CN1066589A - The production technology of hydrolyzed pearl powder - Google Patents
The production technology of hydrolyzed pearl powder Download PDFInfo
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- CN1066589A CN1066589A CN92104156A CN92104156A CN1066589A CN 1066589 A CN1066589 A CN 1066589A CN 92104156 A CN92104156 A CN 92104156A CN 92104156 A CN92104156 A CN 92104156A CN 1066589 A CN1066589 A CN 1066589A
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- powder
- margarita
- pearl powder
- hydrolyzed pearl
- solution
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- Coloring Foods And Improving Nutritive Qualities (AREA)
Abstract
The present invention relates to a kind of technology with the Margarita hydrolysis, it is characterized in that Margarita powder and strong inorganic acid reaction, generate the inorganic salt of the various elements that do not contain organic components, the various elements that still kept former Margarita, after water-soluble, under the situation of adding preservative agent not, can long preservation and not corrupt, the mixture of produced simultaneously aminosal and peptide can be used for medicine, food and cosmetics after reclaiming.This technology is pollution-free, and acid solution can fully reclaim, and reuses.
Description
The present invention relates to a kind of technology with the Margarita hydrolysis, the hydrolyzed pearl powder that uses this technology to make is the inorganic salt that does not contain the various elements of Organic substance composition, thereby can improve the additive of mineral water grade, also can be used as medicine, food, the additive of cosmetics etc.
The preparation technology of existing soluble pearl powder [see number of patent application: 90109538.9] selects the carbonate of the mineral in the organic acid displacement Margarita for use, generates compound carboxylic salts or amino acid salts.Though these complex salt are to the human body beneficial, its aqueous solution is to be difficult to long preservation and stay-in-grade under the situation of adding preservative agent not, therefore can not be as the additive of mineral water.Because can not there be any organic acid to exist in the mineral water, so the organic acid hydrolyzed pearl powder can not be added in the mineral water in order to improve the water quality of mineral water, can make water (1-3 month) rotten corruption in long-time on the contrary.
The production technology that the purpose of this invention is to provide a kind of hydrolyzed pearl powder, hydrolyzed pearl powder with this prepared, it is the inorganic salt that does not contain the various elements of Organic substance composition, water-soluble back is under the situation of adding preservative agent not, can long preservation and not corrupt, hydrolyzed pearl powder with this explained hereafter also can be used as medicine simultaneously, the additive of foods and cosmetics.
Technological process of the present invention is:
(1) with about crushing pearl to 200 order.
(2) strong acid (hydrochloric acid, sulphuric acid etc.) of preparation 3N-6N.Before preparation, carry out vacuum distilling once earlier, with pb in the further reduction acid solution and the content of cd, so just can guarantee the food sanitation standard 0.001mg/g of the content (pb, cd) of heavy metal in the acid solution far below national regulation.
(3) Margarita powder is constantly being joined in the acid solution for preparing under the condition of stirring, between the weight ratio 10%-50% of Margarita powder and solution.
(4) pearl powder solution for preparing was placed 12-24 hour at normal temperatures.
(5) this solution is injected into hollow fiber uf membrane system, and the starting drive operation.This moment concentrating protein and peptide of mobile solution before the film, the solution that the sees through film inorganic salt of multielement that then concentrating.So just make that protein in the pearl powder solution and peptide and inorganic salt are separated.
(6) distinguish before the collection membrane and the solution behind the film.Inorganic salt solution is put into vacuum drying system carry out drying, be heated to 100～110 ℃ simultaneously gradually and carry out the deacidification processing.Dry deacidification 4-6 hour stopped to heat postcooling 2-5 hour, take out dry pulverize a little product.
(7) solution of the protein collected and peptide being put into vacuum drying system carries out dry deacidification and handles 100～110 ℃ of temperature, time 4-6 hour, cool off and take out dry after 3-5 hour, its final dry powder is peptide and amino acid whose mixture, can be used for medicine, food and cosmetics.
The production technology of hydrolyzed pearl powder of the present invention adopts inorganic acid fluid that the mineral in the Margarita is fully cemented out, simultaneously with the scleroprotein hydrolysis.See Table a hydrolyzed pearl powder not.Table two hydrolyzed pearl powder (10% concentration).Table three hydrolyzed pearl powder (15% concentration).
Table one is hydrolyzed pearl powder not
From table, be not difficult to find out that the Margarita powder after the hydrolysis has still kept the various elements of Margarita, this Margarita inorganic salt, pure, pure white, add in the mineral water as clear as crystal, not prolongation in time and putrid and deteriorated, do not produce precipitation or float yet, isolated peptide and aminoacid can utilize as food, cosmetics, the additive of medicine.The vacuum drying deacidifying process fully reclaims acid solution, and acid solution is repeatedly used, and has also fully eliminated the acid vapor problem of environment pollution caused simultaneously.
