CN106343156A - Mixed type feed additive majoram extract water-soluble preparation and preparation method thereof - Google Patents
Mixed type feed additive majoram extract water-soluble preparation and preparation method thereof Download PDFInfo
- Publication number
- CN106343156A CN106343156A CN201610663725.8A CN201610663725A CN106343156A CN 106343156 A CN106343156 A CN 106343156A CN 201610663725 A CN201610663725 A CN 201610663725A CN 106343156 A CN106343156 A CN 106343156A
- Authority
- CN
- China
- Prior art keywords
- water
- bovis seu
- seu bubali
- adeps bovis
- acid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000000284 extract Substances 0.000 title claims abstract description 70
- 238000002360 preparation method Methods 0.000 title claims abstract description 44
- 239000003674 animal food additive Substances 0.000 title claims abstract description 26
- BDAGIHXWWSANSR-UHFFFAOYSA-N Formic acid Chemical compound OC=O BDAGIHXWWSANSR-UHFFFAOYSA-N 0.000 claims abstract description 70
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims abstract description 45
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims abstract description 42
- 235000019253 formic acid Nutrition 0.000 claims abstract description 35
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims abstract description 33
- JVTAAEKCZFNVCJ-UHFFFAOYSA-N lactic acid Chemical compound CC(O)C(O)=O JVTAAEKCZFNVCJ-UHFFFAOYSA-N 0.000 claims abstract description 30
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 22
- 239000004310 lactic acid Substances 0.000 claims abstract description 15
- 235000014655 lactic acid Nutrition 0.000 claims abstract description 15
- 238000002156 mixing Methods 0.000 claims abstract description 11
- 239000007788 liquid Substances 0.000 claims abstract description 9
- 238000000034 method Methods 0.000 claims abstract 2
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims description 40
- OSWFIVFLDKOXQC-UHFFFAOYSA-N 4-(3-methoxyphenyl)aniline Chemical compound COC1=CC=CC(C=2C=CC(N)=CC=2)=C1 OSWFIVFLDKOXQC-UHFFFAOYSA-N 0.000 claims description 33
- 229910021529 ammonia Inorganic materials 0.000 claims description 20
- 239000000203 mixture Substances 0.000 claims description 14
- 229910001220 stainless steel Inorganic materials 0.000 claims description 14
- 239000010935 stainless steel Substances 0.000 claims description 14
- 235000013305 food Nutrition 0.000 claims description 10
- 238000011049 filling Methods 0.000 claims description 7
- 230000004044 response Effects 0.000 claims description 7
- 238000003756 stirring Methods 0.000 claims description 7
- 239000000463 material Substances 0.000 claims description 4
- 238000006243 chemical reaction Methods 0.000 abstract description 9
- 230000000844 anti-bacterial effect Effects 0.000 abstract description 6
- VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 abstract 1
- 235000011114 ammonium hydroxide Nutrition 0.000 abstract 1
- 238000001816 cooling Methods 0.000 abstract 1
- 238000001914 filtration Methods 0.000 abstract 1
- 238000012856 packing Methods 0.000 abstract 1
- 230000001954 sterilising effect Effects 0.000 abstract 1
- 239000002253 acid Substances 0.000 description 15
- 239000003651 drinking water Substances 0.000 description 8
- 235000020188 drinking water Nutrition 0.000 description 8
- 230000000694 effects Effects 0.000 description 8
- 241001465754 Metazoa Species 0.000 description 7
- 235000005979 Citrus limon Nutrition 0.000 description 6
- VZTDIZULWFCMLS-UHFFFAOYSA-N ammonium formate Chemical compound [NH4+].[O-]C=O VZTDIZULWFCMLS-UHFFFAOYSA-N 0.000 description 6
- 239000007853 buffer solution Substances 0.000 description 6
- 230000021615 conjugation Effects 0.000 description 6
- 238000001556 precipitation Methods 0.000 description 6
- 239000002994 raw material Substances 0.000 description 6
- 150000003839 salts Chemical class 0.000 description 6
- MGSRCZKZVOBKFT-UHFFFAOYSA-N thymol Chemical compound CC(C)C1=CC=C(C)C=C1O MGSRCZKZVOBKFT-UHFFFAOYSA-N 0.000 description 6
