CN108004024A - A kind of ginkgo leaf cigarette is applied with quick-fried pearl essential oil and preparation method thereof and in cigarette - Google Patents
A kind of ginkgo leaf cigarette is applied with quick-fried pearl essential oil and preparation method thereof and in cigarette Download PDFInfo
- Publication number
- CN108004024A CN108004024A CN201810041028.8A CN201810041028A CN108004024A CN 108004024 A CN108004024 A CN 108004024A CN 201810041028 A CN201810041028 A CN 201810041028A CN 108004024 A CN108004024 A CN 108004024A
- Authority
- CN
- China
- Prior art keywords
- ginkgo leaf
- cigarette
- quick
- fried pearl
- essential oil
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0003—Compounds of unspecified constitution defined by the chemical reaction for their preparation
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/061—Use of materials for tobacco smoke filters containing additives entrapped within capsules, sponge-like material or the like, for further release upon smoking
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0007—Aliphatic compounds
- C11B9/0015—Aliphatic compounds containing oxygen as the only heteroatom
- C11B9/0019—Aliphatic compounds containing oxygen as the only heteroatom carbocylic acids; Salts or esters thereof
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/022—Refining
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/025—Recovery by solvent extraction
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/027—Recovery of volatiles by distillation or stripping
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Life Sciences & Earth Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Materials Engineering (AREA)
- Medicines Containing Plant Substances (AREA)
- Medicinal Preparation (AREA)
Abstract
The present invention provides a kind of ginkgo leaf cigarette quick-fried pearl essential oil and preparation method thereof and the application in volume.The ginkgo leaf cigarette is that 1.0 2.0h of stirring at normal temperature to solution clear, is obtained after 100nm ceramic membrane filters under the conditions of rotating speed is 200 300r/min by ginkgo leaf molecular distillation thing, Span80 surfactants and Glycerin, mixed triester with caprylic acid capric acid solvent with quick-fried pearl essential oil.The ginkgo leaf molecular distillation thing is that first by ginkgo leaf progress ultra high pressure extraction, to carry out molecular distillation again obtained.The folium ginkgo essential oil that the present invention modulates can directly apply in the quick-fried pearl of cigarette as core, have good compatibility with quick-fried pearl wall material, apply it in cigarette, this perfume is coordinated with tobacco, and the soft exquisiteness of flue gas, pleasant impression is comfortable, improves the sense organ comfort level of cigarette.
Description
Technical field
The present invention relates to cigarette flavors field, specifically a kind of ginkgo leaf cigarette quick-fried pearl essential oil and its preparation side
Method and applied in cigarette.
Background technology
Quick-fried pearl cigarette is pre-filled with one or more flavored capsules, smoker in filter tip and can be selected in sucking process
Property by capsule pinch it is quick-fried, release fragrance.In recent years, domestic tobacco enterprise has carried out extensive work, quick-fried pearl in terms of quick-fried pearl research and development
In additive in addition to traditional Peppermint essential oil, further comprises various tastes essence（Fruity, aroma, cloves etc.）, effect
It is different.As national cigarette industry situation day is becoming tight, the competition of cigarette product is fiercer, this also means that to cigarette product
Technology content require higher, cigarette need to further upgrade optimization with quick-fried pearl.Key technology is molded by furtheing investigate quick-fried pearl, into one
Step expands quick-fried pearl essence species, improves essence dicyandiamide solution, abundant wall material system, optimization moulding process, is the quick-fried pearl of Creating Special
Cigarette product, the only way for strengthening enterprise competitiveness.
Ginkgo（Also known as Gong Sunshu, gingko）It is Gymnospermae Ginkgoaceae plant, is seeds most ancient on the current earth
One of.Ginkgo has the laudatory title of " giant panda of plant kingdom ", is to study " living fossil " that ancient times earth geology becomes deeply, is arranged by country
For two level rare and protected trees.China's gingko resource owning amount accounts for 75% or so of world's total amount, occupies first place in the world.Domestic big portion
The ginkgo of region-by-region is artificial cultivation, is mainly distributed on the provinces and cities such as Hubei, Zhejiang, Anhui, Fujian, Henan, Sichuan.Suizhou, hubei
Thousands of ancient ginkgo are grown among the remote mountains of one band, are that the big intensive sheet of ancient Ginkgo population in the world four falls it
One.
