following steps: by 1- methyl -3- butyl imidazole 4 mass parts of ionotropic glutamate liquid and the mixing of 6 mass parts of glucose, uniform stirring 50min act on 40min under 700W microwave, 110 mass parts of deionized water are added, obtain mixed solution；55 mass parts of active carbon powder are added in mixed solution, stirring is equal It is even, 50min is impregnated, 900W ultrasonic wave disperses 35min, 35min is acted under 600W microwave, filters, filter residue is taken, in 90 DEG C of temperature Lower vacuum drying 18h, obtains modified active powdered carbon.
The clean face powder, preparation method thereof 10. a kind of amino acid is had no time, which comprises the following steps: cornstarch is dissolved in 800 In the deionized water of ~ 1000 mass parts；Sodium lauroyl glutamate, trehalose, 3-o- ethylascorbyl, carnosine, Chinese medicine are mentioned Take the powder of object after mixing, at room temperature 20 ~ 30min of fluidization dispersions；Corn starch solution is sprayed onto fluidization dispersions On powder, temperature is controlled at 50 ~ 70 DEG C, and air mass flow is 800 ~ 1200m during controlling fluidization dispersions³/h；After having sprayed, continue In 50 ~ 70 DEG C of 30 ~ 60min of fluidization dispersion, dried material；Material after drying is that amino acid is had no time clean face powder.