- 239000000843 powder Substances 0.000 description 4
- WEVYAHXRMPXWCK-UHFFFAOYSA-N Acetonitrile Chemical compound CC#N WEVYAHXRMPXWCK-UHFFFAOYSA-N 0.000 description 3
- 244000248349 Citrus limon Species 0.000 description 3
- 244000131522 Citrus pyriformis Species 0.000 description 3
- 239000005844 Thymol Substances 0.000 description 3
- 239000000654 additive Substances 0.000 description 3
- 230000000996 additive effect Effects 0.000 description 3
- HHTWOMMSBMNRKP-UHFFFAOYSA-N carvacrol Natural products CC(=C)C1=CC=C(C)C(O)=C1 HHTWOMMSBMNRKP-UHFFFAOYSA-N 0.000 description 3
- 235000007746 carvacrol Nutrition 0.000 description 3
- 210000004027 cell Anatomy 0.000 description 3
- 238000011161 development Methods 0.000 description 3
- WYXXLXHHWYNKJF-UHFFFAOYSA-N isocarvacrol Natural products CC(C)C1=CC=C(O)C(C)=C1 WYXXLXHHWYNKJF-UHFFFAOYSA-N 0.000 description 3
- 229960000790 thymol Drugs 0.000 description 3
- 102000004190 Enzymes Human genes 0.000 description 2
- 108090000790 Enzymes Proteins 0.000 description 2
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 2
- 239000003242 anti bacterial agent Substances 0.000 description 2
- 229940088710 antibiotic agent Drugs 0.000 description 2
- 230000003115 biocidal effect Effects 0.000 description 2
- RECUKUPTGUEGMW-UHFFFAOYSA-N carvacrol Chemical compound CC(C)C1=CC=C(C)C(O)=C1 RECUKUPTGUEGMW-UHFFFAOYSA-N 0.000 description 2
- 230000008859 change Effects 0.000 description 2
- 238000004140 cleaning Methods 0.000 description 2
- 238000001514 detection method Methods 0.000 description 2
- 239000004459 forage Substances 0.000 description 2
- 239000004615 ingredient Substances 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 244000005700 microbiome Species 0.000 description 2
- 210000003470 mitochondria Anatomy 0.000 description 2
- 239000000419 plant extract Substances 0.000 description 2
- 239000000243 solution Substances 0.000 description 2
- FRXSZNDVFUDTIR-UHFFFAOYSA-N 6-methoxy-1,2,3,4-tetrahydroquinoline Chemical compound N1CCCC2=CC(OC)=CC=C21 FRXSZNDVFUDTIR-UHFFFAOYSA-N 0.000 description 1
- 241001061264 Astragalus Species 0.000 description 1
- 206010059866 Drug resistance Diseases 0.000 description 1
- 241000282894 Sus scrofa domesticus Species 0.000 description 1
- 230000002159 abnormal effect Effects 0.000 description 1
- 230000009471 action Effects 0.000 description 1
- 229910000147 aluminium phosphate Inorganic materials 0.000 description 1
- 150000001413 amino acids Chemical class 0.000 description 1
- 239000002260 anti-inflammatory agent Substances 0.000 description 1
- 230000001741 anti-phlogistic effect Effects 0.000 description 1
- 235000006533 astragalus Nutrition 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 150000007822 carvacrol derivatives Chemical group 0.000 description 1
- 210000000170 cell membrane Anatomy 0.000 description 1
- 239000013522 chelant Substances 0.000 description 1
- 230000002079 cooperative effect Effects 0.000 description 1
- 230000029087 digestion Effects 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 239000003640 drug residue Substances 0.000 description 1
- 210000002472 endoplasmic reticulum Anatomy 0.000 description 1
- 230000002708 enhancing effect Effects 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 238000009313 farming Methods 0.000 description 1
- 235000021050 feed intake Nutrition 0.000 description 1
- 239000003205 fragrance Substances 0.000 description 1
- 238000004817 gas chromatography Methods 0.000 description 1
- 239000004519 grease Substances 0.000 description 1
- 230000009931 harmful effect Effects 0.000 description 1
- 230000036039 immunity Effects 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 235000013372 meat Nutrition 0.000 description 1
- 244000000010 microbial pathogen Species 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 235000015097 nutrients Nutrition 0.000 description 1
- 210000003463 organelle Anatomy 0.000 description 1
- 150000007524 organic acids Chemical class 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 150000002989 phenols Chemical class 0.000 description 1
