CN108435005A - It is a kind of emulsification liquid detergent preparation process in waste liquid circulation utilize device - Google Patents
It is a kind of emulsification liquid detergent preparation process in waste liquid circulation utilize device Download PDFInfo
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- CN108435005A CN108435005A CN201810283211.9A CN201810283211A CN108435005A CN 108435005 A CN108435005 A CN 108435005A CN 201810283211 A CN201810283211 A CN 201810283211A CN 108435005 A CN108435005 A CN 108435005A
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- Prior art keywords
- emulsification
- liquid detergent
- waste liquid
- primary
- preparation process
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- 239000007788 liquid Substances 0.000 title claims abstract description 119
- 239000003599 detergent Substances 0.000 title claims abstract description 46
- 238000004945 emulsification Methods 0.000 title claims abstract description 43
- 230000004087 circulation Effects 0.000 title claims abstract description 35
- 239000002699 waste material Substances 0.000 title claims abstract description 34
- 238000002360 preparation method Methods 0.000 title claims abstract description 26
- 238000003756 stirring Methods 0.000 claims abstract description 35
- 238000002156 mixing Methods 0.000 claims abstract description 27
- 239000000839 emulsion Substances 0.000 claims abstract description 26
- 238000006243 chemical reaction Methods 0.000 claims abstract description 18
- 239000006185 dispersion Substances 0.000 claims abstract description 17
- 239000012530 fluid Substances 0.000 claims abstract description 13
- 238000005070 sampling Methods 0.000 claims abstract description 9
- 239000004576 sand Substances 0.000 claims abstract description 9
- 208000028659 discharge Diseases 0.000 claims abstract description 8
- 238000004062 sedimentation Methods 0.000 claims abstract description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 30
- 239000000463 material Substances 0.000 claims description 26
- 239000006260 foam Substances 0.000 claims description 17
- 230000010355 oscillation Effects 0.000 claims description 11
- 238000003825 pressing Methods 0.000 claims description 9
- 239000008367 deionised water Substances 0.000 claims description 8
- 229910021641 deionized water Inorganic materials 0.000 claims description 8
- 239000000523 sample Substances 0.000 claims description 7
- NJPPVKZQTLUDBO-UHFFFAOYSA-N novaluron Chemical compound C1=C(Cl)C(OC(F)(F)C(OC(F)(F)F)F)=CC=C1NC(=O)NC(=O)C1=C(F)C=CC=C1F NJPPVKZQTLUDBO-UHFFFAOYSA-N 0.000 claims description 6
- 238000010438 heat treatment Methods 0.000 claims description 5
- 229910052751 metal Inorganic materials 0.000 claims description 3
- 239000002184 metal Substances 0.000 claims description 3
- 238000005498 polishing Methods 0.000 claims description 3
- 230000008021 deposition Effects 0.000 claims 1
- 239000004480 active ingredient Substances 0.000 abstract description 14
- 239000004615 ingredient Substances 0.000 description 17
- 230000000694 effects Effects 0.000 description 15
- 238000010586 diagram Methods 0.000 description 13
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 8
- 238000003860 storage Methods 0.000 description 8
- 239000003729 cation exchange resin Substances 0.000 description 5
- 238000005516 engineering process Methods 0.000 description 5
- 238000001914 filtration Methods 0.000 description 5
- 238000004519 manufacturing process Methods 0.000 description 5
- 238000005259 measurement Methods 0.000 description 5
- 238000012545 processing Methods 0.000 description 5
- NWUYHJFMYQTDRP-UHFFFAOYSA-N 1,2-bis(ethenyl)benzene;1-ethenyl-2-ethylbenzene;styrene Chemical compound C=CC1=CC=CC=C1.CCC1=CC=CC=C1C=C.C=CC1=CC=CC=C1C=C NWUYHJFMYQTDRP-UHFFFAOYSA-N 0.000 description 4
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 4
- PPBRXRYQALVLMV-UHFFFAOYSA-N Styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 description 4
- 239000003957 anion exchange resin Substances 0.000 description 4
- 238000000034 method Methods 0.000 description 4
- 238000005406 washing Methods 0.000 description 4
- 230000008878 coupling Effects 0.000 description 3
- 238000010168 coupling process Methods 0.000 description 3
- 238000005859 coupling reaction Methods 0.000 description 3
- 230000007613 environmental effect Effects 0.000 description 3
- 230000004927 fusion Effects 0.000 description 3
- 239000012528 membrane Substances 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- 238000005192 partition Methods 0.000 description 3
- 239000000843 powder Substances 0.000 description 3
- 230000008569 process Effects 0.000 description 3
- 238000001223 reverse osmosis Methods 0.000 description 3
- 239000002351 wastewater Substances 0.000 description 3
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 2
- 150000001768 cations Chemical class 0.000 description 2
- 238000004140 cleaning Methods 0.000 description 2
- 238000005520 cutting process Methods 0.000 description 2
- 238000011161 development Methods 0.000 description 2
- 230000018109 developmental process Effects 0.000 description 2
- 230000007246 mechanism Effects 0.000 description 2
- 150000007522 mineralic acids Chemical class 0.000 description 2
- 238000003032 molecular docking Methods 0.000 description 2
- 239000004745 nonwoven fabric Substances 0.000 description 2
- 239000000741 silica gel Substances 0.000 description 2
- 229910002027 silica gel Inorganic materials 0.000 description 2
- 229910052938 sodium sulfate Inorganic materials 0.000 description 2
- 235000011152 sodium sulphate Nutrition 0.000 description 2
- 229910001220 stainless steel Inorganic materials 0.000 description 2
- 239000010935 stainless steel Substances 0.000 description 2
- 230000001954 sterilising effect Effects 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 241000124033 Salix Species 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 230000009471 action Effects 0.000 description 1
- 230000004913 activation Effects 0.000 description 1
- 239000002671 adjuvant Substances 0.000 description 1
- 230000032683 aging Effects 0.000 description 1
- 150000001450 anions Chemical class 0.000 description 1
- 230000004888 barrier function Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 125000002091 cationic group Chemical group 0.000 description 1
- 239000003610 charcoal Substances 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000002242 deionisation method Methods 0.000 description 1
