CN107630259A - Multi-functional summer is with the preparation method of refrigerant sense fabric - Google Patents
Multi-functional summer is with the preparation method of refrigerant sense fabric Download PDFInfo
- Publication number
- CN107630259A CN107630259A CN201710915823.0A CN201710915823A CN107630259A CN 107630259 A CN107630259 A CN 107630259A CN 201710915823 A CN201710915823 A CN 201710915823A CN 107630259 A CN107630259 A CN 107630259A
- Authority
- CN
- China
- Prior art keywords
- functional
- refrigerant sense
- parts
- fiber
- peppermint oil
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Landscapes
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
- Chemical Or Physical Treatment Of Fibers (AREA)
Abstract
Preparation method the invention discloses multi-functional summer with refrigerant sense fabric, it is concretely comprised the following steps：By peppermint oil and emulsifier solution pre-emulsification, add wall material solution and continue to emulsify, stirring reaction, add crosslinking agent reaction, dry peppermint oil microcapsule；Polyamide, jade powder and microcapsules are added in batch mixer and premixed, melting extrusion in extruder is placed into, obtains multi-functional refrigerant sense fibre section；Fibre section and auxiliary agent are put into screw extruder and carry out melt spinning, produces multi-functional refrigerant sense fiber；Multi-functional refrigerant sense fiber, flaxen fiber, cotton fiber, cocoon fiber are taken by weight, and blending by mixed yarn looming weaving, thermal finalization, is finally post-processed into mixed yarn, produces multi-functional summer with refrigerant sense fabric.Have the beneficial effect that：Preparation method of the present invention improves the added value of fabric, and preparation method is simple, convenient operation and control, steady quality, and production efficiency is high, is easy to large-scale industrial production.
Description
Technical field
The present invention relates to garment material field, more particularly to multi-functional summer is with the preparation method of refrigerant sense fabric.
Background technology
Human body is an airframe systems open, with compared with strong adaptability.When environment changes, human body is most fast
Adaptation reaction is the change of the circulatory system, and caused heat in vivo is carried to skin by it, and by perspiring, evaporation is scattered to increase
Heat.If sweat effectively can not be transmitted and evaporated so that the substantial amounts of heat of aggregation in vivo, will have influence on the comfort of human body, also
Probably due to hyperpyrexia triggers fatigue and reaction of trembling, or even reduce Human Stamina.Human body is passing through gaseous state sweat always
Moisture is lost, this is extremely important to keeping human body thermal balance and comfortableness, and this process depends on body state and the gas of surrounding
Environment is waited, is also largely influenceed by clothes physical property, clothes are the interaction media of environment and human body hot and humid area.
Clothes are not only to be covered in one on skin by kinetoplast, and can be adjusted with the skin heat to be changed because motion state is different
Function interaction is saved, and the latter is played regulatory role, the heat-moisture transfer attribute of clothes is to determine that human body gathers in motion
Heat and caused sweat actively can be delivered to outside clothes, so as to radiating and humidifying, are improved comfortableness, are still stopped in clothes
In dress-human body microenvironment, the key factor of human heat and wet comfort sense is reduced.It is especially all in the case where environment temperature is higher
When enclosing environment temperature close to body surface temperature, human body sweat in motion process flashes to as important factor, and
As human body and the clothes of surrounding environment heat-moisture transfer medium, its wet transitive attribute has non-to the radiating and humidifying of human body in motion
Often important meaning.Therefore, how lasting cooling feeling is kept in outdoor high temperature, turns into the problem of ordinary people is of interest.
Facing to such a demand from terminal consumer, function cool feeling absorbing sweat garment material just arises at the historic moment, in addition, summer weather is scorching
Heat, skin are easily perspired and sensitive, therefore it is required that fabric pliability is high, has no stimulation of the skin.
Prior art such as Authorization Notice No. is CN103184603B Chinese invention patent, discloses a kind of super cool feeling polyester
Fiber blend yarn and its spinning method for genuine, the mixed yarn is by super cool feeling polyester fiber 30%-100% and other fiber 70%-0% groups
It is the fibers such as tencel, Modal, viscose glue, cotton, bamboo fibre, terylene into, other fibers, by blowing, cotton carding, simultaneously on cotton spinning equipment
Bar, rove, spun yarn, the special process spinning of winding procedure.Multiple fiber blending in the mixed yarn, have complementary advantages between fiber,
With changeable style, not only with ventilative, comfortable and easy to wear, feel cunning the is glutinous characteristic of moisture absorption, and there is instantaneous temperature reduction effect, connect
There is 1-2 ° of moment is nice and cool, sunshine irradiates to have the 5-6 ° of cool feeling temperature difference after touching skin, skin can be wet by skin surface sweat after perspiring
Aspiration is transported to fabric face and dissipated, but the fabric flexibility is inadequate, and it is inadequate to wear comfort.