- 239000002574 poison Substances 0.000 description 1
- 231100000614 poison Toxicity 0.000 description 1
- 229920001282 polysaccharide Polymers 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
- 230000028327 secretion Effects 0.000 description 1
- 239000013049 sediment Substances 0.000 description 1
- 230000035943 smell Effects 0.000 description 1
- 210000001082 somatic cell Anatomy 0.000 description 1
- 210000004233 talus Anatomy 0.000 description 1
- 231100000419 toxicity Toxicity 0.000 description 1
- 230000001988 toxicity Effects 0.000 description 1
Landscapes
- Fodder In General (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
Abstract
The invention discloses a mixed type feed additive majoram extract water-soluble preparation and a preparation method thereof. The mixed type feed additive majoram extract water-soluble preparation is a mixed type feed additive product of which a majoram extract can be dissolved in water according to an optional ratio. The preparation method comprises the following steps: (1) placing methanoic acid in a reaction kettle; (2) feeding ammonia water into the methanoic acid from bottom to top; (3) after complete reaction, adding citric acid, lactic acid and acetic acid; (4) placing the majoram extract in another reaction kettle; (5) feeding propylene glycol as a feed additive into the majoram extract; (6) after complete mixing, adding liquid finished in the step (3); (7) cooling; (8) filtering; and (9) checking and packing. The product produced by the method has high sterilizing and antibacterial effects.
Description
Technical field
The present invention relates to field of feed additive technology is and in particular to a kind of mixed feed additive Adeps Bovis seu Bubali extract water
Solubility preparation and preparation method thereof.
Background technology
China's feed industry is started in 20 century 70 middle and late stage, and forage yield from 1992 leaps to the second in the world
Position, from 2011, forage yield has exceeded the U.S. and has occupied No. 1 in the world.Through the development of more than 30 years, China's feed industry was
Define and consult including feed processing industry, feedstuff industry, feed additive industry, feed manufacturing machine industry and feed branch
Educate, quality safety etc. is the complete feed industry system supporting.The development developing into propulsion modern farming of feed industry, carries
High people's living standard has made major contribution.Also some problems, abuse of antibiotics are occurred in that in this quick evolution
Become industry stain, cause a lot of harmful effects.Nonreactive cultivation has become the main trend of present animal husbandry development, and natural
Plant extract be cancel antibiotic after protect one of staple product of animal.
Conventional plant extract has garlicin, Adeps Bovis seu Bubali extract, Herba Epimedii extract, astragalus polysaccharidess etc., is added to and raises
Bactericidal antiphlogistic, enhancing immunity can be played in material, promote growth, food calling etc. to act on, and drug residue free, not cause change
Different, it is Substitutes For Antibiotic well.
The main component of Adeps Bovis seu Bubali extract is carvacrol and thymol, is unique in catalogue of feed additive varieties and medicine
The material of all presence in thing additive catalogue, the application in cultivation has multiple efficacies.
1st, Adeps Bovis seu Bubali extract is the antibacterial growth-promoting additive that the Ministry of Agriculture's approval uses, and has and remarkably promotes animal life
Long effect, its unique abnormal smells from the patient can stimulate searches for food, and increases feed intake, and the activity of its phenols can stimulate digestion the secretion of enzyme, energy
Enough promoting nutrient to digest and assimilate, improving efficiency of feed utilization, thus reaching somatotrophic purpose.
