CN106754115A - A kind of preparation technology of the Dendrobium officinale alcohol rich in active substance of plant - Google Patents
A kind of preparation technology of the Dendrobium officinale alcohol rich in active substance of plant Download PDFInfo
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- CN106754115A CN106754115A CN201611028644.7A CN201611028644A CN106754115A CN 106754115 A CN106754115 A CN 106754115A CN 201611028644 A CN201611028644 A CN 201611028644A CN 106754115 A CN106754115 A CN 106754115A
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- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12G—WINE; PREPARATION THEREOF; ALCOHOLIC BEVERAGES; PREPARATION OF ALCOHOLIC BEVERAGES NOT PROVIDED FOR IN SUBCLASSES C12C OR C12H
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- C12H—PASTEURISATION, STERILISATION, PRESERVATION, PURIFICATION, CLARIFICATION OR AGEING OF ALCOHOLIC BEVERAGES; METHODS FOR ALTERING THE ALCOHOL CONTENT OF FERMENTED SOLUTIONS OR ALCOHOLIC BEVERAGES
- C12H1/00—Pasteurisation, sterilisation, preservation, purification, clarification, or ageing of alcoholic beverages
- C12H1/003—Pasteurisation, sterilisation, preservation, purification, clarification, or ageing of alcoholic beverages by a biochemical process
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Abstract
The present invention provides a kind of preparation technology of the Dendrobium officinale alcohol rich in active substance of plant, belongs to medicines and health protection food technology field.The present invention is selected by the selection of dendrobium candidum raw material, pretreatment of raw material, base liquor, active material is extracted, concentrate decreasing concentration, digest clarification, production cycle etc. proposes a kind of preparation technology of new Dendrobium officinale alcohol.The present invention, with wine as carrier, with the means that are extracted as of its active material, improves the utilization ratio of raw material, reduces cost with the fresh stem of dendrobium candidum as unique raw material.The alcoholic strength of the Dendrobium officinale alcohol that the present invention is prepared is at 38 42 degree；Color and luster is micro- yellow, glittering and translucent；The sweet and tasty net, long times of aftertaste of alcohol, medicine perfume (or spice) are pleasant；Viscosity is higher, convergence effect is good；Rich in polysaccharide and essential amino acid, micro- isoreactivity material.Preparation technology of the present invention is with short production cycle, and raw material availability is high, and any food additives, gentle, the involved equipment simple and regular of processing conditions, easily operation are not used.
Description
Technical field
The invention belongs to medicines and health protection food technology field, more particularly to a kind of preparation technology of Dendrobium officinale alcohol, specifically
It is a kind of preparation technology of the Dendrobium officinale alcohol rich in active substance of plant.
Background technology
Dendrobium officinale alcohol, belongs to health-care white spirit, and its technical field is related to the assembled alcoholic drinks technique with white wine as base liquor.Tradition
Dendrobium officinale alcohol be mainly in white wine or rice wine addition including the several kinds of Chinese medicinal materials including dendrobium candidum, fruit, carbohydrate thing
Matter, by the means such as ultra-fine grinding, prolonged immersion, stirring, temperature control, makes to contain more rich effective component and local flavor in wine
Material.At present, dendrobium officinale health wine is mostly by the way of traditional steeping in wine, make various effective components in dendrobium candidum from
So diffusion, during time-consuming for this kind of method, and the activity substance content in wine is low, or even some active materials cannot be introduced into wine, makes
Low into raw material utilization efficiency, the health care effect that make dendrobium candidum has in itself is had a greatly reduced quality.
The Dendrobium officinale alcohol preparing process being currently known still suffers from many defects, such as, and the processing mode of raw material, multi-source
In Tiepi Fengdou or dry product, the process technology to its upstream lacks monitoring, causes the active component of raw material to be susceptible to oxygen
Change or degrade.Although being mentioned in some patents dry powder can be replaced using the fresh pure stem of dendrobium candidum, tool is not proposed
The processing mode to fresh pure stem of body.The wall breaking technology of dendrobium candidum cell, what is had is not crushed, and has plenty of mechanical lapping
Into fine powder, this is possible to bring active material insufficient or some bitter substances unhelpful to human body of extraction to be entrained in wine.
