CN106387986A - Re-dried tobacco leaf secondary fermentation product - Google Patents

Abstract

The invention provides a re-dried tobacco leaf secondary fermentation product, which is a fermentation product prepared from a mixture of re-dried tobacco leaves and plants by virtue of a liquid-state fermentation process, wherein the re-dried tobacco leaves are obtained by conducting primary solid-state fermentation on at least one of flue-cured tobacco, sun-cured tobacco and aromatic tobacco in a storage process; the plants include one or more of fresh flowers, melons and fruits, vegetables and Chinese herbal medicines; the mass ratio of the re-dried tobacco leaves to the plants ranges from (3 to 1) to (1 to 3); and the re-dried tobacco leaf secondary fermentation product is any one of a fermentation broth, powder or granules formed by drying a fermentation material and an extract of the fermentation broth. According to the re-dried tobacco leaf secondary fermentation product provided by the invention, the mass content of sorbic acid substances is less than 0.001%, so that bad taste, color change and dirt caused by excessively high content of the sorbic acid substances are avoided.

Description

A kind of redried leaf tobacco ferment in second time product

Technical field

A kind of the present invention relates to tobacco material tunning field, more particularly it relates to redrying cigarette Leaf ferment in second time product.

Background technology

Buccal cigarette is to enter to grow up by some Nicotiana tabacum L.s through special handling or the raw material containing tobacco component to make The oral cavity of user, thus the satisfaction brought of the Nicotiana tabacum L. enjoying non smoke form and pleasant sensation.With traditional cigarette Cigarette raw material is different, due to the harmful components of the master, sidestream smoke and Pintsch process of generation of not burning, Smokeless tobacco articles are considered as a kind of safer Medicated cigarette substitute products.And it is good for smoking with various countries Kang Wenti gives more sustained attention, and the Tobacco Control dynamics continuing to increase, and smokeless tobacco articles are undoubtedly thermophilic cigarette people The replacement Sexual behavior mode of group.In countries such as the U.S., Sweden, Folium Nicotianae preparatum, chewing tobacco have long history, buccal cigarette Materials safety also received long-term market validation.Representational smokeless on European ＆ American Market at present Tobacco product manufacturer has Sweden's match (Swedish Match AB), German Po Shier Nicotiana tabacum L. group The smokeless tobacco company (US smokeless Tobacco Co.) of (Poschl Tobacco Group), the U.S., R.J. Rainolds Tobacco CO..Countries in the world tobacco business is research and development and the market of smokeless tobacco raw material Promote as the important directions solving Nicotiana tabacum L. future development.There is depth in the consumption habit of Nicotiana tabacum L. and mode The change carved, taking the U.S. as a example, the tobacco material total volume of retail sales is 86,000,000,000 dollars within 2007, and smokeless cigarette The total volume of retail sales of straw-made articless is 4,400,000,000 dollars, alreadys exceed the retail sales (4,200,000,000 dollars) of traditional cigar, Traditional cigarette consumption figure is declined with annual 4% speed simultaneously, and meanwhile, smokeless tobacco raw material Consumption figure is just increased with the speed of 6-7%, and market potential is more huge.Domestic smokeless tobacco articles also in Starting stage, market also there is no the product of independent research, core technology and research and development of products also in blank In the stage, domestic smokeless tobacco articles not only will cater to the consumer of Chinese-style cigarette style on taste, simultaneously Differentiated products targetedly with regional characteristic should be provided.

In buccal cigarette, most important raw material is tobacco material.The tobacco material using at present, typically takes from biography System cigarette industry raw material, for example by Nicotiana tabacum L. after drying after alcohol metallization processes (i.e. fermentation technology) Obtained from one time fermentation raw material, as buccal cigarette tobacco material after pulverizing to this one time fermentation raw material, Or this one time fermentation raw material is carried out after solvent extraction, with its extracting solution or through spraying to extracting solution The dried powder of mist is as buccal cigarette tobacco material.

Remain a need for the buccal cigarette tobacco material of more tastes.

Content of the invention

The present invention has filled up the blank that tobacco product raw material sucked by domestic no wet-fermentation type, provides one kind to contain The raw material of the mouth containing tobacco product of Nicotiana tabacum L. ferment in second time product, meets domestic smokeless tobacco raw material production enterprise The demand of industry.