2nd, Adeps Bovis seu Bubali extract has very strong surface-active action, can readily penetrate through pathogenic microorganism cell membrane, promote
Large quantity of moisture gathers in the cell and causes somatic cells to expand, and causes membranolysises, thalline is dead；Also can ooze after entering cell
Enter organelle (as endoplasmic reticulum, mitochondrion, ribosome etc.), stoping mitochondrion from drawing oxygen makes cell be choked to death.
3 and feedstuff in Multiple components, exist such as between enzyme preparation, organic acid, amino-acid chelate, common antibiotics etc.
Cooperative effect, is used in conjunction with effect more excellent.
4th, meat fragrance can be significantly improved, and improve Carnis Sus domestica system waterpower.
5th, toxicity is low, using safety；No Drug resistance, noresidue, no withdrawal time.
6th, use cost is low, high financial profit.According to experiment, relatively low addition just can reach good bactericidal effect.
On market, existing Adeps Bovis seu Bubali extract is most is added in the form of powder.Because Adeps Bovis seu Bubali extract is originally as grease
Matter, wherein most of materials are practically insoluble in water, so basic being added in feedstuff with powder form is used.But so there is also
The inconvenience of some interpolations and because usage amount low brought mixing homogeneity such as is difficult to ensure that at the unfavorable factor.
Content of the invention
The technical problem to be solved is to provide one kind to have a safety feature, the mixed feed of high financial profit
The water-soluble preparation of additive Adeps Bovis seu Bubali extract.
The technical problem to be solved employs the following technical solutions to realize:
A kind of water-soluble preparation of mixed feed additive Adeps Bovis seu Bubali extract, this water-soluble preparation of Adeps Bovis seu Bubali extract can be with any
Ratio is miscible with water, will not separate out oil bloom or precipitation, has good dispersibility.Miscible water is in gb/t 6682-2008
The tertiary effluent of regulation.
The water-soluble preparation of above-mentioned Adeps Bovis seu Bubali extract is made up of the component of following parts by weight: formic acid 20-30, ammonia 10-20,
Lactic acid 5-10, acetic acid 5-10, citric acid 5-10, propylene glycol 20-30, Adeps Bovis seu Bubali extract 2-10.Raw materials used it is food stage.
The preparation method of the water-soluble preparation of above-mentioned Adeps Bovis seu Bubali extract is as follows:
(1) formic acid is placed in stainless steel cauldron (band temperature control)；
(2) ammonia is slowly introducing in formic acid upwards by bottom, and guarantees that temperature is maintained at 60-90 DEG C；Formic acid and ammonia
Reaction forms ammonium formate, forms weak acid-weak acid and mild base salt conjugation buffer solution system with formic acid；
(3), after question response is complete, adds citric acid, lactic acid, acetic acid, dissolving, stir 20-30 minute mix homogeneously；
(4) cool to standing under room temperature；
(5) add Adeps Bovis seu Bubali extract in another reactor；
(6) feed additive propylene glycol is passed through in Adeps Bovis seu Bubali extract；
(7), after mixing completely, the liquid that step (4) is completed, mix homogeneously are added；
(8) filtered using 200 mesh stainless steel filters；
(9) each component content and index, filling and package are checked.
The detection method of above-mentioned Adeps Bovis seu Bubali extract is gas chromatography, and mobile phase used is acetonitrile: 1 ‰ phosphoric acid solutions=
2.5: 97.5 (v: v), Detection wavelength is 210nm, and flow velocity is 1ml/min, and column temperature is room temperature.
The present invention passes through to add necessary emulsified component, makes Adeps Bovis seu Bubali extract enter emulsified state, thus being allowed to reach with water
To perfectly miscible state, added by drinking-water, perfection solves adds not enough the asking of mixing homogeneity in inconvenience and powder
Topic.And, add Adeps Bovis seu Bubali extract in drinking-water, can be very good to suppress the growth of microorganism in water, reach cleaning drinking-water, prevent
Only block the effect of waterline, be the developing direction of following drinking water for animals.