Mostly below 60 degree, this ignores the non-polar material to the alcohol-soluble of some in dendrobium candidum to the alcoholic strength of the base liquor for being used
The extraction of matter.Known Dendrobium officinale alcohol is in order to reach the clear on color and luster, it is impossible to further improve polysaccharide, the polypeptide in wine
Deng the content of Large molecule active material.
When compatibility of the preparing process of largely known Dendrobium officinale alcohol between the different Chinese medicines of protrusion, ignore
The clarification link of wine body, substantially all by the way of ancient natural subsidence, therefore due to some sedimentations in wine or cohesion speed
The presence of the slow and colloidal activity material of temperature influence is spent, these tradition are steep in wine and are likely to be formed gradually after filling sub-bottle
Allow the offending precipitation of people.Dendrobium candidum usage amount and with the compatibility of other Chinese medicines in terms of, traditional Dendrobium officinale alcohol
Effective component is complicated, and they are not fully beneficial compositions, or even there is the Antagonistic reaction between different medicinal materials, meanwhile, this
Planting technique also makes the fragrance component of Dendrobium officinale alcohol with obvious flavour of a drug, and is brought very to its follow-up mouthfeel improvement aspect
Big obstacle.Finally, the main pharmacodynamics composition in many Dendrobium officinale alcohols is not from dendrobium candidum, used as traditional Chinese medicinal material raw materials
One of, the addition of dendrobium candidum only accounts for the ratio of very little, due to being influenceed by other raw materials, its leachable also not right and wrong
Chang Duo, and easily with them there are various chemical reactions.
The content of the invention
The present invention provides a kind of preparation technology of the Dendrobium officinale alcohol rich in active substance of plant, and the design innovation wine
Style.The present invention is in the selection of dendrobium candidum raw material, pretreatment of raw material, base liquor selection, active material extraction, concentration decreasing concentration, enzymolysis
Clarification, production cycle, color and luster, viscosity, liquor body style design etc. have carried out a series of improvement and innovation, it is therefore an objective to solve existing
With the presence of Dendrobium officinale alcohol preparation technology problem.The present invention is with wine with the fresh stem of dendrobium candidum as unique raw material
Carrier, with the means that are extracted as of its active material, improves the utilization ratio of raw material, and reduces cost makes dendrobium candidum to human body
Tonic function is farthest played.The object of the invention is realized by following technical proposals：
A kind of preparation technology of the Dendrobium officinale alcohol rich in active substance of plant, comprises the following steps：
1) fresh dendrobium candidum stem is taken, dried process is carried out after being finished through freeze thawing, boiling, make its water content control 35
~50%；
2) stem of dendrobium candidum is cut into rod-short, is put into base liquor, it is size-reduced, ultrasonically treated after, Soakage extraction；
3) after placing 28~30 days, filtering makes separation of solid and liquid, reclaims stem of noble dendrobium fragment, adds base liquor, repeats aforesaid operations,
Double-steeping 25~28 days；
4) after the 55th~58 day, filtering adds base liquor as solvent, and water-bath refluxing extraction collects ethanol extract, then add
Enter the new base liquor of equivalent, secondary back is extracted, the ethanol extract of refluxing extraction twice is mixed after filtering, squeezing；
5) above-mentioned stem of noble dendrobium fragment is washed with water, adds water the aqueous extract that filtered after boiling to obtain, then to addition in the residue of filtering
The water of equivalent, through microwave, boil treatment after carry out filtering to obtain secondary aqueous extract, aqueous extract will merge twice；
6) above-mentioned aqueous extract being concentrated, it is mixed with ethanol extract, the alcoholic strength for making Dendrobium officinale alcohol is reduced to 38~
42 degree, by step 5) residue after water extraction is added in the dendrobium wine after decreasing concentration, continues to impregnate 2~3 months；
7) after the 120th day, in the dendrobium wine after decreasing concentration, pectase and papain are added, 3~5 is reacted at room temperature
My god, it is subsequently placed at a temperature of -10 DEG C~-4 DEG C, natural subsidence 7~12 days, the wine liquid of upper strata clarification is dendrobium candidum magma
Wine.
