CN107880648A - A kind of waterborne digital printing dye sublimation ink-jet ink - Google Patents
A kind of waterborne digital printing dye sublimation ink-jet ink Download PDFInfo
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- CN107880648A CN107880648A CN201711285225.6A CN201711285225A CN107880648A CN 107880648 A CN107880648 A CN 107880648A CN 201711285225 A CN201711285225 A CN 201711285225A CN 107880648 A CN107880648 A CN 107880648A
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- ink
- digital printing
- dye sublimation
- jet ink
- printing dye
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/30—Inkjet printing inks
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/30—Inkjet printing inks
- C09D11/32—Inkjet printing inks characterised by colouring agents
- C09D11/328—Inkjet printing inks characterised by colouring agents characterised by dyes
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/30—Inkjet printing inks
- C09D11/38—Inkjet printing inks characterised by non-macromolecular additives other than solvents, pigments or dyes
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Inks, Pencil-Leads, Or Crayons (AREA)
- Ink Jet (AREA)
Abstract
The invention discloses a kind of waterborne digital printing dye sublimation ink-jet ink, belong to heat sublimation ink technical field.The heat sublimation ink-jet ink includes following each component by mass percentage：Resin 1~10%, mill base 5~50%, solvent 10~50%, sterilization antiseptic 0.1~1%, pH adjusting agent 0.1~1%, wetting agent 0.1~3%, deionized water 10~50%.The heat sublimation ink has the stability of preferably printing fluency, and sharpness is high, substantially increases quick-drying, printing effect is good, is also got a promotion for the applicability of EPSON MT4114 shower nozzles.
Description
Technical field
The present invention relates to technical field of ink, and in particular to a kind of waterborne digital printing dye sublimation ink-jet ink.
Background technology
Heat sublimation ink (also known as thermal transfer ink) is exactly that the disperse dyes low energy, easily to distil are fabricated to digital printing
Ink, it is printed upon on transfer paper, can be within the most short time by image making to exquisite porcelain, metal, very by heating
In the materials such as silk, chemical fiber fabric, the market needs and the requirement of environmental protection, heat sublimation ink that are especially suitable for individualized development are mostly
Prepared by the disperse dyes of weaving, color and good weatherability of the disperse dyes due to its saturation, so being printed in weaving
Catch and have a wide range of applications, be still one of primary raw material of printing and dyeing industry so far.However, existing heat sublimation ink
Shower nozzle is frequently resulted in use the problem of poor fluency, plug occurs, flying print is ineffective, and stability is inadequate,
Sharpness deficiency, rate of drying is slower, and granular sensation is more apparent, and then directly affects the yield rate of textile printing technique, to user
Cause huge loss.
The content of the invention
For overcome the deficiencies in the prior art, it is an object of the invention to provide a kind of waterborne digital printing dye sublimation ink-jet
Ink, the heat sublimation ink have the stability of preferably printing fluency, and sharpness is high, substantially increases quick-drying, prints
Effect is good, is also got a promotion for the applicability of EPSON MT4114 shower nozzles.
To solve the above problems, the technical solution adopted in the present invention is as follows：
A kind of waterborne digital printing dye sublimation ink-jet ink, it includes following each component by mass percentage：Resin 1
~10%, mill base 5~50%, solvent 10~50%, sterilization antiseptic 0.1~1%, pH adjusting agent 0.1~1%, wetting agent 0.1
~3%, deionized water 10~50%.
As the preferred embodiment of the present invention, the mill base is made up of following component by mass percentage：Toner
15~30%, NMF 20~30%, dispersant 5~15%, dispersion aids 0.5~1.5%, bactericide 0.5~1%, pH are adjusted
Save agent 0.2~0.5%, deionized water 40~80%.
As the preferred embodiment of the present invention, the viscosity of the mill base is 10~50Mpa.s, surface tension be 40~
50mN/m；The particle diameter of the mill base is 100~120nm of D50, D90<300nm.