The content of the invention
It is an object of the invention to provide a kind of added value for improving Fypro, preparation method is simple, steady quality,
Production efficiency is high, and fabric has refrigerant sense and mint flavored, glossiness and soft-touch good multi-functional summer with refrigerant sense face
The preparation method of material.
The present invention is directed to the problem of being mentioned in above-mentioned technology, and the technical scheme taken is：Multi-functional summer is with refrigerant sense face
The preparation method of material, including prepared by peppermint oil microcapsule, prepared by multi-functional refrigerant sense fibre section, multi-functional refrigerant sense fiber system
Standby, multi-functional summer is prepared with refrigerant sense fabric, and preparation method concretely comprises the following steps：
It is prepared by peppermint oil microcapsule：Peppermint oil 20-30 parts, wall material 42-55 parts, emulsifying agent 2-3 parts, crosslinking agent are taken by weight
0.01-0.02 parts, the wall material solution that concentration is 1.3-1.7% and the emulsifier solution that concentration is 0.4-0.7% are first prepared, then will be thin
Lotus oil and emulsifier solution pre-emulsification 50-70s, then add wall material solution and continue to emulsify 2-4min, then adjust pH to 3-4, after
Continue and react 12-16min under conditions of temperature is 35-45 DEG C, stir speed (S.S.) is 500-700r/min, be then cooled to 2-10
DEG C, pH is adjusted to 9-10, is eventually adding crosslinking agent reaction 10-20min, spray drying, produces the microcapsules that fineness is 1-5 μm, on
It is that weight ratio is 1 to state wall material:0.9-1.1 gelatin and Arabic gum, the gelatin in the wall material is in the solution with polycation
Form is present, and it can be with producing electrostatic interaction in solution with Arabic gum existing for polyanion, and electric charge attracts each other and shape
Into negative ions complex compound, solubility reduces and condenses encystation, and the microencapsulated forms for the peppermint oil microcapsule that the step obtains are steady
Fixed, distinct, its surface is smooth, and cyst wall densification does not rupture, and wall material can not only play a protective role to peppermint oil, makes thin
Lotus oil high temperature resistant, delays its decomposition, reaches the effect of embedding, and can significantly reduce the rate of volatilization of peppermint oil, more has
Continue muchly to play its effect beneficial to essential oil, the effect of sustained release can be reached；
It is prepared by multi-functional refrigerant sense fibre section：It is 100 by weight ratio:0.7-1:0.28-0.35 polyamide, jade powder and thin
Lotus oil microcapsule is added in batch mixer and premixed, then raw material is put into melting extrusion in double screw extruder, cool drying, i.e., much
Function refrigerant sense fibre section, above-mentioned jade powder are surface-treated with silane coupler and titanate coupling agent, surface treatment
The particle diameter reduction of jade powder and distribution narrow afterwards so that the oil factor of jade powder is decreased obviously, and can effectively reduce the table of jade powder
Face can, so as to reduce the generation of jade powder agglomeration, polyamide in the step, jade powder and peppermint oil microcapsule it is reasonable
Proportioning enables jade powder and peppermint oil microcapsule dispersed in polyamide melt, and agglomeration will not occur, and to poly-
The mobility and spinnability of acid amides melt influence less, while jade powder and the compounding use of peppermint oil microcapsule additive can be big
The big refrigerant sense for improving polyamide, effect is far better than single additive；
It is prepared by multi-functional refrigerant sense fiber：Multi-functional refrigerant sense fibre section and auxiliary agent are put into screw rod, component, spinneret temperature
Respectively 245-255 DEG C, 260-270 DEG C, 235-245 DEG C, winding speed is to be carried out in 380-420m/min screw extruder
Melt spinning, multi-functional refrigerant sense fiber being produced, above-mentioned additive dosage is the 0.3-0.5% of multi-functional refrigerant sense fibre section,
