CN108442134A - Milk filaments non-woven fabrics lace dyestuff and its dyeing - Google Patents
Milk filaments non-woven fabrics lace dyestuff and its dyeing Download PDFInfo
- Publication number
- CN108442134A CN108442134A CN201810352597.4A CN201810352597A CN108442134A CN 108442134 A CN108442134 A CN 108442134A CN 201810352597 A CN201810352597 A CN 201810352597A CN 108442134 A CN108442134 A CN 108442134A
- Authority
- CN
- China
- Prior art keywords
- woven fabrics
- parts
- dyeing
- milk filaments
- lace
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/16—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using dispersed, e.g. acetate, dyestuffs
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
- D06M13/35—Heterocyclic compounds
- D06M13/352—Heterocyclic compounds having five-membered heterocyclic rings
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
- D06M13/402—Amides imides, sulfamic acids
- D06M13/432—Urea, thiourea or derivatives thereof, e.g. biurets; Urea-inclusion compounds; Dicyanamides; Carbodiimides; Guanidines, e.g. dicyandiamides
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
- D06M13/46—Compounds containing quaternary nitrogen atoms
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M16/00—Biochemical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. enzymatic
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/64—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds without sulfate or sulfonate groups
- D06P1/651—Compounds without nitrogen
- D06P1/65106—Oxygen-containing compounds
- D06P1/65131—Compounds containing ether or acetal groups
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/653—Nitrogen-free carboxylic acids or their salts
- D06P1/6533—Aliphatic, araliphatic or cycloaliphatic
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/673—Inorganic compounds
- D06P1/67333—Salts or hydroxides
- D06P1/6735—Salts or hydroxides of alkaline or alkaline-earth metals with anions different from those provided for in D06P1/67341
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/673—Inorganic compounds
- D06P1/67333—Salts or hydroxides
- D06P1/6735—Salts or hydroxides of alkaline or alkaline-earth metals with anions different from those provided for in D06P1/67341
- D06P1/67358—Halides or oxyhalides
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/02—Material containing basic nitrogen
- D06P3/04—Material containing basic nitrogen containing amide groups
- D06P3/043—Material containing basic nitrogen containing amide groups using dispersed dyes
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P5/00—Other features in dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form
- D06P5/02—After-treatment
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/02—Natural fibres, other than mineral fibres
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Dispersion Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Microbiology (AREA)
- Coloring (AREA)
Abstract
The invention discloses a kind of milk filaments non-woven fabrics lace dyestuff and its dyeings.The milk filaments non-woven fabrics lace dyestuff includes the component of following parts by weight：0.2 0.3 parts of disperse orange S 4RL, 0.7 0.8 parts of dispersed ruby S 5BL, deep blue 0.3 0.4 parts of the HGL of dispersion, 0.4 0.6 parts of glacial acetic acid, 7 10 parts of neutral salt, 0.1 0.2 parts of lauryl glucosyl, 0.1 0.2 parts of paregal O, 95 105 parts of water.Beneficial effects of the present invention are：There is good color fastness to light with the milk filaments non-woven fabrics lace that dyeing obtains by the milk filaments non-woven fabrics lace.
Description
Technical field
The present invention relates to dyestuff, more particularly to a kind of milk filaments non-woven fabrics lace dyestuff and its dyeing.
Background technology
Milk filaments exactly by liquid milk separation, remove obtained milk protein after water, in addition softener, is made milk
Slurries are spun into milk protein fiber then by wet spinning process and scientific disposal, and being further spun into can be with the ox of woven fabric
Milk silk.
The Chinese patent of Publication No. CN104420340A discloses a kind of dyeing of milk filaments；The dyeing according to
Secondary includes 5 configuration dye liquor, dyeing, fixation, washing, soap boiling, washing steps；Dye liquor includes working solution, with citric acid, phosphoric acid hydrogen
Disodium or acetic acid, sodium acetate adjust pH value to 4.5；Paregal O of the working solution containing 2% dyestuff and 0.4g/L；In dyeing, bath
It is 1: 50 than control, begin dye at 30 DEG C, then is warming up to 80 DEG C, heat preservation dyeing 80min.