The invention discloses a kind of redried leaf tobacco ferment in second time product, it is the mixing of redried leaf tobacco and plant The tunning that thing is prepared by liquid-state fermentation technology, wherein said redried leaf tobacco passes through flue-cured tobacco, dry in the sun At least one in cigarette and Turkish tobaccos carries out first time solid fermentation in storage process and obtains, wherein institute State plant be one or more of flower, melon fruits and vegetables, Chinese herbal medicine, wherein said redried leaf tobacco with The mass ratio of described plant is 3:1 to 1:3, wherein said redried leaf tobacco ferment in second time product be fermentation liquid, Any one in the powder being formed after fermented product is dry or granule, the extract of fermentation liquid.

Preferably, wherein used in liquid fermentation process, microorganism is antibacterial, actinomycetes, funguses, ferment The combination of one or more of mother.

It is highly preferred that the microorganism being used is lactic acid bacteria, yeast, bacillus bifiduss, huge spore bar Bacterium, bacillus subtilises, thermophilic actinomycetes, enterobacter cloacae, unwrapping wire root nodule bacteria, Pseudomonas alba One of or several combinations.

In the redried leaf tobacco ferment in second time product of the present invention, the mass content of Pyrusussuriensiss acid is less than 0.001%.

Advantages of the present invention：

1st, the redried leaf tobacco ferment in second time product of the present invention is the ferment in second time product of redrying Nicotiana tabacum L. and plant, Comprise tobacco source fragrance matter and plant source fragrance matter, fragrance is abundanter.Nicotiana tabacum L. ferment in second time product Remove rich in multiple hydrolytic enzyme, such as protease, amylase, Digestive Enzyme, pectase, SOD enzyme etc., simultaneously Due to depth fermentation, the macromolecular substances Degradation and Transformation in plant is to be more easy to absorbed small-molecule substance, Also contain abundant aminoacid, oligosaccharide, dietary fiber, fatty acid and mineral element.Therefore, this Bright redried leaf tobacco ferment in second time product nutrient enriches, and has health care, and the present invention is secondary by Nicotiana tabacum L. Tunning is applied to not only provide the selection of more diversification in buccal cigarette raw material on style taste, more It is important that unbalanced to nutrition intake, digest and assimilate poor crowd and have clear improvement, in addition also delay Aging, resisting fatigue, effect of enhancing immunity.

2nd, the different collocation of tobacco extract raw material can obtain the tobacco extract of different taste types, thus obtaining Obtain the buccal cigarette raw material of different taste types, such as adopt flue-cured tobacco and dry in the sun cigarette mass ratio 1：1 collocation is realized fragrant Taste is strong, strength is sufficient, have the tobacco extract of dry in the sun cigarette feature, and such as adopts flue-cured tobacco, cabo With tobacco leaf fragment mass ratio 2：1：1 combination realize fresh and sweet note, strength moderate there is Chinese-style cigarette The tobacco extract of feature style.

3 it is surprising that redrying Nicotiana tabacum L. ferment in second time product GC with Headspace-MS full scan by the present invention Figure can with merely through the contrast of solid fermentation (i.e. one time fermentation) tobacco particle thing GC with Headspace-MS full scan figure Find out, after ferment in second time, at 16-17min in spectrogram, chromatographic peak substantially diminishes, through library searching, At this, chromatographic peak is Pyrusussuriensiss acid, and that is, in Nicotiana tabacum L. ferment in second time product, Determination of sorbic substantially reduces, Find through quantitative Analysis, Determination of sorbic can as little as less than 0.001%.Although sorbic acid is a kind of to people The safe and harmless natural antiseptic agent of body, but when its concentration is excessive, often there is undesirable acid smell, Although the mouthfeel that tradition is lighted with suction type Medicated cigarette no affects, may potentially affect the mouth of buccal cigarette When sense, therefore the redrying Nicotiana tabacum L. ferment in second time product of the present invention are used as buccal cigarette raw material, because of Determination of sorbic Reduce and improve mouthfeel, experiment shows, product of the present invention has the fermentation fragrance of flavour feature. In addition, sorbic acid is easy to oxidized in atmosphere and variable color, leads to suck tobacco product and send out dirt also with variable color, Determination of sorbic is reduced by ferment in second time, the probability of mouth containing tobacco product variable color can be greatly reduced.