As a kind of specific embodiment of the dendrobium candidum preparation technology rich in active substance of plant of the present invention,
The dendrobium candidum original plasm wine is carried out into hook tune, optimizes the mouthfeel of wine body, be made the iron sheet rich in active material and smell coordination
Dendrobium wine.
As a kind of specific embodiment of the dendrobium candidum preparation technology rich in active substance of plant of the present invention,
Step 1) in, the concrete operations of the freeze thawing are：By fresh dendrobium candidum as more than 1h is freezed at -20 DEG C, then move to
Normal temperature, after melting completely, freezes, multigelation 2~3 times again；The digestion time is 15~30min；At the drying
Using baking oven or baking box, drying temperature is 50~60 DEG C to reason, and continuous 2~4 bakings bakee the time for 6~7h every time, dry every time
Roasting interval time is no less than 12h.
As a kind of specific embodiment of the dendrobium candidum preparation technology rich in active substance of plant of the present invention,
Step 2) in, the length of the quarter butt is 1~3cm, and the alcoholic strength of the base liquor is 60~68 degree, the base liquor and dendrobium candidum
Amount ratio be 1.5L：200g；The ultrasonically treated time is 15~20min.
As a kind of specific embodiment of the dendrobium candidum preparation technology rich in active substance of plant of the present invention,
Step 3) in, the number of degrees of the base liquor are 60~68 degree, and the base liquor is 1.5L with the amount ratio of dendrobium candidum：200g.
As a kind of specific embodiment of the dendrobium candidum preparation technology rich in active substance of plant of the present invention,
Step 4) in, the number of degrees of the base liquor are 60~68 degree, and the base liquor is 0.3~0.7L with the amount ratio of dendrobium candidum：200g；
The temperature of the water-bath backflow is 55~65 DEG C, and the time is 1~2h.
As a kind of specific embodiment of the dendrobium candidum preparation technology rich in active substance of plant of the present invention,
Step 5) in, the water of the washing stem of noble dendrobium fragment is normal-temperature water or the water no more than 4 DEG C, the addition and dendrobium candidum of the water
Amount ratio be 1.5L:200g；The boiling time is 8~12min, and the microwave time is 5~7min.
As a kind of specific embodiment of the dendrobium candidum preparation technology rich in active substance of plant of the present invention,
Step 6) it is described concentration aqueous extract amount be concentration before amount 70~80%.
As a kind of specific embodiment of the dendrobium candidum preparation technology rich in active substance of plant of the present invention,
The addition of the pectase is 0.5~1g/L；The addition of the papain is 0.2~0.5g/L.
The present invention also provides a kind of Dendrobium officinale alcohol rich in active substance of plant, and the Dendrobium officinale alcohol uses above-mentioned system
Standby technique is prepared.
Existing Dendrobium officinale alcohol, in terms of raw material, with the addition of including the several kinds of Chinese medicinal materials including dendrobium candidum, at material
Mainly to dry product ultra-fine grinding, extracting mode is mainly prolonged immersion to reason, and aid in stir, the means such as temperature control, most
Make to contain more rich effective component in wine eventually.This traditional mode steep in wine, complicated component, the strange taste bitter taste in some wine
Flavour of a drug are difficult to eradicate, and effective component is mainly by natural diffuseness, and time-consuming for this kind of method, cause the activity substance content in wine
It is low, or even during some active materials cannot be introduced into wine, cause that raw material utilization efficiency is low, finished wine wine body is unstable, easy
Precipitation is formed, the further development of Dendrobium officinale alcohol is constrained.
