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CN107217495A - A kind of preparation method of hollow nylon blend polyester lightweight push-and-pull paulin coating cloth - Google Patents

A kind of preparation method of hollow nylon blend polyester lightweight push-and-pull paulin coating cloth Download PDF

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Publication number
CN107217495A
CN107217495A CN201710607679.4A CN201710607679A CN107217495A CN 107217495 A CN107217495 A CN 107217495A CN 201710607679 A CN201710607679 A CN 201710607679A CN 107217495 A CN107217495 A CN 107217495A
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CN
China
Prior art keywords
coating
paulin
hollow nylon
pull
preparation
Prior art date
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Pending
Application number
CN201710607679.4A
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Chinese (zh)
Inventor
王旭
吴文中
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
ANHUI PLATO COATED FABRICS Co Ltd
Original Assignee
ANHUI PLATO COATED FABRICS Co Ltd
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Publication date
Application filed by ANHUI PLATO COATED FABRICS Co Ltd filed Critical ANHUI PLATO COATED FABRICS Co Ltd
Priority to CN201710607679.4A priority Critical patent/CN107217495A/en
Publication of CN107217495A publication Critical patent/CN107217495A/en
Pending legal-status Critical Current

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    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06N—WALL, FLOOR, OR LIKE COVERING MATERIALS, e.g. LINOLEUM, OILCLOTH, ARTIFICIAL LEATHER, ROOFING FELT, CONSISTING OF A FIBROUS WEB COATED WITH A LAYER OF MACROMOLECULAR MATERIAL; FLEXIBLE SHEET MATERIAL NOT OTHERWISE PROVIDED FOR
    • D06N3/00—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof
    • D06N3/0002—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof characterised by the substrate
    • D06N3/0006—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof characterised by the substrate using woven fabrics
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    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06B—TREATING TEXTILE MATERIALS USING LIQUIDS, GASES OR VAPOURS
    • D06B15/00—Removing liquids, gases or vapours from textile materials in association with treatment of the materials by liquids, gases or vapours
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06B—TREATING TEXTILE MATERIALS USING LIQUIDS, GASES OR VAPOURS
    • D06B3/00—Passing of textile materials through liquids, gases or vapours to effect treatment, e.g. washing, dyeing, bleaching, sizing, impregnating
    • D06B3/10—Passing of textile materials through liquids, gases or vapours to effect treatment, e.g. washing, dyeing, bleaching, sizing, impregnating of fabrics
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    • D06C—FINISHING, DRESSING, TENTERING OR STRETCHING TEXTILE FABRICS
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    • D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
    • D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
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    • D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
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    • D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M15/643—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds containing silicon in the main chain
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    • D06N3/00—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof
    • D06N3/0002—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof characterised by the substrate
    • D06N3/0015—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof characterised by the substrate using fibres of specified chemical or physical nature, e.g. natural silk
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    • D06N3/00—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof
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    • D06N3/0015—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof characterised by the substrate using fibres of specified chemical or physical nature, e.g. natural silk
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    • D06N3/00—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof
    • D06N3/0056—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof characterised by the compounding ingredients of the macro-molecular coating
    • D06N3/0061—Organic fillers or organic fibrous fillers, e.g. ground leather waste, wood bark, cork powder, vegetable flour; Other organic compounding ingredients; Post-treatment with organic compounds
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    • D06N3/00—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof
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    • D06N3/0063—Inorganic compounding ingredients, e.g. metals, carbon fibres, Na2CO3, metal layers; Post-treatment with inorganic compounds
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    • D06N3/00—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof
    • D06N3/12—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof with macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. gelatine proteins
    • D06N3/14—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof with macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. gelatine proteins with polyurethanes
    • D06N3/146—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof with macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. gelatine proteins with polyurethanes characterised by the macromolecular diols used
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    • D06N3/00—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof
    • D06N3/12—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof with macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. gelatine proteins
    • D06N3/14—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof with macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. gelatine proteins with polyurethanes
    • D06N3/147—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof with macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. gelatine proteins with polyurethanes characterised by the isocyanates used
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    • D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
    • D06M2101/16—Synthetic fibres, other than mineral fibres
    • D06M2101/30—Synthetic polymers consisting of macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
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    • D06M2101/16—Synthetic fibres, other than mineral fibres
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    • D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
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    • D06N2209/00—Properties of the materials
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  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
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  • Chemical Kinetics & Catalysis (AREA)
  • Dispersion Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Inorganic Chemistry (AREA)
  • Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)