- 239000000428 dust Substances 0.000 description 1
- 230000005611 electricity Effects 0.000 description 1
- 230000001804 emulsifying effect Effects 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000000945 filler Substances 0.000 description 1
- 238000011049 filling Methods 0.000 description 1
- 230000001771 impaired effect Effects 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 229910052738 indium Inorganic materials 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- 238000011068 loading method Methods 0.000 description 1
- 230000013011 mating Effects 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 230000001590 oxidative effect Effects 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 238000010008 shearing Methods 0.000 description 1
- 239000008234 soft water Substances 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 230000006641 stabilisation Effects 0.000 description 1
- 238000011105 stabilization Methods 0.000 description 1
- 239000004094 surface-active agent Substances 0.000 description 1
- 239000008399 tap water Substances 0.000 description 1
- 235000020679 tap water Nutrition 0.000 description 1
- 229910021642 ultra pure water Inorganic materials 0.000 description 1
- 239000012498 ultrapure water Substances 0.000 description 1
- 239000003643 water by type Substances 0.000 description 1
- 235000014101 wine Nutrition 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F23/00—Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
- B01F23/40—Mixing liquids with liquids; Emulsifying
- B01F23/41—Emulsifying
- B01F23/411—Emulsifying using electrical or magnetic fields, heat or vibrations
- B01F23/4111—Emulsifying using electrical or magnetic fields, heat or vibrations using vibrations
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F23/00—Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
- B01F23/40—Mixing liquids with liquids; Emulsifying
- B01F23/43—Mixing liquids with liquids; Emulsifying using driven stirrers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F31/00—Mixers with shaking, oscillating, or vibrating mechanisms
- B01F31/80—Mixing by means of high-frequency vibrations above one kHz, e.g. ultrasonic vibrations
- B01F31/83—Mixing by means of high-frequency vibrations above one kHz, e.g. ultrasonic vibrations comprising a supplementary stirring element
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F2101/00—Mixing characterised by the nature of the mixed materials or by the application field
- B01F2101/4505—Mixing ingredients comprising detergents, soaps, for washing, e.g. washing machines
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
Abstract
The invention discloses the waste liquid circulations in a kind of emulsification liquid detergent preparation process to utilize device, including primary reaction chamber, the primary reaction chamber both sides are connected with feeding equipment and tanning device by primary feed tube and primary discharge nozzle respectively, primary reaction chamber includes tank body, tank base is equipped with turbulent pump by square support, tank body side is connected with waste liquid circulation by waste fluid inlet tube and circulation fluid delivery pipe respectively and utilizes device, and emulsion dispersion device is installed at the top of square support, waste liquid circulation includes grid cistern using device, the grid cistern sequentially passes through transporting conduit and is connected with primary sedimentation pond, temperature control mixing chamber and sand filter, and it is equipped between sampling by branched pipe between primary sedimentation pond and temperature control mixing chamber；Main component is shaken and is activated, remained surface active ingredient to greatest extent, improve the washability of liquid detergent, and comprehensively utilize the remaining liq of liquid detergent, increase operation rate by the emulsification and stirring for improving liquid detergent.
Description
Technical field
The present invention relates to liquid detergent preparing technical field, the waste liquid circulation in specially a kind of emulsification liquid detergent preparation process
Utilize device.
Background technology
Prevailing with technology development and environmental protection concept, global articles for washing will tend to diversification, but energy saving, water-saving,
Efficiently, product that is mild, easy to use and meeting safety and environmental requirement by be the development of current and future cleaning product master
Flow direction.
It is well known that containing largely the filler anhydrous sodium sulphate without any cleaning function, mass fraction are more than in washing powder
40%, great waste is caused in terms of resource and the energy, can also be caused dust pollution in production, is unfavorable for environmental protection.And
Liquid detergent with resourceful and inexpensive water instead of anhydrous sodium sulphate, using biodegradable surfactant as main component
And it is aided with phosphorus-free adjuvant and compounds.Due to liquid detergent have production technology is easy, performance is mild, it is non-stimulated, easy to dissolve, make
The features such as with facilitating, overcomes some disadvantages of washing powder, have developed rapidly, be gradually accepted by people.
But also there is its deficiency as a kind of emerging promising fluid product, that is, liquid detergent detergency is not
By force, to find out its cause, being exactly during liquid detergent produces, surface active ingredient can not be preferably merged with solvent,
This results in the liquid detergent active constituent content designed according to production standard relatively low, and due to during preparation, effectively
The activity of ingredient cannot be excited adequately, and the practical effect of later stage liquid detergent is influenced.An and more main problem
It is, in existing technology, generally directly uses tap water, contain a large amount of ion in this water, it will serious shadow
Ring the fusion and use of surface active ingredient.
In existing technical solution, a kind of liquid detergent preparation facilities such as application No. is 201420799572.6 announcements,
Liquid detergent can be quickly prepared, and realizes automatic addition raw material, temperature automatically controlled, automatic stirring, automatic cycle, there is production effect
Rate is high, the feature that product quality is stable, uniformly mixed.