Milk filaments non-woven fabrics lace is that milk filaments sewing is formed pattern on non-woven fabrics, is then dissolved non-woven fabrics, only
The pattern that remaining milk filaments are sewn into is formed by lace.Disperse red S-2GFL or disperse blue are generally used in the prior art
HGL dyes milk filaments as dyestuff.But using disperse red S-2GFL or disperse blue HGL as dyestuff, using
Although the color fastness to light of milk filaments non-woven fabrics lace prepared by above-mentioned milk filaments dyeing makes moderate progress, but still can not expire
The requirement of sufficient people, has much room for improvement.
Invention content
The object of the present invention is to provide a kind of milk filaments non-woven fabrics lace dyestuffs.It is used by the milk filaments non-woven fabrics lace
The milk filaments non-woven fabrics lace that dyeing obtains has good color fastness to light.
The present invention above-mentioned technical purpose technical scheme is that：
A kind of milk filaments non-woven fabrics lace dyestuff, includes the component of following parts by weight：
0.2-0.3 parts of disperse orange S-4RL, 0.7-0.8 parts of dispersed ruby S-5BL, dispersion deep blue HGL 0.3-0.4 parts, ice vinegar
0.4-0.6 parts sour, 7-10 parts of neutral salt, 0.1-0.2 parts of lauryl glucosyl, 0.1-0.2 parts of paregal O, water 95-105
Part.
By using above-mentioned technical proposal, disperse orange S-4RL, dispersed ruby S-5BL, the deep blue HGL of dispersion are dispersion dye
Material.Milk filaments alkaline resistance properties is poor, and dye-uptake is low under alkaline environment, and glacial acetic acid is used to adjust the pH value of dyestuff to acidity, increases
The dye-uptake of strong milk filaments.The addition of neutral salt can reduce the solubility of protein in milk filaments, and can saltout protein,
To reduce hydrolysis of the protein in dyeing in milk filaments, color fastness is improved.Lauryl glucosyl belongs to nonionic table
Face activating agent alkyl glycosides, is colourless transparent liquid, soluble easily in water, is relatively soluble in common organic solvent, has hydrophilic polarity
The long-chain molecule of group and hydrophobic non-polar group.Paregal O is nonionic surfactant, and main component is polyoxyethylene
Fatty alcohol ether, is creamy white or ecru ointment shape, congeals to the cold, soluble easily in water, in steady in hard water, acid solution or lye
Determine state.
The present invention is further arranged to：The neutral salt is at least one of sodium sulphate, potassium sulfate.
By using above-mentioned technical proposal, sodium sulphate, potassium sulfate are water-soluble preferably, and are common neutral salt, inexpensive
It is easy to get.Sulfate ion in sodium sulphate and potassium sulfate can improve the stability of protein conformation in milk filaments, to reduce
Hydrolysis of the protein in dyeing, improves color fastness in milk filaments.
Another goal of the invention of the present invention is to provide a kind of dyeing of milk filaments non-woven fabrics lace, including walks as follows
Suddenly：
Step 1：First so that the non-woven fabrics in milk filaments non-woven fabrics lace is dissolved with water, discharges；
Step 2：The milk filaments non-woven fabrics lace that step 1 obtains is added in above-mentioned dyestuff, after being heated to 125-135 DEG C, is protected
Warm 50-70min, dyeing discharge after the completion of dyeing；
Step 3：The milk filaments non-woven fabrics lace that step 2 obtains is added to the water, functional finishing agent is added, is impregnated, sizing；
According to parts by weight, the functional finishing agent includes following component：
1-2 parts of antiseptic, 3-5 parts of ultra-violet absorber, 1-4 parts of antistatic agent, 1-2 parts of color fixing agent.
By using above-mentioned technical proposal, when being dyed using above-mentioned dyestuff, milk filaments need at 125-135 DEG C
It can be dyed, improve the color fastness after dyeing.Antiseptic can assign lace anti-microbial property, and ultra-violet absorber can
The good uvioresistant performance of lace is assigned, antistatic agent can assign lace good resistance, reduce electric conductivity, color fixing agent energy
Enough enhance the bond strength of dyestuff and milk filaments.