The invention has the beneficial effects as follows:
1st, the water-soluble preparation of Adeps Bovis seu Bubali extract of the present invention has and uses safety, secondary to the no any poison of growth of animal makees
With, noresidue, animal, human body and production equipment are corroded low simultaneously.
2nd, the water-soluble preparation of Adeps Bovis seu Bubali extract of the present invention additionally adds acid ingredient, under sour environment, in Adeps Bovis seu Bubali extract
Carvacrol and thymol can produce collaborative with acid, play more preferable bactericidal action and more preferable phagostimulating effect.
3rd, the water-soluble preparation of Adeps Bovis seu Bubali extract of the present invention can be miscible with water with arbitrary proportion, will not separate out oil bloom or heavy
Form sediment, there is good dispersibility.
Specific embodiment
In order that technological means, creation characteristic, reached purpose and effect that the present invention realizes are easy to understand, tie below
Close specific embodiment, the present invention is expanded on further.
Embodiment 1
A kind of water-soluble preparation of mixed feed additive Adeps Bovis seu Bubali extract, formic acid 20-30, ammonia 10-20, lactic acid 7.5, second
Acid 7.5, citric acid 7.5, propylene glycol 25, Adeps Bovis seu Bubali extract 6.Raw materials used it is food stage.
The preparation method of the water-soluble preparation of above-mentioned Adeps Bovis seu Bubali extract is as follows:
(1) formic acid is placed in stainless steel cauldron (band temperature control)；
(2) ammonia is slowly introducing in formic acid upwards by bottom, and guarantees that temperature is maintained at 60-90 DEG C；Formic acid and ammonia
Reaction forms ammonium formate, forms weak acid-weak acid and mild base salt conjugation buffer solution system with formic acid；
(3), after question response is complete, adds citric acid, lactic acid, acetic acid, dissolving, stir 20-30 minute mix homogeneously；
(4) cool to standing under room temperature；
(5) add Adeps Bovis seu Bubali extract in another reactor；
(6) feed additive propylene glycol is passed through in Adeps Bovis seu Bubali extract；
(7), after mixing completely, the liquid that step (4) is completed, mix homogeneously are added；
(8) filtered using 200 mesh stainless steel filters；
(9) each component content and index, filling and package are checked.
This water-soluble preparation of Adeps Bovis seu Bubali extract can be miscible with water with arbitrary proportion, will not separate out oil bloom or precipitation, have
Good dispersibility.Miscible water is tertiary effluent specified in gb/t 6682-2008.
Embodiment 2
A kind of water-soluble preparation of mixed feed additive Adeps Bovis seu Bubali extract, formic acid 30, ammonia 10, lactic acid 10, acetic acid 5, lemon
Lemon acid 10, propylene glycol 20, Adeps Bovis seu Bubali extract 10.Raw materials used it is food stage.
The preparation method of the water-soluble preparation of above-mentioned Adeps Bovis seu Bubali extract is as follows:
(1) formic acid is placed in stainless steel cauldron (band temperature control)；
(2) ammonia is slowly introducing in formic acid upwards by bottom, and guarantees that temperature is maintained at 60-90 DEG C；Formic acid and ammonia
Reaction forms ammonium formate, forms weak acid-weak acid and mild base salt conjugation buffer solution system with formic acid；
(3), after question response is complete, adds citric acid, lactic acid, acetic acid, dissolving, stir 20-30 minute mix homogeneously；
(4) cool to standing under room temperature；
(5) add Adeps Bovis seu Bubali extract in another reactor；
(6) feed additive propylene glycol is passed through in Adeps Bovis seu Bubali extract；
(7), after mixing completely, the liquid that step (4) is completed, mix homogeneously are added；
(8) filtered using 200 mesh stainless steel filters；
(9) each component content and index, filling and package are checked.
This water-soluble preparation of Adeps Bovis seu Bubali extract can be miscible with water with arbitrary proportion, will not separate out oil bloom or precipitation, have
Good dispersibility.Miscible water is tertiary effluent specified in gb/t 6682-2008.