Ginkgo leaf has multiple biological activities and medical value, such as anti-oxidant, removing human body is certainly as a kind of Chinese herbal medicine
By base, improve blood flow, increase brain blood supply and other effects.Ginkgo leaf primary medicinal component is flavonoids and lactone compound
（Content is more than 24.0%）, the chromocor compound having now been found that has rutin, radix astragali, isoquercitin, kaempferol etc., lactone
Compound has ginkgolides and Bilobalide, can assign the medicinal herbs smell of uniqueness, has the prospect as essence spice for cigarette.
But ginkgo leaf in the achievement in research of report is seen at present and is used for field of medicaments more.The present inventor was studying
Find to handle obtained Folium Ginkgo volatile oil extract simply by steam distillation in journey, be added in cigarette have compared with
Big negative effect, miscellaneous gas is more, and oral cavity is uncomfortable, and the naturally sense of fragrance is poor, can not meet to make as cigarette additive
With requiring.
The content of the invention
The purpose of the present invention is in view of the deficiencies of the prior art, provide a kind of ginkgo leaf cigarette quick-fried pearl essential oil and its preparation side
Method and applied in cigarette.The folium ginkgo essential oil allocated has obvious herbal breath, and overall aromatic style is comfortable, association
Adjust, naturally, the quick-fried pearl of cigarette is prepared as oil-soluble content, there is good compatibility, quick-fried pearl shaping with quick-fried pearl wall material
Qualification rate is high, and the abnormal phenomenon such as solid pearl, permeability, bias, rupture is less.After quick-fried pearl in cigarette filter rod is pinched brokenly, ginkgo leaf
Distinctive medicinal herbs fragrance is obvious, and personalized note protrudes, this perfume is coordinated with tobacco, and the soft exquisiteness of flue gas, pleasant impression is comfortable, improves
The sense organ comfort level of cigarette；The free-radical contents in there is removing cigarette mainstream flue gas during cigarette is burnt and sucked at the same time.
To reach above-mentioned purpose, technical solution provided by the invention is：A kind of quick-fried pearl essential oil of ginkgo leaf cigarette, it is special
Sign is that to be formed by the material allocation of following percentage by weight：
Ginkgo leaf molecular distillation thing 0.5-3%
Span80 surfactants 0.05-0.2%
Glycerin, mixed triester with caprylic acid capric acid surplus
The gross weight of above-mentioned substance is 100%；Wherein described ginkgo leaf molecular distillation thing is by after fresh ginkgo leaf impurity elimination, cleaning
Cut into pieces after draining, the alcohol solvent that concentration is 40%-70% is added according to 1: 10~1: 20 solid-liquid ratio, and after mixing sealing
Insert in high-pressure bottle, using deionized water as pressure matchmaker, apply 200-500MPa pressure at normal temperatures and extracted, the dwell time is
20-40min, material residue is filtered to remove after release, is concentrated in vacuo to the ginkgo leaf leaching liquor that relative density is 1.140-1.160, then
It is 100-200Pa in pressure, vapo(u)rizing temperature is 45-60 DEG C, material flow 1-2mL/min, and knifing rotating speed is 350~450r/
The light component obtained under conditions of min after molecular distillation.
The preparation method of the quick-fried pearl essential oil of a kind of ginkgo leaf cigarette provided by the invention, it is characterised in that comprise the following steps that：
（1）It will first drain away the water after fresh ginkgo leaf impurity elimination, cleaning, cut into pieces, added according to 1: 10~1: 20 solid-liquid ratio
Concentration is the alcohol solvent of 40%-70%, inserts the mixed material in high-pressure bottle after mixing sealing, using deionized water as pressure
Matchmaker, applies 200-500MPa pressure and is extracted at normal temperatures, dwell time 20-40min, material residue is filtered to remove after release,
It is 1.140-1.160 to be concentrated in vacuo to relative density, obtains ginkgo leaf leaching liquor；
（2）By step（1）Ginkgo leaf leaching liquor after middle concentration is 100-200Pa, vapo(u)rizing temperature 45-60 in distillation pressure
DEG C, material flow 1-2mL/min, knifing rotating speed collects light group after carrying out molecular distillation under conditions of being 350~450r/min
Point, it is ginkgo leaf molecular distillation thing；
（3）Prepare raw material according to following percentage by weight：Step（2）The ginkgo leaf molecular distillation thing 0.5-3% of middle preparation,
Span80 surfactant 0.05-0.2%, surplus are Glycerin, mixed triester with caprylic acid capric acid solvent；And above-mentioned material is put into carry successively and is stirred
In the container for mixing device, stirring at normal temperature 1.0-2.0h is passed through to solution clear under the conditions of rotating speed is 200-300r/min
It is the quick-fried pearl essential oil of ginkgo leaf cigarette after 100nm ceramic membrane filters.