The present invention is further arranged to：The antiseptic is biguanides antiseptic.
By using above-mentioned technical proposal, biguanides antiseptic makes cell surface by the effect of block cell lysozyme
Structural degeneration and destroy bacterium.
The present invention is further arranged to：The biguanides antiseptic is hexamethylene.
By using above-mentioned technical proposal, hexamethylene has wide spectrum, long-term efficient sterilizing
Ability, toxicity after testing after the qualitative fungicide for nontoxic rank, and it is completely nonirritant to skin and mucosa, and can be complete
Biodegradation, unique sterilization mechanism not will produce any drug resistance；Colourless or light amber supernatant liquid, it is water-soluble compared with
It is good, colorless and odorless, pH 7-8.
The present invention is further arranged to：The ultra-violet absorber selects Benzotriazole Ultraviolet Stabilizer.
By using above-mentioned technical proposal, Benzotriazole Ultraviolet Stabilizer be in ultra-violet absorber yield it is maximum,
The most a kind of product of kind, there is higher absorbancy index in 300-385nm；Before absorbing light, ultra-violet absorber with
The form of phenol compound exists, because the electron density on oxygen atom is much larger than the electron density on triazole theheterocyclic nitrogen atom,
Therefore be allowed to that stronger alkalinity is presented, the absorption of light makes electron density mainly be shifted on triazole theheterocyclic nitrogen atom from oxygen atom, makes phenol
More acid, the richer alkalinity of nitrogen-atoms, proton, which is quickly transferred on nitrogen-atoms, forms tautomer.This tautomer is
Unstable, extra energy security can be converted to thermal energy, be returned to more stable ground state.Entire interconversion processes efficiency pole
Height almost can be repeated ad infinitum, and here it is compounds to have the reason of photostability.
The present invention is further arranged to：The Benzotriazole Ultraviolet Stabilizer is one kind in UV-P, UV-327.
By using above-mentioned technical proposal, the chemical name of UV-P is three nitrogen of 2- (2 '-hydroxyls -5 '-aminomethyl phenyl) benzo
Azoles, can strong absorbing wavelength be 270-340nm ultraviolet light；Appearance is colourless or pale yellow crystals；Can be dissolved in gasoline, benzene,
A variety of organic solvents such as acetone, solubility is minimum in water, is not decomposed by concentrated base, concentrated acid, it can be with heavy metal ion chemical combination
At salt；The ultraviolet light of 270~280nm wavelength can be absorbed；Stability in transparent article is compared with articles colored more preferable.UV-327
Chemical name be 2- (2 '-hydroxyls -3 ', 5 '-di-tert-butyl-phenyls) -5- chlorobenzotriazoles, pale yellow powder, fusing point 156
DEG C, have toxicity low, absorbs the features such as UV resistance is strong.
The present invention is further arranged to：The antistatic agent selects quaternary ammonium salt antistatic agent.
By using above-mentioned technical proposal, quaternary ammonium salt antistatic agent belongs to cationic, and static elasticity eliminating effect is good, absorption
Ability is strong, but heat resistance is poor, is easy to happen thermal decomposition.
The present invention is further arranged to：The quaternary ammonium salt antistatic agent is stearyl trimethyl ammonium chloride, dilauryl
One kind in alkyl dimethyl ammonium chloride.
By using above-mentioned technical proposal, stearyl trimethyl ammonium chloride can be dissolved in alcohol and hot water；With cation, it is non-from
Sub- surfactant or dyestuff have good compatibility, avoid and anion surfactant, dyestuff or additive compatibility.Dilauryl
Alkyl dimethyl ammonium chloride is white or yellowish lotion, is soluble in polar solvent, is slightly soluble in water；With cation, nonionic, both sexes from
Sub- surfactant has good compatibility；Easily it is adsorbed to negatively charged surface；The fiber for bonding balling-up can be made to become
It is fluffy and soft.