Present invention process is made to overcome the problem that presently, there are from raw material selection, pretreatment, base liquor selection and extraction
The preparations of the several respects to Dendrobium officinale alcohol such as standby technique are improved optimization, and specific innovation and improvement are as follows：
1st, the selection of raw material：The present invention, as starting and unique raw material, does not have other things using the fresh stem of dendrobium candidum
Matter is added, and composition is simple in making the wine prepared, and other medicine constituents are not mixed, keeps the original delicate fragrance of dendrobium candidum and color
Pool.
2nd, the pretreatment of raw material：De-enzyme broken wall can promote the dissolution of polysaccharide material using boiling after multigelation 2~3 times；
Dried process temperature is no more than 60 DEG C, to its water content in certain scope, promotes the formation of fragrance；Pulverization process is used and cut
Rod-short is cut into, it is broken in the rotation of wine high speed, reduce the oxidation of active material and the dissolution of bitter substance.
3rd, the selection of base liquor：The alcoholic strength of base liquor is improved to 60~68 degree.
4th, extraction and preparation technique：1. impregnation process：After stem of noble dendrobium material is broken into homogenate, it is immersed in wine, ultrasonication is put
Put room temperature, intermittence stirring；2. filtering squeezing：Filtering, squeezes out the wine that can not be flowed out certainly, and separation of solid and liquid is added new again
Base liquor, double-steeping；3. refluxing extraction：Base liquor is added as solvent, 60 DEG C of water-baths, refluxing extraction improves fat by heating up
The dissolution of soluble substance；4. water boils extraction：Washing stem of noble dendrobium fragment, plus deionized water, boil, microwave, twice water extraction, increase water-soluble
The dissolution of property material；5. decreasing concentration is concentrated：Merge above-mentioned aqueous extract twice, concentration mixes with dipping wine liquid；Dendrobium candidum is residual
Slag, is added in the dendrobium wine after decreasing concentration, continues to impregnate, to extend the extraction time of active material.6. enzymolysis clarification：Add fruit
In wine after glue enzyme, papain to decreasing concentration, stand at low temperature accelerates the precipitation of insoluble matter.
5th, whole technological process preparation time is no more than 2 months, and the ageing time is 3 months or so.
6th, the wine body characteristicses of dendrobium wine
Color and luster：Clear, micro- Huang
Viscosity：Colloidal, convergence effect is good
Alcoholic strength：Between 38-42 degree
Mouthfeel standard：Alcohol is sweet and tasty net, and long times of aftertaste, medicine perfume (or spice) is pleasant
Activity substance content：In finished wine obtained by this law, polyoses content is not less than 5.0g/L；Total free amino acid contains
Amount is not less than 0.6g/L, wherein, lysine is not less than 0.03g/L, phenylalanine and is not less than 0.02g/L, threonine and is not less than
0.02g/L, isoleucine be not less than 0.02g/L, leucine be not less than 0.04g/L, valine be not less than 0.02g/L (above six
Plant amino acid and be essential amino acid)；The content of trace element：Iron is not less than 1.5mg/L, zinc and is not less than 0.7mg/L, manganese
It is not less than 3.0mg/L, chromium and is not less than 0.007mg/L.
Beneficial effects of the present invention：The alcoholic strength of the Dendrobium officinale alcohol that the present invention is prepared is between 38-42 degree；Color and luster is micro-
It is yellow, glittering and translucent；The sweet and tasty net, long times of aftertaste of alcohol, medicine perfume (or spice) are pleasant；Viscosity is higher, convergence effect is good；Rich in polysaccharide and human body
The new Dendrobium officinale alcohol of essential amino acid, micro- isoreactivity material.Preparation technology of the present invention is with short production cycle, raw material profit
It is high with rate, any food additives, gentle, the involved equipment simple and regular of processing conditions, easily operation are not used.
Brief description of the drawings
Fig. 1 is Dendrobium officinale alcohol preparation technology flow chart of the present invention rich in active material.
