CN106758378B - A kind of textile dyeing increases deep functional agent and preparation method thereof, application - Google Patents
A kind of textile dyeing increases deep functional agent and preparation method thereof, application Download PDFInfo
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- CN106758378B CN106758378B CN201710020124.XA CN201710020124A CN106758378B CN 106758378 B CN106758378 B CN 106758378B CN 201710020124 A CN201710020124 A CN 201710020124A CN 106758378 B CN106758378 B CN 106758378B
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/38—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using reactive dyes
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/64—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds without sulfate or sulfonate groups
- D06P1/651—Compounds without nitrogen
- D06P1/65106—Oxygen-containing compounds
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/64—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds without sulfate or sulfonate groups
- D06P1/651—Compounds without nitrogen
- D06P1/65106—Oxygen-containing compounds
- D06P1/65118—Compounds containing hydroxyl groups
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/64—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds without sulfate or sulfonate groups
- D06P1/651—Compounds without nitrogen
- D06P1/65106—Oxygen-containing compounds
- D06P1/65131—Compounds containing ether or acetal groups
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Abstract
The invention discloses a kind of textile dyeings to increase deep functional agent and preparation method thereof, application, and the formula that the textile dyeing increases deep functional agent is as follows, in parts by weight for：1-5 parts of barbaloin, 1-5 parts of alkyl glycosides, 2-8 parts of flavones ethylene glycol, 70 parts of water；The preparation method that the textile dyeing increases deep functional agent is to be stood after each ingredient in above-mentioned formula is mixed evenly to obtain the final product；The textile dyeing increases deep functional agent and is applied to during the direct dyes of fabric or the dyeing process of reactive dye.Ingredient is simple and environmentally friendly in the formula of the deep functional agent of textile dyeing increasing of the present invention, it is easy to use, dyeing need not be changed and add new equipment, it can be widely applied to direct dyes, the reactive dyeing of silk, wool, cotton, fiber crops, regenerated celulose fibre fabric and blended union fabric, it is remarkably improved color depth and color fastness, dye dosage can be reduced simultaneously, reduced energy expenditure and sewage discharge, had a extensive future.
Description
Technical field
The invention belongs to textile dyeing fields, and in particular to a kind of textile dyeing increases deep functional agent and preparation method thereof, answers
With.
Background technology
Traditional textile dyeing is susceptible to poor color fastness, such as paint low not depth, dye-uptake, crock fastness, washing jail
The problems such as degree difference.If the usual poor fabric of color fastness encounters rainwater, sweat and rubbed by the external world, it will produce color and fall off
It fades, especially the deep and bright-coloured fabric of color and luster, discolouration phenomena are more prominent；In addition having in the dyestuff of these colour fadings that fall off
Machine molecule and heavy metal ion etc. are likely to be absorbed by the body and be detrimental to health by skin, and are wearing or washing
Other dirty fabrics can be also contaminated in the process, and inconvenience is brought to life.In order to improve fabric color fastness, some prints are often added
Dye auxiliary agent, such as when for using direct dyes and reactive dyeing, sodium chloride is often added as dyeing accelerant；And
And addition sodium carbonate is also needed for reactive dyeing（Or sodium bicarbonate）As dye fixing agent, however through these conventional prints
The quality of dye auxiliary agent institute printed fabrics still cannot be satisfied the application demand of high-end customer.
Patent CN201310636510.3 discloses a kind of deep-dyeing agent, preparation method and improves dyed textiles color fastness
Method, pass through amido organosilicon, ternary polymerization organosilicon, secondary alcohol polyoxyethylene ether, octadecyldimethyl ethoxy season
Ammonium salt, alkyl ketene, paraffin emulsifier and water are prepared to obtain deep-dyeing agent, and dyed fabric is then impregnated deep-dyeing agent dressing liquid
In, through centrifugal dehydration and drying, then at 190 DEG C of high-temperature process, obtain with the fabric for increasing deep function.Although being arranged through its increasing is deep
Fabric color fastness it is high and soft, but the deep-dyeing agent increase it is deep arrange be after dyeing process, and need it is soaking,
Dehydration, drying and high-temperature process, increase dyeing process.