Auxiliary agent is that weight ratio is 1:0.7-0.9:0.13-0.15 calcium chloride, rare earth ion and lactic acid, D-lactic acid and dextrorotation in lactic acid
The weight ratio of lactic acid is 1:0.2-0.3, D-lactic acid and L-lactic acid rational proportion can enable lactic acid as chlorination in lactic acid
The carrier agent of calcium and rare earth ion, the dispersiveness and stabilizer of calcium chloride and rare earth ion are improved, can preferably be acted on poly-
Amide molecule, the in addition addition of lactic acid can also make fiber be easy to colour, increase gloss and soft-touch, the controllability of the auxiliary agent
Good, the addition of auxiliary agent can hinder or destroy the formation of hydrogen bond between polyamide molecule, by reducing polyamide molecule interphase interaction
To reduce its melt viscosity, the addition of trace assistant can improve the processing characteristics of multi-functional refrigerant sense fibre section, make more work(
Can refrigerant sense fibre section obtain can spinnability greatly improve, and be not easy fracture of wire, finally improve the performance of multi-functional refrigerant sense fiber,
The peppermint oil microcapsule and jade powder that are prepared are coated in fiber by the multi-functional refrigerant sense fiber, have fiber refrigerant
Sense and mint flavored, also with the slow releasing function of peppermint oil microcapsule, the timeliness of long stapled refrigerant sense and mint flavored can be prolonged
Property；
Multi-functional summer is prepared with refrigerant sense fabric：Multi-functional refrigerant sense fiber 40-60 parts, flaxen fiber 5-15 are taken by weight
Part, cotton fiber 15-25 parts, cocoon fiber 8-15 parts, blending, by mixed yarn looming weaving, thermal finalization, are finally put into mixed yarn
Post-processed in dressing liquid, produce multi-functional summer is with refrigerant sense fabric, the composition and its parts by weight of above-mentioned dressing liquid：It is thin
Lotus oil microcapsule 3-5 parts, propylene glycol glycidyl ether 19-22 parts, aziridine 5-10 parts, ethylene urea 2-3 parts, polyurethane
0.8-1.2 parts, Tween-20 1-2 parts, water 80-90 parts, the arrangement liquid energy crosslink with fiber, effectively keep fibrous polymer
Thing chain molecule is connected to each other, and makes to be maintained between molecule on chain on relative position, strengthens the wrinkle resistance of fabric, and make peppermint
Oil microcapsule is readily adsorbed in web surface, strong to fabric affinity, fabric is had a feel of smooth, soft, wash resistant, and
There is the presence of peppermint oil microcapsule in collated web surface and fiber gap, and form is complete, does not have broken wall phenomenon,
The refrigerant sense of fabric is further enhanced, the fabric has refreshing, anti-inflammation, wears refrigerant advantage, and the fabric is easy
In coloring, absorbing sweat effect is good, have no stimulation of the skin, glossiness and soft-touch are good, also with peppermint oil microcapsule
Slow releasing function, can extend fabric refrigerant sense and mint flavored it is ageing.
Compared with prior art, the advantage of the invention is that：1）Preparation method of the present invention improves the attached of Fypro
Value added, preparation method is simple, convenient operation and control, steady quality, and production efficiency is high, is easy to large-scale industrial production；2）Should
Multi-functional summer has refreshing, anti-inflammation with refrigerant sense fabric, wears refrigerant advantage, and the fabric be easy to coloring,
Absorbing sweat effect is good, have no stimulation of the skin, glossiness and soft-touch are good；3）The fabric has the feel of smooth, soft,
Wash resistant, and have the presence of peppermint oil microcapsule in collated web surface and fiber gap, the form of microcapsules is complete,
There is no broken wall phenomenon, the fabric utilizes the slow releasing function of peppermint oil microcapsule, can extend the refrigerant sense and mint flavored of fabric
It is ageing；4）Jade powder and peppermint oil microcapsule are embedded with multi-functional refrigerant sense fiber in the fabric, fiber can be improved
Water-wash resistance, and then improve the water-wash resistance of fabric.