Abstract

The invention discloses a kind of preparation method of hollow nylon blend polyester lightweight push-and-pull paulin coating cloth, blending woven is carried out with hollow nylon fiber using nylon fiber and polyester fiber and twisted filament and obtains scrim material, due to the unique cavity structure of hollow nylon fiber, it is woven go out yarn weaved fabric there is good heat-proof quality；Then base fabric is subjected to the water-proof finish before coating, the waterproofing agent of organosilicon being made is compounded using compositions such as octamethylcy-clotetrasiloxane, Long carbon chain trimethoxy silanes, the water repellency of scrim surfaces can be improved, and provide necessary basic for the resistance to hydrostatic pressure of final products, it can also prevent coating adhesive from penetrating into fabric another side, it is ensured that coating film forming is uniform；Finally in base fabric using it is positive and negative brush twice by the way of carry out the brushing of polyurethane coating glue, the soft, coating of waterproof is obtained, simultaneously because containing the nanometer titanium dioxide of certain component in coating, with certain anti-ultraviolet effect, the weatherability of raising coating.

Description

A kind of preparation method of hollow nylon blend polyester lightweight push-and-pull paulin coating cloth
Technical field
The present invention relates to coating cloth technical field, more particularly to a kind of hollow nylon blend polyester lightweight push-and-pull paulin coating The preparation method of cloth.
Background technology
Coating cloth is mainly on the basis of cloth is coated with one layer of material with specific function using special process, makes cloth Material adds special function, so also referred to as functional coat fabric.Sun-proof, waterproof, fire-retardant etc. can be divided into according to function Coating cloth, due to it is excellent the characteristics of can be widely applied to the fields such as clothes, tent, transport, national defence.Outdoor push-and-pull paulin is widely used in The fields such as outdoor activities, business activity, with the advantage such as waterproof, sun-proof, but are due to that heaviness causes to store inconvenient, this needs The tarpaulin material of push-and-pull paulin is modified accordingly, while the tarpaulin that traditional technique is made does not have heat-insulated work With especially being used in summer, what space in tarpaulin can be suitable is sultry, it is impossible to meet the life requirement of people, this is accomplished by pair The fabric and coating of push-and-pull paulin tarpaulin are carried out modified accordingly and optimized, and obtain collecting light, tension, solid, heat-insulated with one The coating cloth of body.
The content of the invention
The object of the invention is exactly to be pushed away to make up the defect of prior art there is provided a kind of hollow nylon blend polyester lightweight Draw the preparation method of paulin coating cloth.
The present invention is achieved by the following technical solutions：
A kind of preparation method of hollow nylon blend polyester lightweight push-and-pull paulin coating cloth, including step in detail below：
（1）Quality such as common nylon chopped fiber and polyester fiber and twisting with the fingers are obtained and twisted filament is stand-by, then with hollow nylon fiber Blending woven is carried out according to certain mass ratio, plain woven base fabric is obtained；
（2）Base fabric is immersed in water-proof aagent 20-30 minutes, the base fabric after dipping is then used into pressure calendering, control Certain speed and pick-up rate, then the base fabric after calendering is finally repeated single-steeping, rolled in 150-170 DEG C of drying Light, drying operation, obtain waterproof base fabric before coating；
（3）Polyurethane coating glue of the viscosity in 6000CP or so has been configured, first polyurethane coating glue has been applied using vertical brushing The tow sides of the waterproof base fabric before coating are brushed, gross thickness 0.28-0.3mm is controlled, at 150-160 DEG C after dry 10-15 minutes Take out and carry out my horizontal brushing, control gross thickness 0.35-0.38mm, finally control 16-18 ms/min of speed, temperature control 170-175 DEG C it is dried.
A kind of preparation method of hollow nylon blend polyester lightweight push-and-pull paulin coating cloth, step（1）Described in and twist with the fingers Silk carries out blending woven with hollow nylon fiber according to certain mass ratio, refers to according to simultaneously twisted filament：Hollow nylon fiber 1:2 Ratio carries out mixed weaving.
A kind of preparation method of hollow nylon blend polyester lightweight push-and-pull paulin coating cloth, step（2）Described in control Certain speed and pick-up rate specifically refers to the speed with 10m/min, and pick-up rate is controlled in 30-35%.
A kind of preparation method of hollow nylon blend polyester lightweight push-and-pull paulin coating cloth, step（2）Described in waterproof Finishing agent refers to the waterproofing agent of organosilicon being made up of certain technique, and specific preparation technology is as follows：（1）By the silica of prestox ring four The deionized water that 2-2.5 times of total amount is measured is added after alkane and 0.1-0.15% TMAH are well mixed, is heated to 90-95 DEG C, stirring reaction is cooled to 60-65 DEG C after 90-120 minutes, adds octamethylcy-clotetrasiloxane quality 2-3% ethene Ethyl triethoxy silicane alkane, 2.5-3% Long carbon chain trimethoxy silane is continuously heating to 110-120 DEG C, after reacting 60-90 minutes Vacuumize 30-40 minutes, add total reactant quality 30-40% isopropanol, continue to stir 20-30 minutes, produce organosilicon and answer Compound；（2）Appropriate isomerous tridecanol polyoxyethylene ether 1305 is mixed with organic silicon composite, solid content is obtained for 25-28% Water-proof aagent.