Specific embodiment
In order to make the purpose , technical scheme and advantage of the present invention be clearer, it is right below in conjunction with drawings and Examples
The present invention is further elaborated.It should be appreciated that the specific embodiments described herein are merely illustrative of the present invention, and
It is not used in the restriction present invention.
Embodiment 1
The preparation technology of Dendrobium officinale alcohol of the present invention is as follows：
1) the fresh dendrobium candidum stems of 200g are taken, as 1.5h is freezed at -20 DEG C, normal temperature is then moved to, treats to melt completely
Afterwards, freeze again, multigelation 3 times, be then placed in steamer, boiling 30min completes de-enzyme；Dry, be then placed in baking oven,
It is continuous at 55 DEG C to bakee 3 times, the time is bakeed every time for 6h, the interval time for bakeing every time is 12h；Make the aqueous of dendrobium candidum stem
Amount control is 40%.
2) the dendrobium candidum stem after will be baked cuts into the quarter butt of 2~3cm, is put into the base liquor that alcoholic strength is 65 degree,
Consumption is 1.5L, then size-reduced, 90% power ultrasonic treatment 20min, Soakage extraction.
3) after placing 28 days, filtering makes separation of solid and liquid, squeezes out and is unable to direct current wine out, reclaims stem of noble dendrobium fragment, again
To the base liquor 1.5L that alcoholic strength is 65 degree is added in the liquid of separation of solid and liquid, filtering, squeezing, reclaimer operation, double-steeping are repeated
25 days.
4) after the 56th day, used as solvent, 60 DEG C of water-bath refluxing extraction 2h collect ethanol for filtering, addition 0.4L, 65 degree of base liquors
Extract solution, adds 0.4L, 65 degree of base liquors as solvent again, and secondary back is extracted, and refluxing extraction twice is mixed after filtering, squeezing
Ethanol extract, about 3.6L.
5) stem of noble dendrobium fragment is washed using normal-temperature water, is subsequently adding 1.5L water, water extraction is filtered to obtain after boiling 10min
Liquid, adds 1.5L water, microwave treatment 7min secondary aqueous extract to be filtered to obtain after boiling, will be carried twice in the residue of filtering
Take liquid to merge, about 2.9L.
6) above-mentioned aqueous extract is concentrated to 2.1L, it is mixed with the ethanol extract of 3.6L, obtain the iron sheet stone of decreasing concentration
Dry measure used in former times wine, alcoholic strength is 40 degree or sos, by step 5) during the dendrobium candidum residue that obtains adds the dendrobium wine to decreasing concentration, continuation leaching
Stain 2 months.
7) after the 120th day, in the dendrobium wine after decreasing concentration, pectase 0.5g/L, papain 0.3g/L, room temperature are added
Lower reaction 4 days, then as at a temperature of -4 DEG C, natural subsidence 7 days carefully removes the wine liquid of upper strata clarification, and about 5L obtains iron sheet stone
Dry measure used in former times original plasm wine.
8) hook tune is carried out to above-mentioned original plasm wine, on the premise of retaining the distinctive fragrant and taste of dendrobium candidum, optimizes the mouth of wine body
Sense, is finally made the Dendrobium officinale alcohol rich in active material and smell coordination.
9) Dendrobium officinale alcohol being made is placed more than one month, treats that it is slowly aging, is stirred, filling sub-bottle.
Embodiment 2
The preparation technology of Dendrobium officinale alcohol of the present invention is as follows：
1) the fresh dendrobium candidum stems of 400g are taken, as 2h is freezed at -20 DEG C, normal temperature is then moved to, after melting completely,
Freeze again, multigelation 3 times, be then placed in steamer, boiling 25min completes de-enzyme；Dry, be then placed in baking oven, 60
It is continuous at DEG C to bakee 2 times, the time is bakeed every time for 7h, the interval time for bakeing every time is 14h；Make the water content of dendrobium candidum stem
Control is 45%.
2) the dendrobium candidum stem after will be baked cuts into the quarter butt of 3cm, is put into the base liquor that alcoholic strength is 63 degree, consumption
It is 3L, then size-reduced, 90% power ultrasonic treatment 15min, Soakage extraction.