In summary technical solution and reality there are the problem of, and combine the technical solution being widely used at present, also
Existing major defect is mainly reflected in the following aspects：First, existing preparation facilities is only simply stirred energy
Power does not account for into emulsification, activation capacity, and which results in above-mentioned problem, active ingredient mixing is uneven, and
It is active insufficient, actual washing demand cannot be met, secondly, many underproof waste water are will produce during preparation, and
This effluent part is containing many active ingredients in fact, but these active ingredients cannot be but effectively utilized, can only
It is wasted, results in waste of resources.
Invention content
In order to overcome the shortcomings of prior art, the waste liquid that the present invention is provided in a kind of emulsification liquid detergent preparation process follows
Ring utilizes device, improves the emulsification and stirring of liquid detergent, and main component is shaken and is activated, and remains surface work to greatest extent
Property ingredient, keeps the comparison of ingredients of liquid detergent uniform, improves the washability of liquid detergent, and comprehensively utilize the raffinate of liquid detergent
Body can be utilized after treatment, increases operation rate again, can effectively solve the problem that the problem of background technology proposes.
The technical solution adopted by the present invention to solve the technical problems is：
A kind of waste liquid circulation in emulsification liquid detergent preparation process utilizes device, including primary reaction chamber described primary anti-
Room both sides are answered to be respectively equipped with primary feed tube and primary discharge nozzle, the primary feed tube is connected with feeding equipment, the primary
Discharge nozzle is connected with tanning device, and the primary reaction chamber includes tank body, and the tank base is fixedly mounted by square support
There are turbulent pump, the tank body side to be connected with waste liquid circulation by waste fluid inlet tube and circulation fluid delivery pipe respectively and utilize device,
And emulsion dispersion device is installed at the top of square support；
The waste liquid circulation includes grid cistern using device, and the grid cistern sequentially passes through the connection of transporting conduit
There are primary sedimentation pond, temperature control mixing chamber and sand filter, and is equipped with by branched pipe between primary sedimentation pond and temperature control mixing chamber
Between sampling, the temperature control mixing chamber includes liquid collecting tank, and the liquid collecting tank center is equipped with stirring rod, and solid on liquid collecting top tank structure
Dingan County is equipped with heating tube, and temperature sensor is installed at the distal center of the stirring rod.
As a kind of preferred technical solution of the present invention, the turbulent flow pump is equipped with several equally distributed liquid outlets,
Outlet tube is respectively connected on the liquid outlet, the outlet tube is equipped with several scattered holes of overflowing.
As a kind of preferred technical solution of the present invention, be respectively equipped at the top of liquid collecting tank auxiliary material addition integrated pipe and go from
Sub- water adding tube.
As a kind of preferred technical solution of the present invention, foamed filter plate, the foamed filter are equipped at the top of liquid collecting tank
Foam pressing plate of dispelling is installed on plate by connecting rod.
As a kind of preferred technical solution of the present invention, the branched pipe is equipped with connecting sleeve, includes between the sampling
Probe tube, the probe tube inside is equipped with the connecting pole coordinated with connecting sleeve, and closure valve is equipped in connecting sleeve.
As a kind of preferred technical solution of the present invention, the emulsion dispersion device includes emulsion reactor and kettle cover, institute
It states by buckling airtight connection between emulsion reactor and kettle cover, and pedestal is installed in the non-central location of kettle cover, institute
It states and is equipped with bearing holder (housing, cover) in pedestal, agitating shaft is equipped with by bearing in the bearing holder (housing, cover), conducting tube, institute are equipped at the center of agitating shaft
It states transporting pipe end and is installed with emulsification pump
As a kind of preferred technical solution of the present invention, stirring accessory lobes are installed on the outside of agitating shaft, adjacent
Swing stirring ball is equipped with by spring between stirring accessory lobes, the emulsification pump and is passed through between the stirring accessory lobes of bottommost
The fitting contact of honeycomb orifice plate, honeycomb hole board bottom portion is directly connected to emulsification pump.
As a kind of preferred technical solution of the present invention, taken by the sliding being engraved on inner wall at the top of the emulsion reactor
Plate is equipped with foamed filter plate, and foam pressing plate of dispelling is equipped with by connecting rod on the foamed filter plate.
As a kind of preferred technical solution of the present invention, the agitating shaft is in " saying " font, and the stirring accessory lobes are in " Y "
Font connects between the agitating shaft and stirring accessory lobes in such a way that polishing metal silk is in oblique pull, the agitating shaft and transporting
The metallic rod of mutual oblique is installed between pipe.
As a kind of preferred technical solution of the present invention, on the square support between the turbulent flow pump and emulsion dispersion device
It is installed with ultrasonic oscillation device.
Compared with prior art, the beneficial effects of the invention are as follows：The present invention improves the emulsification and stirring of liquid detergent, promotes
The mixing of liquid detergent ingredient, and main component is shaken and is activated also by the way that ultrasonic oscillation device is arranged during this,
And carry out that foam Over can also be prevented during emulsification treatment fusion, avoid surface active ingredient become foam cannot
It incorporates, in addition periodically the foam of generation is incorporated, surface active ingredient is remained to greatest extent, makes the comparison of ingredients of liquid detergent
Uniformly；And directly comprehensively utilize the waste water of its generation again during preparation, it can be directly by it after treatment
Active ingredient uses again, avoids the waste of active ingredient, but also can prevent pollution environment.