Embodiment
The present invention program is described further below by embodiment：
Embodiment 1：
Multi-functional summer is with the preparation method of refrigerant sense fabric, including prepared by peppermint oil microcapsule, multi-functional refrigerant sense fiber is cut
Prepared by piece, prepared by multi-functional refrigerant sense fiber, multi-functional summer is prepared with refrigerant sense fabric, and preparation method concretely comprises the following steps：
1）It is prepared by peppermint oil microcapsule：30 parts of peppermint oil, 45 parts of wall material, 3 parts of emulsifying agent, 0.012 part of crosslinking agent are taken by weight,
The wall material solution that concentration is 1.7% and the emulsifier solution that concentration is 0.45% are first prepared, then peppermint oil and emulsifier solution is pre-
65s is emulsified, wall material solution is then added and continues to emulsify 2min, then adjusts pH to 3.8, it is 38 DEG C, stir speed (S.S.) to continue in temperature
To react 12min under conditions of 700r/min, 10 DEG C are then cooled to, pH is adjusted to 9.2, is eventually adding crosslinking agent reaction 20min,
Spray drying, the microcapsules that fineness is 1-5 μm are produced, above-mentioned wall material is that weight ratio is 1:0.92 gelatin and Arabic gum, should
Gelatin in wall material exists in the form of polycation in the solution, it can with solution with Arabic existing for polyanion
Glue produces electrostatic interaction, and electric charge attracts each other and forms negative ions complex compound, and solubility reduces and condenses encystation, and the step obtains
The microencapsulated forms of the peppermint oil microcapsule arrived are stable, and distinct, its surface is smooth, and cyst wall densification does not rupture, and wall material is not
Peppermint oil can only be played a protective role, make peppermint oil high temperature resistant, delay its decomposition, reach the effect of embedding, and can be with
The rate of volatilization of peppermint oil is significantly reduced, essential oil is more beneficial for and continues muchly to play its effect, the effect of sustained release can be reached
Fruit；
2）It is prepared by multi-functional refrigerant sense fibre section：It is 100 by weight ratio:1:0.28 polyamide, jade powder and peppermint oil are micro-
Capsule is added in batch mixer and premixed, then raw material is put into melting extrusion in double screw extruder, cool drying, is produced multi-functional clear
Cool fiber is cut into slices, and above-mentioned jade powder is surface-treated with silane coupler and titanate coupling agent, jade after surface treatment
The particle diameter of powder reduces and distribution narrow so that and the oil factor of jade powder is decreased obviously, and can effectively reduce the surface energy of jade powder, from
And reducing the generation of jade powder agglomeration, the rational proportion of polyamide, jade powder and peppermint oil microcapsule makes in the step
Obtain jade powder and peppermint oil microcapsule can be dispersed in polyamide melt, agglomeration will not occur, and polyamide is melted
The mobility and spinnability of body influence less, while jade powder and the compounding use of peppermint oil microcapsule additive can greatly improve
The refrigerant sense of polyamide, effect is far better than single additive；
3）It is prepared by multi-functional refrigerant sense fiber：Multi-functional refrigerant sense fibre section and auxiliary agent are put into screw rod, component, spinneret temperature
Degree is respectively 255 DEG C, 260 DEG C, 245 DEG C, and winding speed is to carry out melt spinning in 380m/min screw extruder, i.e., much
Function refrigerant sense fiber, above-mentioned additive dosage are the 0.5% of multi-functional refrigerant sense fibre section, and auxiliary agent is that weight ratio is 1:
0.7:0.15 calcium chloride, rare earth ion and lactic acid, the weight of D-lactic acid and L-lactic acid ratio is 1 in lactic acid:0.2, lactic acid
Middle D-lactic acid and L-lactic acid rational proportion can enable lactic acid improve chlorination as calcium chloride and the carrier agent of rare earth ion
The dispersiveness and stabilizer of calcium and rare earth ion, can preferably act on polyamide molecule, and the addition of lactic acid in addition can also make
Fiber is easy to colour, increases gloss and soft-touch, and the controllability of the auxiliary agent is good, and the addition of auxiliary agent can hinder or destroy polyamides
The formation of hydrogen bond between amine molecule, its melt viscosity is reduced by reducing polyamide molecule interphase interaction, trace assistant adds
The processing characteristics of multi-functional refrigerant sense fibre section can be improved by entering, make multi-functional refrigerant sense fibre section obtain can spinnability significantly
Improve, and be not easy fracture of wire, finally improve the performance of multi-functional refrigerant sense fiber, the multi-functional refrigerant sense fiber will be prepared
Peppermint oil microcapsule and jade powder are coated in fiber, fiber is had refrigerant sense and mint flavored so that its woven face prepared
Material with refreshing, anti-inflammation, wear refrigerant advantage, and the fabric lining is easy to colour, absorbing sweat effect is good, to skin
Have no stimulation, glossiness and soft-touch it is good, also with the slow releasing function of peppermint oil microcapsule, can prolong long stapled
Refrigerant sense and mint flavored it is ageing.