As the preferred embodiment of the present invention, the preparation method of the mill base is as follows：Deionized water, molten is put into successively
Agent, sterilization antiseptic, pH adjusting agent, 20min is stirred under 500r/min rotating speed；Then dispersion aids is put into, continues to stir
Until solution is integrally limpid；Input dispersant continues stirring until solution is integrally limpid；Put into rotating speed of the toner in 500r/min
Lower stirring 20min；Then all materials are added into horizontal mill (a diameter of 0.1~0.5mm of zirconium oxide bead, zirconium pearl loading
For 70~90%, grinding capacity is 1~1.5Kg) in, 12~15h, grinding temperature are ground under 1000~2000r/min rotating speed
Spend for 30~50 DEG C.
As the preferred embodiment of the present invention, the NMF in paste formula is selected from ethylene glycol, diethylene glycol, three
At least one of ethylene glycol, 1,2 propane diols, glycerine, 1,5 pentanediols, D-sorbite, EG-1；The pH adjusting agent is selected from
Ammoniacal liquor, triethanolamine, EDETATE SODIUM, middle one kind of the sodium of EDTA tetra-；The dispersion aids is selected from OP-7, OP-10, OP-15, NP-
7th, NP-10, NP-15 at least one of；The dispersant be selected from the REAX 88B of virtue Wei Shiweike companies, REAX 88A,
At least one of REAX 80D, REAX83A, REAX 85A；The toner be selected from black toner, blue toner, red toner,
At least one of yellow toner.Wherein, black toner is selected from C.I. disperse violets 27, C.I. disperse blues 366, C.I. disperse blues
26th, C.I. disperse orange 25s, C.I. disperse oranges 37, C.I. scattered orange 119, C.I. disperse yellows 54, C.I. disperse 64, C.I. and disperseed
At least two in 242；Blue toner is selected from C.I. Disperse Blue-56s, C.I. disperse blue 60s, C.I. disperse blues 91, C.I. disperse blues
One kind in 359；Red toner is selected from C.I. disperse reds 50, C.I. disperse red 60s, C.I. disperse reds 65, C.I. disperse reds 239
In one kind；Yellow toner is in C.I. disperse yellows 7, C.I. disperse yellows 54, C.I. dispersion yellow 64s, C.I. disperse yellows 100
It is a kind of.
As the preferred embodiment of the present invention, the resin is selected from PVP-K10, PVP- of BASF joint-stock company production
K20, PVP-K30, PVP-K40, PVP-K50, TEGO Viscoplus 3000, the TEGO of the German high paint company production of enlightening
At least one of Viscoplus 3010, TEGO Viscoplus 3030.
As the preferred embodiment of the present invention, the secondary solvent is selected from ethylene glycol, diethylene glycol, triethylene glycol, 1,2
Propane diols, glycerine, 1,5 pentanediols, D-sorbite, glycerin ether, ethylene glycol monobutyl ether, diethylene glycol monomethyl ether, diethylene glycol
At least one of ether, diethylene glycol monobutyl ether, triethylene glycol butyl ether.
As the preferred embodiment of the present invention, the pH adjusting agent is selected from ammoniacal liquor, triethanolamine, EDETATE SODIUM, EDTA
One kind in four sodium.
As the preferred embodiment of the present invention, the wetting agent is selected from Ai Fu Konas Chemical Co., Ltd.
AFCONA3522, AFCON3580, AFCON3581, AFCONA3585, German Ming Ling chemical companies production METOLAT355,
METOLA362, METOLAT364, METOLA365, U.S.'s Hensel step group324、168、169、At least one of LF-37.
In above-mentioned ink set, deionized water, for adjusting ink viscosity and surface tension, helps as bulk solvent
In the solvability of the system of raising；Secondary solvent be used for adjust ink viscosity and surface tension, effectively improve system moisture retention,
Quick-drying, fluency, further improve solvability；Sterilization antiseptic can reduce, suppress the breeding of various algae bacteriums, carry
High stability of ink；PH adjusting agent is used for the pH of regulation system, it is possible to increase the stability and applicability of ink.Wetting agent plays
The effect of surface tension is adjusted, control system water and oil balance, lifts the mobility and levelability of ink.Resin plays scattered, increasing
Thick, hydrotropy effect, it is possible to increase printing quick-drying, level-dyeing property and glossiness.Color source of the mill base as ink, imitates printing
Fruit bright colors saturation.
