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CN106474827A - A kind of antibacterial filter core and its preparation method and application - Google Patents

A kind of antibacterial filter core and its preparation method and application Download PDF

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Publication number
CN106474827A
CN106474827A CN201610863803.9A CN201610863803A CN106474827A CN 106474827 A CN106474827 A CN 106474827A CN 201610863803 A CN201610863803 A CN 201610863803A CN 106474827 A CN106474827 A CN 106474827A
Authority
CN
China
Prior art keywords
filter core
carbon composite
nanometer copper
copper carbon
composite particle
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201610863803.9A
Other languages
Chinese (zh)
Inventor
李超
杜晓凤
连崑
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Suzhou Research Institute Of Xi''an Jiao Tong University
Suzhou Academy of Xian Jiaotong University
Original Assignee
Suzhou Research Institute Of Xi''an Jiao Tong University
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Suzhou Research Institute Of Xi''an Jiao Tong University filed Critical Suzhou Research Institute Of Xi''an Jiao Tong University
Priority to CN201610863803.9A priority Critical patent/CN106474827A/en
Publication of CN106474827A publication Critical patent/CN106474827A/en
Pending legal-status Critical Current

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D39/00Filtering material for liquid or gaseous fluids
    • B01D39/14Other self-supporting filtering material ; Other filtering material
    • B01D39/20Other self-supporting filtering material ; Other filtering material of inorganic material, e.g. asbestos paper, metallic filtering material of non-woven wires
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D39/00Filtering material for liquid or gaseous fluids
    • B01D39/14Other self-supporting filtering material ; Other filtering material
    • B01D39/16Other self-supporting filtering material ; Other filtering material of organic material, e.g. synthetic fibres
    • B01D39/18Other self-supporting filtering material ; Other filtering material of organic material, e.g. synthetic fibres the material being cellulose or derivatives thereof
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2239/00Aspects relating to filtering material for liquid or gaseous fluids
    • B01D2239/04Additives and treatments of the filtering material
    • B01D2239/0407Additives and treatments of the filtering material comprising particulate additives, e.g. adsorbents
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2239/00Aspects relating to filtering material for liquid or gaseous fluids
    • B01D2239/04Additives and treatments of the filtering material
    • B01D2239/0442Antimicrobial, antibacterial, antifungal additives
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2239/00Aspects relating to filtering material for liquid or gaseous fluids
    • B01D2239/10Filtering material manufacturing

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Filtering Materials (AREA)
  • Water Treatment By Sorption (AREA)

Abstract

The invention discloses a kind of antibacterial filter core and its preparation method and application, the antibacterial filter core has extremely strong antibacterial action, has extremely strong lethal effect to Escherichia coli, staphylococcus aureus, it is adaptable to purification of water quality in the short time.A kind of antibacterial filter core, the filter core include Nanometer Copper carbon composite particle and cellulose.The filter core is made up of Nanometer Copper carbon composite particle and cellulose.The weight ratio of the Nanometer Copper carbon composite particle and the cellulose is(8~12):1.The particle diameter of the Nanometer Copper carbon composite particle is 20 50nm.A kind of preparation method of antibacterial filter core, Nanometer Copper carbon composite and cellulose is mixed, is placed in the die cavity of mould and calcines, and then cools down drying forming.