4）Multi-functional summer is prepared with refrigerant sense fabric：It is to take multi-functional 55 parts of refrigerant sense fiber, flaxen fiber 6 by weight
Part, 23 parts of cotton fiber, 8 parts of cocoon fiber, by mixed yarn looming weaving, thermal finalization, finally put into dressing liquid and post-processed,
Produce multi-functional summer is with refrigerant sense fabric, the composition and its parts by weight of above-mentioned dressing liquid：5 parts of peppermint oil microcapsule, the third two
19 parts of alcohol glycidol ether, 10 parts of aziridine, 2 parts of ethylene urea, 1.2 parts of polyurethane, 1 part of Tween-20,90 parts of water, should
Arrange liquid energy to crosslink with fiber, effectively keep fibre-forming polymer chain molecule to be connected to each other, make to protect between molecule on chain
Hold on relative position, strengthen the wrinkle resistance of fabric, and peppermint oil microcapsule is readily adsorbed in web surface, to fabric parent
It is strong with power, make fabric that there is the feel of smooth, soft, wash resistant, and have peppermint in collated web surface and fiber gap
The presence of oil microcapsule, and form is complete, does not have broken wall phenomenon, further enhances the refrigerant sense of fabric, and the fabric has clear
It is cool to refresh oneself, anti-inflammation, wear refrigerant advantage, and the fabric be easy to coloring, absorbing sweat effect is good, have no stimulation of the skin,
Glossiness and soft-touch are good, also with the slow releasing function of peppermint oil microcapsule, can extend the refrigerant sense of fabric and thin
Lotus taste it is ageing.
Embodiment 2：
Multi-functional summer, it was concretely comprised the following steps with the preparation method of refrigerant sense fabric：
1）It is prepared by peppermint oil microcapsule：20 parts of peppermint oil, 55 parts of wall material, 2 parts of emulsifying agent, 0.02 part of crosslinking agent are taken by weight,
First prepare the wall material solution that concentration is 1.3% and the emulsifier solution that concentration is 0.7%, then by peppermint oil and the pre- breast of emulsifier solution
Change 50s, then add wall material solution and continue to emulsify 4min, then adjust pH to 3, continue temperature be 45 DEG C, stir speed (S.S.) be
16min is reacted under conditions of 500r/min, is then cooled to 3 DEG C, pH is adjusted to 10, is eventually adding crosslinking agent reaction 13min, spraying
Dry, produce the microcapsules that fineness is 1-5 μm, above-mentioned wall material is that weight ratio is 1:1.1 gelatin and Arabic gum；
2）It is prepared by multi-functional refrigerant sense fibre section：It is 100 by weight ratio:0.7:0.35 polyamide, jade powder and peppermint oil
Microcapsules are added in batch mixer and premixed, then raw material is put into melting extrusion in double screw extruder, cool drying, are produced multi-functional
Refrigerant sense fibre section, above-mentioned jade powder are surface-treated with silane coupler and titanate coupling agent；
3）It is prepared by multi-functional refrigerant sense fiber：Multi-functional refrigerant sense fibre section and auxiliary agent are put into screw rod, component, spinneret temperature
Degree is respectively 245 DEG C, 270 DEG C, 235 DEG C, and winding speed is to carry out melt spinning in 420m/min screw extruder, i.e., much
Function refrigerant sense fiber, above-mentioned additive dosage are the 0.3% of multi-functional refrigerant sense fibre section, and auxiliary agent is that weight ratio is 1:
0.9:0.13 calcium chloride, rare earth ion and lactic acid, the weight of D-lactic acid and L-lactic acid ratio is 1 in lactic acid:0.3.
4）Multi-functional summer is prepared with refrigerant sense fabric：Multi-functional 43 parts of refrigerant sense fiber, flaxen fiber 15 are taken by weight
Part, cotton fiber 15-256 parts, 15 parts of cocoon fiber, blending, by mixed yarn looming weaving, thermal finalization, are finally put into mixed yarn
Post-processed in dressing liquid, produce multi-functional summer is with refrigerant sense fabric, the composition and its parts by weight of above-mentioned dressing liquid：It is thin
3 parts of lotus oil microcapsule, 22 parts of propylene glycol glycidyl ether, 5 parts of aziridine, 3 parts of ethylene urea, 0.8 part of polyurethane, tell
Warm -20 2 parts, 80 parts of water.