The present invention preferably technical solution：The step（1）In fresh ginkgo leaf derive from Suizhou, hubei Luoyang town ginkgo
Paddy.
The present invention preferably technical solution：The operating pressure of the ceramic membrane pipe fitting is 0.10-0.20MPa, temperature 25-
30 DEG C, the main purpose of ceramic membrane filter is to remove impurity and insoluble matter a small amount of in essential oil system.
A kind of application in cigarette of the quick-fried pearl essential oil of ginkgo leaf cigarette provided by the invention, it is characterised in that：Will be above-mentioned
After Fruit storage 10-20min, material is wrapped up with the dripping pill being placed in pill dripping machine rubber cement tank with quick-fried pearl essential oil for ginkgo leaf cigarette
Cigarette is made with quick-fried pearl according to the preparation process of dripping pill in the curing agent for expecting and being placed in contain in ball device, and in filter tow forming process
It is middle that the positioning of quick-fried pearl is applied in filter stick.
The advantage of the invention is that：
（1）Raw material selected by the present invention is fresh ginkgo leaf, relative to dried Chinese medicine ginkgo leaf, in fresh ginkgo leaf
Volatile ingredient it is more, fragrance is more natural, comfortable, true to nature.
（2）The main function of Glycerin, mixed triester with caprylic acid capric acid is dispersing and dissolving ginkgo leaf molecular distillation thing in the present invention, has raw material
The advantages that cost is low, colorless and odorless, viscosity are low, not oxidizable, stable system.
（3）The folium ginkgo essential oil that the present invention modulates can directly apply in the quick-fried pearl of cigarette as core, with quick-fried pearl wall material
With good compatibility, quick-fried pearl online production shaping qualification rate is high, the abnormal phenomenon such as solid pearl, permeability, bias, rupture compared with
It is few.
（4）After quick-fried pearl in cigarette filter rod is pinched brokenly, the distinctive medicinal herbs fragrance of ginkgo leaf is obvious, and personalized note protrudes,
This perfume is coordinated with tobacco, and the soft exquisiteness of flue gas, pleasant impression is comfortable, improves the sense organ comfort level of cigarette；Burnt and sucked at the same time in cigarette
Have effects that to remove free-radical contents in cigarette mainstream flue gas in journey.
Embodiment
Below in conjunction with specific embodiment, the present invention is described in further detail.A kind of ginkgo leaf cigarette quick-fried pearl essence
Oil, it is characterised in that formed by the material allocation of following percentage by weight：
Ginkgo leaf molecular distillation thing 0.5-3%
Span80 surfactants 0.05-0.2%
Glycerin, mixed triester with caprylic acid capric acid surplus
Wherein described ginkgo leaf molecular distillation thing is by being cut into pieces after being drained after fresh ginkgo leaf impurity elimination, cleaning, according to 1: 10
~1: 20 solid-liquid ratio adds concentration and is the alcohol solvent of 40%-70%, and is inserted after mixing sealing in high-pressure bottle, with deionization
Water is pressure matchmaker, applies 200-500MPa pressure at normal temperatures and is extracted, dwell time 20-40min, is filtered to remove after release
Material residue, is concentrated in vacuo to the ginkgo leaf leaching liquor that relative density is 1.140-1.160, then in pressure be 100-200Pa, and distillation is warm
Spend for 45-60 DEG C, material flow 1-2mL/min, obtained under conditions of knifing rotating speed is 350~450r/min after molecular distillation
Light component.The fresh ginkgo leaf is collected in Suizhou, hubei Luoyang town ginkgo paddy.