Description

A kind of antibacterial filter core and its preparation method and application
Technical field
The present invention relates to a kind of antibacterial filter core, the preparation method of the antibacterial filter core and the antibacterial filter core are in purifier Application.
Background technology
The water resources problems of China is faced with formidable challenges, and drinking water safety is the task of top priority of China.According to world health Survey of organization, the disease in the whole world 70% are relevant with drinking water pollution.Cholera, dysentery and the malaria that the whole world is caused because of water pollution Number is more than 50,000,000.There are 1.9 hundred million people ill every year in China, 60,000 people die from the disease that water pollution causes, and Chinese Government is Drinking water safety is listed in scientific and technological key special subjects.
Use cost is cheap, the water purification catridge of low-carbon (LC) is farthest improving the research side that drinking water quality is filter core To.Filter core mainly has following a few classes at present:Active carbon filter core, with extremely strong suction-operated, typically adsorbable is more than 10 μm Particle;PP melt-blown filter, filter core accuracy rating 0.5-100 μm, the impurity of different-grain diameter can be retained;Ceramic element, is a kind of new Type environment-friendly filter element, filtering accuracy reach 0.1 μm, for removing the solid particle in the liquid in water, plating solution, running water.Although These filter cores have a certain effect to purification of water quality, but the process for microorganism in water, and filter core also has very big development space.
Content of the invention
For the problems referred to above, it is an object of the invention to provide a kind of antibacterial filter core and its preparation method and application, should Antibacterial filter core has extremely strong antibacterial action, has extremely strong lethal effect to Escherichia coli, staphylococcus aureus in the short time, Suitable for purification of water quality.
For reaching above-mentioned purpose, the technical solution used in the present invention is as follows:
A kind of antibacterial filter core, the filter core include Nanometer Copper carbon composite particle and cellulose.
Preferably, the filter core is made up of Nanometer Copper carbon composite particle and cellulose.
Preferably, the weight ratio of the Nanometer Copper carbon composite particle and the cellulose is(8~12):1.
Preferably, the particle diameter of the Nanometer Copper carbon composite particle is 20-50nm.
A kind of preparation method of antibacterial filter core, Nanometer Copper carbon composite and cellulose is mixed, is placed on the type of mould Calcine in chamber, then cool down drying forming.
Preferably, 0.5-1.5h is calcined at a temperature of 140-160 DEG C.
Preferably, the weight ratio of the Nanometer Copper carbon composite particle and the cellulose is(8~12):1.
Preferably, the particle diameter of the Nanometer Copper carbon composite particle is 20-50nm.
Application of the described antibacterial filter core in purifier.
The present invention adopts technique scheme, has the advantage that compared to existing technology:
The material of water purification cup filter element includes Nanometer Copper carbon composite particle, can realize the adsorption function of conventional filter core, realizes Absorption to fine solid particles impurity, while also have to Escherichia coli, golden yellow Portugal in extremely strong antibacterial action, short time Grape coccus has extremely strong lethal effect, it is adaptable to purification of water quality.
Description of the drawings
Accompanying drawing 1a carries out the photo after sterilized test for control group filter core;
Filter core of the accompanying drawing 1b used by the water purifying cup of the present invention carries out the photo after sterilized test.
Specific embodiment
Below in conjunction with the accompanying drawings presently preferred embodiments of the present invention is described in detail, so that advantages and features of the invention energy It is easier to be understood by the person skilled in the art.
Filter core includes Nanometer Copper carbon composite particle and cellulose, be by particle diameter for 20-50nm Nanometer Copper carbon Composite material granular and cellulose are bonded, and the weight ratio of Nanometer Copper carbon composite particle and cellulose is(8~12):1, Preferably 10:1, filter core, is the cylinder of a height of 5cm or more than 5cm.Nanometer Copper carbon composite is patent application US2012/ Material disclosed in 0021222.
The preparation method of the filter core is as follows:With Nanometer Copper carbon composite particle and cellulose as raw material, by 10:1 Part by weight is mixed, and the raw material for mixing is seated in calcining a period of time in the die cavity of mould, so that cellulose is heated Fully bond with Nanometer Copper carbon composite particle, then cool down drying forming.Wherein, the temperature of calcining is 140-160 DEG C, forges The burning time is 0.5-1.5h, calcines 1h preferably at 150 DEG C.The particle diameter of Nanometer Copper carbon composite particle is 20-50nm.
By active carbon filter core of the prior art as a control group, the filter core respectively to control group filter core and the present invention is carried out Antibacterial ability is tested, specific as follows:At room temperature, two kinds of in type filter cores are placed in the bacterial solution of quantitative concentrations, plus Wriggling pump circulation 10min, using the bacterial concentration in solution before and after colony counting method test loop, control group filter core and the present invention The antibacterial ability test result of filter core is respectively referring to accompanying drawing 1a and 1b.As a result show to kill in the filter core 410min used by the present invention More than 98% bacterium in stagnant water, meets drinking water standard, as a result referring specifically to table 1.
Table 1
Time 10min
For colibacillary sterilizing rate 98.76%
Above-described embodiment technology design only to illustrate the invention and feature, are a kind of preferred embodiments, its object is to allow Person skilled in the art will appreciate that present disclosure and implements according to this, can not limit the protection model of the present invention with this Enclose.Equivalence changes or modification that all Spirit Essences according to the present invention are made, should all be included within the scope of the present invention.