As the preferred embodiment of the present invention, the heat sublimation ink-jet ink is manufactured according to the following steps：
1) deionized water of formula ratio, solvent, sterilization antiseptic, pH adjusting agent are put into material barrel in order,
20min is stirred under 500r/min rotating speed；The wetting agent for adding formula ratio continues to stir, untill solution is integrally limpid；Add
The resin for entering formula ratio continues to stir, untill treating that solution is integrally limpid；
2) mill base for adding formula ratio stirs 20min under 500r/min rotating speed；Then with 0.22 μm of hydrophylic filter membranes with
0.45 μm of hydrophylic filter membranes is combined to be filtered, and is produced.
Compared with prior art, the beneficial effects of the present invention are：
Waterborne digital stamp heat sublimation ink of the present invention has the stability of preferably printing fluency, sharp keen
Degree is high, substantially increases quick-drying, and printing effect is good, is also got a promotion for the applicability of EPSON MT4114 shower nozzles, meets
Industrial needs.
Embodiment
The present invention is described in further detail with reference to embodiment.
A kind of waterborne digital printing dye sublimation ink-jet ink, it includes following each component by mass percentage：Resin 1
~10%, mill base 5~50%, solvent 10~50%, sterilization antiseptic 0.1~1%, pH adjusting agent 0.1~1%, wetting agent 0.1
~3%, deionized water 10~50%.
In above-mentioned formula, mill base is made up of following component by mass percentage：Toner 15~30%, NMF 20~
30%th, dispersant 5~15%, dispersion aids 0.5~1.5%, bactericide 0.5~1%, pH adjusting agent 0.2~0.5%, go from
Sub- water 40~80%.The viscosity of above mill base is 10~50Mpa.s, surface tension is 40~50mN/m；The particle diameter of the mill base
For 100~120nm of D50, D90<300nm；Its preparation method is as follows：Deionized water, solvent, sterilization antiseptic, pH are put into successively
Conditioning agent, 20min is stirred under 500r/min rotating speed；Then dispersion aids is put into, continues stirring until solution is integrally limpid；
Input dispersant continues stirring until solution is integrally limpid；Input toner stirs 20min under 500r/min rotating speed；Then will
All materials add horizontal mill, and (a diameter of 0.1~0.5mm of zirconium oxide bead, zirconium pearl loading are 70~90%, grind capacity
For 1~1.5Kg) in, 12~15h is ground under 1000~2000r/min rotating speed, grinding temperature is 30~50 DEG C.With colouring
NMF in slurry formula is selected from ethylene glycol, diethylene glycol, triethylene glycol, 1,2 propane diols, glycerine, 1,5 pentanediols, sorb
At least one of sugar alcohol, EG-1；PH adjusting agent selected from ammoniacal liquor, triethanolamine, EDETATE SODIUM, the sodium of EDTA tetra- middle one kind；Help
Dispersant be selected from OP-7, OP-10, OP-15, NP-7, NP-10, NP-15 at least one of；It is real big that dispersant is selected from virtue dimension
At least one of the REAX 88B of gram company, REAX 88A, REAX 80D, REAX 83A, REAX 85A；Toner is selected from black
At least one of toner, blue toner, red toner, yellow toner.Wherein, black toner be selected from C.I. disperse violets 27,
C.I. disperse blue 366, C.I. disperse blues 26, C.I. disperse orange 25s, C.I. disperse oranges 37, C.I. scattered orange 119, C.I. disperse
Huang 54, C.I. disperse 64, C.I. disperses in 242 at least two；Blue toner is selected from C.I. Disperse Blue-56s, C.I. disperse blues
60th, one kind in C.I. disperse blues 91, C.I. disperse blues 359；Red toner be selected from C.I. disperse reds 50, C.I. disperse red 60s,
C.I. one kind in disperse red 65, C.I. disperse reds 239；Yellow toner is selected from C.I. disperse yellows 7, C.I. disperse yellows 54, C.I.
One kind in dispersion yellow 64, C.I. disperse yellows 100.