3) after placing 30 days, filtering makes separation of solid and liquid, squeezes out and is unable to direct current wine out, reclaims stem of noble dendrobium fragment, again
To the base liquor 3L that alcoholic strength is 63 degree is added in the liquid of separation of solid and liquid, filtering, squeezing, reclaimer operation, double-steeping 28 are repeated
My god.
4) after the 58th day, used as solvent, 60 DEG C of water-bath refluxing extraction 1.5h collect second for filtering, addition 1.4L, 63 degree of base liquors
Alcohol extract, adds 1.4L, 63 degree of base liquors as solvent again, and secondary back is extracted, and backflow twice is mixed after filtering, squeezing and is carried
The ethanol extract for taking, about 8.5L.
5) stem of noble dendrobium fragment is washed using normal-temperature water, is subsequently adding 3L water, water extraction is filtered to obtain after boiling 12min
Liquid, adds 3L water, microwave treatment 7min secondary aqueous extract to be filtered to obtain after boiling, will be extracted twice in the residue of filtering
Liquid is merged, about 5.9L.
6) above-mentioned aqueous extract is concentrated to 5.2L, it is mixed with the ethanol extract of 8.5L, obtain the iron sheet stone of decreasing concentration
Dry measure used in former times wine, alcoholic strength is 42 degree or sos, by step 5) during the dendrobium candidum residue that obtains adds the dendrobium wine to decreasing concentration, continuation leaching
Stain 2 months.
7) after the 120th day, in the dendrobium wine after decreasing concentration, pectase 1g/L, papain 0.5g/L are added, at room temperature
Reaction 5 days, then as at a temperature of -8 DEG C, natural subsidence 10 days carefully removes the wine liquid of upper strata clarification, and about 13L obtains iron sheet stone
Dry measure used in former times original plasm wine.
8) hook tune is carried out to above-mentioned original plasm wine, on the premise of retaining the distinctive fragrant and taste of dendrobium candidum, optimizes the mouth of wine body
Sense, is finally made the Dendrobium officinale alcohol rich in active material and smell coordination.
9) Dendrobium officinale alcohol being made is placed more than one month, treats that it is slowly aging, is stirred, filling sub-bottle.
Embodiment 3
The preparation technology of Dendrobium officinale alcohol of the present invention is as follows：
1) the fresh dendrobium candidum stems of 600g are taken, as 1h is freezed at -20 DEG C, normal temperature is then moved to, after melting completely,
Freeze again, multigelation 2 times, be then placed in steamer, boiling 25min completes de-enzyme；Dry, be then placed in baking oven, 60
It is continuous at DEG C to bakee 3 times, the time is bakeed every time for 6h, the interval time for bakeing every time is 14h；Make the water content of dendrobium candidum stem
Control is 50%.
2) the dendrobium candidum stem after will be baked cuts into the quarter butt of 2~3cm, is put into the base liquor that alcoholic strength is 68 degree,
Consumption is 4.5L, then size-reduced, 90% power ultrasonic treatment 15min, Soakage extraction.
3) after placing 28 days, filtering makes separation of solid and liquid, squeezes out and is unable to direct current wine out, reclaims stem of noble dendrobium fragment, again
To the base liquor 4.5L that alcoholic strength is 68 degree is added in the liquid of separation of solid and liquid, filtering, squeezing, reclaimer operation, double-steeping are repeated
25 days.
4) after the 58th day, used as solvent, 60 DEG C of water-bath refluxing extraction 2h collect ethanol for filtering, addition 1.5L, 68 degree of base liquors
Extract solution, adds 1.5L, 68 degree of base liquors as solvent again, and secondary back is extracted, and refluxing extraction twice is mixed after filtering, squeezing
Ethanol extract, about 12L.