Embodiment one, the preparation method of the quick-fried pearl essential oil of a kind of ginkgo leaf cigarette, it is characterised in that comprise the following steps that：
（1）It will first drain away the water, cut into pieces after fresh ginkgo leaf impurity elimination, cleaning, it is molten to add ethanol according to 1: 10 solid-liquid ratio
Agent（Concentration is 70%）, the mixed material is inserted in high-pressure bottle after mixing sealing, using deionized water as pressure matchmaker, at normal temperatures
Apply 400MPa pressure to be extracted, dwell time 20min, is filtered to remove material residue after release, is concentrated in vacuo to relative density
For 1.140-1.160, ginkgo leaf leaching liquor is obtained；
（2）Ginkgo leaf leaching liquor after concentration is subjected to molecular distillation（Distillation pressure is 150Pa, and vapo(u)rizing temperature is 50 DEG C, material
Flow velocity is 2mL/min, knifing rotating speed 350r/min）The light component obtained afterwards is ginkgo leaf molecular distillation thing；
（3）Prepare the raw material of following percentage by weight：Step（2）In ginkgo leaf molecular distillation thing 2%；Span80 surface-actives
Agent 0.05%；Remaining 97.95% is Glycerin, mixed triester with caprylic acid capric acid solvent；And above-mentioned material will be put into agitating device successively
In container, stirring at normal temperature 1.5h is to solution clear under the conditions of rotating speed is 300r/min, through 100nm ceramic membranes（Pressure is
0.10-0.20MPa, temperature are 25-30 DEG C,）It is the as quick-fried pearl essential oil of ginkgo leaf cigarette after filtering.
Embodiment two, the preparation method of the quick-fried pearl essential oil of a kind of ginkgo leaf cigarette, it is characterised in that comprise the following steps that：
（1）It will first drain away the water, cut into pieces after fresh ginkgo leaf impurity elimination, cleaning, it is molten to add ethanol according to 1: 12 solid-liquid ratio
Agent（Concentration is 55%）, the mixed material is inserted in high-pressure bottle after mixing sealing, using deionized water as pressure matchmaker, at normal temperatures
Apply 200MPa pressure to be extracted, dwell time 30min, material residue is filtered to remove after release, is concentrated in vacuo to relative density
For 1.140-1.160, ginkgo leaf leaching liquor is obtained；
（2）Ginkgo leaf leaching liquor after concentration is subjected to molecular distillation（Distillation pressure is 200Pa, and vapo(u)rizing temperature is 60 DEG C, material
Flow velocity is 1mL/min, knifing rotating speed 450r/min）The light component obtained afterwards is ginkgo leaf molecular distillation thing；
（3）Prepare the raw material of following percentage by weight：Step（2）In ginkgo leaf molecular distillation thing 1.5%；Live on Span80 surfaces
Property agent 0.1%；Remaining 98.4% is Glycerin, mixed triester with caprylic acid capric acid solvent；Above-mentioned material is put into the container with agitating device successively
In, stirring at normal temperature 1.0h is to solution clear under the conditions of rotating speed is 250r/min, through 100nm ceramic membranes（Pressure is 0.10-
0.20MPa, temperature are 25-30 DEG C,）It is as folium ginkgo essential oil after filtering.
Embodiment three, the preparation method of the quick-fried pearl essential oil of a kind of ginkgo leaf cigarette, it is characterised in that comprise the following steps that：
（1）It will first drain away the water, cut into pieces after fresh ginkgo leaf impurity elimination, cleaning, it is molten to add ethanol according to 1: 20 solid-liquid ratio
Agent（Concentration is 45%）, the mixed material is inserted in high-pressure bottle after mixing sealing, using deionized water as pressure matchmaker, at normal temperatures
Apply 280MPa pressure to be extracted, dwell time 35min, is filtered to remove material residue after release, is concentrated in vacuo to relative density
For 1.140-1.160, ginkgo leaf leaching liquor is obtained；
（2）Ginkgo leaf leaching liquor after concentration is subjected to molecular distillation（Distillation pressure is 120Pa, and vapo(u)rizing temperature is 45 DEG C, material
Flow velocity is 1.5mL/min, knifing rotating speed 320r/min）The light component obtained afterwards is ginkgo leaf molecular distillation thing；
（3）Prepare the raw material of following percentage by weight：Step（2）In ginkgo leaf molecular distillation thing 2.5%；Live on Span80 surfaces
Property agent 0.2%；Remaining 97.3% is Glycerin, mixed triester with caprylic acid capric acid solvent.Above-mentioned material is put into the container with agitating device successively
In, stirring at normal temperature 1.0h is to solution clear under the conditions of rotating speed 260r/min, through 100nm ceramic membranes（Pressure is 0.10-
0.20MPa, temperature are 25-30 DEG C,）It is as folium ginkgo essential oil after filtering.