Description of the drawings
Fig. 1 is the overall structure diagram of the present invention；
Fig. 2 is side structure schematic diagram of the present invention；
Fig. 3 is that the secondary water conservancy diversion of the present invention rotates plate structure schematic diagram；
Fig. 4 is deionized water feeding mechanism structural schematic diagram of the present invention；
Fig. 5 is tanning device structural schematic diagram of the present invention；
Fig. 6 is skid rail structure diagram of the present invention；
Fig. 7 is the canned liquid storage bucket internal structure schematic diagram of the present invention；
Fig. 8 is feeding equipment structural schematic diagram of the present invention；
Fig. 9 is that waste liquid circulation of the present invention utilizes apparatus structure schematic diagram；
Figure 10 is temperature control mixing chamber structural schematic diagram of the present invention；
Figure 11 is structural schematic diagram between present invention sampling；
Figure 12 is cryogenic thermostat reaction kettle structural schematic diagram of the present invention；
Figure 13 is block ring cover structure schematic diagram of the present invention；
Figure label：1- primary reaction chambers；2- primary feed tubes；3- primary discharge nozzles；4- feeding equipments；The canned dresses of 5-
It sets；6- tank bodies；7- square supports；8- turbulent flows pump；9- emulsion dispersion devices；10- slides attachment strap；11- exports end pipe；12- is polished
Wire；13- metallic rods；14- ultrasonic oscillation devices；
401- major ingredient feed pipes；402- auxiliary material supplementary devices；403- oblique pull V-type cutting ferrules；404- waveform feeding end pipes；
405- auxiliary material points deposit case；406- auxiliary material delivery pipes；407- liquid pumps；408- check valves；409- multi-port converters；410- is sprayed
Shower；411- short-acting mixing chambers temporarily；412- blenders；413- circulating pipes；
The 501- shape of falling Qian holders；The inverted T shaped holders of 502-；The canned conveyer belts of 503-；The canned fixed disks of 504-；505- docking are defeated
Send band；506- sliding rails；507- sliding blocks；The canned liquid storage buckets of 508-；509- telescopic rods；510- lifting motors；511- racks；512- into
Liquid pipe；513- measurement pipes；514- closes liquid bar；515- inlet openings；516- check valves；517- closes soft silica gel umbrella crown；518- is closed
Motor；
801- liquid outlets；802- outlet tubes；803-, which overflows, dissipates hole；
901- emulsion reactors；902- kettle covers；903- is buckled；904- pedestals；905- bearing holder (housing, cover)s；906- agitating shafts；907-
Conducting tube；908- emulsification pumps；909- stirs accessory lobes；910- swings stirring ball；911- honeycomb orifice plates；
1001- foamed filter plates；1002- dispels foam pressing plate；
1101- circulation pipes；1102- circulating pumps；1103- casings；1104- grade water conservancy diversion rotor plate；1105- trident prongs
Frame；1106- coupling bars；1107- ring sets；1108- deflectors；
1501- handles tank body；1501- water inlet pipes；Tube in 1503-；1504- partition boards；1505- temporary rooms；1506- is ultrapure
Water tank；1507- reverse osmosis membranes；1508- cation exchange resin layers；1509- anion exchange resin layers；1510- embedded grooves；
1511- multistage filters；1512- stands surge tank；1513- check valves；1514- ultraviolet sterilizing lamps；1515- suction pumps；
1516- multimedium coarse filtration plates；1517- non-woven fabrics filter layers；1518- coarse sand filter layers；1519- fine sand filter layers；1520- activity
Charcoal filter layer；
1601- waste fluid inlet tubes；1602- circulation fluid delivery pipes；1603- grid cisterns；1604- transporting conduits；1605-
Primary sedimentation pond；1606- temperature control mixing chambers；1607- sand filters；1608- branched pipes；Between 1609- samplings；1610- liquid collecting tanks；
1611- stirring rod；1612- heating tubes；1613- temperature sensors；1614- auxiliary materials add integrated pipe；1615- deionized waters are added
Pipe；1616- connecting sleeves；1617- probe tubes；1618- connecting poles；1619- closure valves；
1701- autoclave bodies；1702- A-frames；1703- inner circulating tubes；1704- collector tubes；1705-L type outlet tubes；
Baffle is flowed in 1706-；1707- electric hot plates；1708- block ring covers；1709- fine filtering nets；1710- forward direction deflectors；1711-
Reverse guide plate；1712- foraminous net covers.
Specific implementation mode
Following will be combined with the drawings in the embodiments of the present invention, and technical solution in the embodiment of the present invention carries out clear, complete
Site preparation describes, it is clear that described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.It is based on
Embodiment in the present invention, it is obtained by those of ordinary skill in the art without making creative efforts every other
Embodiment shall fall within the protection scope of the present invention.
As shown in figure 1 to figure 13, the present invention provides a kind of liquid detergent process units with emulsion dispersion function, including
Primary reaction chamber 1,1 both sides of the primary reaction chamber are respectively equipped with primary feed tube 2 and primary discharge nozzle 3, the primary feed
Pipe 2 is connected with feeding equipment 4, and the primary discharge nozzle 3 is connected with tanning device 5, and the primary reaction chamber 1 includes tank body 6, institute
It states 6 bottom of tank body and turbulent flow pump 8 is installed with by square support 7,6 top of the tank body is connected with deionization by diversion pipe
Water supply, 6 side of the tank body are connected with waste liquid by waste fluid inlet tube 1601 and circulation fluid delivery pipe 1602 respectively and follow
Ring utilizes device, and is installed with emulsion dispersion device 9 at 7 top of square support.