Brief description

Fig. 1 is the redried leaf tobacco ferment in second time product GC with Headspace-MS full scan figure of the present invention

Fig. 2 is the GC with Headspace-MS full scan figure of one time fermentation tobacco particle thing

Specific embodiment

In order that the objects, technical solutions and advantages of the present invention become more apparent, with reference to embodiments, The present invention will be described in further detail.It should be appreciated that specific embodiment described herein is only used To explain the present invention, it is not intended to limit the present invention.

Embodiment 1

Is produced from Yunnan low temperature sterilization after shredding after the cleaning of Flos Carthami big gold dollar redried leaf tobacco, add roseleaf, redrying Nicotiana tabacum L. is 3 with the mass ratio of roseleaf:1, then inoculation yeast carry out wet-mixed fermentation, sweat Parameter is as follows：Bacillus subtilises are transferred to liquid seed culture medium from slant medium and activated for two generations Afterwards, access equipped with the 250mL triangular flask of 100mL liquid fermentation medium, inoculum concentration 4% (v/v), 30.C, 120r/rain cultivate 20 hours, and now the OD600 of culture medium is about 6.0, culture fluid It is centrifuged 20 minutes with 4000r/min, with aseptic water washing, centrifugation, finally plus sterilized water vibration shakes up, Used time is diluted to the microbial inoculum of bacterium number 108/mL.Claim tobacco shred and the Flos Rosae Rugosae of the good moisture of pre-balance to 13% 300 grams of petal mixture is put in plastic bag, does blank with the tobacco shred processing without microbial inoculum, in temperature 30 DEG C, the constant temperature and humidity incubator artificial fermentation of relative humidity 65%.

Embodiment 2

Redried leaf tobacco K326 is produced in Yunnan, the big gold dollar of redried leaf tobacco Flos Carthami is produced according to 1 in Yunnan:1 ratio mixing After pulverizing, add Yunnan Fructus Canarii albi, Nicotiana tabacum L. is 1 with the mass ratio of roseleaf：1, then inoculation yeast, double Discrimination bacillus, lactobacilluss mixed fermentation, after fermentation, product carries out lyophilization, obtains water activity 0.6Aw Following fermentation powder.

Table 1 below list in redried leaf tobacco ferment in second time product fragrance matter with through a solid fermentation Redried leaf tobacco contrasts

It can be seen that, after ferment in second time, the type of fragrance matter increased a lot, has greatly enriched fragrance Species.

Claims (4)

1. a kind of redried leaf tobacco ferment in second time product is it is characterised in that it is the mixing of redried leaf tobacco and plant The tunning that thing is prepared by liquid-state fermentation technology, wherein said redried leaf tobacco pass through by flue-cured tobacco, dry in the sun cigarette and At least one in Turkish tobaccos carries out first time solid fermentation in storage process and obtains, and wherein said plant is The matter of one or more of flower, melon fruits and vegetables, Chinese herbal medicine, wherein said redried leaf tobacco and described plant Amount ratio is 3:1 to 1:3, wherein said redried leaf tobacco ferment in second time product be fermentation liquid, fermented product be dried after shape Any one in the powder becoming or granule, the extract of fermentation liquid.

2. redried leaf tobacco ferment in second time product according to claim 1 is it is characterised in that wherein liquid Used in sweat, microorganism is antibacterial, actinomycetes, funguses, the combination of one or more of yeast.

3. redried leaf tobacco ferment in second time product according to claim 1 is it is characterised in that used Microorganism is lactic acid bacteria, yeast, bacillus bifiduss, bacillus megaterium, bacillus subtilises, thermophilic are put One of line bacterium, enterobacter cloacae, unwrapping wire root nodule bacteria, Pseudomonas alba or several combinations.

4. redried leaf tobacco ferment in second time product according to claim 1 is it is characterised in that wherein Pyrusussuriensiss The mass content of acid is less than 0.001%.