Example IV, the preparation method of the quick-fried pearl essential oil of a kind of ginkgo leaf cigarette, it is characterised in that comprise the following steps that：
（1）It will first drain away the water, cut into pieces after fresh ginkgo leaf impurity elimination, cleaning, it is molten to add ethanol according to 1: 16 solid-liquid ratio
Agent（Concentration is 55%）, the mixed material is inserted in high-pressure bottle after mixing sealing, using deionized water as pressure matchmaker, at normal temperatures
Apply 380MPa pressure to be extracted, dwell time 32min, material residue is filtered to remove after release, is concentrated in vacuo to relative density
For 1.140-1.160, ginkgo leaf leaching liquor is obtained.
（2）Ginkgo leaf leaching liquor after concentration is subjected to molecular distillation（Distillation pressure is 140Pa, and vapo(u)rizing temperature is 55 DEG C,
Material flow is 1.5mL/min, knifing rotating speed 450r/min）The light component obtained afterwards is ginkgo leaf molecular distillation thing；
（3）Prepare the raw material of following percentage by weight：Step（2）In ginkgo leaf molecular distillation thing 3%；Span80 surface-actives
Agent 0.15%；Remaining 96.85% is Glycerin, mixed triester with caprylic acid capric acid solvent, and above-mentioned material is put into the container with agitating device successively
In, stirring at normal temperature 1.5h is to solution clear under the conditions of rotating speed is 300r/min, through 100nm ceramic membranes（Pressure is 0.10-
0.20MPa, temperature are 25-30 DEG C,）It is as folium ginkgo essential oil after filtering.
Embodiment five, by the ginkgo leaf cigarette prepared in embodiment 1 with quick-fried pearl essential oil, by Fruit storage 10-20min
Afterwards, with reference to the conventional production process of the quick-fried pearl of enterprises cigarette, with the dripping pill lapping that is placed in pill dripping machine rubber cement tank and
It is placed in the curing agent contained in ball device and cigarette is made with quick-fried pearl according to the preparation process of dripping pill, and detects the performance for preparing quick-fried pearl, its inspection
Survey the result shows that：Folium ginkgo essential oil has good compatibility, quick-fried pearl is molded online as oil-soluble content with quick-fried pearl wall material
Effect stability, product qualification rate reach more than 98%, and the abnormal phenomenon such as solid pearl, permeability, bias, rupture is less.
Embodiment six：By ginkgo leaf cigarette prepared by embodiment 1-4 quick-fried pearl essential oil, difference Fruit storage 10-20min
Afterwards, with reference to the conventional production process of the quick-fried pearl of enterprises cigarette, with the dripping pill lapping that is placed in pill dripping machine rubber cement tank and
It is placed in the curing agent contained in ball device and cigarette is made with quick-fried pearl according to the preparation process of dripping pill, and by quick-fried pearl in filter tow forming process
Positioning is applied in filter stick, and four kinds of cigarette are then made, and is evaluated with reference to State Bureau's standard of smokeing panel test, and is pinched in aspiration procedure
Break quick-fried pearl.Group of smokeing panel test is made of 13 cigarette sensory evaluation experts, using secretly commenting mode to carry out sensory evaluation and give a mark, and with
Blank cigarette is contrasted, its Analyses Methods for Sensory Evaluation Results is as shown in table 1.
And aspirated respectively, and use cigarette with quick-fried pearl essential oil cigarette using the ginkgo leaf cigarette being added with embodiment 1-4
Gas collector and electron spin resonance, analysis detect quick-fried pearl and pinch brokenly rear folium ginkgo essential oil to cigarette mainstream flue gas free radical
The elimination effect of content, the results are shown in Table 2.
Note：+, free-radical contents rise；-, free-radical contents reduce
The quick-fried pearl prepared using folium ginkgo essential oil can be seen that by above-mentioned smoking result, after being pinched brokenly during cigarette smoking,
Sensory effects evaluation score significantly improves, and application effect is more notable.The distinctive medicinal herbs fragrance of ginkgo leaf is obvious, personalized note
Prominent, this perfume is coordinated with tobacco, and the soft exquisiteness of flue gas, pleasant impression is comfortable, improves the sense organ comfort level of cigarette；Fired at the same time in cigarette
Have effects that to remove free-radical contents in cigarette mainstream flue gas during suction.