Embodiment 3
A kind of water-soluble preparation of mixed feed additive Adeps Bovis seu Bubali extract, formic acid 20, ammonia 20, lactic acid 5, acetic acid 10, lemon
Lemon acid 5, propylene glycol 30, Adeps Bovis seu Bubali extract 2.Raw materials used it is food stage.
The preparation method of the water-soluble preparation of above-mentioned Adeps Bovis seu Bubali extract is as follows:
(1) formic acid is placed in stainless steel cauldron (band temperature control)；
(2) ammonia is slowly introducing in formic acid upwards by bottom, and guarantees that temperature is maintained at 60-90 DEG C；Formic acid and ammonia
Reaction forms ammonium formate, forms weak acid-weak acid and mild base salt conjugation buffer solution system with formic acid；
(3), after question response is complete, adds citric acid, lactic acid, acetic acid, dissolving, stir 20-30 minute mix homogeneously；
(4) cool to standing under room temperature；
(5) add Adeps Bovis seu Bubali extract in another reactor；
(6) feed additive propylene glycol is passed through in Adeps Bovis seu Bubali extract；
(7), after mixing completely, the liquid that step (4) is completed, mix homogeneously are added；
(8) filtered using 200 mesh stainless steel filters；
(9) each component content and index, filling and package are checked.
This water-soluble preparation of Adeps Bovis seu Bubali extract can be miscible with water with arbitrary proportion, will not separate out oil bloom or precipitation, have
Good dispersibility.Miscible water is tertiary effluent specified in gb/t 6682-2008.
Embodiment 4
A kind of water-soluble preparation of mixed feed additive Adeps Bovis seu Bubali extract, formic acid 30, ammonia 20, lactic acid 10, acetic acid 10, lemon
Lemon acid 10, propylene glycol 30, Adeps Bovis seu Bubali extract 10.Raw materials used it is food stage.
The preparation method of the water-soluble preparation of above-mentioned Adeps Bovis seu Bubali extract is as follows:
(1) formic acid is placed in stainless steel cauldron (band temperature control)；
(2) ammonia is slowly introducing in formic acid upwards by bottom, and guarantees that temperature is maintained at 60-90 DEG C；Formic acid and ammonia
Reaction forms ammonium formate, forms weak acid-weak acid and mild base salt conjugation buffer solution system with formic acid:
(3), after question response is complete, adds citric acid, lactic acid, acetic acid, dissolving, stir 20-30 minute mix homogeneously；
(4) cool to standing under room temperature；
(5) add Adeps Bovis seu Bubali extract in another reactor；
(6) feed additive propylene glycol is passed through in Adeps Bovis seu Bubali extract；
(7), after mixing completely, the liquid that step (4) is completed, mix homogeneously are added；
(8) filtered using 200 mesh stainless steel filters；
(9) each component content and index, filling and package are checked.
This water-soluble preparation of Adeps Bovis seu Bubali extract can be miscible with water with arbitrary proportion, will not separate out oil bloom or precipitation, have
Good dispersibility.Miscible water is tertiary effluent specified in gb/t 6682-2008.
Embodiment 5
A kind of water-soluble preparation of mixed feed additive Adeps Bovis seu Bubali extract, formic acid 20, ammonia 10, lactic acid 5, acetic acid 5, Fructus Citri Limoniae
Acid 5, propylene glycol 20, Adeps Bovis seu Bubali extract 2.Raw materials used it is food stage.
The preparation method of the water-soluble preparation of above-mentioned Adeps Bovis seu Bubali extract is as follows:
(1) formic acid is placed in stainless steel cauldron (band temperature control)；
(2) ammonia is slowly introducing in formic acid upwards by bottom, and guarantees that temperature is maintained at 60-90 DEG C；Formic acid and ammonia
Reaction forms ammonium formate, forms weak acid-weak acid and mild base salt conjugation buffer solution system with formic acid；
(3), after question response is complete, adds citric acid, lactic acid, acetic acid, dissolving, stir 20-30 minute mix homogeneously；
(4) cool to standing under room temperature；
(5) add Adeps Bovis seu Bubali extract in another reactor；
(6) feed additive propylene glycol is passed through in Adeps Bovis seu Bubali extract；
(7), after mixing completely, the liquid that step (4) is completed, mix homogeneously are added；
(8) filtered using 200 mesh stainless steel filters；
(9) each component content and index, filling and package are checked.
