CN106699618A - Mechanical device for producing carbocistein - Google Patents
Mechanical device for producing carbocistein Download PDFInfo
- Publication number
- CN106699618A CN106699618A CN201510792897.0A CN201510792897A CN106699618A CN 106699618 A CN106699618 A CN 106699618A CN 201510792897 A CN201510792897 A CN 201510792897A CN 106699618 A CN106699618 A CN 106699618A
- Authority
- CN
- China
- Prior art keywords
- machine
- alanine
- mechanical device
- filter
- centrifuge
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C319/00—Preparation of thiols, sulfides, hydropolysulfides or polysulfides
- C07C319/14—Preparation of thiols, sulfides, hydropolysulfides or polysulfides of sulfides
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C319/00—Preparation of thiols, sulfides, hydropolysulfides or polysulfides
- C07C319/26—Separation; Purification; Stabilisation; Use of additives
- C07C319/28—Separation; Purification
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
The invention discloses a mechanical device for producing carbocistein. The device belongs to the production field of amino acids. The mechanical device comprises a ceramic reaction kettle (1), a filter (2), a centrifugal machine (3), a drying machine (4), and a packaging machine (5); a first raw material inlet (6) is arranged on the ceramic reaction kettle (1), a first slurry pump and a pipeline (7) are arranged between the ceramic reaction kettle (1) and the filter (2), a solid outlet (8) is arranged on the filter (2), a second slurry pump and a pipeline (9) are arranged between the ceramic reaction kettle (1) and the centrifugal machine (3), a liquid outlet (10) is arranged on the centrifugal machine (3), a first conveyor (11) is arranged between the centrifugal machine (3) and the drying machine (4), a second conveyor (12) is arranged between the drying machine (4) and the packaging machine (5), and a packaging bag inlet (13) and a finished product outlet (14) are arranged on the packaging machine (5).
Description
Technical field
The invention belongs to amino acids production field, more particularly to a kind of mechanical device for producing vinegar sulphur alanine as raw material batch with cysteine hydrochloride monohydrate.
Background technology
Vinegar sulphur alanine, outward appearance is white crystalline powder, insoluble in cold water, ethanol and acetone and other organic solvent, is soluble in acid and alkaline aqueous solution.Vinegar sulphur alanine is widely used：1. pharmaceutically as expectorant, can reduce bronchial mucous secretion, the viscosity of phlegm declines and is easy to expectoration, thus can be used for for treating the not congruent patient of thick sputum, dys-expectoration, pulmonary ventilation function that chronic bronchitis, pulmonary emphysema, pulmonary tuberculosis, bronchial astehma etc. cause；2. can be used for the synthesis of multi-medicament, be a kind of important medicine intermediate and industrial chemicals；3., in daily life as hair finishing agent and conditioning agent, can act also as anti-acne medicine and use.The technique for producing vinegar sulphur alanine is more, can be used different raw materials to pass through different routes final product is obtained, the present invention is with cysteine hydrochloride monohydrate as primary raw material, expected supplemented by monoxone, liquefied ammonia, activated carbon, refined hydrochloric acid, with ceramic reactor, filter, centrifuge, drying machine, packing machine as equipment, vinegar sulphur alanine is obtained by operations such as acid adding reaction, decolorization filtering, centrifugation, drying, packagings.The process units have using common apparatus combination, simple production process, three-waste free discharge, without series of advantages such as high-temperature high-voltage reaction, low production cost and the high, good product qualities of yield.
The content of the invention
Present invention mainly solves problem be to provide a kind of mechanical device for producing vinegar sulphur alanine, the device produces vinegar sulphur alanine with ceramic reactor, filter, centrifuge, drying machine, packing machine as equipment with cysteine hydrochloride monohydrate, monoxone, liquefied ammonia, activated carbon, refined hydrochloric acid as raw material.
The technical solution adopted by the present invention is：
A kind of mechanical device for producing vinegar sulphur alanine, including：Ceramic reactor 1, filter 2, centrifuge 3, drying machine 4, packing machine 5；Ceramic reactor 1 is provided with the first material inlet 6, the first shurry pump and pipeline 7 are provided between ceramic reactor 1 and filter 2, filter 2 is provided with solid outlet 8, the second shurry pump and pipeline 9 are provided between ceramic reactor 1 and centrifuge 3, centrifuge 3 is provided with liquid outlet 10, and the first conveyer 11 is provided between centrifuge 3 and drying machine 4, and second conveyor 12 is provided between drying machine 4 and packing machine 5, packing machine 5 is provided with packaging bag import 13, product outlet 14.
Further technical scheme of the invention is：
First, second described shurry pump is stainless steel shurry pump, and corresponding pipeline is polyethylene pipe, and the second shurry pump is two-way conveying.
First, second described conveyer is scraper conveyor.
Described ceramic reactor is 5 tonnes.
Described drying machine is vacuum drier.
The beneficial effects of the invention are as follows：There is provided a kind of mechanical device for producing vinegar sulphur alanine, the device is using common apparatus combination, simple structure, easy to operate, reaction condition be gentle, pollution-free waste discharge, product vinegar sulphur alanine is widely used, as the synthesis of expectorant and multi-medicament, it is being pharmaceutically a kind of important medicine intermediate and industrial chemicals；In daily life as hair finishing agent and conditioning agent, can act also as anti-acne medicine and use.