Among the above, the effect of feeding equipment 4 is to provide liquid detergent major ingredient and auxiliary material, and since liquid detergent configured
In general requirement in journey is required to configure liquid detergent one by one according to ratio requirement, in the present embodiment, tank
Dress mode is improved, described in detail below：
The feeding equipment 4 is made of major ingredient feed pipe 401 and auxiliary material supplementary device 402, passes through 401 He of major ingredient feed pipe
Auxiliary material supplementary device 402 adds major ingredient and auxiliary material respectively, and the outlet end of the major ingredient feed pipe 401 passes through oblique pull V-type cutting ferrule 403
It is fixedly mounted on 6 inner wall of tank body, is socketed with multi-port converters 409 in the end of major ingredient feed pipe 401, the multiport turns
The outlet end of parallel operation 409 is equipped with spray shower head 410, improves major ingredient and enters the uniformity being distributed in the process.
The auxiliary material supplementary device 402 includes being fixedly mounted on waveform feeding end pipe 404 on 6 inner wall of tank body and several
A auxiliary material point deposits case 405, and the auxiliary material point is deposited case 405 and connect with waveform feeding end pipe 404 by auxiliary material delivery pipe 406,
405 bottom of case is deposited in each auxiliary material point and is equipped with liquid pump 407, and the liquid pump 407 is fixedly mounted on auxiliary by check valve 408
The inlet of material conveying tube 406, passes through above structure so that auxiliary material by mixing, is done so before entering in the reaction chamber
The advantage is that auxiliary material can be avoided to contact in advance first, chemically react between each other, and enters major ingredient reative cell in auxiliary material
Moment before, and can adequately be mixed.
As the preferred of present embodiment, the junction of each auxiliary material delivery pipe 406 and waveform feeding end pipe 404 also
Interim short-acting mixing chamber 411 is installed, blender 412, the waveform are installed at 411 top of interim short-acting mixing chamber
Feeding end pipe 404 directly connect with interim 411 bottom of short-acting mixing chamber or by circulating pipe 413 and interim short-acting mixing chamber 411
Connection.
For liquid detergent, specific prepare completes to also need to be packed or be bottled later, due to being liquid
State needs carry out quantitative as desired canned, and in present embodiment, canned mode is improved, described in detail below：
The tanning device 5 includes the shape of falling Qian holder 501, and 501 side of the shape of falling Qian holder is installed with inverted T shaped branch
Frame 502,501 upper surface of the shape of falling Qian holder are equipped with canned conveyer belt 503, pass through the conveying of 503 timing of canned conveyer belt
Come over, equidistantly canned fixed disk 504 is uniformly installed on the canned conveyer belt 503, for carrying tinning box, and tank
503 both ends of dress conveyer belt are respectively equipped with docking conveyer belt 505, have got well later tinning and institute for conveying tinning box and loading
It states 502 front of inverted T shaped holder and is equipped with sliding rail 506, canned liquid storage bucket 508 is equipped with by sliding block 507 on the sliding rail 506,
The position of canned liquid storage bucket 508 is controlled by sliding rail 506 and sliding block 507, the sliding block 507 passes through telescopic rod 509 and lifting electricity
Machine 510 connects, and 509 inside of the telescopic rod is equipped with the rack 511 engaged with 510 rotation axis gear of lifting motor, passes through tooth
The meshing relation of wheel and rack 511 controls the lengthwise position of canned liquid storage bucket 508 using lifting motor 510.
As the preferred of present embodiment, the 508 outlet at bottom end of canned liquid storage bucket is equipped with inlet tube 512, and in tank
The outlet end for filling liquid storage bucket 508 is equipped with columned measurement pipe 513, and the measurement pipe 513, which is internally provided with, closes liquid bar 514, passes through
Measurement pipe 513 is set and closes each canned quality of the determination that the relative position relation between liquid bar 514 can be quantitatively, accurately
It is again convenient, it is equipped with inlet opening 515 in the bottom of measurement pipe 513, the inlet opening 515 is internally provided with check valve 516, passes through feed liquor
515 feed liquor of hole, can fast and accurately feed liquor, and the check valve 516 being arranged can prevent liquid from pouring in down a chimney, described to close liquid bar 514
End is installed with closing soft silica gel umbrella crown 517, and is installed at the top for closing liquid bar 514 and is closed motor 518.
Wherein, the turbulent flow pump 8 is equipped with several equally distributed liquid outlets 801, is all connected on the liquid outlet 801
There are outlet tube 802, the outlet tube 802 to be equipped with several scattered holes 803 of overflowing, current stabilization pump 8 can be realized by liquid storage pipe 802
Action of turbulent flow, it is large number of due to outlet tube 802, its whole can be scatter as needed, and in present embodiment
In, in order to further promote dispersion effect, numerous scattered holes 803 of overflowing often is set on outlet tube 802, is improved actual
Shunting effect.
Preferably, it is installed with ultrasonic wave on the square support 7 between the turbulent flow pump 8 and emulsion dispersion device 9
Rocking equipment 14, in the present embodiment, the application of ultrasonic oscillation device 14 are extremely wide, such as application No. is
A kind of wines accelerating ageing device disclosed in 200620006630.0 just applies similar ultrasonic oscillation device in the application,
Its main operation principle is：Using high frequency oscillation caused by ultrasonic oscillation device, frequency of oscillation can be in 20KHZ
Within the scope of~160KHZ, the experiment that limited number of time can also be carried out according to actual demand obtains best frequency of oscillation, can be with
Accelerate composition or the mutual effect of substance, the chemical changes such as biochemical variation, oxidation is caused in addition to this can also to match
It closes and installs cooling device and heating device around media Containers, improve the effect of mixing, and ultrasonic wave has penetrability, it can
It is activated with shaking the ingredient directed contact with, the barrier that can also be penetrated between other structures is shaken.