Patent CN201610104901.4 discloses a kind of high-efficiency fiber deep dyeing promoter and preparation method thereof, uses first
Base sodium naphthalene sulfonate, sodium lignin sulfonate, organosilicon alkanes monomer, methacryloxypropyl trimethoxy silane, bisphenol-A ring
Deep-dyeing agent is prepared in oxygen lotion, salicylate, organic acid, nano-titanium dioxide, emulsifier, initiator and deionized water.It should
Material composition used by invention is complicated and more, and preparation time is long, is unfavorable for large-scale popularization use.
Invention content
The technical issues of solution：In order to solve the problems such as traditional textile dyeing is susceptible to poor color fastness, one kind is provided
Environmental protection and good novel fabric deep dyeing functional agent of application prospect and preparation method thereof, application.
Technical solution：A kind of deep functional agent of textile dyeing increasing, the formula which increases deep functional agent is as follows, with weight
Part is calculated as：
1-5 parts of barbaloin
1-5 parts of alkyl glycosides
2-8 parts of flavones ethylene glycol
70 parts of water.
Further, the flavones ethylene glycol is the ginkgo water extract of content 30%, and it is limited to be purchased from hundred million promise chemicals of Ningbo
Company.
A kind of textile dyeing increases the preparation method of deep functional agent, the preparation method is that：It weighs each raw material by above-mentioned formula,
Barbaloin, alkyl glycosides, flavones ethylene glycol and water are mixed evenly, is then stored at room temperature at least 1 hour and is contaminated to get fabric
Color increases deep functional agent.
A kind of textile dyeing increases the application of deep functional agent, and the textile dyeing increases the direct dye that deep functional agent is applied to fabric
During the dyeing process of material or reactive dye.
In above-mentioned technical proposal, the specific method of the application is：
1）After preparing direct dyes, 80 DEG C are warming up to, textile dyeing is added and increases deep functional agent, after stirring evenly, then puts
Enter fabric；
2）Sodium chloride is added at 80 DEG C after 5 min of constant temperature dyeing and promotees dye, then after dyeing 40 min, takes out fabric, 60 DEG C
Hot water wash 3 times, cold water are washed 3 times, drying.
In above-mentioned technical proposal, the specific method of the application is：
1）After preparing reactive dye, 80 DEG C are warming up to, textile dyeing is added and increases deep functional agent, after stirring evenly, then puts
Enter fabric；
2）Sodium chloride is added at 80 DEG C after 5 min of constant temperature dyeing and promotees dye, then after dyeing 20 min, sodium carbonate or carbon is added
Sour hydrogen sodium, then dye and take out fabric after 30 min, 60 DEG C of hot water wash 3 times, cold water is washed 3 times, drying.
In above-mentioned technical proposal, the fabric includes silk, wool, cotton, fiber crops, regenerated celulose fibre fabric or blended friendship
Woven fabric.
In above-mentioned technical proposal, the dosage that the textile dyeing increases deep functional agent and direct dyes or reactive dye is：5-
30 mL/L textile dyeings increase deep functional agent：1-5% o.w.f direct dyess or reactive dye.
In above-mentioned technical proposal, the dosage of the sodium chloride is 10 g/L, and the bath raio is 1:40, the direct dyes
Dosage is 1-5% o.w.f, and the dosage that the textile dyeing increases deep functional agent is 5-30 mL/L.
In above-mentioned technical proposal, the dosage of the sodium chloride is 30 g/L, and the bath raio is 1:40, the reactive dye
Dosage is 1-5% o.w.f, and the dosage that the textile dyeing increases deep functional agent is 5-30mL/L；When fabric is cotton, fiber crops, regeneration fibre
When cellulose fiber fabric or blended union fabric, 10-25 g/L sodium carbonate is selected；When fabric is silk or wool, 5- is selected
15 g/L sodium bicarbonates.
Advantageous effect：
1）Barbaloin, alkyl glycosides and flavones ethylene glycol are used in the formula of the present invention, these ingredients are in textile printing and dyeing
Using uncommon, furthermore we find that, dyeing rate and adsorption effect of the dyestuff to fiber can be improved in barbaloin in formula,
Improve color depth；Alkyl glycosides can be improved dyestuff and act on the fixation of fiber, promote hydroxyl, carboxyl and the dyestuff formationization on fiber
Key is learned, color fastness and color depth effect can be improved；Osmotic effect of the dyestuff to fiber can be improved in flavones ethylene glycol；These types of ingredient lacks
One can not, be used in conjunction with each other, played good deep dyeing functional effect jointly.