Claims (5)
1. the quick-fried pearl essential oil of a kind of ginkgo leaf cigarette, it is characterised in that formed by the material allocation of following percentage by weight：
Ginkgo leaf molecular distillation thing 0.5-3%
Span80 surfactants 0.05-0.2%
Glycerin, mixed triester with caprylic acid capric acid surplus
Wherein described ginkgo leaf molecular distillation thing is by being cut into pieces after being drained after fresh ginkgo leaf impurity elimination, cleaning, according to 1: 10
~1: 20 solid-liquid ratio adds concentration and is the alcohol solvent of 40%-70%, and is inserted after mixing sealing in high-pressure bottle, with deionization
Water is pressure matchmaker, applies 200-500MPa pressure at normal temperatures and is extracted, dwell time 20-40min, is filtered to remove after release
Material residue, is concentrated in vacuo to the ginkgo leaf leaching liquor that relative density is 1.140-1.160, then in pressure be 100-200Pa, and distillation is warm
Spend for 45-60 DEG C, material flow 1-2mL/min, obtained under conditions of knifing rotating speed is 350~450r/min after molecular distillation
Light component.
2. a kind of ginkgo leaf cigarette preparation method of quick-fried pearl essential oil, it is characterised in that comprise the following steps that：
（1）It will first drain away the water after fresh ginkgo leaf impurity elimination, cleaning, cut into pieces, added according to 1: 10~1: 20 solid-liquid ratio
Concentration is the alcohol solvent of 40%-70%, inserts the mixed material in high-pressure bottle after mixing sealing, using deionized water as pressure
Matchmaker, applies 200-500MPa pressure and is extracted at normal temperatures, dwell time 20-40min, material residue is filtered to remove after release,
It is 1.140-1.160 to be concentrated in vacuo to relative density, obtains ginkgo leaf leaching liquor；
（2）By step（1）Ginkgo leaf leaching liquor after middle concentration is 100-200Pa, vapo(u)rizing temperature 45-60 in distillation pressure
DEG C, material flow 1-2mL/min, knifing rotating speed collects light group after carrying out molecular distillation under conditions of being 350~450r/min
Point, it is ginkgo leaf molecular distillation thing；
（3）Prepare raw material according to following percentage by weight：Step（2）The ginkgo leaf molecular distillation thing 0.5-3% of middle preparation,
Span80 surfactant 0.05-0.2%, surplus are Glycerin, mixed triester with caprylic acid capric acid solvent；And above-mentioned material is put into carry successively and is stirred
In the container for mixing device, stirring at normal temperature 1.0-2.0h is passed through to solution clear under the conditions of rotating speed is 200-300r/min
It is the quick-fried pearl essential oil of ginkgo leaf cigarette after 100nm ceramic membrane filters.
A kind of 3. preparation method of the quick-fried pearl essential oil of ginkgo leaf cigarette according to claim 2, it is characterised in that：The step
（1）In fresh ginkgo leaf derive from Suizhou, hubei Luoyang town ginkgo paddy.
A kind of 4. preparation method of the quick-fried pearl essential oil of ginkgo leaf cigarette according to claim 2, it is characterised in that：The ceramics
The operating pressure of membrane tube part is 0.10-0.20MPa, and temperature is 25-30 DEG C.
A kind of 5. application in cigarette of the quick-fried pearl essential oil of ginkgo leaf cigarette described in claim 1 or 2, it is characterised in that：
By above-mentioned ginkgo leaf cigarette with quick-fried pearl essential oil after Fruit storage 10-20min, with the dripping pill being placed in pill dripping machine rubber cement tank
Lapping and be placed in the curing agent contained in ball device cigarette be made with quick-fried pearl according to the preparation process of dripping pill, and filter tow into
The positioning of quick-fried pearl is applied in filter stick during type.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810041028.8A CN108004024A (en) | 2018-01-16 | 2018-01-16 | A kind of ginkgo leaf cigarette is applied with quick-fried pearl essential oil and preparation method thereof and in cigarette |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810041028.8A CN108004024A (en) | 2018-01-16 | 2018-01-16 | A kind of ginkgo leaf cigarette is applied with quick-fried pearl essential oil and preparation method thereof and in cigarette |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108004024A true CN108004024A (en) | 2018-05-08 |