5) stem of noble dendrobium fragment is washed using 3 DEG C of water, is subsequently adding 4.5L water, water extraction is filtered to obtain after boiling 12min
Liquid is taken, adds 4.5L water, microwave treatment 7min that secondary aqueous extract is filtered to obtain after boiling in the residue of filtering, will twice
Extract solution is merged, about 8.5L.
6) above-mentioned aqueous extract is concentrated to 8.1L, it is mixed with the ethanol extract of 12L, obtain the dendrobium candidum of decreasing concentration
Wine, alcoholic strength is 42 degree or sos, by step 5) during the dendrobium candidum residue that obtains adds the dendrobium wine to decreasing concentration, continuation dipping
2 months.
7) after the 120th day, in the dendrobium wine after decreasing concentration, pectase 0.8g/L, papain 0.2g/L, room temperature are added
Lower reaction 4 days, then as at a temperature of -4 DEG C, natural subsidence 10 days carefully removes the wine liquid of upper strata clarification, and about 20L obtains iron sheet
Stem of noble dendrobium original plasm wine.
8) hook tune is carried out to above-mentioned original plasm wine, on the premise of retaining the distinctive fragrant and taste of dendrobium candidum, optimizes the mouth of wine body
Sense, is finally made the Dendrobium officinale alcohol rich in active material and smell coordination.
9) Dendrobium officinale alcohol being made is placed more than one month, treats that it is slowly aging, is stirred, filling sub-bottle.
Dendrobium candidum colours of wine prepared by embodiment 1~3, mouthfeel, perfume (or spice), taste and the concrete property rich in active material with
The characteristic of existing Dendrobium officinale alcohol is contrasted, as a result as shown in table 1 below：
The Dendrobium officinale alcohol of the preparation of 1 embodiment of table 1~3 and the Character Comparison of existing Dendrobium officinale alcohol
As can be seen from the above table, the Dendrobium officinale alcohol that prepared by the inventive method is in terms of outward appearance, fragrance, the sticky and degree of convergence
It is substantially better than existing Dendrobium officinale alcohol, and the present invention prepares the polyoses content being rich in Dendrobium officinale alcohol about in 5.8mg/
ML, and existing polyoses content only has 0.92mg/mL；The total amino acid content being rich in Dendrobium officinale alcohol of the present invention about exists
0.70mg/mL, and existing amino acid content is only 0.22mg/mL, and six kinds of amino acid needed by human contain in wine of the present invention
Amount is also apparently higher than existing Dendrobium officinale alcohol；Meanwhile, rich in things such as calcium, magnesium and iron, manganese, zinc in wine prepared by the present invention
Matter, and the content of calcium and magnesium is substantially relatively low in existing Dendrobium officinale alcohol, and it is nearly no detectable the trace meter unit of needed by human body
Element.Therefore, during preparation method of the present invention can fully extract the active substance of plant in dendrobium candidum and transfer them to wine, improve
The nutritive value of finished wine, is a kind of Dendrobium officinale alcohol rich in active substance of plant.
Presently preferred embodiments of the present invention is the foregoing is only, is not intended to limit the invention, it is all in essence of the invention
Any modification, equivalent and improvement made within god and principle etc., should be included within the scope of the present invention.