In above-mentioned ink set, resin be selected from BASF joint-stock company production PVP-K10, PVP-K20, PVP-K30,
PVP-K40, PVP-K50, TEGO Viscoplus 3000, the TEGO Viscoplus of the German high paint company production of enlightening
3010th, at least one of TEGO Viscoplus 3030.Secondary solvent is selected from ethylene glycol, diethylene glycol, triethylene glycol, 1,2
Propane diols, glycerine, 1,5 pentanediols, D-sorbite, glycerin ether, ethylene glycol monobutyl ether, diethylene glycol monomethyl ether, diethylene glycol
At least one of ether, diethylene glycol monobutyl ether, triethylene glycol butyl ether.PH adjusting agent is selected from ammoniacal liquor, triethanolamine, EDTA bis-
One kind in sodium, the sodium of EDTA tetra-.AFCONA3522, AFCON3580 of the wetting agent selected from Ai Fu Konas Chemical Co., Ltd.,
AFCON3581, AFCONA3585, German Ming Ling chemical companies production METOLAT355, METOLA362, METOLAT364,
METOLA365, U.S.'s Hensel step group324、168、169、
At least one of LF-37.
Above-mentioned heat sublimation ink-jet ink is manufactured according to the following steps：
1) deionized water of formula ratio, solvent, sterilization antiseptic, pH adjusting agent are put into material barrel in order,
20min is stirred under 500r/min rotating speed；The wetting agent for adding formula ratio continues to stir, untill solution is integrally limpid；Add
The resin for entering formula ratio continues to stir, untill treating that solution is integrally limpid；2) mill base of formula ratio is added 500r/min's
20min is stirred under rotating speed；Then with 0.22 μm of hydrophylic filter membranes with 0.45 μm of hydrophylic filter membranes is combined is filtered, produce.
Embodiment 1：Black heat sublimation ink-jet ink
A kind of waterborne digital printing dye sublimation ink-jet ink, it includes following each component by mass percentage：Resin
10%th, mill base 30%, solvent 20%, sterilization antiseptic 0.5%, pH adjusting agent 0.5%, wetting agent 1.5%, deionized water
37.5%.
Above-mentioned heat sublimation ink-jet ink is manufactured according to the following steps：
1) deionized water of formula ratio, solvent, sterilization antiseptic, pH adjusting agent are put into material barrel in order,
20min is stirred under 500r/min rotating speed；The wetting agent for adding formula ratio continues to stir, untill solution is integrally limpid；Add
The resin for entering formula ratio continues to stir, untill treating that solution is integrally limpid；
2) mill base for adding formula ratio stirs 20min under 500r/min rotating speed；Then with 0.22 μm of hydrophylic filter membranes with
0.45 μm of hydrophylic filter membranes is combined to be filtered, and is produced.
Embodiment 2：Blue heat sublimation ink-jet ink
A kind of waterborne digital printing dye sublimation ink-jet ink, it includes following each component by mass percentage：Resin
8%th, mill base 40%, solvent 10%, sterilization antiseptic 0.1%, pH adjusting agent 0.8%, wetting agent 2.1%, deionized water 39%.
Preparation method is the same as embodiment 1.
Embodiment 3：Red heat sublimation ink-jet ink
A kind of waterborne digital printing dye sublimation ink-jet ink, it includes following each component by mass percentage：Resin
5%th, mill base 45%, solvent 15%, sterilization antiseptic 1%, pH adjusting agent 1%, wetting agent 2%, deionized water 31%.
Preparation method is the same as embodiment 1.
Embodiment 4：Yellow heat sublimation ink-jet ink
A kind of waterborne digital printing dye sublimation ink-jet ink, it includes following each component by mass percentage：Resin
1%th, mill base 15%, solvent 50%, sterilization antiseptic 0.8%, pH adjusting agent 0.1%, wetting agent 3%, deionized water 30.1%.
Preparation method is the same as embodiment 1.