The present invention is further arranged to：The color fixing agent selects one kind in color fixing agent Y, color fixing agent M.
By using above-mentioned technical proposal, color fixing agent Y is water white transparency thick liquid, can be made into solid through drying；Chemistry
Group become dicyandiamide formaldehyde resin water solubility initial reduced body, be highly soluble in water, with unionized, cationic surfactant or sun from
Subtype synthetic resin initial reduced body is used in mixed way, can not be mixed with anionic dyes, anion surfactant；Meet hard water, strong
Acid, highly basic, tannic acid, rongalite and a large amount of sulfate, hypochlorite etc. will produce precipitation.Color fixing agent M is dissolved in water and 2% vinegar
Acid；It is reacted with copper acetate by color fixing agent Y and is made, can shared with cationic or nonionic surface active agent, it can not be with the moon
Ionic dyes or surfactant bathe use together.
In conclusion the invention has the advantages that：
1, neutral salt is added in dyestuff, reduces the solubility of protein in milk filaments, exists to reduce protein in milk filaments
Hydrolysis when dyeing；
2, neutral salt selects potassium sulfate and sodium sulphate containing sulfate ion, and albumen in milk filaments is improved using sulfate ion
The stability of texture elephant reduces hydrolysis of the protein in dyeing in milk filaments, improves color fastness.
Specific implementation mode
Disperse orange S-4RL, dispersed ruby S-5BL, the deep blue HGL of dispersion, disperse red S-2GFL are purchased from Zhejiang Long Sheng groups
Limited liability company；
Glacial acetic acid, sodium sulphate, potassium sulfate are commercial product；
Lauryl glucosyl is purchased from Guangzhou Ying Hong Chemical Co., Ltd.s；
Paregal O is purchased from ten thousand new material Co., Ltds in Guangzhou；
Hexamethylene is purchased from Jinan Yuan Shui Chemical Industry Science Co., Ltd；
UV-P, UV-327 are purchased from Guangzhou Te Lei Chemical Co., Ltd.s；
Stearyl trimethyl ammonium chloride, dilauryl ammonium chloride are purchased from Suzhou Yuan Tairun Chemical Co., Ltd.s；
Color fixing agent Y and color fixing agent M are purchased from Shandong Ka Ya Chemical Co., Ltd.s.
The component table of table 1, embodiment 1-5 milk filaments non-woven fabrics lace dyestuffs
The preparation method of embodiment 1-5 milk filaments non-woven fabrics lace dyestuffs is as follows：
A kind of preparation method of milk filaments non-woven fabrics lace dyestuff, includes the following steps：
Weigh disperse orange S-4RL, dispersed ruby S-5BL, the deep blue HGL of dispersion, glacial acetic acid, neutral salt, lauryl glucosyl,
Paregal O, water are uniformly mixed.
Table 2, embodiment 6-10 milk filaments non-woven fabrics lace Technological parameters tables
Dyestuff used in embodiment 6-10 is corresponded to using the milk filaments non-woven fabrics lace dyestuff prepared according to embodiment 1-5.
Wherein, 6 corresponding embodiment 1 of embodiment, 7 corresponding embodiment 2 of embodiment, 8 corresponding embodiment 3 of embodiment, embodiment 9, which corresponds to, to be implemented
Example 4,10 corresponding embodiment 5 of embodiment.
The dyeing of embodiment 6-10 milk filaments non-woven fabrics laces is as follows：
A kind of dyeing of milk filaments non-woven fabrics lace, includes the following steps：
Step 1：First water-bath 2h in the water by milk filaments non-woven fabrics lace in 100 DEG C, makes non-woven fabrics dissolve, and discharging is weighed；
Step 2：The milk filaments non-woven fabrics lace that step 1 is obtained is added in dyestuff, bath raio 1：20, it after heating, keeps the temperature, dye
Color discharges after the completion of dyeing；
Step 3：The milk filaments non-woven fabrics lace that step 2 obtains is added to the water, functional finishing agent is added, is impregnated, sizing.