The emulsion dispersion device 9 includes emulsion reactor 901 and kettle cover 902, the emulsion reactor 901 and kettle cover
By buckling 903 airtight connections between 902, convenient for opening and closing, and by the connection of closed structure, convenient for keeping emulsification
State consistency inside reaction kettle, and it is installed with pedestal 904 in the non-central location of kettle cover 902, in the pedestal 904
Equipped with bearing holder (housing, cover) 905, agitating shaft 906 is equipped with by bearing in the bearing holder (housing, cover) 905, is carried by the mixing effect of agitating shaft 906
The high uniformity coefficient of material mixing, is convenient for emulsion dispersion, conducting tube 907, the conducting tube is equipped at the center of agitating shaft 906
907 ends are installed with emulsification pump 908, are installed with stirring accessory lobes 909 in 906 outside of agitating shaft, stirring accessory lobes 909 carry
The sweep area of height stirring is equipped with swing stirring ball 910 by spring between adjacent stirring accessory lobes 909, destroys and formed
Stable circulation is stirred, keeps its mixing effect more preferable, the emulsification pump 908 and is led between the stirring accessory lobes 909 of bottommost
The fitting contact of honeycomb orifice plate 911 is crossed, 911 bottom of honeycomb orifice plate is directly connected to emulsification pump 908.
In the present embodiment, electric energy is the source of 908 power of emulsification pump, it, will be electric mainly by the support of electric power
It can be converted into the high-speed rotating power of bearing, will need blended product under the powerful shearing force of the high speed rotation generation of bearing
Crush, emulsify, to being come out from the bottom discharge of emulsification pump, the pump housing mainly by being formed outside pump chamber and inside pump chamber,
The material mainly used outside pump chamber is the stainless steel product of model SS316, and such material is wear-resisting, is not easy to get rusty, pump chamber
Internal structure is equally made of stainless steel, and has strong corrosive, wearability, to more good than external
Some oxidizing liquids are preferably segmented, impaired without leading to the pump housing, it is continuous that emulsification pump can be used for multi-phase fluid medium
Emulsification or dispersion, play the role of conveying simultaneously for the liquid medium of low-viscosity, can also realize that powder, liquid proportional connect
Continuous mixing.
As the preferred of present embodiment, the agitating shaft 906 is in " saying " font, and the stirring accessory lobes 909 are in " Y " word
Type connects between the agitating shaft 906 and stirring accessory lobes 909 in such a way that polishing metal silk 12 is in oblique pull, the agitating shaft
The metallic rod 13 of mutual oblique is installed between 906 and conducting tube 907.
In the present embodiment, 901 top of the emulsion reactor is equipped with by the sliding attachment strap 10 being engraved on inner wall
Foamed filter plate 1001 is equipped with foam pressing plate 1002 of dispelling by connecting rod on the foamed filter plate 1001.
Involve range in the control emulsification generation foam of foamed filter plate 1001 among the above, and in this process,
And the excessive foam generated then can be all pressed into solution by foam pressing plate 1002 of dispelling by the compacting of pressing plate, to reach
Eliminate the purpose of emulsification foam.
As preferred embodiment, it is equipped with output end pipe 11 in the bottom centre of the emulsion reactor 901, it is described defeated
Go out end pipe 11 and the circulation loop that circulating pump 1102 forms closure is connected by circulation pipe 1101, passes through set in 11 end of output end pipe
Pipe 1103 is equipped with secondary water conservancy diversion rotor plate 1104, and the output end of the circulation pipe 1101 is located under foamed filter plate 1001
The liquid of needs is carried out circulate operation by side by ringing, so that emulsifying effectiveness is more preferable, more uniform.
It further illustrates, the secondary water conservancy diversion rotor plate 1104 includes trident prong frame 1105, the trident prong
1105 center of frame is installed with coupling bar 1106, and the coupling bar 1106 is equipped with ring set 1107,1107 appearance of the ring set
Face is installed with equally distributed deflector 1108, and the deflector 1108 is in willow leaf shape, and dispersing liquid destroys original
Circulation balance so that more disorderly, the effect of raising emulsification and stirring of fluid circulation.
First, deionized water is exactly by water by cation exchange resin, then the cation in water is absorbed by resin, is set
Cationic H on fat+It is displaced in water, and with the corresponding inorganic acid of cation composition in water, the water containing such inorganic acid
Pass through anion exchange resin OH again-It is displaced in water, and water is combined into the H+ in water, this i.e. deionized water.
The deionized water feeding mechanism includes processing tank body 1501, is divided at the top and bottom of 1501 both sides of processing tank body
Not She You water inlet pipe 1502 and middle tube 1503, and handle in tank body 1501 and divided for temporary room 1505 and ultrapure by partition board 1504
Water tank 1506,1504 bottom of the partition board is connect by reverse osmosis membrane 1507 with processing 1501 bottom surface of tank body, in the reverse osmosis
The both sides of permeable membrane 1507 are respectively equipped with cation exchange resin layer 1508 and anion exchange resin layer 1509, the temporary room
It is installed with several groups embedded groove 1510 on 1505 inner walls, by Embedded mounting means, is conveniently replaceable filter layer, it is described
Multistage filter 1511 is movably installed with by snap fit in embedded groove 1510, and the arrival end of the water inlet pipe 1502 is located at
1511 top of multistage filter.
Wherein, cation exchange resin layer 1508 is commonly styrene type storng-acid cation exchange resin, anion
Exchange resin layer 1509 is commonly styrene type strong alkalinity anion.