This water-soluble preparation of Adeps Bovis seu Bubali extract can be miscible with water with arbitrary proportion, will not separate out oil bloom or precipitation, have
Good dispersibility.Miscible water is tertiary effluent specified in gb/t 6682-2008.
The present invention passes through to add necessary emulsified component, makes Adeps Bovis seu Bubali extract enter emulsified state, thus being allowed to reach with water
To perfectly miscible state, added by drinking-water, perfection solves adds not enough the asking of mixing homogeneity in inconvenience and powder
Topic.And, add Adeps Bovis seu Bubali extract in drinking-water, can be very good to suppress the growth of microorganism in water, reach cleaning drinking-water, prevent
Only block the effect of waterline, be the developing direction of following drinking water for animals.
A kind of water-soluble preparation of Adeps Bovis seu Bubali extract according to the present invention additionally adds acid ingredient, under sour environment, Adeps Bovis seu Bubali
Carvacrol in extract and thymol can be produced with acid and work in coordination with, and plays more preferable bactericidal action and more preferable food calling effect
Really.
Ultimate principle and principal character and the advantages of the present invention of the present invention have been shown and described above.The technology of the industry
, it should be appreciated that the present invention is not restricted to the described embodiments, the simply explanation described in above-described embodiment and description is originally for personnel
The principle of invention, without departing from the spirit and scope of the present invention, the present invention also has various changes and modifications, these changes
Change and improvement both falls within scope of the claimed invention.Claimed scope by appending claims and its
Equivalent thereof.
Claims (4)
1. the water-soluble preparation of a kind of mixed feed additive Adeps Bovis seu Bubali extract, can be miscible with water with arbitrary proportion, and its feature exists
In being made up of the component of following parts by weight: formic acid 20-30, ammonia 10-20, lactic acid 5-10, acetic acid 5-10, citric acid 5-10,
Propylene glycol 20-30, Adeps Bovis seu Bubali extract 2-10.
2. the water-soluble preparation of mixed feed additive Adeps Bovis seu Bubali extract according to claim 1 is it is characterised in that used former
Material is food stage.
3. mixed feed additive liquid acidity regulator according to claim 1 is it is characterised in that above-mentioned miscible use
Water is tertiary effluent specified in gb/t 6682-2008.
4. a kind of method preparing the water-soluble preparation of Adeps Bovis seu Bubali extract described in any one of claim 1-3 it is characterised in that step such as
Under:
(1) formic acid is placed in stainless steel cauldron；
(2) ammonia is slowly introducing in formic acid upwards by bottom, and guarantees that temperature is maintained at 60-90 DEG C；
(3), after question response is complete, adds citric acid, lactic acid, acetic acid, dissolving, stir 20-30 minute mix homogeneously；
(4) cool to standing under room temperature；
(5) add Adeps Bovis seu Bubali extract in another reactor；
(6) feed additive propylene glycol is passed through in Adeps Bovis seu Bubali extract；
(7), after mixing completely, the liquid that step (4) is completed, mix homogeneously are added；
(8) filtered using 200 mesh stainless steel filters；
(9) each component content and index, filling and package are checked.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610663725.8A CN106343156A (en) | 2016-08-15 | 2016-08-15 | Mixed type feed additive majoram extract water-soluble preparation and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610663725.8A CN106343156A (en) | 2016-08-15 | 2016-08-15 | Mixed type feed additive majoram extract water-soluble preparation and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106343156A true CN106343156A (en) | 2017-01-25 |
Family
ID=57844416