2）Ingredient is simple and environmentally friendly in the formula of the deep functional agent of textile dyeing increasing of the present invention, easy to use, no
It needs to change dyeing and adds new equipment.
3）The textile dyeing of the present invention increases deep functional agent and can be widely applied to silk, wool, cotton, fiber crops, regenerated cellulose fibre
The direct dyes of dimensional fabric and blended union fabric, reactive dyeing.
4）The textile dyeing of the present invention increases deep functional agent and is remarkably improved the color depth and color fastness of textile dyeing, while can drop
Low dye dosage reduces energy expenditure and sewage discharge, is a kind of new dyeing function increasing that is environmentally friendly, effective and having application prospect
Strong agent.
Specific implementation mode
For a further understanding of the present invention, the preferred embodiment of the invention is described with reference to embodiment, still
It should be appreciated that these descriptions are only the feature and advantage further illustrated the present invention, rather than to the claims in the present invention
Limitation.
Embodiment 1
A kind of textile dyeing increases deep functional agent, and the formula which increases deep functional agent is as follows, in parts by weight for：
1 part of barbaloin
1 part of alkyl glycosides
2 parts of flavones ethylene glycol
70 parts of water.
Wherein, the flavones ethylene glycol is the ginkgo water extract of content 30%, is purchased from the hundred million limited public affairs of promise chemicals of Ningbo
Department.
The preparation method of above-mentioned fabrics deep dyeing functional agent is：It weighs each raw material by above-mentioned formula, by barbaloin, alkyl
Glucosides, flavones ethylene glycol and water are mixed evenly, and are then stored at room temperature 1 hour and increase deep functional agent to get textile dyeing.
Embodiment 2
A kind of textile dyeing increases deep functional agent, and the formula which increases deep functional agent is as follows, in parts by weight for：
3 parts of barbaloin
3 parts of alkyl glycosides
5 parts of flavones ethylene glycol
70 parts of water.
Wherein, the flavones ethylene glycol is the ginkgo water extract of content 30%, is purchased from the hundred million limited public affairs of promise chemicals of Ningbo
Department.
The preparation method of above-mentioned fabrics deep dyeing functional agent is：It weighs each raw material by above-mentioned formula, by barbaloin, alkyl
Glucosides, flavones ethylene glycol and water are mixed evenly, and are then stored at room temperature 3 hours and increase deep functional agent to get textile dyeing.
Embodiment 3
A kind of textile dyeing increases deep functional agent, and the formula which increases deep functional agent is as follows, in parts by weight for：
5 parts of barbaloin
5 parts of alkyl glycosides
8 parts of flavones ethylene glycol
70 parts of water.
Wherein, the flavones ethylene glycol is the ginkgo water extract of content 30%, is purchased from the hundred million limited public affairs of promise chemicals of Ningbo
Department.
The preparation method of above-mentioned fabrics deep dyeing functional agent is：It weighs each raw material by above-mentioned formula, by barbaloin, alkyl
Glucosides, flavones ethylene glycol and water are mixed evenly, and are then stored at room temperature 2 hours and increase deep functional agent to get textile dyeing.
The application of above-mentioned fabrics deep dyeing functional agent, the textile dyeing increase the direct dye that deep functional agent is applied to fabric
During the dyeing process of material or reactive dye.The fabric include silk, wool, cotton, fiber crops, regenerated celulose fibre fabric or
Blended union fabric.
By taking the textile dyeing prepared by embodiment 2 increases deep functional agent as an example, its concrete application is described in detail below：
1 direct dyes of application examples contaminates cotton
The dosage of each material is in dyeing process：
Direct red 2b： 3 %（o.w.f）
Textile dyeing increases deep functional agent： 15 mL/L
Sodium chloride： 10 g/L
Bath raio： 1:40；
The weight ratio of fabric and water when the bath raio refers to dyeing, 1:40 indicate to need 1g textile dyeings in dye bath
Add 40g water；
The concrete technology of dyeing process is：
1）After preparing direct red 2b, 80 DEG C are warming up to, textile dyeing is added and increases deep functional agent, after stirring evenly, then puts
Enter cotton；
2）Sodium chloride is added at 80 DEG C after 5 min of constant temperature dyeing and promotees dye, then after dyeing 40 min, takes out cotton, 60 DEG C of heat
Washing 3 times, cold water is washed 3 times, drying.