Embodiment 3：
Multi-functional summer is with the preparation method of refrigerant sense fabric：
1）25 parts of peppermint oil, 48 parts of wall material, 2.5 parts of emulsifying agent, 0.015 part of crosslinking agent are taken by weight, and wall material is that weight ratio is
1:1 gelatin and Arabic gum, the wall material solution that concentration is 1.5% and the emulsifier solution that concentration is 0.5% are first prepared, then will be thin
Lotus oil and emulsifier solution pre-emulsification 60s, then add wall material solution and continue to emulsify 3min, then adjust pH to 3.5, continue in temperature
Spend for 40 DEG C, stir speed (S.S.) be 600r/min under conditions of react 14min, be then cooled to 6 DEG C, pH is adjusted to 9.5, is eventually adding
Crosslinking agent reacts 15min, spray drying, produces the peppermint oil microcapsule that fineness is 1-5 μm；
2）It is 100 by weight ratio:0.8:0.3 polyamide, it is surface-treated with silane coupler and titanate coupling agent
Jade powder and peppermint oil microcapsule, which are added in batch mixer, to be premixed, then raw material is put into melting extrusion in double screw extruder, is cooled down
Dry, produce multi-functional refrigerant sense fibre section；
3）By multi-functional refrigerant sense fibre section and auxiliary agent be put into screw rod, component, spinneret temperature be respectively 250 DEG C, 265 DEG C,
240 DEG C, winding speed is to carry out melt spinning in 400m/min screw extruder, produces multi-functional refrigerant sense fiber, above-mentioned
Additive dosage is the 0.4% of multi-functional refrigerant sense fibre section, and auxiliary agent is that weight ratio is 1:0.8:0.14 calcium chloride, rare earth
Ion and lactic acid, the weight of D-lactic acid and L-lactic acid ratio is 1 in lactic acid:0.25；
4）Multi-functional 50 parts of refrigerant sense fiber, 10 parts of flaxen fiber, 20 parts of cotton fiber, 12 parts of cocoon fiber, blending are taken by weight
Into mixed yarn, mixed yarn looming weaving, is finally put into containing 4 parts of peppermint oil microcapsule, propylene glycol glycidyl ether thermal finalization
20 parts, 8 parts of aziridine, 2.5 parts of ethylene urea, 1 part of polyurethane, 1.5 parts of Tween-20,85 parts of water dressing liquid in carry out
Post processing, produces multi-functional summer with refrigerant sense fabric.
Embodiment 4：
Multi-functional summer is with the performance test of refrigerant sense fabric：
The fabric of embodiment 1, embodiment 2 and embodiment 3 is set to test group, common commercially available polyamide fabric is set to control group 1,
Common commercially available refrigerant fabric is set to control group 2, carries out refrigerant sense test respectively.
Refrigerant sense is tested：Changes in temperature sensing tester is contacted using instantaneous touch cool feeling Q-max as index：By simulating hand contact surface
The change of caused heat calculates the degree of cool feeling after material, and result of calculation is as shown in table 1.
Table 1：Refrigerant sense test result
As shown in Table 1, the refrigerant sense Q-max of the embodiment of the present invention 1, embodiment 2 and the fabric of embodiment 3 is more than control group 1 and right
According to group 2, illustrate that the multi-functional summer that preparation method of the present invention obtains is good with the cooling effect of refrigerant sense fabric.
Routine operation in the operating procedure of the present invention is well known to those skilled in the art, herein without repeating.
Technical scheme is described in detail embodiment described above, it should be understood that it is described above only
For the specific embodiment of the present invention, it is not intended to limit the invention, all any modifications made in the spirit of the present invention,
Supplement or similar fashion replacement etc., should be included in the scope of the protection.
Claims (10)
1. multi-functional summer is with the preparation method of refrigerant sense fabric, including prepared by peppermint oil microcapsule, multi-functional refrigerant sense fiber
Prepared by section, prepared by multi-functional refrigerant sense fiber, multi-functional summer is prepared with refrigerant sense fabric, it is characterised in that：Described is more
Function refrigerant sense fiber preparation process is：Multi-functional refrigerant fibre section and auxiliary agent are put into screw extruder and carry out melting spinning
Silk, produces multi-functional refrigerant fiber.
2. multi-functional refrigerant sense fiber according to claim 1, it is characterised in that：Described multi-functional refrigerant sense fiber system
Screw rod, component, the spinneret temperature of screw extruder are respectively 245-255 DEG C, 260-270 DEG C, 235-245 DEG C in standby step,
Winding speed is 380-420m/min.
3. multi-functional refrigerant sense fiber according to claim 1, it is characterised in that：Described multi-functional refrigerant sense fiber system
Additive dosage is the 0.3-0.5% of multi-functional refrigerant sense fibre section in standby step, and auxiliary agent is that weight ratio is 1:0.7-0.9:
0.13-0.15 calcium chloride, rare earth ion and lactic acid, the weight of D-lactic acid and L-lactic acid ratio is 1 in lactic acid:0.2-0.3.