A kind of preparation method of hollow nylon blend polyester lightweight push-and-pull paulin coating cloth, step（3）Described in poly- ammonia Ester coating adhesive is uniformly made according to certain composition proportion dispersed with stirring, and its composition proportion is：Polyoxypropyleneglycol 100-105 parts, 25-30 parts of isocyanates, 45-50 parts of dibutyl phthalate, 2-2.5 parts of dibutyl tin laurate are received 30-35 parts of titanium dioxide of rice, 4-5 parts of BTA.
It is an advantage of the invention that：The present invention first using nylon fiber, simultaneously with hollow nylon fiber enter with polyester fiber by twisted filament Row blending woven obtains scrim material, due to the unique cavity structure of hollow nylon fiber, internal reservoir still air, it is woven go out Yarn weaved fabric compared with common woven fabric, its mass area ratio is the 70% of same thickness, and its surface area is big, with good Good heat-proof quality；Then base fabric is subjected to the water-proof finish before coating, using octamethylcy-clotetrasiloxane, Long carbon chain trimethoxy The waterproofing agent of organosilicon that the compositions such as base silane compounding is made, can improve the water repellency of scrim surfaces, and be the resistance to of final products Hydrostatic pressing provides necessary basic, moreover it is possible to prevent coating adhesive from penetrating into fabric another side, it is ensured that coating film forming is uniform；Finally in base On cloth using it is positive and negative brush twice by the way of carry out the brushing of polyurethane coating glue, by control polyurethane coating glue viscosity, The parameters such as coating layer thickness, speed, baking temperature, obtain the soft, coating of waterproof, simultaneously because containing certain component in coating Nanometer titanium dioxide, with certain anti-ultraviolet effect, improves the weatherability of coating.
A kind of preparation method of hollow nylon blend polyester lightweight push-and-pull paulin coating cloth of the present invention, obtained product with it is general Logical push-and-pull paulin coating cloth is compared, thinner and lighter, convenient for collecting, and will not influence its tear, fracture strength because of frivolous, simultaneously With good thermal insulation, temperature suitable under push-and-pull paulin is able to maintain that.
Embodiment
A kind of preparation method of hollow nylon blend polyester lightweight push-and-pull paulin coating cloth, including step in detail below：
（1）Quality such as common nylon chopped fiber and polyester fiber and twisting with the fingers are obtained and twisted filament is stand-by, then with hollow nylon fiber According to 1:2 mass ratio carries out blending woven, obtains plain woven base fabric；
（2）Base fabric is immersed in water-proof aagent 20 minutes, the base fabric after dipping is then used into pressure calendering, 10m/ is controlled Min speed, pick-up rate 30%, then the base fabric after calendering is finally repeated into single-steeping, calendering, baking in 150 DEG C of drying Dry run, obtains waterproof base fabric before coating；
（3）Polyurethane coating glue of the viscosity in 6000CP or so has been configured, first polyurethane coating glue has been applied using vertical brushing The tow sides of the waterproof base fabric before coating are brushed, gross thickness 0.28mm is controlled, taking out progress after being dried 10 minutes at 150 DEG C, I crouches Formula brushing, controls gross thickness 0.35mm, finally controls 16 ms/min of speed, and 170 DEG C of temperature control is dried.
A kind of preparation method of described hollow nylon blend polyester lightweight push-and-pull paulin coating cloth, step（2）Described in Water-proof aagent refer to the waterproofing agent of organosilicon being made up of certain technique, specific preparation technology is as follows：（1）By prestox ring The deionized water of 2 times of amounts of total amount is added after tetrasiloxane and 0.1% TMAH are well mixed, 90 DEG C are heated to, Stirring reaction is cooled to 60 DEG C after 90 minutes, add the VTES of octamethylcy-clotetrasiloxane quality 2%, 2.5% Long carbon chain trimethoxy silane, is continuously heating to 110 DEG C, reaction is vacuumized 30 minutes after 60 minutes, adds overall reaction The isopropanol of amount of substance 30%, continues to stir 20 minutes, produces organic silicon composite；（2）By appropriate isomerous tridecanol polyoxy second Alkene ether 1305 is mixed with organic silicon composite, obtains the water-proof aagent that solid content is 25%.
A kind of preparation method of described hollow nylon blend polyester lightweight push-and-pull paulin coating cloth, step（3）Described in Polyurethane coating glue be uniformly to be made according to certain composition proportion dispersed with stirring, its composition proportion is：PPOX 100 parts of glycol, 25 parts of isocyanates, 45 parts of dibutyl phthalate, 2 parts of dibutyl tin laurate, nanometer titanium dioxide 30 Part, 4 parts of BTA.