Brief description of the drawings：
If Fig. 1 is structure of the invention and process flow diagram.
Specific embodiment
The particular content that vinegar sulphur alanine most preferred embodiment is produced using the mechanical device is further illustrated below in conjunction with the accompanying drawings：
Embodiment：
1. in 900 kilograms of cysteine hydrochloride monohydrate being sent into ceramic reactor 1 by the first material inlet 6 being arranged on ceramic reactor 1,3000 liters of monoxones are added by same import, start agitator, rotating speed is 30 revs/min, and cysteine hydrochloride monohydrate and monoxone are mixed into thick liquid；Liquefied ammonia is now added by same import, stop adding liquefied ammonia when the pH value of liquid in kettle reaches 10, continue stirring reaction adds 20 kilograms by same import activated carbon after 2 hours, while the temperature of reaction solution is brought up into 60 DEG C, stirring reaction is decolourized 0.5 hour；The solidliquid mixture of reaction is sent into filter 2 by the first shurry pump and pipeline 7 that are arranged between ceramic reactor 1 and filter 2 after decolouring to filter, filter cake is discharged by the solid outlet 8 being arranged on filter 2 and reclaimed, liquid portion is sent ceramic reactor 1 back to and continues to stir by the first shurry pump and pipeline 7 that are arranged between ceramic reactor 1 and filter 2, the first material inlet 6 by being arranged on ceramic reactor 1 adds the refined hydrochloric acid of 10 equivalents while stirring, it is 3 to adjust pH value, then the stirred crystallization in cooling, obtains the solidliquid mixture of vinegar sulphur alanine.
2. the solidliquid mixture of vinegar sulphur alanine is sent into centrifuge 3 by the second shurry pump and pipeline 9 that are arranged between ceramic reactor 1 and centrifuge 3 carries out separation of solid and liquid, liquid portion is discharged by the liquid outlet 10 being arranged on centrifuge 3 and reclaimed, and solid portion is vinegar sulphur crystalline alanine body.
3. vinegar sulphur crystalline alanine body is sent into drying machine 4 by the first conveyer 11 being arranged between centrifuge 3 and drying machine 4 to be dried, vinegar sulphur alanine pulvis is obtained after drying 4 hours at a temperature of 80 DEG C, vinegar sulphur alanine pulvis is sent into packing machine 5 by the second conveyor 12 being arranged between drying machine 4 and packing machine 5, by the batch feeding packaging bag of packaging bag import 13 being arranged on packing machine 5, the product outlet 14 after pulvis packaging is finished by being arranged on packing machine 5 discharges.
Certainly, the present invention also has other implementation methods, and the improvement of any technology, principle and the technique done under without departing from spiritual background of the invention is within the scope of the present invention.
Claims (4)
1. a kind of mechanical device for producing vinegar sulphur alanine, including：Ceramic reactor（1）, filter（2）, centrifuge（3）, drying machine（4）, packing machine（5）；It is characterized in that：Ceramic reactor（1）It is provided with the first material inlet（6）, ceramic reactor（1）And filter（2）Between be provided with the first shurry pump and pipeline（7）, filter（2）It is provided with solid outlet（8）, ceramic reactor（1）And centrifuge（3）Between be provided with the second shurry pump and pipeline（9）, centrifuge（3）It is provided with liquid outlet（10）, centrifuge（3）And drying machine（4）Between be provided with the first conveyer（11）, drying machine（4）And packing machine（5）Between be provided with second conveyor（12）, packing machine（5）It is provided with packaging bag import（13）, product outlet（14）；Described ceramic reactor is 5 tonnes.
2. a kind of mechanical device for producing vinegar sulphur alanine as claimed in claim 1, it is characterised in that：First, second described shurry pump is stainless steel shurry pump, and corresponding pipeline is polyethylene pipe, and the second shurry pump is two-way conveying.
3. a kind of mechanical device for producing vinegar sulphur alanine as claimed in claim 1, it is characterised in that：First, second described conveyer is scraper conveyor.
4. a kind of mechanical device for producing vinegar sulphur alanine as claimed in claim 1, it is characterised in that：Described drying machine is vacuum drier.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510792897.0A CN106699618A (en) | 2015-11-18 | 2015-11-18 | Mechanical device for producing carbocistein |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510792897.0A CN106699618A (en) | 2015-11-18 | 2015-11-18 | Mechanical device for producing carbocistein |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106699618A true CN106699618A (en) | 2017-05-24 |
Family
ID=58933063
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510792897.0A Pending CN106699618A (en) | 2015-11-18 | 2015-11-18 | Mechanical device for producing carbocistein |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106699618A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109566599A (en) * | 2018-12-25 | 2019-04-05 | 南京健邦锦源医疗仪器有限公司 | A kind of exfoliated cell preservative fluid |
-
2015
- 2015-11-18 CN CN201510792897.0A patent/CN106699618A/en active Pending
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109566599A (en) * | 2018-12-25 | 2019-04-05 | 南京健邦锦源医疗仪器有限公司 | A kind of exfoliated cell preservative fluid |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| WD01 | Invention patent application deemed withdrawn after publication | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20170524 |