Claims (10)
1. a kind of preparation technology of the Dendrobium officinale alcohol rich in active substance of plant, it is characterised in that comprise the following steps：
1) take fresh dendrobium candidum stem, dried process carried out after being finished through freeze thawing, boiling, make its water content control 35~
50%；
2) stem of dendrobium candidum is cut into rod-short, is put into base liquor, it is size-reduced, ultrasonically treated after, Soakage extraction；
3) after placing 28~30 days, filtering makes separation of solid and liquid, reclaims stem of noble dendrobium fragment, adds base liquor, repeats aforesaid operations, secondary
Dipping 25~28 days；
4) after the 55th~58 day, filtering adds base liquor as solvent, and water-bath refluxing extraction is collected ethanol extract, added
The new base liquor of amount, secondary back is extracted, and the ethanol extract of refluxing extraction twice is mixed after filtering, squeezing；
5) wash above-mentioned stem of noble dendrobium fragment with water, adds water the aqueous extract that filtered after boiling to obtain, then to filtering residue in add equivalent
Water, through microwave, boil treatment after carry out filtering to obtain secondary aqueous extract, aqueous extract will merge twice；
6) above-mentioned aqueous extract is concentrated, it is mixed with ethanol extract, the alcoholic strength of Dendrobium officinale alcohol is reduced to 38~42 degree,
By step 5) residue after water extraction is added in the dendrobium wine after decreasing concentration, continues to impregnate 2~3 months；
7) after the 120th day, in the dendrobium wine after decreasing concentration, pectase and papain are added, at room temperature reaction 3~5 days, so
After be placed at a temperature of -10 DEG C~-4 DEG C, natural subsidence 7~12 days, upper strata clarification wine liquid be dendrobium candidum original plasm wine.
2. as claimed in claim 1 a kind of preparation technology of the Dendrobium officinale alcohol rich in active substance of plant, it is characterised in that will
The dendrobium candidum original plasm wine carries out hook tune, optimizes the mouthfeel of wine body, is made the iron sheet stone rich in active material and smell coordination
Dry measure used in former times wine.
3. as claimed in claim 1 a kind of preparation technology of the Dendrobium officinale alcohol rich in active substance of plant, it is characterised in that step
It is rapid 1) in, the concrete operations of the freeze thawing are：By fresh dendrobium candidum as more than 1h is freezed at -20 DEG C, then move to often
Temperature, after melting completely, freezes, multigelation 2~3 times again；The digestion time is 15~30min；The dried process
Using baking oven or baking box, drying temperature is 50~60 DEG C, continuous 2~4 bakings, and the time is bakeed every time for 6~7h, is bakeed every time
Interval time is no less than 12h.
4. as claimed in claim 1 a kind of preparation technology of the Dendrobium officinale alcohol rich in active substance of plant, it is characterised in that step
It is rapid 2) in, the length of the quarter butt is 1~3cm, and the alcoholic strength of the base liquor is 60~68 degree, the base liquor and dendrobium candidum
Amount ratio is 1.5L：200g；The ultrasonically treated time is 15~20min.
5. as claimed in claim 1 a kind of preparation technology of the Dendrobium officinale alcohol rich in active substance of plant, it is characterised in that step
It is rapid 3) in, the number of degrees of the base liquor are 60~68 degree, and the base liquor is 1.5L with the amount ratio of dendrobium candidum：200g.
6. as claimed in claim 1 a kind of preparation technology of the Dendrobium officinale alcohol rich in active substance of plant, it is characterised in that step
It is rapid 4) in, the number of degrees of the base liquor are 60~68 degree, and the base liquor is 0.3~0.7L with the amount ratio of dendrobium candidum：200g；Institute
The temperature for stating water-bath backflow is 55~65 DEG C, and the time is 1~2h.
7. as claimed in claim 1 a kind of preparation technology of the Dendrobium officinale alcohol rich in active substance of plant, it is characterised in that step
It is rapid 5) in, the water of the washing stem of noble dendrobium fragment is normal-temperature water or the water no more than 4 DEG C, the addition of the water and dendrobium candidum
Amount ratio is 1.5L:200g；The boiling time is 8~12min, and the microwave time is 5~7min.
8. as claimed in claim 1 a kind of preparation technology of the Dendrobium officinale alcohol rich in active substance of plant, it is characterised in that step
It is rapid 6) described in concentration aqueous extract amount be concentration before amount 70~80%.
9. as claimed in claim 1 a kind of preparation technology of the Dendrobium officinale alcohol rich in active substance of plant, it is characterised in that institute
The addition for stating pectase is 0.5~1g/L；The addition of the papain is 0.2~0.5g/L.
10. a kind of Dendrobium officinale alcohol rich in active substance of plant, it is characterised in that the Dendrobium officinale alcohol uses the right
It is required that 1 to 9 preparation technology is prepared.
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