Claims (5)

1. a kind of preparation method of hollow nylon blend polyester lightweight push-and-pull paulin coating cloth, it is characterised in that including following tool Body step：
（1）Quality such as common nylon chopped fiber and polyester fiber and twisting with the fingers are obtained and twisted filament is stand-by, then with hollow nylon fiber Blending woven is carried out according to certain mass ratio, plain woven base fabric is obtained；
（2）Base fabric is immersed in water-proof aagent 20-30 minutes, the base fabric after dipping is then used into pressure calendering, control Certain speed and pick-up rate, then the base fabric after calendering is finally repeated single-steeping, rolled in 150-170 DEG C of drying Light, drying operation, obtain waterproof base fabric before coating；
（3）Polyurethane coating glue of the viscosity in 6000CP or so has been configured, first polyurethane coating glue has been applied using vertical brushing The tow sides of the waterproof base fabric before coating are brushed, gross thickness 0.28-0.3mm is controlled, at 150-160 DEG C after dry 10-15 minutes Take out and carry out my horizontal brushing, control gross thickness 0.35-0.38mm, finally control 16-18 ms/min of speed, temperature control 170-175 DEG C it is dried.
2. a kind of preparation method of hollow nylon blend polyester lightweight push-and-pull paulin coating cloth according to claim 1, its It is characterised by, step（1）Described in and twisted filament and hollow nylon fiber carry out blending woven according to certain mass ratio, refer to According to simultaneously twisted filament：Hollow nylon fiber 1:2 ratio carries out mixed weaving.
3. a kind of preparation method of hollow nylon blend polyester lightweight push-and-pull paulin coating cloth according to claim 1, its It is characterised by, step（2）Described in the certain speed of control and pick-up rate specifically refer to speed with 10m/min, mangle Rate is controlled in 30-35%.
4. a kind of preparation method of hollow nylon blend polyester lightweight push-and-pull paulin coating cloth according to claim 1, its It is characterised by, step（2）Described in water-proof aagent refer to the waterproofing agent of organosilicon being made up of certain technique, it is specific to prepare Technique is as follows：（1）Total amount is added after octamethylcy-clotetrasiloxane and 0.1-0.15% TMAH are well mixed The 2-2.5 times of deionized water measured, is heated to 90-95 DEG C, stirring reaction is cooled to 60-65 DEG C after 90-120 minutes, adds eight first Basic ring tetrasiloxane quality 2-3% VTES, 2.5-3% Long carbon chain trimethoxy silane continues to heat up To 110-120 DEG C, reaction is vacuumized 30-40 minutes after 60-90 minutes, adds total reactant quality 30-40% isopropanol, after Continuous stirring 20-30 minutes, produces organic silicon composite；（2）By appropriate isomerous tridecanol polyoxyethylene ether 1305 and organosilicon Compound is mixed, and obtains the water-proof aagent that solid content is 25-28%.
5. a kind of preparation method of hollow nylon blend polyester lightweight push-and-pull paulin coating cloth according to claim 1, its It is characterised by, step（3）Described in polyurethane coating glue be uniformly to be made according to certain composition proportion dispersed with stirring, its Composition proportion is：100-105 parts of polyoxypropyleneglycol, 25-30 parts of isocyanates, 45-50 parts of dibutyl phthalate, two 2-2.5 parts of dibutyl tin laurate, 30-35 parts of nanometer titanium dioxide, 4-5 parts of BTA.
CN201710607679.4A 2017-07-24 2017-07-24 A kind of preparation method of hollow nylon blend polyester lightweight push-and-pull paulin coating cloth Pending CN107217495A (en)

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CN110126315A (en) * 2019-05-30 2019-08-16 吴江市达派纺织有限公司 A kind of cloth calendering PVB production technology
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CN115467172A (en) * 2022-09-21 2022-12-13 浙江东进新材料有限公司 Preparation method of ultra-light thin waterproof coating fabric and coating device
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Application publication date: 20170929