Comparative example 1
The Chinese patent of Publication No. CN104420340A is selected to be dyed as a comparison case 1 to milk filaments non-woven fabrics lace,
Specific dyeing includes the following steps：
(a) dye liquor is prepared：The working solution for configuring disperse red S-2GFL and the 0.4g/L paregal O containing 2wt%, with citric acid, phosphorus
Sour disodium hydrogen or acetic acid, sodium acetate adjusting pH value to 4.5, bath raio 1: 50；
(b) it dyes：First water-bath 2h in the water by milk filaments non-woven fabrics lace in 100 DEG C, makes non-woven fabrics dissolve, and discharging is weighed；
Milk filaments non-woven fabrics lace is put into working solution and is dyed, 30 DEG C of dyes that begin are warming up to 80 DEG C, heat preservation dyeing 80min；
(c) fixation：Milk filaments non-woven fabrics lace is immersed in 85 DEG C of soda ash solution and carry out fixation, the fixation time is 20-
40min；
(d) it washes：Milk filaments non-woven fabrics lace is cleaned with clear water；
(e) soap boiling：Soap boiling is carried out to milk filaments non-woven fabrics lace in the solution of the 0.25-0.4g/L containing gleditsia sinensis, soap boiling temperature is
80℃；
(f) it washes：Milk filaments non-woven fabrics lace is cleaned with clear water.
With reference to GB/T 8427-2008《The textile color fastness of resistance to artificial light》What testing example 6-10 and comparative example 1 obtained
The color fastness to light of milk filaments non-woven fabrics lace.
With reference to GB/T 12703.2-2009《The evaluation part 2 of textile antistatic property：Surface density of charge》Test implementation
The antistatic performance for the milk filaments non-woven fabrics lace that example 6-10 and comparative example 1 obtain.
With reference to GB/T 21655.1-2008《The evaluation (part 1) of textile absorbing fast-drying：Individual event composite test method》
The Moisture absorbing ＆ quick drying property for the milk filaments non-woven fabrics lace that testing example 6-10 and comparative example 1 obtain.
With reference to GB/T 20944.1-2007《The evaluation part 1 of antibacterial textile performance：Agar diffusion method》Test implementation
The anti-microbial property for the milk filaments non-woven fabrics lace that example 6-10 and comparative example 1 obtain.
The color fastness to light testing record sheet of table 3, embodiment 6-10 and comparative example 1
The antistatic performance testing record sheet of table 4, embodiment 6-10 and comparative example 1
The absorbing fast-drying testing record sheet of table 5, embodiment 6-10 and comparative example 1
The testing record sheet of the anti-microbial property of table 6, embodiment 6-10 and comparative example 1
From table 2-5 it is found that compared to comparative example 1, milk filaments non-woven fabrics prepared by dyestuff and dyeing using the present invention is not
Only there is better color fastness to light, but also there is good antistatic performance, absorbing fast-drying performance and anti-microbial property.
This specific embodiment is only explanation of the invention, is not limitation of the present invention, people in the art
Member can as needed make the present embodiment the modification of not creative contribution after reading this specification, but as long as at this
It is all protected by Patent Law in the right of invention.
Claims (10)
1. a kind of milk filaments non-woven fabrics lace dyestuff, it is characterized in that：Include the component of following parts by weight：
0.2-0.3 parts of disperse orange S-4RL, 0.7-0.8 parts of dispersed ruby S-5BL, dispersion deep blue HGL 0.3-0.4 parts, ice vinegar
0.4-0.6 parts sour, 7-10 parts of neutral salt, 0.1-0.2 parts of lauryl glucosyl, 0.1-0.2 parts of paregal O, water 95-105
Part.
2. milk filaments non-woven fabrics lace dyestuff according to claim 1, it is characterized in that：The neutral salt be sodium sulphate,
At least one of potassium sulfate.