4. multi-functional refrigerant sense fiber according to claim 1, it is characterised in that：Described peppermint oil microcapsule prepares step
The composition of peppermint oil microcapsule and its parts by weight are in rapid：Peppermint oil 20-30 parts, wall material 42-55 parts, emulsifying agent 2-3 parts, crosslinking
Agent 0.01-0.02 parts, wall material are that weight ratio is 1:0.9-1.1 gelatin and Arabic gum.
5. multi-functional refrigerant sense fiber according to claim 1, it is characterised in that：Described peppermint oil microcapsule prepares step
The concentration of wall material solution is 1.3-1.7% in rapid, and the concentration of emulsifier solution is 0.4-0.7%.
6. multi-functional refrigerant sense fiber according to claim 1, it is characterised in that：Described peppermint oil microcapsule prepares step
The pH of stirring reaction is 3-4 in rapid, and temperature is 35-45 DEG C, stir speed (S.S.) 500-700r/min, time 12-16min；Hand over
The temperature of connection reaction is 2-10 DEG C, pH 9-10, time 10-20min.
7. multi-functional refrigerant sense fiber according to claim 1, it is characterised in that：Described peppermint oil microcapsule prepares step
The fineness of peppermint oil microcapsule is 1-5 μm in rapid.
8. multi-functional refrigerant sense fiber according to claim 1, it is characterised in that：Described multi-functional refrigerant sense fiber is cut
The weight ratio of polyamide, jade powder and peppermint oil microcapsule is 100 in piece preparation process:0.7-1:0.28-0.35, jade powder are used
Silane coupler and titanate coupling agent are surface-treated.
9. multi-functional refrigerant sense fiber according to claim 1, it is characterised in that：Described multi-functional summer refrigerant sense
The composition of refrigerant sense fabric and its parts by weight are in fabric preparation process：Multi-functional refrigerant sense fiber 40-60 parts, flaxen fiber 5-15
Part, cotton fiber 15-25 parts, cocoon fiber 8-15 parts.
10. multi-functional summer according to claim 1 is with the preparation method of refrigerant sense fabric, it is characterised in that：Described
Multi-functional summer is with the composition of dressing liquid and its parts by weight in refrigerant sense fabric preparation process：Peppermint oil microcapsule 3-5 parts, third
Glycol glycidol ether 19-22 parts, aziridine 5-10 parts, ethylene urea 2-3 parts, polyurethane 0.8-1.2 parts, Tween-20
1-2 parts, water 80-90 parts.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710915823.0A CN107630259A (en) | 2017-09-30 | 2017-09-30 | Multi-functional summer is with the preparation method of refrigerant sense fabric |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710915823.0A CN107630259A (en) | 2017-09-30 | 2017-09-30 | Multi-functional summer is with the preparation method of refrigerant sense fabric |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107630259A true CN107630259A (en) | 2018-01-26 |
Family
ID=61105078
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710915823.0A Pending CN107630259A (en) | 2017-09-30 | 2017-09-30 | Multi-functional summer is with the preparation method of refrigerant sense fabric |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107630259A (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114686998A (en) * | 2022-04-21 | 2022-07-01 | 浙江锦事达化纤有限公司 | Cool nylon yarn and preparation process thereof |
| CN114960012A (en) * | 2022-05-31 | 2022-08-30 | 广东电网有限责任公司 | Cool fabric, preparation method thereof and gloves |
| CN116145274A (en) * | 2022-12-12 | 2023-05-23 | 南通赛晖科技发展股份有限公司 | Cool comfortable fabric and preparation method thereof |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1664113A (en) * | 2005-03-23 | 2005-09-07 | 李上辉 | Anion materials, modified leather materials thereby, and use thereof |
| CN104178356A (en) * | 2014-09-05 | 2014-12-03 | 南京泽朗生物科技有限公司 | Preparation method of mint essence oil microcapsule and application of mint essence oil microcapsule in tobacco |
| CN104195668A (en) * | 2014-08-19 | 2014-12-10 | 浙江华峰氨纶股份有限公司 | Preparation method of multifunctional cool polyurethane elastic fiber |