2 direct dyes dyeing silk habotai of application examples
The dosage of each material is in dyeing process：
Direct indigo plant GL： 2%（o.w.f）
Textile dyeing increases deep functional agent： 15mL/L
Sodium chloride： 10g/L
Bath raio： 1:40；
The concrete technology of dyeing process is：
1）After preparing direct indigo plant GL, 80 DEG C are warming up to, textile dyeing is added and increases deep functional agent, after stirring evenly, then puts
Enter Real Silk Habotai；
2）Sodium chloride is added at 80 DEG C after 5 min of constant temperature dyeing and promotees dye, then after dyeing 40 min, takes out Real Silk Habotai,
60 DEG C of hot water wash 3 times, cold water is washed 3 times, drying.
3 Dyeing of Cotton Fabric with Reactive Dyes of application examples
The dosage of each material is in dyeing process：
Reactive brilliant red GB： 3 %（o.w.f）
Textile dyeing increases deep functional agent： 10 mL/L
Sodium chloride： 30 g/L
Sodium carbonate： 20 g/L
Bath raio： 1:40；
The concrete technology of dyeing process is：
1）After preparing reactive brilliant red GB, 80 DEG C are warming up to, textile dyeing is added and increases deep functional agent, after stirring evenly, then
It is put into cotton；
2）Sodium chloride is added at 80 DEG C after 5 min of constant temperature dyeing and promotees dye, then after dyeing 20 min, sodium carbonate is added, then contaminate
Take out cotton after 30 min of color, 60 DEG C of hot water wash 3 times, cold water is washed 3 times, drying.
4 reactive dye dyeing silk habotai of application examples
The dosage of each material is in dyeing process：
Active golden yellow KG： 2 %（o.w.f）
Textile dyeing increases deep functional agent： 10 mL/L
Sodium chloride： 20 g/L
Sodium bicarbonate： 6 g/L
Bath raio： 1:40；
The concrete technology of dyeing process is：
1）After preparing active golden yellow KG, 80 DEG C are warming up to, textile dyeing is added and increases deep functional agent, after stirring evenly, then
It is put into Real Silk Habotai；
2）Sodium chloride is added at 80 DEG C after 5 min of constant temperature dyeing and promotees dye, then after dyeing 20 min, sodium bicarbonate is added, then
It dyes and takes out Real Silk Habotai after 30 min, 60 DEG C of hot water wash 3 times, cold water is washed 3 times, drying.
The textile dyeing of the present invention increases direct dyes, reactive dye, textile dyeing used in the application of deep functional agent and increases
Deep functional agent, sodium chloride, sodium carbonate and sodium bicarbonate dosage be not limited to use above example, occurrence can be according to dyestuff
Type, the property of fabric, dyeing etc. carry out adjustment appropriate.
In order to better illustrate the performance that the textile dyeing prepared by the present invention increases deep functional agent, we have done following comparison
Experiment：
1 direct dyes of comparative example contaminates cotton
The dosage of each material is in dyeing process：
Direct red 2b： 3 %（o.w.f）
Sodium chloride： 10 g/L
Bath raio： 1:40；
The concrete technology of dyeing process is：
1）After preparing direct red 2b, 80 DEG C, after stirring evenly are warming up to, cotton is placed into；
2）Sodium chloride is added at 80 DEG C after 5 min of constant temperature dyeing and promotees dye, then after dyeing 40 min, takes out cotton, 60 DEG C of heat
Washing 3 times, cold water is washed 3 times, drying.
2 direct dyes dyeing silk habotai of comparative example
The dosage of each material is in dyeing process：
Direct indigo plant GL： 2 %（o.w.f）
Sodium chloride： 10 g/L
Bath raio： 1:40；
The concrete technology of dyeing process is：
1）After preparing direct indigo plant GL, 80 DEG C, after stirring evenly are warming up to, silk is placed into；
2）Sodium chloride is added at 80 DEG C after 5 min of constant temperature dyeing and promotees dye, then after dyeing 40 min, takes out silk, 60 DEG C
Hot water wash 3 times, cold water are washed 3 times, drying.