Family
ID=62050770
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810041028.8A Pending CN108004024A (en) | 2018-01-16 | 2018-01-16 | A kind of ginkgo leaf cigarette is applied with quick-fried pearl essential oil and preparation method thereof and in cigarette |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN108004024A (en) |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109111990A (en) * | 2018-10-09 | 2019-01-01 | 湖北中烟工业有限责任公司 | Utilize the method and its application of wax in impulse electric field efficient removal olive oil |
| CN110184121A (en) * | 2019-04-29 | 2019-08-30 | 深圳市永沣香料有限公司 | Cigarette quick-fried pearl essential oil and the preparation method and application thereof |
| CN111040876A (en) * | 2019-12-19 | 2020-04-21 | 云南瑞升烟草技术（集团）有限公司 | Preparation method of natural spice suitable for cigarette bead blasting |
| CN111035054A (en) * | 2019-11-27 | 2020-04-21 | 内蒙古昆明卷烟有限责任公司 | Method for preparing tar extract with aroma characteristics from waste cigarette butts and application of tar extract in cigarettes |
| CN111713736A (en) * | 2020-06-28 | 2020-09-29 | 潮州市泥香陶瓷新材料有限公司 | Environment-friendly ceramic blasting bead for cigarettes and manufacturing method |
| CN113491672A (en) * | 2020-04-07 | 2021-10-12 | 成都百裕制药股份有限公司 | A dripping pill containing bilobalide as effective component and its preparation method |
| CN113796575A (en) * | 2021-09-15 | 2021-12-17 | 成都生制堂生物科技有限公司 | Natural compound essential oil for cigarette bead blasting and preparation method thereof |
Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103087825A (en) * | 2011-11-08 | 2013-05-08 | 江西中烟工业有限责任公司 | Desmodium styracifolium extract and preparation method and application thereof |
| CN104886554A (en) * | 2015-04-30 | 2015-09-09 | 山东圣健生物科技有限公司 | Pomander soft capsule and preparation method thereof |
| CN105028689A (en) * | 2015-06-24 | 2015-11-11 | 洛阳国花坊牡丹生物科技有限公司 | Preparation method of peony seed oil and ginkgo oil blended edible oil |
| CN106333384A (en) * | 2016-11-01 | 2017-01-18 | 湖北中烟工业有限责任公司 | Mixed type tobacco molecular distillation light component electronic tobacco liquid and preparation method thereof |
| CN106753787A (en) * | 2016-11-29 | 2017-05-31 | 湖北中烟工业有限责任公司 | A kind of cigarette quick-fried pearl lemon-mint essential oil and its preparation method and application |
| CN107034018A (en) * | 2017-04-27 | 2017-08-11 | 河南中烟工业有限责任公司 | A kind of quick-fried pearl aloe flavour of cigarette and its application in cigarette |
| CN107510091A (en) * | 2017-08-16 | 2017-12-26 | 湖北中烟工业有限责任公司 | A kind of preparation method of the quick-fried pearl essential oil of cigarette |
-
2018
- 2018-01-16 CN CN201810041028.8A patent/CN108004024A/en active Pending
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103087825A (en) * | 2011-11-08 | 2013-05-08 | 江西中烟工业有限责任公司 | Desmodium styracifolium extract and preparation method and application thereof |
| CN104886554A (en) * | 2015-04-30 | 2015-09-09 | 山东圣健生物科技有限公司 | Pomander soft capsule and preparation method thereof |
| CN105028689A (en) * | 2015-06-24 | 2015-11-11 | 洛阳国花坊牡丹生物科技有限公司 | Preparation method of peony seed oil and ginkgo oil blended edible oil |
| CN106333384A (en) * | 2016-11-01 | 2017-01-18 | 湖北中烟工业有限责任公司 | Mixed type tobacco molecular distillation light component electronic tobacco liquid and preparation method thereof |
| CN106753787A (en) * | 2016-11-29 | 2017-05-31 | 湖北中烟工业有限责任公司 | A kind of cigarette quick-fried pearl lemon-mint essential oil and its preparation method and application |
| CN107034018A (en) * | 2017-04-27 | 2017-08-11 | 河南中烟工业有限责任公司 | A kind of quick-fried pearl aloe flavour of cigarette and its application in cigarette |
| CN107510091A (en) * | 2017-08-16 | 2017-12-26 | 湖北中烟工业有限责任公司 | A kind of preparation method of the quick-fried pearl essential oil of cigarette |
Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109111990A (en) * | 2018-10-09 | 2019-01-01 | 湖北中烟工业有限责任公司 | Utilize the method and its application of wax in impulse electric field efficient removal olive oil |
| CN110184121A (en) * | 2019-04-29 | 2019-08-30 | 深圳市永沣香料有限公司 | Cigarette quick-fried pearl essential oil and the preparation method and application thereof |