| CN106592251A (en) * | 2016-11-17 | 2017-04-26 | 上海应用技术大学 | Microcapsule finishing agent for cool and refreshing functional fabric and preparation method |
-
2017
- 2017-09-30 CN CN201710915823.0A patent/CN107630259A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1664113A (en) * | 2005-03-23 | 2005-09-07 | 李上辉 | Anion materials, modified leather materials thereby, and use thereof |
| CN104195668A (en) * | 2014-08-19 | 2014-12-10 | 浙江华峰氨纶股份有限公司 | Preparation method of multifunctional cool polyurethane elastic fiber |
| CN104178356A (en) * | 2014-09-05 | 2014-12-03 | 南京泽朗生物科技有限公司 | Preparation method of mint essence oil microcapsule and application of mint essence oil microcapsule in tobacco |
| CN106592251A (en) * | 2016-11-17 | 2017-04-26 | 上海应用技术大学 | Microcapsule finishing agent for cool and refreshing functional fabric and preparation method |
Non-Patent Citations (3)
| Title |
|---|
| 中国科学技术协会: "《2014-2015 稀土科学技术 学科发展报告》", 30 April 2016, 中国科学技术出版社 第1版 * |
| 杨一: ""薄荷油微胶囊的制备及其应用"", 《中国优秀硕士学位论文全文数据库（电子期刊） 工程科技Ⅰ辑》 * |
| 黄玉媛等: "《精细化工配方 常用原料手册》", 31 March 1998, 广东科技出版社 第1版 * |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114686998A (en) * | 2022-04-21 | 2022-07-01 | 浙江锦事达化纤有限公司 | Cool nylon yarn and preparation process thereof |
| CN114686998B (en) * | 2022-04-21 | 2023-10-13 | 浙江锦事达化纤有限公司 | Cool nylon yarn and preparation process thereof |
| CN114960012A (en) * | 2022-05-31 | 2022-08-30 | 广东电网有限责任公司 | Cool fabric, preparation method thereof and gloves |
| CN114960012B (en) * | 2022-05-31 | 2023-08-11 | 广东电网有限责任公司 | Cool sense fabric and glove |
| CN116145274A (en) * | 2022-12-12 | 2023-05-23 | 南通赛晖科技发展股份有限公司 | Cool comfortable fabric and preparation method thereof |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN103276464B (en) | A kind of manufacture method of chinlon high functionality cooling filament | |
| CN106498541B (en) | A kind of ecological antibiotic height sense polyester fiber and its production method | |
| CN105908269B (en) | Manufacturing method of special-shaped hollow warmth keeping polyester drawn textured yarn | |
| CN111172619A (en) | Fiber, preparation method, application and textile thereof | |
| CN103088459B (en) | Polyamide-based cooling fiber and yarn | |
| CN103653279A (en) | Underwear and production method thereof | |
| CN107630259A (en) | Multi-functional summer is with the preparation method of refrigerant sense fabric | |
| CN108411402A (en) | A kind of garment material based on one-D nano zinc oxide polyester antibacterial plastic concentrate | |
| CN105887279B (en) | A kind of wash-and-wear of shirt fabric and preparation method thereof | |
| CN105177739A (en) | Two-component round hollow cross-shaped special-shaped high-absorbent complex fiber and production method thereof | |
| CN107488907A (en) | A kind of mixed yarn of bamboo fibre, cotton fiber and chemical fibre | |
| CN107740200A (en) | Multi-functional refrigerant sense fiber | |
| CN110117853A (en) | Multi-functional cashmere blended yarn and preparation method thereof | |
| CN107805949A (en) | Multi-functional summer is with refrigerant sense fabric | |
| CN105113052A (en) | Cool-sense polyester fiber | |
| CN112760784A (en) | Preparation process of nylon-polyester blended fabric with cool feeling | |
| CN105862208B (en) | Preparation processing method with the wool blended hosiery yarns of moisture absorption heating function | |
| CN111962296A (en) | Aerogel textile fabric and preparation method thereof | |
| CN107761189A (en) | A kind of preparation method of the refreshing anti-bacterial fibre of super fine denier suction ice | |
| CN113322577B (en) | Wadding with antibacterial flame-retardant warm-keeping function and preparation method thereof | |
| CN101240462B (en) | Method for preparing acrylics-protein-copper salt composite antistatic fiber | |
| CN105671679A (en) | High-moisture-conducting and heat-insulating fibers | |
| CN107012531A (en) | A kind of ice-cold rapid-curing cutback hydrophilic polyesters fiber and preparation method thereof | |
| CN107280113A (en) | The fabric and processing method of a kind of sun-proof radiation protection | |
| CN110468463A (en) | A kind of high-end knitting fabric and its processing method |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20180126 |