3 Dyeing of Cotton Fabric with Reactive Dyes of comparative example
The dosage of each material is in dyeing process：
Reactive brilliant red GB： 3 %（o.w.f）
Sodium chloride： 30 g/L
Sodium carbonate： 20 g/L
Bath raio： 1:40；
The concrete technology of dyeing process is：
1）After preparing reactive brilliant red GB, 80 DEG C, after stirring evenly are warming up to, cotton is placed into；
2）Sodium chloride is added at 80 DEG C after 5 min of constant temperature dyeing and promotees dye, then after dyeing 20 min, sodium carbonate is added, then contaminate
Take out cotton after 30 min of color, 60 DEG C of hot water wash 3 times, cold water is washed 3 times, drying.
4 reactive dye dyeing silk habotai of comparative example
The dosage of each material is in dyeing process：
Active golden yellow KG： 2 %（o.w.f）
Sodium chloride： 20 g/L
Sodium bicarbonate： 6 g/L
Bath raio： 1:40；
The concrete technology of dyeing process is：
1）After preparing active golden yellow KG, 80 DEG C, after stirring evenly are warming up to, Real Silk Habotai is placed into；
2）Sodium chloride is added at 80 DEG C after 5 min of constant temperature dyeing and promotees dye, then after dyeing 20 min, sodium bicarbonate is added, then
It dyes and takes out Real Silk Habotai after 30 min, 60 DEG C of hot water wash 3 times, cold water is washed 3 times, drying.
5 reactive dye dyeing silk habotai of comparative example
The dosage of each material is in dyeing process：
Active golden yellow KG： 2 %（o.w.f）
Functional agent A： 10 mL/L
Sodium chloride： 20 g/L
Sodium bicarbonate： 6 g/L
Bath raio： 1:40；
Wherein, increase deep functional agent compared to the textile dyeing in application examples 4（Embodiment 2）, the functional agent A in this comparative example
Lack barbaloin in formula, other formulas are with preparation process with embodiment 2, and details are not described herein.
The concrete technology of dyeing process is：
1）After preparing active golden yellow KG, 80 DEG C are warming up to, functional agent A is added, after stirring evenly, places into silk electricity
Power is spun；
2）Sodium chloride is added at 80 DEG C after 5 min of constant temperature dyeing and promotees dye, then after dyeing 20 min, sodium bicarbonate is added, then
It dyes and takes out Real Silk Habotai after 30 min, 60 DEG C of hot water wash 3 times, cold water is washed 3 times, drying.
6 reactive dye dyeing silk habotai of comparative example
The dosage of each material is in dyeing process：
Active golden yellow KG： 2 %（o.w.f）
Functional agent B： 10 mL/L
Sodium chloride： 20 g/L
Sodium bicarbonate： 6 g/L
Bath raio： 1:40；
Wherein, increase deep functional agent compared to the textile dyeing in application examples 4（Embodiment 2）, the functional agent B in this comparative example
Lack alkyl glycosides in formula, other formulas are with preparation process with embodiment 2, and details are not described herein.
The concrete technology of dyeing process is：
1）After preparing active golden yellow KG, 80 DEG C are warming up to, functional agent B is added, after stirring evenly, places into silk electricity
Power is spun；
2）Sodium chloride is added at 80 DEG C after 5 min of constant temperature dyeing and promotees dye, then after dyeing 20 min, sodium bicarbonate is added, then
It dyes and takes out Real Silk Habotai after 30 min, 60 DEG C of hot water wash 3 times, cold water is washed 3 times, drying.
7 reactive dye dyeing silk habotai of comparative example
The dosage of each material is in dyeing process：
Active golden yellow KG： 2 %（o.w.f）
Functional agent C： 10 mL/L
Sodium chloride： 20 g/L
Sodium bicarbonate： 6 g/L
Bath raio： 1:40；
Wherein, increase deep functional agent compared to the textile dyeing in application examples 4（Embodiment 2）, the functional agent C in this comparative example
Lack flavones ethylene glycol in formula, other formulas are with preparation process with embodiment 2, and details are not described herein.