Claims (9)

1. a kind of antibacterial filter core, it is characterised in that:The filter core includes Nanometer Copper carbon composite particle and cellulose.
2. antibacterial filter core according to claim 1, it is characterised in that:The filter core by Nanometer Copper carbon composite particle and Cellulose is constituted.
3. antibacterial filter core according to claim 1, it is characterised in that:The Nanometer Copper carbon composite particle and the fibre Tieing up plain weight ratio is(8~12):1.
4. antibacterial filter core according to claim 1, it is characterised in that:The particle diameter of the Nanometer Copper carbon composite particle is 20-50nm.
5. a kind of preparation method of antibacterial filter core, it is characterised in that:Nanometer Copper carbon composite and cellulose are mixed, is placed on Calcine in the die cavity of mould, then cool down drying forming.
6. preparation method according to claim 5, it is characterised in that:0.5-1.5h is calcined at a temperature of 140-160 DEG C.
7. preparation method according to claim 5, it is characterised in that:The Nanometer Copper carbon composite particle and the fibre Tieing up plain weight ratio is(8~12):1.
8. antibacterial filter core according to claim 5, it is characterised in that:The particle diameter of the Nanometer Copper carbon composite particle is 20-50nm.
9. application of the antibacterial filter core any one of claim 1-4 in purifier.
CN201610863803.9A 2016-09-29 2016-09-29 A kind of antibacterial filter core and its preparation method and application Pending CN106474827A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201610863803.9A CN106474827A (en) 2016-09-29 2016-09-29 A kind of antibacterial filter core and its preparation method and application

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201610863803.9A CN106474827A (en) 2016-09-29 2016-09-29 A kind of antibacterial filter core and its preparation method and application

Publications (1)

Publication Number Publication Date
CN106474827A true CN106474827A (en) 2017-03-08

Family

ID=58269051

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201610863803.9A Pending CN106474827A (en) 2016-09-29 2016-09-29 A kind of antibacterial filter core and its preparation method and application

Country Status (1)

Country Link
CN (1) CN106474827A (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108743419A (en) * 2018-08-16 2018-11-06 苏州清馨健康科技有限公司 Antibacterial removes stain toothpaste
CN113109229A (en) * 2021-02-25 2021-07-13 中科检测技术服务(广州)股份有限公司 Method for testing antibacterial performance of filter element of water purifier

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1255400A (en) * 1999-12-07 2000-06-07 李儒林 Water-clarifying filter and its making method and application
CN101524605A (en) * 2009-04-09 2009-09-09 吉林大学 Individual soldier water purifier applying composite nano water purifying material
US20120021222A1 (en) * 2006-02-10 2012-01-26 Kun Lian Carbon-Encased Metal Nanoparticles and Sponges, Methods of Synthesis, and Methods of Use
CN102580405A (en) * 2012-02-14 2012-07-18 厦门建霖工业有限公司 Multifunction carbon rod filter cartridge and manufacturing method thereof
CN104692667A (en) * 2015-02-11 2015-06-10 陕西科技大学 Method for preparing porous glass filter element for water purifier
CN105731559A (en) * 2016-02-03 2016-07-06 惠州市银嘉环保科技有限公司 Ultrafiltration anti-microbial activated carbon bar and preparation method thereof

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1255400A (en) * 1999-12-07 2000-06-07 李儒林 Water-clarifying filter and its making method and application
US20120021222A1 (en) * 2006-02-10 2012-01-26 Kun Lian Carbon-Encased Metal Nanoparticles and Sponges, Methods of Synthesis, and Methods of Use
CN101524605A (en) * 2009-04-09 2009-09-09 吉林大学 Individual soldier water purifier applying composite nano water purifying material
CN102580405A (en) * 2012-02-14 2012-07-18 厦门建霖工业有限公司 Multifunction carbon rod filter cartridge and manufacturing method thereof
CN104692667A (en) * 2015-02-11 2015-06-10 陕西科技大学 Method for preparing porous glass filter element for water purifier
CN105731559A (en) * 2016-02-03 2016-07-06 惠州市银嘉环保科技有限公司 Ultrafiltration anti-microbial activated carbon bar and preparation method thereof

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
朱企新 等译: "《固液分离》", 30 April 1990 *

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108743419A (en) * 2018-08-16 2018-11-06 苏州清馨健康科技有限公司 Antibacterial removes stain toothpaste
CN113109229A (en) * 2021-02-25 2021-07-13 中科检测技术服务(广州)股份有限公司 Method for testing antibacterial performance of filter element of water purifier

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Application publication date: 20170308

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