Performance test：
Using embodiment 1~4 as test group, certain domestic heat sublimation ink as blank group, sprayed using EPSON MT4114
Head printer carries out thermal transfer print image on transfer paper, in print procedure, the printing smoothness of determination test group and blank group
Property and stability；Then it is transferred on Se Dingbu, middle low temperature drying, and is determined under 205~225 DEG C, 25~35S with Pyrograph machine
Its sharpness and quick-drying.
Specific experiment method is as follows：
1st, fluency method of testing：Use in EPSON5113 industrial nozzles with the continuously printing 20 of 30~40 ㎡/H speed
㎡, determine its disconnected porosity；
2nd, stability test method：Use in EPSON5113 industrial nozzles with the continuously printing 100 of 30~40 ㎡/H speed
㎡, determine its disconnected porosity；
3rd, sharpness method of testing：The special heat-transferring printing paper of ink-jet is printed using EPSON5113 industrial nozzles, used
The heat sublimation ink of embodiment 1~4 and comparative example 1~4 prints 4P, 6P, 8P, 10P, 26 English of 12P sizes respectively
New roman character, more minimum visible writing；
4th, quick-drying method of testing：The heat sublimation ink of embodiment 1~4 and comparative example 1~4 is passed through into EPSON5113
Industrial nozzle prints 100% color lump respectively, is then stained with whether survey has substantially to fall with heat-transferring printing paper in 1,2,3,4,5min period
Color, obtain surface drying time.
It the results are shown in Table 1.
The performance test results of table 1 contrast
From table 1, waterborne digital printing dye sublimation ink-jet ink of the present invention is applied to all kinds of domestic EPSON
MT4114 printers, there is preferably printing fluency and stability, sharpness is high, substantially increases quick-drying, printing effect
Good, saturation degree bright in luster is high.
Above-mentioned embodiment is only the preferred embodiment of the present invention, it is impossible to the scope of protection of the invention is limited with this,
The change and replacement for any unsubstantiality that those skilled in the art is done on the basis of the present invention belong to institute of the present invention
Claimed scope.
Claims (10)
- A kind of 1. waterborne digital printing dye sublimation ink-jet ink, it is characterised in that：It includes following by mass percentage each Component：Resin 1~10%, mill base 5~50%, solvent 10~50%, sterilization antiseptic 0.1~1%, pH adjusting agent 0.1~ 1%th, wetting agent 0.1~3%, deionized water 10~50%.
- 2. waterborne digital printing dye sublimation ink-jet ink according to claim 1, it is characterised in that：The mill base is by following Component by mass percentage is made：Toner 15~30%, NMF 20~30%, dispersant 5~15%, dispersion aids 0.5~1.5%, bactericide 0.5~1%, pH adjusting agent 0.2~0.5%, deionized water 40~80%.
- 3. waterborne digital printing dye sublimation ink-jet ink according to claim 2, it is characterised in that：The viscosity of the mill base It is 40~50mN/m for 10~50Mpa.s, surface tension；The particle diameter of the mill base is D50100~120nm, D90<300nm.
- 4. waterborne digital printing dye sublimation ink-jet ink according to claim 2, it is characterised in that：The preparation of the mill base Method is as follows：Deionized water, solvent, sterilization antiseptic, pH adjusting agent are put into successively, are stirred under 500r/min rotating speed 20min；Then dispersion aids is put into, continues stirring until solution is integrally limpid；Input dispersant continues stirring until solution is whole Body is limpid；Input toner stirs 20min under 500r/min rotating speed；Then all materials are added in horizontal mill, 12~15h is ground under 1000~2000r/min rotating speed, grinding temperature is 30~50 DEG C.
- 5. waterborne digital printing dye sublimation ink-jet ink according to claim 2, it is characterised in that：The NMF is selected from At least one in ethylene glycol, diethylene glycol, triethylene glycol, 1,2 propane diols, glycerine, 1,5 pentanediols, D-sorbite, EG-1 Kind；The pH adjusting agent selected from ammoniacal liquor, triethanolamine, EDETATE SODIUM, the sodium of EDTA tetra- middle one kind；The dispersion aids is selected from At least one of OP-7, OP-10, OP-15, NP-7, NP-10, NP-15；The dispersant is selected from virtue Wei Shiweike companies REAX 88B, REAX 88A, REAX 80D, REAX 83A, at least one of REAX 85A；The toner is selected from black color At least one of powder, blue toner, red toner, yellow toner.