The concrete technology of dyeing process is：
1）After preparing active golden yellow KG, 80 DEG C are warming up to, functional agent C is added, after stirring evenly, places into silk electricity
Power is spun；
2）Sodium chloride is added at 80 DEG C after 5 min of constant temperature dyeing and promotees dye, then after dyeing 20 min, sodium bicarbonate is added, then
It dyes and takes out Real Silk Habotai after 30 min, 60 DEG C of hot water wash 3 times, cold water is washed 3 times, drying.
Performance test
Correlated performance test is carried out to the fabric dyed by application examples 1-4 and comparative example 1-7 below.
Test method
Colorfastness to rubbing：According to GB/T 3920- 2008《Textile color stability tests colour fastness to rubbing》Method uses
Two methods of dry friction and wet friction differentiate the staining degree of fabric；
Color fastness to washing：GB/T 3921.2-2008 according to national standards《Textile color stability tests fastness to soaping》
Test
K/S values are tested：Yarn dyed fabric is folded 4 layers, using 600 color measuring and matching systems of Datacolor, measures PRINTED FABRIC
K/S values, measure 4 at be averaged.K/S values are bigger, indicate that material is stronger to the absorbability of light, fabric color is deeper.
Test result
With Real Silk Habotai fabric（56 g/m2）And cotton fabric（105 g/m2）After the technology of the present invention, above-mentioned each application
Example and the comparison of comparative example various performance parameters are as follows：
Note：Friction, 3 grades of soaping fastness are qualification, and 5 grades best；K/S values are the bigger the better, and illustrate that color is deeper.
It is compared with comparative example 1-4 from application examples 1-4：Application examples 1-4 is added to the deep functional agent of increasing, acts on cotton, true
After the fabrics such as silk, color depth value K/S numerical value biggers, and there is preferable colorfastness to rubbing and washing fastness.Comparative example 1-4 processing
Cotton, real silk fabric K/S values are relatively low, and color fastness is poor.
It is compared with comparative example 5,6,7 from application examples 4：Function deep-dyeing agent lacks barbaloin composition in comparative example 5, dye
The K/S values of fabric after color, crock fastness and washing fastness are below application examples 4；Function deep-dyeing agent lacks alkyl sugar in comparative example 6
Glycosides composition, the K/S values of fabric after dyeing, crock fastness and washing fastness are below application examples 4；Function increases deep in comparative example 7
Agent lacks flavones ethylene glycol composition, and the K/S values of fabric after dyeing, crock fastness and washing fastness are below application examples 4.
The foregoing description of the disclosed embodiments enables those skilled in the art to implement or use the present invention.
Various modifications to these embodiments will be apparent to those skilled in the art, as defined herein
General Principle can be realized in other embodiments without departing from the spirit or scope of the present invention.Therefore, of the invention
It is not intended to be limited to the embodiments shown herein, and is to fit to and the principles and novel features disclosed herein phase one
The widest range caused.
Claims (9)
1. a kind of textile dyeing increases deep functional agent, which is characterized in that the formula that the textile dyeing increases deep functional agent is as follows, with weight
Part is calculated as：
1-5 parts of barbaloin
1-5 parts of alkyl glycosides
2-8 parts of flavones ethylene glycol
70 parts of water.
2. textile dyeing according to claim 1 increases deep functional agent, which is characterized in that the textile dyeing increases deep functional agent
Preparation method be：It weighs each raw material, barbaloin, alkyl glycosides, flavones ethylene glycol and water is mixed equal by above-mentioned formula
It is even, it is then stored at room temperature at least 1 hour and increases deep functional agent to get textile dyeing.
3. textile dyeing according to claim 1 increases the application of deep functional agent, which is characterized in that the textile dyeing increases deep
Functional agent is applied to during the direct dyes of fabric or the dyeing process of reactive dye.
4. textile dyeing according to claim 3 increases the application of deep functional agent, which is characterized in that the specific side of the application
Method is：
1）After preparing direct dyes, 80 DEG C are warming up to, textile dyeing is added and increases deep functional agent, after stirring evenly, places into and knits
Object；
2）Sodium chloride is added at 80 DEG C after constant temperature dyeing 5min and promotees dye, then after dyeing 40min, takes out fabric, 60 DEG C of hot water wash 3
Secondary, cold water is washed 3 times, drying.