Accompanying drawing: vacuum drying deacidification system schematic, wherein
1. inorganic salt solution bottle 2. condensing tubes
3. strong acid solution catcher 4. condensing tubes
5. strong acid solution catcher 6. automatic constant-temperature electrocaloric effects
7. acid vapor nertralizer and gas dryer bottle
Embodiment 1
Get Margarita powder 100 grams, be dissolved in the 1000ml3N hydrochloric acid, (15-24 ℃) placed 24 hours at normal temperatures, pass through hollow fiber uf membrane system then, solution 800ml behind the taking-up film, put into vacuum drying deacidification system (as accompanying drawing) and carry out dry deacidification processing, start vacuum pump, automatic constant-temperature electrocaloric effect 6 is heated up gradually, at this moment the acid solution in the inorganic salt solution bottle is vaporized gradually, and steam is condensed into acid solution (cooling water is open-minded when pump startup) again by condensing tube 2,4, be collected in the strong acid solution catcher 3,5.As have the acid gas that is condensed or not and continue acid vapor nertralizer and gas dryer bottle 7 by NaOH or KOH are housed.The purpose of taking this measure is to guarantee no noxious gas emission, contaminated air.Acid solution amount before the acid solution summation that condensation is got off and the evaporation equates substantially, and is and purer than it, thereby can repeatedly use.Dry deacidification is handled, and temperature is that 105 ℃ of times are 4 hours, stops to heat postcooling 3 hours.Take out after the termination of pumping and get 80.1 gram dry powder after block is pulverized.Sample analysis the results are shown in Table two.400mg is dissolved in the 1000ml Laoshan Spring Water with this dry powder, and water quality is as clear as crystal, places after 1 year, still keeps original transparency, any precipitation float do not occur.
Embodiment 2
Get Margarita powder 150 grams, be dissolved in the 1000ml 6N sulphuric acid, at room temperature (15-26 ℃) placed 12 hours.Then by hollow fiber uf membrane system, get solution 800ml behind the film, the dry deacidification of carrying out is similarly to Example 1 handled, 110 ℃ of treatment temperatures, the time is 6 hours, at last dry powder 120.5 grams, sample analysis the results are shown in Table three.400mg is dissolved in the 1000ml Laoshan Spring Water with this dry powder, and water quality is as clear as crystal, places after 1 year, still keeps original transparency, any precipitation or float do not occur.
Claims (1)
- A kind of production technology of hydrolyzed pearl powder is characterized in that:The Margarita powder the pulverized ratio in 10%-15% be not dissolved in strong acid (hydrochloric acid or the sulphuric acid) solution of 3N-6N under the condition of stirring, at room temperature placed 12-24 hour, filter with hollow fiber uf membrane system then, before the film of collecting respectively, liquid is put into vacuum drying system respectively and is carried out dry deacidification handle under 100-110 ℃ of temperature behind the film, obtains hydrolyzed pearl powder dry powder and peptide, ispol dry powder.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN92104156A CN1066589A (en) | 1992-06-08 | 1992-06-08 | The production technology of hydrolyzed pearl powder |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN92104156A CN1066589A (en) | 1992-06-08 | 1992-06-08 | The production technology of hydrolyzed pearl powder |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN1066589A true CN1066589A (en) | 1992-12-02 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN92104156A Pending CN1066589A (en) | 1992-06-08 | 1992-06-08 | The production technology of hydrolyzed pearl powder |
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| CN (1) | CN1066589A (en) |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1039880C (en) * | 1993-04-24 | 1998-09-23 | 于圣德 | Marine natural biological compounded active matter and making method thereof |
| CN1058050C (en) * | 1995-03-03 | 2000-11-01 | 辽宁珍珠保健品公司 | Beer containing pearl and producing method thereof |
| CN1063048C (en) * | 1997-10-21 | 2001-03-14 | 门摩西 | Water soluble pearl powder and its processing technique |
| CN106974877A (en) * | 2017-03-24 | 2017-07-25 | 北海市宝珠林海洋科技有限公司 | A kind of pearl creme acted on whitening spot-removing and preparation method thereof |
| CN110668907A (en) * | 2019-10-09 | 2020-01-10 | 福州三合元生物科技有限公司 | Preparation method of hydrolyzed amino acid |
-
1992
- 1992-06-08 CN CN92104156A patent/CN1066589A/en active Pending
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1039880C (en) * | 1993-04-24 | 1998-09-23 | 于圣德 | Marine natural biological compounded active matter and making method thereof |
| CN1058050C (en) * | 1995-03-03 | 2000-11-01 | 辽宁珍珠保健品公司 | Beer containing pearl and producing method thereof |
| CN1063048C (en) * | 1997-10-21 | 2001-03-14 | 门摩西 | Water soluble pearl powder and its processing technique |
| CN106974877A (en) * | 2017-03-24 | 2017-07-25 | 北海市宝珠林海洋科技有限公司 | A kind of pearl creme acted on whitening spot-removing and preparation method thereof |
| CN110668907A (en) * | 2019-10-09 | 2020-01-10 | 福州三合元生物科技有限公司 | Preparation method of hydrolyzed amino acid |
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