Preferably, the middle tube 1503, which is connected with, stands surge tank 1512, in the water inlet pipe 1502 and middle tube
It is equipped with check valve 1513 on 1503, ultraviolet sterilizing lamp is equipped in the processing tank body 1501 and standing surge tank 1512
1514,1514 bottom of standing surge tank is equipped with suction pump 1515.
As preferred embodiment, the multistage filter 1511 includes multimedium coarse filtration plate 1516, the multimedium
The lower section of coarse filtration plate 1516 by being equipped with non-woven fabrics filter layer 1517, coarse sand filter layer 1518, fine sand filter layer 1519 under upper successively
With activated carbon filter layer 1520, thick impurity, suspended matter and variegated peculiar smell etc. are filtered successively, improves the preparative capacibility of deionized water,
Reduce economic cost.
The waste liquid circulation includes grid cistern 1603 using device, and the grid cistern 1603 sequentially passes through transporting
Conduit 1604 is connected with primary sedimentation pond 1605, temperature control mixing chamber 1606 and sand filter 1607, and in 1605 He of primary sedimentation pond
By branched pipe 1608 equipped with 1609 between sampling between temperature control mixing chamber 1606, the temperature control mixing chamber 1606 includes liquid collecting tank
1610,1610 center of the liquid collecting tank is equipped with stirring rod 1611, and is installed with heating tube on 1610 inner wall of liquid collecting tank
1612, temperature sensor 1613 is installed at the distal center of the stirring rod 1611.
Preferably, auxiliary material addition integrated pipe 1614 and deionized water adding tube are respectively equipped at 1610 top of liquid collecting tank
1615, it is equipped with foamed filter plate 1001 at 1610 top of liquid collecting tank, is equipped with and is dispelled by connecting rod on the foamed filter plate 1001
Foam pressing plate 1002.
As preferred embodiment, the branched pipe 1608 is equipped with connecting sleeve 1616,1609 packet between the sampling
Probe tube 1617 is included, 1617 inside of the probe tube is equipped with the connecting pole 1618 coordinated with connecting sleeve 1616, and in connector sleeve
Closure valve 1619 is equipped in pipe 1616.
Further include cryogenic thermostat reaction kettle, the cryogenic thermostat reaction kettle includes autoclave body 1701,1701 bottom of the autoclave body
Center is equipped with A-frame 1702, and is installed with inner circulating tube 1703, the inner circulating tube at 1702 center of A-frame
1703 tops are installed with collector tube 1704, and the collector tube 1704 extends to 1701 bottom of autoclave body, and in inner circulating tube
1703 two bottom sides are installed with L-type outlet tube 1705 respectively, are installed on 1701 inner wall of autoclave body and L-type outlet tube
1705 mating interior stream baffles 1706, the interior stream baffle 1706 are in inverted " L " font, the inner circulating tube 1703 and interior stream baffle
It is installed with electric hot plate 1707 on 1706, and is equipped with emulsification pump 908 between inner circulating tube 1703 and interior stream baffle 1706,
908 outside of the emulsification pump is coated with block ring cover 1708, and the block ring cover 1708 includes fine filtering net 1709, the essence
1709 outside of thin filter screen by being equipped with positive deflector 1710, reverse guide plate 1711 and foraminous net cover 1712 except interior successively.
Among the above, cryogenic thermostat reaction kettle is the preposition structure of external raising mixed effect, that is to say, that the device
It is before being located at emulsion dispersion device 9.
In summary：
(1) present invention by be arranged emulsion dispersion device, improve the emulsification and stirring of liquid detergent, promote liquid detergent at
The mixing divided, and main component is shaken and is activated also by the way that ultrasonic oscillation device is arranged during this, and emulsified
Foam Over can also be prevented during processing fusion, avoiding surface active ingredient and becoming foam cannot incorporate, in addition
Periodically the foam of generation is incorporated, surface active ingredient is remained to greatest extent, keeps the comparison of ingredients of liquid detergent uniform；
(2) and during preparation deionized water is directly acquired so that the preparation effect of liquid detergent is more preferable, due to going
Ionized water is soft water, and during emulsification and stirring, syncretizing effect is more preferable；
(3) and after liquid detergent has prepared it can carry out rapidly quantitative canned, avoid and put for a long time
Setting influences the property of liquid detergent；
(4) feed add during, by optimize adding method, for the major ingredient of single mass, directly into
Row addition, but for the auxiliary material of a variety of properties, before addition, by independent conveying, and before it will enter,
It is mixed rapidly, reaches auxiliary material and uniformly mix, equally distributed purpose；
(5) and during preparation the waste water for directly comprehensively utilizing its generation again, can be straight after treatment
It connects and uses its active ingredient again, avoid the waste of active ingredient, but also pollution environment can be prevented；
(6) during preparation, promote to merge by way of cryogenic thermostat, improve the efficiency of reaction, and then whole
Production efficiency on upper promotion integrated artistic, meets generation demand.
It is obvious to a person skilled in the art that invention is not limited to the details of the above exemplary embodiments, Er Qie
In the case of without departing substantially from spirit or essential attributes of the invention, the present invention can be realized in other specific forms.Therefore, no matter
From the point of view of which point, the present embodiments are to be considered as illustrative and not restrictive, and the scope of the present invention is by appended power
Profit requires rather than above description limits, it is intended that all by what is fallen within the meaning and scope of the equivalent requirements of the claims
Variation is included within the present invention.Any reference signs in the claims should not be construed as limiting the involved claims.