5. textile dyeing according to claim 3 increases the application of deep functional agent, which is characterized in that the specific side of the application
Method is：
1）After preparing reactive dye, 80 DEG C are warming up to, textile dyeing is added and increases deep functional agent, after stirring evenly, places into and knits
Object；
2）Sodium chloride is added at 80 DEG C after constant temperature dyeing 5min and promotees dye, then after dyeing 20min, sodium carbonate or sodium bicarbonate is added,
It dyes again and takes out fabric after 30min, 60 DEG C of hot water wash 3 times, cold water is washed 3 times, drying.
6. the textile dyeing according to claim 3 or 4 or 5 increases the application of deep functional agent, which is characterized in that the fabric packet
Include silk, wool, cotton, fiber crops, regenerated celulose fibre fabric or blended union fabric.
7. textile dyeing according to claim 6 increases the application of deep functional agent, which is characterized in that the textile dyeing increases deep
The dosage of functional agent and direct dyes or reactive dye is：5-30mL/L textile dyeings increase deep functional agent：1-5% o.w.f are direct
Dyestuff or reactive dye.
8. textile dyeing according to claim 4 increases the application of deep functional agent, which is characterized in that the dosage of the sodium chloride
For 10g/L, the bath raio is 1:40, the dosage of the direct dyes is 1-5% o.w.f, and the textile dyeing increases deep functional agent
Dosage be 5-30mL/L.
9. textile dyeing according to claim 5 increases the application of deep functional agent, which is characterized in that the dosage of the sodium chloride
For 30g/L, the bath raio is 1:40, the dosage of the reactive dye is 1-5% o.w.f, and the textile dyeing increases deep functional agent
Dosage be 5-30mL/L；When fabric is cotton, fiber crops, regenerated celulose fibre fabric or blended union fabric, 10-25g/ is selected
L sodium carbonate；When fabric is silk or wool, 5-15g/L sodium bicarbonates are selected.
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| CN109944092B (en) * | 2019-03-05 | 2021-08-24 | 上海兴康化工有限公司 | Short-process wool dyeing process using reactive dye |
| CN112746336A (en) * | 2020-12-24 | 2021-05-04 | 苏州经贸职业技术学院 | Degumming agent for silk fabric, preparation method of degumming agent and degumming method for silk fabric |
| CN114438803B (en) * | 2022-01-26 | 2023-05-12 | 内蒙古工业大学 | Cashmere fiber dyeing deepening method and deepening agent |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102383319A (en) * | 2011-06-16 | 2012-03-21 | 北京泛博化学股份有限公司 | Deepening agent and preparation method thereof |
| CN104846669A (en) * | 2015-05-23 | 2015-08-19 | 青岛东昌瑞纺织品有限公司 | Textile dye |
| CN105671945A (en) * | 2016-04-12 | 2016-06-15 | 湖州吉昌丝绸有限公司 | Environment-friendly deepening agent applicable to polyester fiber |
| CN106192475A (en) * | 2016-09-13 | 2016-12-07 | 广州市番禺区协运来化工用品有限公司 | A kind of fiber deep dyeing promoter and preparation thereof |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS56112583A (en) * | 1980-02-01 | 1981-09-04 | Nikka Chemical Ind Co Ltd | Color darkening agent of polyester fiber dyed article |
-
2017
- 2017-01-12 CN CN201710020124.XA patent/CN106758378B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102383319A (en) * | 2011-06-16 | 2012-03-21 | 北京泛博化学股份有限公司 | Deepening agent and preparation method thereof |
| CN104846669A (en) * | 2015-05-23 | 2015-08-19 | 青岛东昌瑞纺织品有限公司 | Textile dye |
| CN105671945A (en) * | 2016-04-12 | 2016-06-15 | 湖州吉昌丝绸有限公司 | Environment-friendly deepening agent applicable to polyester fiber |
| CN106192475A (en) * | 2016-09-13 | 2016-12-07 | 广州市番禺区协运来化工用品有限公司 | A kind of fiber deep dyeing promoter and preparation thereof |
Non-Patent Citations (2)
| Title |
|---|
| 染整前处理绿色助剂及新型前处理工艺;刘旭峰;《日用化学品科学》;20070831;第30卷(第8期);第21-24页 * |
| 银杏叶中黄酮的水提取及HPLC测定;邓永智等;《福建分析测试》;20011231(第2期);第1393-1396页 * |
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