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610663725.8A Pending CN106343156A (en) | 2016-08-15 | 2016-08-15 | Mixed type feed additive majoram extract water-soluble preparation and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106343156A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109430539A (en) * | 2018-12-28 | 2019-03-08 | 潍坊加易加生物科技有限公司 | A kind of silage fermentation promotor and preparation method thereof and its application |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101120758A (en) * | 2007-09-20 | 2008-02-13 | 成都枫澜科技有限公司 | Liquid acidifier and preparation method |
| CN103719562A (en) * | 2013-12-13 | 2014-04-16 | 安徽泰格维生素实业有限公司 | Novel acidifying agent and preparation method thereof |
| CN105616484A (en) * | 2016-01-29 | 2016-06-01 | 黄利文 | Soluble origanum oil premix and preparation method thereof |
-
2016
- 2016-08-15 CN CN201610663725.8A patent/CN106343156A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101120758A (en) * | 2007-09-20 | 2008-02-13 | 成都枫澜科技有限公司 | Liquid acidifier and preparation method |
| CN103719562A (en) * | 2013-12-13 | 2014-04-16 | 安徽泰格维生素实业有限公司 | Novel acidifying agent and preparation method thereof |
| CN105616484A (en) * | 2016-01-29 | 2016-06-01 | 黄利文 | Soluble origanum oil premix and preparation method thereof |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109430539A (en) * | 2018-12-28 | 2019-03-08 | 潍坊加易加生物科技有限公司 | A kind of silage fermentation promotor and preparation method thereof and its application |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN104642259B (en) | A kind of livestock and poultry ecological cultivation method and livestock and poultry product | |
| CN105175166A (en) | Fertilizer special for organic tea and preparing method of fertilizer | |
| CN106912697A (en) | A kind of deodorant pig feed and preparation method thereof | |
| CN104472865A (en) | Method for preparing silage | |
| CN107473868A (en) | A kind of tealeaves upgrading synergy organic-inorganic set meal fertilizer and preparation method thereof | |
| CN102008009A (en) | Ferment feed synergist and preparation method thereof | |
| DE3024076A1 (en) | METHOD FOR PRODUCING A PREPARATION CONTAINING MINERALS | |
| CN101112221B (en) | Chinese herbal medicine feed additive for accelerating the growth of animals and use method thereof | |
| CN105981936A (en) | Production methods of dairy cow selenium-enriched feed and selenium-enriched milk | |
| CN102731184A (en) | Method for preparing base fertilizer for sweet-scented osmanthus fragrant Chinese chestnut tree | |
| CN107173571A (en) | One boar food | |
| CN101744346A (en) | Natural food preservative taking pine needle as raw material and preparation method thereof | |
| CN105379966B (en) | A kind of water-soluble allicin mixture and preparation method thereof | |
| CN104150989B (en) | Utilize the method that feces of livestock and poultry makes compost | |
| CN106343156A (en) | Mixed type feed additive majoram extract water-soluble preparation and preparation method thereof | |
| CN103005146A (en) | Production method of captive Tibetan chicken manure fermentation feed | |
| CN103483054A (en) | Multifunctional composite fertilizer for preventing and treating vegetable death and preparation method thereof | |
| CN107056441A (en) | A kind of preparation method of the bio-feritlizer containing willow leaf | |
| CN107827513A (en) | A kind of preparation method of the water-soluble fertilizer containing amino acid | |
| KR101834749B1 (en) | Manufacturing Method of Animal Feed Additives Comprising Artemisia Capillaris, Houttuynia Cordata, and Perilla Frutescens | |
| CN107056536A (en) | A kind of bio-fertilizer containing ferment residue and preparation method thereof | |
| CN106748379A (en) | A kind of method that bamboo shoots waste water produces Liquid Fertilizer | |
| CN106472692A (en) | A kind of preparation of acidified with citric acid milk powder and application process | |
| CN105622295A (en) | Organic fertilizer and preparing method thereof | |
| CN106417918A (en) | Livestock and poultry additive containing selenium and EM probiotics and application of additive |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20170125 |
|
| RJ01 | Rejection of invention patent application after publication |