- 6. waterborne digital printing dye sublimation ink-jet ink according to claim 1, it is characterised in that：The resin be selected from bar PVP-K10, PVP-K20, PVP-K30, PVP-K40, PVP-K50 of Si Fu joint-stock companies production, the German high paint company life of enlightening At least one of the TEGO Viscoplus 3000 of production, TEGO Viscoplus 3010, TEGO Viscoplus 3030.
- 7. waterborne digital printing dye sublimation ink-jet ink according to claim 1, it is characterised in that：The secondary solvent choosing From ethylene glycol, diethylene glycol, triethylene glycol, 1,2 propane diols, glycerine, 1,5 pentanediols, D-sorbite, glycerin ether, ethylene glycol At least one of monobutyl ether, diethylene glycol monomethyl ether, diethylene glycol ether, diethylene glycol monobutyl ether, triethylene glycol butyl ether.
- 8. waterborne digital printing dye sublimation ink-jet ink according to claim 1, it is characterised in that：The pH adjusting agent choosing One kind from ammoniacal liquor, triethanolamine, EDETATE SODIUM, the sodium of EDTA tetra-.
- 9. waterborne digital printing dye sublimation ink-jet ink according to claim 1, it is characterised in that：The wetting agent is selected from AFCONA3522, AFCON3580 of Ai Fu Konas Chemical Co., Ltd., AFCON3581, AFCONA3585, the bright icepro chemistry of Germany METOLAT355, METOLA362, METOLAT364, METOLA365, the U.S.'s Hensel of company's production step group 324、168、169、At least one of LF-37.
- 10. waterborne digital printing dye sublimation ink-jet ink according to claim 1, it is characterised in that：The heat sublimation spray Ink is manufactured according to the following steps：1) deionized water of formula ratio, solvent, sterilization antiseptic, pH adjusting agent are put into material barrel in order, in 500r/ 20min is stirred under min rotating speed；The wetting agent for adding formula ratio continues to stir, untill solution is integrally limpid；Add formula The resin of amount continues to stir, untill treating that solution is integrally limpid；2) mill base for adding formula ratio stirs 20min under 500r/min rotating speed；Then with 0.22 μm of hydrophylic filter membranes and 0.45 μ M hydrophylic filter membranes are combined to be filtered, and is produced.
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| CN109505174A (en) * | 2018-11-21 | 2019-03-22 | 唐山德方化学有限公司 | A kind of silk ink-jet cloth printing technique |
| CN111234610A (en) * | 2020-03-09 | 2020-06-05 | 传美讯电子科技（珠海）有限公司 | Water-based ink-jet pigment color paste and preparation method and application thereof |
| CN111253806A (en) * | 2020-03-02 | 2020-06-09 | 传美讯电子科技（珠海）有限公司 | Structured acrylic dispersing agent and preparation method thereof, and aqueous inkjet thermal transfer printing disperse dye color paste and preparation method thereof |
| CN112940562A (en) * | 2021-03-10 | 2021-06-11 | 珠海君奥新材料科技有限公司 | Novel pyrograph color ink suitable for Epson head |
| CN113529446A (en) * | 2021-07-29 | 2021-10-22 | 浙江海印数码科技有限公司 | High-temperature dispersion direct-injection ink suitable for mulberry spray head and preparation method and application thereof |
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| CN109505174B (en) * | 2018-11-21 | 2021-12-14 | 唐山德方化学有限公司 | Ink-jet printing and dyeing process for silk |
| CN111253806A (en) * | 2020-03-02 | 2020-06-09 | 传美讯电子科技（珠海）有限公司 | Structured acrylic dispersing agent and preparation method thereof, and aqueous inkjet thermal transfer printing disperse dye color paste and preparation method thereof |
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| CN111234610B (en) * | 2020-03-09 | 2022-06-10 | 传美讯电子科技（珠海）有限公司 | Water-based ink-jet pigment color paste and preparation method and application thereof |
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