Claims (10)
1. the waste liquid circulation in a kind of emulsification liquid detergent preparation process utilizes device, including primary reaction chamber (1), described primary anti-
Room (1) both sides are answered to be respectively equipped with primary feed tube (2) and primary discharge nozzle (3), the primary feed tube (2) is connected with charging dress
It sets (4), the primary discharge nozzle (3) is connected with tanning device (5), it is characterised in that：The primary reaction chamber (1) includes tank body
(6), tank body (6) bottom is installed with turbulent flow pump (8) by square support (7), and tank body (6) side passes through respectively
Waste fluid inlet tube (1601) and circulation fluid delivery pipe (1602) are connected with waste liquid circulation and utilize device, and in square support (7)
Top is installed with emulsion dispersion device (9)；
The waste liquid circulation includes grid cistern (1603) using device, and the grid cistern (1603) sequentially passes through transporting
Conduit (1604) is connected with primary sedimentation pond (1605), temperature control mixing chamber (1606) and sand filter (1607), and in primary deposition
By branched pipe (1608) equipped with (1609) between sampling, the temperature control mixing chamber between pond (1605) and temperature control mixing chamber (1606)
(1606) include liquid collecting tank (1610), liquid collecting tank (1610) center is equipped with stirring rod (1611), and in liquid collecting tank
(1610) it is installed with heating tube (1612) on inner wall, temperature is installed at the distal center of the stirring rod (1611)
Sensor (1613).
2. the waste liquid circulation in a kind of emulsification liquid detergent preparation process according to claim 1 utilizes device, feature to exist
In：The turbulent flow pump (8) is equipped with several equally distributed liquid outlets (801), is respectively connected with out on the liquid outlet (801)
Liquid pipe (802), the outlet tube (802) are equipped with several and overflow scattered hole (803).
3. the waste liquid circulation in a kind of emulsification liquid detergent preparation process according to claim 1 utilizes device, feature to exist
In：Auxiliary material addition integrated pipe (1614) and deionized water adding tube (1615) are respectively equipped at the top of liquid collecting tank (1610).
4. the waste liquid circulation in a kind of emulsification liquid detergent preparation process according to claim 1 utilizes device, feature to exist
In：It is equipped with foamed filter plate (1001) at the top of liquid collecting tank (1610), is installed by connecting rod on the foamed filter plate (1001)
It dispels foam pressing plate (1002).
5. the waste liquid circulation in a kind of emulsification liquid detergent preparation process according to claim 1 utilizes device, feature to exist
In：The branched pipe (1608) is equipped with connecting sleeve (1616), and (1609) include probe tube (1617) between the sampling, described
It is equipped with the connecting pole (1618) coordinated with connecting sleeve (1616) on the inside of probe tube (1617), and is set in connecting sleeve (1616)
There is closure valve (1619).
6. the waste liquid circulation in a kind of emulsification liquid detergent preparation process according to claim 1 utilizes device, feature to exist
In：The emulsion dispersion device (9) includes emulsion reactor (901) and kettle cover (902), the emulsion reactor (901) and kettle
Between lid (902) pedestal is installed with by buckle (903) airtight connection, and in the non-central location of kettle cover (902)
(904), bearing holder (housing, cover) (905) is equipped in the pedestal (904), the bearing holder (housing, cover) (905) is interior to be equipped with agitating shaft by bearing
(906), it is equipped with conducting tube (907) at the center of agitating shaft (906), conducting tube (907) end is installed with emulsification pump
(908)。
7. the waste liquid circulation in a kind of emulsification liquid detergent preparation process according to claim 6 utilizes device, feature to exist
In：It is installed with stirring accessory lobes (909) on the outside of agitating shaft (906), passes through spring between adjacent stirring accessory lobes (909)
Be equipped with swing stirring ball (910), the emulsification pump (908) be located at bottommost stirring accessory lobes (909) between pass through honeycomb
Orifice plate (911) fitting contact, honeycomb orifice plate (911) bottom is directly connected to emulsification pump (908).
8. the waste liquid circulation in a kind of emulsification liquid detergent preparation process according to claim 6 utilizes device, feature to exist
In：Foamed filter plate (1001) is equipped with by the sliding attachment strap (10) being engraved on inner wall at the top of the emulsion reactor (901),
Foam pressing plate (1002) of dispelling is installed by connecting rod on the foamed filter plate (1001).
9. the waste liquid circulation in a kind of emulsification liquid detergent preparation process according to claim 6 utilizes device, feature to exist
In：The agitating shaft (906) is in " saying " font, and the stirring accessory lobes (909) are in " Y " font, the agitating shaft (906) and is stirred
It mixes between accessory lobes (909) through polishing metal silk (12) in being connected by way of oblique pull, the agitating shaft (906) and conducting tube
(907) metallic rod (13) of mutual oblique is installed between.
10. the waste liquid circulation in a kind of emulsification liquid detergent preparation process according to claim 1 utilizes device, feature to exist
In：It is installed with ultrasonic oscillation device on square support (7) between the turbulent flow pump (8) and emulsion dispersion device (9)
(14)。
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|---|---|---|---|
| CN201810283211.9A CN108435005A (en) | 2018-04-02 | 2018-04-02 | It is a kind of emulsification liquid detergent preparation process in waste liquid circulation utilize device |
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| CN201810283211.9A CN108435005A (en) | 2018-04-02 | 2018-04-02 | It is a kind of emulsification liquid detergent preparation process in waste liquid circulation utilize device |
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ID=63198679
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| CN201810283211.9A Pending CN108435005A (en) | 2018-04-02 | 2018-04-02 | It is a kind of emulsification liquid detergent preparation process in waste liquid circulation utilize device |
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