3. a kind of dyeing of milk filaments non-woven fabrics lace, it is characterized in that：Include the following steps：
Step 1：First so that the non-woven fabrics in milk filaments non-woven fabrics lace is dissolved with water, discharges；
Step 2：The milk filaments non-woven fabrics lace that step 1 is obtained is added in dyestuff as claimed in claim 1 or 2, is heated to
After 125-135 DEG C, 50-70min is kept the temperature, dyeing discharges after the completion of dyeing；
Step 3：The milk filaments non-woven fabrics lace that step 2 obtains is added to the water, functional finishing agent is added, is impregnated, sizing；
According to parts by weight, the functional finishing agent includes following component：
1-2 parts of antiseptic, 3-5 parts of ultra-violet absorber, 1-4 parts of antistatic agent, 1-2 parts of color fixing agent.
4. the dyeing of milk filaments non-woven fabrics lace according to claim 3, it is characterized in that：The antiseptic is biguanides
Class antiseptic.
5. the dyeing of milk filaments non-woven fabrics lace according to claim 4, it is characterized in that：The biguanides antiseptic
For hexamethylene.
6. the dyeing of milk filaments non-woven fabrics lace according to claim 3, it is characterized in that：The ultra-violet absorber
Select Benzotriazole Ultraviolet Stabilizer.
7. the dyeing of milk filaments non-woven fabrics lace according to claim 6, it is characterized in that：The benzotriazole is purple
Ultraviolet absorbers are one kind in UV-P, UV-327.
8. the dyeing of milk filaments non-woven fabrics lace according to claim 3, it is characterized in that：The antistatic agent is selected
Quaternary ammonium salt antistatic agent.
9. the dyeing of milk filaments non-woven fabrics lace according to claim 8, it is characterized in that：The quaternary ammonium salt resists quiet
Electric agent is one kind in stearyl trimethyl ammonium chloride, dilauryl ammonium chloride.
10. the dyeing of milk filaments non-woven fabrics lace according to claim 1, it is characterized in that：The color fixing agent is selected
One kind in color fixing agent Y, color fixing agent M.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810352597.4A CN108442134B (en) | 2018-04-18 | 2018-04-18 | Dye for milk yarn non-woven fabric lace and dyeing process thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810352597.4A CN108442134B (en) | 2018-04-18 | 2018-04-18 | Dye for milk yarn non-woven fabric lace and dyeing process thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN108442134A true CN108442134A (en) | 2018-08-24 |
| CN108442134B CN108442134B (en) | 2021-02-12 |
Family
ID=63201026
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810352597.4A Active CN108442134B (en) | 2018-04-18 | 2018-04-18 | Dye for milk yarn non-woven fabric lace and dyeing process thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN108442134B (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111254553A (en) * | 2020-03-26 | 2020-06-09 | 上海封林贸易有限公司 | Antibacterial regenerated fiber textile fabric |
Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1514053A (en) * | 2003-07-24 | 2004-07-21 | 青岛工艺美术集团公司 | Water soluble technical method of making cording |
| CN1865555A (en) * | 2005-05-18 | 2006-11-22 | 王启发 | Method for preparing wool comprising milk protein fiber and wool thereby |
| CN1884650A (en) * | 2006-05-23 | 2006-12-27 | 浙江华孚色纺有限公司 | Milk protein fiber mixed color spinning yarn and production method thereof |
| CN102851875A (en) * | 2012-08-30 | 2013-01-02 | 昆山承宇机电科技有限公司 | Dyeing and finishing process for lace fabric |
| CN104273765A (en) * | 2014-11-04 | 2015-01-14 | 苏州艾宸服饰有限公司 | Easily-dyed lace edge fabric for menswear |
| CN104420340A (en) * | 2013-09-09 | 2015-03-18 | 青岛三秀新科技复合面料有限公司 | Milk fiber dyeing technology |
| CN105507038A (en) * | 2014-10-14 | 2016-04-20 | 天津天服三悦服装有限责任公司 | Dyeing method of knitted fabric made of milk protein composite fibers |
-
2018
- 2018-04-18 CN CN201810352597.4A patent/CN108442134B/en active Active