| CN111035054A (en) * | 2019-11-27 | 2020-04-21 | 内蒙古昆明卷烟有限责任公司 | Method for preparing tar extract with aroma characteristics from waste cigarette butts and application of tar extract in cigarettes |
| CN111035054B (en) * | 2019-11-27 | 2022-07-05 | 内蒙古昆明卷烟有限责任公司 | Method for preparing tar extract with aroma characteristics from waste cigarette butts and application of tar extract in cigarettes |
| CN111040876A (en) * | 2019-12-19 | 2020-04-21 | 云南瑞升烟草技术（集团）有限公司 | Preparation method of natural spice suitable for cigarette bead blasting |
| CN113491672A (en) * | 2020-04-07 | 2021-10-12 | 成都百裕制药股份有限公司 | A dripping pill containing bilobalide as effective component and its preparation method |
| CN111713736A (en) * | 2020-06-28 | 2020-09-29 | 潮州市泥香陶瓷新材料有限公司 | Environment-friendly ceramic blasting bead for cigarettes and manufacturing method |
| CN111713736B (en) * | 2020-06-28 | 2022-05-10 | 潮州市泥香陶瓷新材料有限公司 | Environment-friendly ceramic blasting bead for cigarettes and manufacturing method |
| CN113796575A (en) * | 2021-09-15 | 2021-12-17 | 成都生制堂生物科技有限公司 | Natural compound essential oil for cigarette bead blasting and preparation method thereof |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN108004024A (en) | A kind of ginkgo leaf cigarette is applied with quick-fried pearl essential oil and preparation method thereof and in cigarette | |
| CN101444333B (en) | Method of preparing Grosvenor momordica extract and application thereof | |
| CN105029681B (en) | Natural perfume material refined liquid, tobacco juice suitable for tobacco juice for electronic smoke and preparation method thereof | |
| CN107927901A (en) | It is a kind of that the method for tobacco aromaticss and its application in the quick-fried pearl of cigarette are prepared using Glycerin, mixed triester with caprylic acid capric acid | |
| CN101444331B (en) | Ultrahigh-pressure extraction method of honeysuckle flower, wild chrysanthemum and mulberry leaf and application of extract liquid thereof | |
| CN108179066A (en) | It is a kind of for honeysuckle Peppermint essential oil of the quick-fried pearl of cigarette and its preparation method and application | |
| CN106962972B (en) | A kind of counterextraction method for lifting discarded tobacco leaf quality | |
| CN103478885A (en) | Tobacco sheet containing tea flower extractive and preparation method thereof | |
| CN102090712A (en) | Method for preparing coarse extract of peanut shell total flavones and application thereof in cigarettes | |
| CN107319637A (en) | A kind of extracting method of the electronic cigarette basic smoke raw material of tobacco source | |
| CN101838587A (en) | Method for extracting natural Chinese herbal medicinal flavor component and application of extractive thereof | |
| CN102732381B (en) | Preparation method of fermented tobacco Dendranthema indicum essential oil | |
| CN101317691B (en) | Additive agent for rose fragrance type cigarette, preparation and application thereof | |
| CN109156895A (en) | A kind of reduction cigarette smoking dry sensation and irritating filter stick additive, preparation method and the usage | |
| CN101606756A (en) | Green tea cigarette and production method thereof | |
| CN103045370B (en) | Method for preparing cigarette essence containing aloe extractive and application of cigarette essence to cigarettes | |
| CN103497834B (en) | Method for preparing dandelion absolute oil and application of dandelion absolute oil in cigarettes | |
| CN106617253A (en) | Method for preparing electronic cigarette essence from green tea | |
| CN102125299B (en) | Additive for cigarettes and application thereof | |
| CN107802025A (en) | A kind of preparation method of ginkgo biloba p.e and its application in cigarette | |
| CN108113049A (en) | A kind of herbal tea flavored liquids essence, microcapsule essence and its application in cigarette | |
| CN107874318A (en) | A kind of turf composite particles, preparation method and its application in cigarette | |
| CN106010796A (en) | Flavor preparation method, flavor prepared by preparation method and application of flavor | |
| CN108865437A (en) | A kind of cigarette preparation method of perilla seed fragrance and the application in cigarette | |
| CN108395932A (en) | A kind of preparation method of cigarette jasmine oil |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20180508 |