CN108147900A - Effervescent formulation of instant ecology fish guano and preparation method thereof and instant ecological fish guano and preparation method thereof - Google Patents
Effervescent formulation of instant ecology fish guano and preparation method thereof and instant ecological fish guano and preparation method thereof Download PDFInfo
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- CN108147900A CN108147900A CN201810149397.9A CN201810149397A CN108147900A CN 108147900 A CN108147900 A CN 108147900A CN 201810149397 A CN201810149397 A CN 201810149397A CN 108147900 A CN108147900 A CN 108147900A
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05B—PHOSPHATIC FERTILISERS
- C05B7/00—Fertilisers based essentially on alkali or ammonium orthophosphates
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G5/00—Fertilisers characterised by their form
- C05G5/10—Solid or semi-solid fertilisers, e.g. powders
- C05G5/12—Granules or flakes
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Abstract
The present invention provides effervescent formulation of a kind of instant ecological fish guano and preparation method thereof and instant ecological fish guano and preparation method thereof, and in terms of parts by weight, which includes：0.1 0.3 parts of 10 40 parts of Xanthohumate, 10 40 parts of hair-hydrolyzation amino acid powder, 10 25 parts of inorganic fertilizer, micro- 15 parts middle, 0.1 2 parts of probiotics and plant growth regulator.The present invention constructs a kind of complete molten, instant ecological fish guano, can promote algae and mushroom breeding by the quick diffusion of nutrition, dissolved oxygen, carbon dioxide and the plant cell factor, increase water body basicity, so as to build more stable water body.
Description
Technical field
The invention belongs to ecological fish fertilizer technology field, more particularly, to a kind of instant ecological fish guano and preparation method thereof
With the effervescent formulation of instant ecological fish guano and preparation method thereof.
Background technology
With Environmental protection attention degree it is higher and higher, although the river in China, river, lake, library net cage or fence
It is largely removed or is migrated, but pond culture especially high density intensive culture will be over a long time quite China from now on
The aquaculture pattern of mainstream.The pattern rely on high density seed put in a suitable place to breed, feedstuff feeding, chemical fertilizer application, regular drug epidemic prevention, into
And obtain high yield.At present, in the market rich water product mainly based on chemical fertilizer, base manure then mainly based on organic fertilizer, mostly feces of livestock and poultry,
But because application base manure human cost is huge, more and more raisers start directly to supplement organic fertilizer in the breeding process.Tradition
Organic fertilizer derives from a wealth of sources (such as feces of livestock and poultry, cripple, stalk), cheap, lasting using rear fertilizer efficiency, but decomposes slowly,
A large amount of oxygen is consumed when easily growing germ, and decomposing, using the improper hypoxia death for easily causing aquatic livestock.Same duration
Phase can also cause water body muddiness, substrate to deteriorate using the insoluble or not decomposed organic fertilizer of powdery, easily cause water body environment cataclysm.
However, although nutritional ingredient is more single contained by inorganic fertilizer, effect is rapid, and the fertility duration is shorter and easily causes list
The excessive multiplication of one algae.Water column stability is destroyed greatly in high temperature season, and easily causes fish disease.
During current fertilizer application, existing single administration (such as urea, ammonium bicarbonate, potash fertilizer, phosphorus ammonium)；Direct stacking hanging bag is sprinkled
(such as chicken manure hanging bag, pool angle stacking, make compost and splash) is spilt, also has raiser to apply the compound proportioning of organic fertilizer and inorganic fertilizer, but
Instantly, more raisers then select direct commodity in use composite fertilizer or compound organic and inorganic fertilizer to human cost Gao Qi.At present,
Fish guano in the market has paste (such as Fertilizer water paste), powdery (such as chicken manure, fulvic acid) and graininess (such as composite fertilizer), have it is water-soluble and
Insoluble point, but so far there is not yet the ecological fish guano of effervesce dosage form.Also rarely have for intensive aquaculture in formula design
There are the problem of and the dispensing that designs, such as there are the basic eutrophication of water body, feed is largely fed and itself nutrient turns in feed
Rate is insufficient and the problems such as unconverted substance influences aquatic health；Such as in feed N to fish body conversion ratio not
Foot 40%, the substance for largely failing conversion are present in water body and bottom material of pond for breeding in different forms, serious threat aquatic livestock
Health；Moreover nutrient is unbalance in chronic administration composite fertilizer or single chemical fertilizer, most probably aggravation water body, further breaks
Algae phase in pond, bacterium are balanced each other, and then the substance of breeding water body is caused to recycle and is obstructed with energy flow, so as to which animal be caused to give birth to
It is long slowly to occur with disease.Therefore, current fertilizer is often up to the ideal effect less than fertilising institute's phase.
Invention content
The defects of the purpose of the present invention is overcoming the prior art, provides a kind of instant ecological fish guano and its effervescent formulation, profit
With rational ecological fish fertilizer formula combination effervesce technique, and then it is often difficult continual and steady to effectively realize water quality in aquaculture process
The problem of.
To achieve these goals, the first aspect of the present invention provides a kind of instant ecological fish guano, should in terms of parts by weight
Fish guano includes：10-40 parts of Xanthohumate, 10-40 parts of hair-hydrolyzation amino acid powder, 10-25 parts of inorganic fertilizer, middle trace element 1-5
0.1-0.3 parts of part, 0.1-2 parts of probiotics and plant growth regulator.
The second aspect of the present invention provides a kind of preparation method of above-mentioned instant ecological fish guano, which includes：
The donor of Xanthohumate, hair-hydrolyzation amino acid powder, inorganic fertilizer and middle trace element is uniformly mixed, obtains first
Mixed powder；
Part first mixed material with probiotics and plant growth regulator is uniformly mixed, it is mixed to obtain second
Close powder；
Second mixed powder and remaining first mixed powder are uniformly mixed, obtain the instant ecological fish
Fertilizer.
The third aspect of the present invention provides a kind of effervescent formulation of instant ecological fish guano, in terms of parts by weight, the effervesce system
Agent includes：Instant ecological 31.2-112.3 parts of fish guano in claim 1-6 described in any one, 10-40 parts of sodium bicarbonate, winestone
3-15 parts sour, 0.1-3 parts of polyethylene glycol and polyethylene adjoin 0.1-4 parts of pyrrolidone.
The fourth aspect of the present invention provides a kind of preparation method of the effervescent formulation of above-mentioned instant ecological fish guano, and feature exists
In the preparation method includes：
The instant ecological fish guano in part, sodium bicarbonate and part polyethylene are adjoined pyrrolidone ethanol solution and be uniformly mixed, is then squeezed
It presses through sieve to be granulated, obtains the first particle；
Remaining instant ecological fish guano, tartaric acid and remaining polyethylene are adjoined pyrrolidone ethanol solution and be uniformly mixed, so
Sieving is squeezed afterwards to be granulated, and obtains the second particle；
First particle and second particle are uniformly mixed, polyethylene glycol is then added in and carries out tabletting, after dry
Obtain the effervescent formulation of the instant ecological fish guano.
Technical scheme of the present invention has the following advantages that：
(1) present invention constructs a kind of complete molten, instant ecological fish guano, can pass through nutrition, dissolved oxygen, carbon dioxide and plant
The quick diffusion of object cell factor promotes algae and mushroom breeding, increases water body basicity, so as to build more stable water body；
(2) present invention by effervesce technique, it can be achieved that balanced rich water at the middle and upper levels and water transfer function；Cause water energy stream
Efficiency of movement greatly improves；
(3) rich water effect of the invention is fast, provides full nutrition for diatom and monoplast green alga, prevents single algae excessive
Breeding, promotes the balanced sustainable development of water body, even if can also obtain good rich water effect in low temperature season；
(4) present invention utilizes the breeding of bioflocculation bacterium, builds the small ecosystem so that water quality can be for quite a long time
It is interior to keep stablizing, the usage amount of pond fertilizer can be reduced, inhibits cyanobacteria and Euglena wawter bloom in high temperature season.
Other features and advantages of the present invention will be described in detail in subsequent specific embodiment part.
Description of the drawings
Exemplary embodiment of the invention is described in more detail in conjunction with the accompanying drawings, it is of the invention above-mentioned and its
Its purpose, feature and advantage will be apparent, wherein, in exemplary embodiment of the invention, identical reference label
Typically represent same parts.
Fig. 1-1 to Fig. 1-9 respectively illustrates the effervesce of the instant ecological fish guano of addition according to an embodiment of the invention
After preparation in water body bioflocculation structure chart.
Specific embodiment
The preferred embodiment of the present invention is described in more detail below.Although the following describe the preferred implementations of the present invention
Mode, however, it is to be appreciated that may be realized in various forms the present invention without should be limited by embodiments set forth herein.Phase
Instead, these embodiments are provided so that the present invention is more thorough and complete, and can be by the scope of the present invention completely
It is communicated to those skilled in the art.
The first aspect of the present invention provides a kind of instant ecological fish guano, and in terms of parts by weight, which includes：Xanthohumate
10-40 parts, 10-40 parts of hair-hydrolyzation amino acid powder, 10-25 parts of inorganic fertilizer, middle 1-5 parts of trace element, probiotics 0.1-2
0.1-0.3 parts of part and plant growth regulator.
In the present invention, the content of organic matter of hair-hydrolyzation amino acid powder is more than 40%, and the content of amino acid is in 20-40%
Between.
The present invention is introduced simultaneously by water-soluble organic fertilizer, inorganic fertilizer, middle micro-, bioflocculation bacterium rational proportion
Plant cell regulatory factor, can effectively facilitate algal grown, even if can also obtain preferable rich water effect in low temperature water body,
In the water body that organic matter is abundant, by the addition and culture of bioflocculation bacterium, structure population algae (such as diatom and single celled green
Algae) and the small ecological environment of mushroom, water body can be made to keep stable state within considerable time.
In accordance with the present invention it is preferred that the Xanthohumate is SODLUM FULVATE and/or potassium fulvate.
Potassium fulvate is a kind of pure natural minerals activity potassium element fertilizer, and fulvic acid is extracted from plant using biochemical technology
Then potassium fulvate is made with potassium oxide, potassium fulvate includes trace element, rare earth element, plant growth regulator, virus suppression
The multiple nutritional components such as preparation, make that nutrient is more sufficient, supply is more reasonable, are caused when lacking nutrient so as to avoid crop
Various physiological disturbances generation.
In accordance with the present invention it is preferred that the inorganic fertilizer includes sulphur ammonium, monoammonium phosphate and potassium chloride, the sulphur ammonium, phosphoric acid one
The mass ratio of ammonium and potassium chloride is (1-10)：(3-8)：(3-8).
Preferably, in the 1-5 months, the addition mass ratio of sulphur ammonium, monoammonium phosphate and potassium chloride is 4：3：3；The 6-9 months
When, the addition mass ratio of sulphur ammonium, monoammonium phosphate and potassium chloride is 1：1：2；During the 10-12 months, sulphur ammonium, monoammonium phosphate and potassium chloride
It is 2 to add mass ratio：4：4.
In the present invention, inorganic fertilizer mainly provides N, P, K necessary to water body rich water, and can generate part algae photosynthesis institute
The CO needed2。
In accordance with the present invention it is preferred that the donor of the middle trace element includes：Monosilicate, magnesium sulfate, zinc sulfate, sulphur
Sour manganese and ironic citrate；With the total weight of instant ecological fish guano, the monosilicate is 0.4-2wt%, magnesium sulfate 0.4-
1wt%, zinc sulfate 0.02-0.05wt%, manganese sulfate are 0.1-1.5wt% and ironic citrate is 0.1-1wt%.
In the present invention, the middle main required nutrient that algae and fungus grown are provided of trace element.
In accordance with the present invention it is preferred that the probiotics are biological flocculated bacteria；The bioflocculation bacterium bag includes withered grass bud
Spore bacillus bacterium powder and/or rhodococcus erythropolis bacterium powder.
Preferably, the addition mass ratio of the bacillus subtilis bacterium powder and rhodococcus erythropolis bacterium powder is 1-2:1.
In the present invention, the bacterial content of the bacillus subtilis bacterium powder and rhodococcus erythropolis bacterium powder is 20,000,000,000/more than g.
In accordance with the present invention it is preferred that the plant growth regulator includes sour diethylaminoethanol ester and/or α-naphthalene second
Sour sodium.α-naphthaleneacidsodium is preferably high-purity α-naphthaleneacidsodium.
Preferably, when the plant growth regulator is sour diethylaminoethanol ester and α-naphthaleneacidsodium, institute
It is 1-2 to state the mass ratio of sour diethylaminoethanol ester and α-naphthaleneacidsodium:1.
Sour diethylaminoethanol ester (DA-6), molecular formula, C12H25NO2, it is white, light yellow or brown powder crystal,
It is a kind of with wide spectrum and efficient plant growth regulator, activity is wider, and early period can accelerate nutrition life with DA-6, plant
Long, the duration is long, acts on still relatively continuing at low temperature；α-naphthaleneacidsodium (C12H9O2Na) can individually, also and other
Product is used in compounding, can enhance the drought resisting of plant, cold-resistant, disease-resistant, salt resistance alkali, hot-dry wind tolerance ability.
The second aspect of the present invention provides a kind of preparation method of above-mentioned instant ecological fish guano, which includes：
The donor of Xanthohumate, hair-hydrolyzation amino acid powder, inorganic fertilizer and middle trace element is uniformly mixed, obtains first
Mixed powder；
Part first mixed material with probiotics and plant growth regulator is uniformly mixed, it is mixed to obtain second
Close powder；
Second mixed powder and remaining first mixed powder are uniformly mixed, obtain the instant ecological fish
Fertilizer.
In the present invention, each raw material for preparing instant ecological fish guano is fine-powdered, and average grain diameter is 80 mesh.
The third aspect of the present invention provides a kind of effervescent formulation of instant ecological fish guano, in terms of parts by weight, the effervesce system
Agent includes：Instant ecological 31.2-112.3 parts of fish guano in claim 1-6 described in any one, 10-40 parts of sodium bicarbonate, winestone
3-15 parts sour, 0.1-3 parts of polyethylene glycol and polyethylene adjoin 0.1-4 parts of pyrrolidone.
The effervescent formulation of efficiently complete molten ecological fish guano fully considers the unbalanced problem of nutrient in pond waters, by water-soluble
The rational proportion of organic fertilizer and inorganic fertilizer, using effervescent formulation technique, rapidly by the algae cell growth factor, oxygen, titanium dioxide
Carbon and nutrient are quickly sent to algae and water, and improve the basicity on fertilising periphery, can effectively facilitate bacterium and algal grown, right
The population advantage of diatom and single celled green alga is kept, so that breeding water body also quickly can cause water quality by rich water at low temperature
Stable state can be kept within considerable time.Meanwhile in the abundant water body of organic matter, pass through the training of bioflocculation bacterium so that
Itself and algae, zooplankter, organic debris, animal wastes, nutriment etc. form the small ecosystem, accelerate energy in water body
It is flowed with substance, and then reduces feed coefficient, water quality is made to keep stable state within the long duration, in high temperature season, effect is more
Significantly.
In the present invention, polyethylene glycol (PEG4000) and polyethylene adjoin during pyrrolidone (PVP) is respectively effervescent formulation
Lubricant and adhesive.
The fourth aspect of the present invention provides a kind of preparation method of the effervescent formulation of above-mentioned instant ecological fish guano, the preparation side
Method includes：
The instant ecological fish guano in part, sodium bicarbonate and part polyethylene are adjoined pyrrolidone ethanol solution and be uniformly mixed, is then squeezed
It presses through sieve to be granulated, obtains the first particle；
Remaining instant ecological fish guano, tartaric acid and remaining polyethylene are adjoined pyrrolidone ethanol solution and be uniformly mixed, so
Sieving is squeezed afterwards to be granulated, and obtains the second particle；
First particle and second particle are uniformly mixed, polyethylene glycol is then added in and carries out tabletting, after dry
Obtain the effervescent formulation of the instant ecological fish guano.Drying temperature is 50-75 DEG C.
Preferably, the instant ecological fish guano that the instant ecological fish guano in part is 40-80wt%, remaining instant ecological fish
Instant ecological fish guano of the fertilizer for 20-60wt%.
In the present invention, each raw material for preparing the effervescent formulation of instant ecological fish guano is fine-powdered, and average grain diameter is 80 mesh.
The average grain diameter of first particle and the second particle is 30 mesh.
In accordance with the present invention it is preferred that the solid-liquid ratio that the polyethylene adjoins pyrrolidone ethanol solution is 3-10:100, unit is
g/ml。
It further illustrates the present invention by the following examples：
The unit of solid-liquid ratio that the polyethylene of following embodiment configuration adjoins pyrrolidone ethanol solution is g/ml.
Embodiment 1
The present embodiment provides a kind of effervescent formulations of instant ecological fish guano, and in terms of parts by weight, which includes：It is small
40 parts of soda, 15 parts of hair-hydrolyzation amino acid powder, 15 parts of potassium fulvate, 7 parts of sulphur ammonium, 5 parts of monoammonium phosphate, 5 parts of potassium chloride, poly- second
Alkene adjoins 3 parts of pyrrolidone, middle micro- 3 parts, 5 parts of tartaric acid, 1.5 parts of polyethylene glycol (PEG4000), 0.3 part of probiotics,
Sour 0.1 part of diethylaminoethanol ester, 0.1 part of α-naphthaleneacidsodium；Wherein, the donor of the middle trace element is monosilicate
1.5 parts, 0.5 part of magnesium sulfate, 0.05 part of zinc sulfate, 0.45 part of manganese sulfate, 0.5 part of ironic citrate；The probiotics are withered
Careless bacillus bacterium powder, dosage are 0.3 part.
Preparation method is：By each solid material after ultramicro grinding, 80 mesh sieve is crossed, in dry environments, is claimed according to formula
Take corresponding weight；It is 5 that polyethylene, which is adjoined pyrrolidone (PVP-K30) to be prepared into solid-liquid ratio,:100 ethanol solution, when granulation, make
With；By after crushing potassium fulvate, hair-hydrolyzation amino acid powder, sulphur ammonium, monoammonium phosphate, potassium chloride and monosilicate, magnesium sulfate,
Zinc sulfate, manganese sulfate, ironic citrate are uniformly mixed, and obtain the first mixed powder；By the first mixed material of part and Tiny ecosystem system
Agent, sour diethylaminoethanol ester (DA-6) and α-naphthaleneacidsodium have been uniformly mixed, obtain the second mixed powder；By the second mixed powder
Material and remaining first mixed powder are uniformly mixed, and obtain instant ecological fish guano；The instant ecological fish guano of 70wt% is taken, is added in small
Soda and mixing, adjoin pyrrolidone (PVP-K30) ethanol solution using the polyethylene that blowing portion has been configured while stirring, squeezed
30 mesh sieve is granulated, and cuts off to obtain the first particle；The instant ecological fish guano of remaining 30wt% is taken, tartaric acid and mixing are added in, while stirring
It mixes side and pyrrolidone (PVP-K30) ethanol solution is adjoined using the remaining polyethylene being configured of spraying, squeezed 30 mesh sieve and be granulated, and cut
Break to obtain the second particle；First particle and second particle are uniformly mixed, the poly- second two weighed is uniformly added on surface
Alcohol (PEG4000) carry out tabletting, at 65 DEG C wind cold drying to get instant ecological fish guano effervescent formulation.
Embodiment 2
The present embodiment provides a kind of effervescent formulations of instant ecological fish guano, and in terms of parts by weight, which includes：It is small
30 parts of soda, 5 parts of hair-hydrolyzation amino acid powder, 35 parts of potassium fulvate, 10 parts of tartaric acid, 2 parts of sulphur ammonium, 5 parts of monoammonium phosphate, chlorination
5 parts of potassium, polyethylene adjoin 2 parts of pyrrolidone, middle micro- 3 parts, 2.5 parts of polyethylene glycol (PEG4000), sour diethylaminoethanol
0.2 part of ester, 0.3 part of probiotics；Wherein, the donor of the middle trace element be 1.0 parts of monosilicate, 1.0 parts of magnesium sulfate,
0.02 part of zinc sulfate, 0.1 part of manganese sulfate, 0.88 part of ironic citrate；The probiotics be bacillus subtilis bacterium powder, dosage
It is 0.3 part.
Preparation method is：By each solid material after ultramicro grinding, 80 mesh sieve is crossed, in dry environments, is claimed according to formula
Take corresponding weight；It is 5 that polyethylene, which is adjoined pyrrolidone (PVP-K30) to be prepared into solid-liquid ratio,:100 ethanol solution, when granulation, make
With；By potassium fulvate, hair-hydrolyzation amino acid powder, sulphur ammonium, monoammonium phosphate, potassium chloride and monosilicate, magnesium sulfate, zinc sulfate,
Manganese sulfate, ironic citrate are uniformly mixed, and obtain the first mixed powder；It is by the first mixed material of part and bioflocculation bacterium and sour
Diethylaminoethanol ester (DA-6) is uniformly mixed, and obtains the second mixed powder；By the second mixed powder and remaining first mixing
Powder is uniformly mixed, and obtains instant ecological fish guano；The instant ecological fish guano of 60wt% is taken, adds in sodium bicarbonate and mixing, side stirring
Pyrrolidone (PVP-K30) ethanol solution is adjoined in side using the polyethylene that blowing portion has been configured, and squeezed 30 mesh sieve and is granulated, and cut off
First particle；The instant ecological fish guano of remaining 40wt% is taken, tartaric acid and mixing is added in, is matched while stirring using spraying residue
The polyethylene put adjoins pyrrolidone (PVP-K30) ethanol solution, squeezed 30 mesh sieve and is granulated, and cut off to obtain the second particle；By described in
First particle and second particle are uniformly mixed, be uniformly added on surface the polyethylene glycol (PEG4000) that weighs carry out tabletting,
At 65 DEG C wind cold drying to get instant ecological fish guano effervescent formulation.
Embodiment 3
The present embodiment provides a kind of effervescent formulations of instant ecological fish guano, and in terms of parts by weight, which includes：It is small
20 parts of soda, 35 parts of hair-hydrolyzation amino acid powder, 10 parts of potassium fulvate, 2 parts of sulphur ammonium, 6 parts of monoammonium phosphate, 5 parts of potassium chloride, poly- second
Alkene adjoins 3 parts of pyrrolidone, middle micro- 4 parts, 11 parts of tartaric acid, 2.7 parts of polyethylene glycol (PEG4000), α-naphthaleneacidsodium 0.3
Part, 1 part of probiotics；Wherein, the donor of the middle trace element be 2 parts of monosilicate, 0.5 part of magnesium sulfate, zinc sulfate
0.05 part, 0.45 part of manganese sulfate, 1 part of ironic citrate；The probiotics are rhodococcus erythropolis bacterium powder, and dosage is 1 part.
Preparation method is：By each solid material after ultramicro grinding, 80 mesh sieve is crossed, in dry environments, is claimed according to formula
Take corresponding weight；It is 5 that polyethylene, which is adjoined pyrrolidone (PVP-K30) to be prepared into solid-liquid ratio,:100 ethanol solution, when granulation, make
With；By potassium fulvate, hair-hydrolyzation amino acid powder, sulphur ammonium, monoammonium phosphate, potassium chloride and monosilicate, magnesium sulfate, zinc sulfate,
Manganese sulfate, ironic citrate are uniformly mixed, and obtain the first mixed powder；By the first mixed material of part and probiotics and α-naphthalene
Sodium acetate is uniformly mixed, and obtains the second mixed powder；Second mixed powder and remaining first mixed powder are uniformly mixed, obtained
To instant ecological fish guano；The instant ecological fish guano of 50wt% is taken, sodium bicarbonate and mixing is added in, is matched while stirring using blowing portion
The polyethylene put adjoins pyrrolidone (PVP-K30) ethanol solution, squeezed 30 mesh sieve and is granulated, and cut off to obtain the first particle；Take residue
50wt% instant ecological fish guano, tartaric acid and mixing are added in, while stirring using the remaining polyethylene being configured of spraying
Adjoin pyrrolidone (PVP-K30) ethanol solution, squeezed 30 mesh sieve and be granulated, and cut off to obtain the second particle；By first particle and institute
It states the second particle to be uniformly mixed, the polyethylene glycol (PEG4000) that weighs is uniformly added on surface and carries out tabletting, air-cooled at 65 DEG C
The dry effervescent formulation to get instant ecological fish guano.
Embodiment 4
The present embodiment provides a kind of effervescent formulations of instant ecological fish guano, and in terms of parts by weight, which includes：It is small
25 parts of soda, 15 parts of hair-hydrolyzation amino acid powder, 15 parts of potassium fulvate, 7 parts of sulphur ammonium, 8 parts of monoammonium phosphate, 5 parts of potassium chloride, poly- second
Alkene adjoins 3 parts of pyrrolidone, middle micro- 5 parts, 14 parts of tartaric acid, 2.3 parts of polyethylene glycol (PEG4000), probiotics 0.5
Part, 0.1 part of α-naphthaleneacidsodium and sour 0.1 part of diethylaminoethanol ester；Wherein, the donor of the middle trace element is single silicic acid
2 parts of salt, 1 part of magnesium sulfate, 0.05 part of zinc sulfate, 0.45 part of manganese sulfate, 1 part of ironic citrate；The probiotics are withered grass bud
Spore bacillus bacterium powder and rhodococcus erythropolis bacterium powder, bacillus subtilis dosage are 0.3 part, and rhodococcus erythropolis bacterium powder dosage is 0.2 part.
Preparation method is：By each solid material after ultramicro grinding, 80 mesh sieve is crossed, in dry environments, is claimed according to formula
Take corresponding weight；It is 5 that polyethylene, which is adjoined pyrrolidone (PVP-K30) to be prepared into solid-liquid ratio,:100 ethanol solution, when granulation, make
With；By potassium fulvate, hair-hydrolyzation amino acid powder, sulphur ammonium, monoammonium phosphate, potassium chloride and monosilicate, magnesium sulfate, zinc sulfate,
Manganese sulfate, ironic citrate are uniformly mixed, and obtain the first mixed powder；By the first mixed material of part and probiotics, it is sour
Diethylaminoethanol ester (DA-6) and α-naphthaleneacidsodium are uniformly mixed, and obtain the second mixed powder；By the second mixed powder and remain
The first remaining mixed powder is uniformly mixed, and obtains instant ecological fish guano；The instant ecological fish guano of 50wt% is taken, adds in sodium bicarbonate simultaneously
Mixing adjoins pyrrolidone (PVP-K30) ethanol solution using the polyethylene that blowing portion has been configured while stirring, squeezes 30 mesh sieve
It is granulated, cuts off to obtain the first particle；The instant ecological fish guano of remaining 50wt% is taken, tartaric acid and mixing is added in, adopts while stirring
With spraying, remaining polyethylene be configured adjoins pyrrolidone (PVP-K30) ethanol solution, squeezed 30 mesh and sieves granulation, cut off the
Two particles；First particle and second particle are uniformly mixed, the polyethylene glycol weighed is uniformly added on surface
(PEG4000) carry out tabletting, at 65 DEG C wind cold drying to get instant ecological fish guano effervescent formulation.
Test case 1
The effervescent formulation of the instant ecological fish guano of the embodiment of the present invention 4 is added in the small size pond of laboratory, test adds
The bioflocculation structure of pond waters after adding, specifically as shown in Fig. 1-1 to Fig. 1-9.Wherein, laboratory small size pond is organic
250L cultivating pool water bodys are held in glass aquarium (100cm × 60cm × 50cm).
As shown in Fig. 1-1 to Fig. 1-9, biological flocculation structure is initially formed from simply changing to complexity based on der Pilz
Frame structure, around adhere to a small amount of bacterium, subsequently form the biological flocculation of small volume, at the 10th day, the structure of floc sedimentation is also
It is by a relatively simple, almost not it is observed that protozoan and wheel animalcule attachment thereon, during by the 15th day, floc sedimentation volume significantly becomes
Greatly, structure is more complicated, can significantly observe that the planktonic organisms such as cladocera and wheel animalcule are attached to floc sedimentation surface.After 20th day, wadding
The volume change unobvious of group, floc sedimentation color also gradually become sepia by light yellow.Microexamination finds that Floe structure is relatively dredged
There is apparent gap on pine, surface.
Test case 2
The effervescent formulation of instant ecological fish guano of the embodiment of the present invention 4 and the fish guano of control group are launched to Jiangsu Province Yancheng
Haifeng county farm of great Feng areas of city, the biological growth situation and items water body index in water body after test dispensing；Specific experiment side
Method is as follows, and test result is shown in Table 2-6；
Test period is：- 2016 years on the 1st Septembers of September in 2016 30 days；
Test method is：(1) three ponds of uniform specification are selected, size is 80 mu, 2 meters of the depth of water, flooding time, water source
All same；(2) pond stocking model be silver carp (100g/ tails) 100 tails/mu, variegated carp (100g/ tails)：25 tails/mu, crucian 1500
Tail/mu, grass carp：100 tails/mu, bream：200 tails/mu；(3) ecological fish guano of the test group for the embodiment of the present invention 3, control group 1
For ammonium bicarbonate plus calcium superphosphate, control group 2 is certain commercially available fish guano product, and the main component of commercially available fish guano is humic acid；(4) it is of the invention
The fish guano dosage of embodiment 3 is 1kg/ (* meter of mu), and the commercially available fish guano dosage of control group 2 is 1kg/ (* meters of mu), the carbon of control group 1
Ammonium adds the calcium superphosphate dosage to be：Ammonium bicarbonate 2kg/ (* meters of mu)+calcium superphosphate (phosphate fertilizer) 1kg/ (* meters of mu), is the morning 9 with the fertile time
Point；The specifically used time see the table below 1：
1 application date table of table
The water transparency that 2 different time of table measures
Test data unit is cm in table 2.
Table 3 applies fertilizer the variation of front and rear algae composition
The pH value of 4 different time of table
5 different time bioflocculation quantity (mL/L) of table
The variation (mg/L) of 6 different time ammonia nitrogen of table
As shown in table 3, from the experimental data of control group 1 it is found that due to applied chemical fertilizer so that easily break out indigo plant in pond
Algae；From the data of test group it is found that the product of the application present invention can promote the growth of green alga, diatom to a certain extent.
As shown in table 4, the ecological fish rich water matter using the present invention is more stable；Water body is be easy to cause using fertilizer such as chemical fertilizer
Acute variation.
To sum up, by the test data of table 2- tables 6 it is found that control group 1 applies chemical fertilizer, fertilizer efficiency is fast and violent, but the duration is short,
The acute variation of water body is be easy to cause, causes down algae；Control group 2 is commercially available common fish guano, and fertility is insufficient, and the fertilising period is 5-7
My god, labor intensity is big；Instant ecological fish guano of the experimental group for the present invention, duration can reach 10 days or more, can reduce labour
Intensity.
Various embodiments of the present invention are described above, above description is exemplary, and non-exclusive, and
It is not limited to disclosed each embodiment.In the case of without departing from the scope and spirit of illustrated each embodiment, for this skill
Many modifications and changes will be apparent from for the those of ordinary skill in art field.
Claims (10)
1. a kind of instant ecological fish guano, which is characterized in that in terms of parts by weight, which includes：10-40 parts of Xanthohumate, hair
10-40 parts of hydrolyzing amino acid powder, 10-25 parts of inorganic fertilizer, middle 1-5 parts of trace element, 0.1-2 parts of probiotics and plant life
It is conditioning agent 0.1-0.3 parts long.
2. instant ecological fish guano according to claim 1, wherein, the Xanthohumate is SODLUM FULVATE and/or fulvic acid
Potassium.
3. instant ecological fish guano according to claim 1, wherein, the inorganic fertilizer includes sulphur ammonium, monoammonium phosphate and chlorination
Potassium, the mass ratio of the sulphur ammonium, monoammonium phosphate and potassium chloride is (1-10)：(3-8)：(3-8).
4. instant ecological fish guano according to claim 1, wherein, the donor of the middle trace element includes：Monosilicate,
Magnesium sulfate, zinc sulfate, manganese sulfate and ironic citrate；With the total weight of instant ecological fish guano, the monosilicate is 0.4-
2wt%, magnesium sulfate 0.4-1wt%, zinc sulfate 0.02-0.05wt%, manganese sulfate are 0.1-1.5wt% and ironic citrate is
0.1-1wt%.
5. instant ecological fish guano according to claim 1, wherein, the probiotics are biological flocculated bacteria；The life
Object flocculated bacteria includes bacillus subtilis bacterium powder and/or rhodococcus erythropolis bacterium powder.
6. instant ecological fish guano according to claim 1, wherein, the plant growth regulator includes sour lignocaine
Ethyl alcohol ester and/or α-naphthaleneacidsodium.
7. the preparation method of the instant ecological fish guano according to any one in claim 1-6, which is characterized in that the preparation
Method includes：
The donor of Xanthohumate, hair-hydrolyzation amino acid powder, inorganic fertilizer and middle trace element is uniformly mixed, obtains the first mixing
Powder；
Part first mixed material with probiotics and plant growth regulator is uniformly mixed, obtains the second mixed powder
Material；
Second mixed powder and remaining first mixed powder are uniformly mixed, obtain the instant ecological fish guano.
8. a kind of effervescent formulation of instant ecological fish guano, which is characterized in that in terms of parts by weight, which includes：Right
It is required that instant ecological 31.2-112.3 parts of the fish guano in 1-6 described in any one, 10-40 parts of sodium bicarbonate, gather 3-15 parts of tartaric acid
0.1-3 parts of ethylene glycol and polyethylene adjoin 0.1-4 parts of pyrrolidone.
9. the preparation method of the effervescent formulation of instant ecological fish guano according to claim 8, which is characterized in that the preparation side
Method includes：
The instant ecological fish guano in part, sodium bicarbonate and part polyethylene are adjoined pyrrolidone ethanol solution and be uniformly mixed, was then squeezed
Sieve is granulated, and obtains the first particle；
Remaining instant ecological fish guano, tartaric acid and remaining polyethylene are adjoined pyrrolidone ethanol solution and be uniformly mixed, is then squeezed
It presses through sieve to be granulated, obtains the second particle；
First particle and second particle are uniformly mixed, polyethylene glycol is then added in and carries out tabletting, obtained after dry
The effervescent formulation of the instant ecological fish guano.
10. the preparation method of the effervescent formulation of instant ecological fish guano according to claim 9, wherein, the polyethylene adjoins
The solid-liquid ratio of pyrrolidone ethanol solution is 3-10:100, unit g/ml.
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Application publication date: 20180612 |