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1514053A (en) * | 2003-07-24 | 2004-07-21 | 青岛工艺美术集团公司 | Water soluble technical method of making cording |
| CN1865555A (en) * | 2005-05-18 | 2006-11-22 | 王启发 | Method for preparing wool comprising milk protein fiber and wool thereby |
| CN1884650A (en) * | 2006-05-23 | 2006-12-27 | 浙江华孚色纺有限公司 | Milk protein fiber mixed color spinning yarn and production method thereof |
| CN102851875A (en) * | 2012-08-30 | 2013-01-02 | 昆山承宇机电科技有限公司 | Dyeing and finishing process for lace fabric |
| CN104420340A (en) * | 2013-09-09 | 2015-03-18 | 青岛三秀新科技复合面料有限公司 | Milk fiber dyeing technology |
| CN105507038A (en) * | 2014-10-14 | 2016-04-20 | 天津天服三悦服装有限责任公司 | Dyeing method of knitted fabric made of milk protein composite fibers |
| CN104273765A (en) * | 2014-11-04 | 2015-01-14 | 苏州艾宸服饰有限公司 | Easily-dyed lace edge fabric for menswear |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111254553A (en) * | 2020-03-26 | 2020-06-09 | 上海封林贸易有限公司 | Antibacterial regenerated fiber textile fabric |
| CN111254553B (en) * | 2020-03-26 | 2021-02-19 | 刘少华 | Baby sleeping pad made of antibacterial regenerated fiber textile fabric |
Also Published As
| Publication number | Publication date |
|---|---|
| CN108442134B (en) | 2021-02-12 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN101225601B (en) | Multifunctional reactive cotton ultraviolet absorbent, synthetic method and use thereof | |
| WO2018010356A1 (en) | Dyeing method for cationic dyeable polyester/polyester/nylon/spandex fabrics | |
| CN102162195B (en) | Dyeing and finishing process of washable organza fabric | |
| CN1986647A (en) | Antiseptic active cationic dye and its preparing method | |
| CN109457470A (en) | The flame-retardant silk and its preparation method and application prepared using flavones and metal salt | |
| CN106049102A (en) | Fabric color fixing agent for clothing and preparation method thereof | |
| WO2018010355A1 (en) | Dyeing method for polyester/cationic dyeable polyester/nylon/spandex fabric | |
| CN105256613A (en) | Printing and dyeing auxiliary agent, and preparation method and application thereof | |
| CN101974819B (en) | Pretreatment, dyeing and finishing process of pepper fiber woven fabric | |
| CN108049223B (en) | Color fixing agent for reactive dye dyeing and preparation method thereof | |
| CN101117775A (en) | Method for dyeing mercerizing wool or mercerizing wool fabric by yellow chrysanthemum flower dye | |
| CN108442134A (en) | Milk filaments non-woven fabrics lace dyestuff and its dyeing | |
| EP2427539B1 (en) | Bluing composition and method for treating textile articles using the same | |
| CN109576974A (en) | A kind of cotton, nylon fibre blended yarn weaved fabric few watermark dyeing technique | |
| CN110306367B (en) | Edible pigment dyeing method for cashmere fabric and colored cashmere fabric | |
| CN113123125A (en) | Preparation method of pure-mint antibacterial cool fabric and fabric prepared by adopting method | |
| CN1687520A (en) | Dedicated dye for dyeing blend fabric and mixed fabric | |
| CN102127872A (en) | Method for dyeing nylon-containing silver-plated fiber interwoven shell fabric | |
| CN103174019A (en) | Multifunctional chemical system used for scouring and bleaching cotton-polyester blended fabrics and dyeing polyester components in one bath | |
| CN103343459A (en) | Moisture absorption and quick dry sportswear polyamide yarn-pure cotton yarn mixed fabric producing method | |
| CN117418398B (en) | Jean washing auxiliary agent and jean washing method | |
| Rehman et al. | Eco-friendly dyeing of cellulosic fabric using Direct Red 28 and Direct Blue 15 dyes | |
| US20230407557A1 (en) | Method for preparing antimicrobial treatment agent for textile | |
| CN113235302A (en) | Super-concentrated transparent fabric softener | |
| CN108130734A (en) | A kind of natural tea pigment dyeing method based on chitin modified sodolin |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant |