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CN106174683B - A kind of composition and the tobacco juice for electronic smoke containing said composition - Google Patents

A kind of composition and the tobacco juice for electronic smoke containing said composition Download PDF

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Publication number
CN106174683B
CN106174683B CN201610609456.7A CN201610609456A CN106174683B CN 106174683 B CN106174683 B CN 106174683B CN 201610609456 A CN201610609456 A CN 201610609456A CN 106174683 B CN106174683 B CN 106174683B
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percent
tea
wuyi
extract
composition
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CN106174683A (en
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陈群
李斌
陈小明
伊勇涛
操晓亮
蓝洪桥
张峰
向晨
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China Tobacco Fujian Industrial Co Ltd
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China Tobacco Fujian Industrial Co Ltd
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    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/10Chemical features of tobacco products or tobacco substitutes
    • A24B15/16Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/18Treatment of tobacco products or tobacco substitutes
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00Essential oils; Perfumes
    • C11B9/02Recovery or refining of essential oils from raw materials

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Tea And Coffee (AREA)
  • Medicines Containing Plant Substances (AREA)
  • Cosmetics (AREA)

Abstract

The present invention, which provides a kind of composition and the tobacco juice for electronic smoke containing said composition, the composition, to be included:1~4 part of Wuyi cliff tea essential oil, such as 2~3 parts;5~10 parts of Wuyi cliff tea alcohol extract;Such as 7~8 parts;5~12 parts of Wuyi cliff tea water extract;Such as 8~10 parts.Electronic cigarette is used for the tobacco juice for electronic smoke that said composition configures, electronic cigarette is not only had clear and upright far away, mellow fragrant Wuyi cliff tea odor characteristic, and also fragrance enriches coordination, and it is fine and smooth soft, there is preferable plumpness and thick and solid property.

Description

Composition and electronic cigarette liquid containing same
Technical Field
The invention belongs to the technical field of electronic cigarettes, and particularly relates to a composition and electronic cigarette liquid containing the same.
Background
An electronic cigarette is an electronic transmission device that transmits fragrance, nicotine, and the like to the respiratory system by an electronic heating means. As a substitute for the conventional cigarette, the electronic cigarette is very similar to the conventional cigarette in appearance. It simulates the taste of cigarette, but has no ash, no tip, no burning, no open fire and very low harmful matter content.
The electronic cigarette mainly comprises a smoking set and a cartridge, wherein the cartridge is loaded with tobacco juice, and the smoking set atomizes the tobacco juice to generate smoking effect. The electronic cigarette liquid is mainly a product prepared by blending various flavors and fragrances, although the smoke generated by the electronic cigarette liquid has a gap with the real smoking feeling of cigarettes in the aspects of fragrance, taste and the like.
CN104087415A discloses an electronic cigarette liquid with grape flavor and a preparation method thereof. The grape-flavored electronic cigarette liquid is prepared by uniformly mixing propylene glycol, glycerol, 1, 3-butanediol, xylitol liquid, grape juice concentrated solution, edible grape formula essence and the like according to a proportion; wherein the grape juice concentrated solution is obtained by squeezing, extracting, and concentrating by rotary evaporation under reduced pressure; the grape-flavored electronic cigarette liquid comprises the following components in parts by weight: 1-80 parts of propylene glycol, 1-60 parts of glycerol, 1-50 parts of 1, 3-butanediol, 1-30 parts of xylitol solution, 5-10 parts of grape juice concentrated solution and 0.1-2 parts of edible grape formula essence.
Disclosure of Invention
The invention creatively adopts the processes of distillation, alcohol extraction, water extraction and the like to obtain the Wuyi rock tea extract from the Wuyi rock tea, and further prepares the Wuyi rock tea extract into a composition containing the Wuyi rock tea extract by the technologies of compounding, flavor blending, flavor imitation and the like, and further prepares the Wuyi rock tea essence. The composition containing the Wuyi rock tea extract and the Wuyi rock tea essence are applied to electronic cigarette liquid, and the aroma style and the aroma characteristics of the Wuyi rock tea can be integrated into the electronic cigarette liquid, so that the electronic cigarette is endowed with the Wuyi rock tea aroma characteristics of being clear, long-lasting, mellow and fragrant.
An object of the present invention is to obtain a composition, and another object of the present invention is to obtain a Wuyi rock tea essence having the characteristic of Wuyi rock tea aroma. Still another object of the present invention is to obtain an electronic cigarette liquid with the characteristic of wuyi rock tea aroma.
The present invention provides in a first aspect a composition comprising, by weight:
1-4 parts, such as 2-3 parts, of Wuyi rock tea essential oil;
5-10 parts of Wuyi cliff tea alcohol extract; for example, 7 to 8 parts;
5-12 parts of Wuyi rock tea water extract; for example, 8 to 10 parts; wherein,
the Wuyi rock tea essential oil is prepared by the following steps a1) to a 2):
a1) distilling Wuyi rock tea with water vapor, collecting distillate,
a2) performing oil-water separation on the distillate to obtain an oil phase which is the Wuyi rock tea essential oil;
the Wuyi cliff tea alcohol extract is prepared by the following steps b1) to b 2):
b1) mixing the residue of WUYIYAN tea and/or WUYIYAN tea with ethanol or ethanol water solution, extracting under reflux at 60-70 deg.C for 1-2 hr, filtering to obtain ethanol extractive solution,
optionally, repeating the above extraction steps once for the residue after filtration, then combining the ethanol extractive solutions obtained by two extractions,
b2) distilling the ethanol extract under reduced pressure, wherein the vacuum degree of the reduced pressure distillation is 40-60 mbar, the temperature of the reduced pressure distillation is 45-55 ℃, and the obtained distillation residue is the Wuyi rock tea alcohol extract;
the Wuyi rock tea aqueous extract is prepared by the following steps c1) to c 2):
c1) mixing the Wuyi rock tea leaves and/or residues left after extraction of the Wuyi rock tea with water according to the weight ratio of 1: 8-10, carrying out hot reflux extraction at the extraction temperature of 80-90 ℃ for 1-2h, then filtering to obtain a water extract,
optionally, repeating the extraction step once for the residue remaining after filtration, and then combining the water extracts obtained twice,
c2) and distilling the water extract under reduced pressure, wherein the vacuum degree of the reduced pressure distillation is 40-60 mbar, the temperature of the reduced pressure distillation is 50-60 ℃, and the obtained distillation residue is the water extract of the Wuyi rock tea.
In one embodiment, the composition of any of the present invention, wherein step a1) or a2) has one or more of the following characteristics:
in step a1), steam distillation is water distillation;
in the step a1), the temperature of steam is 102-110 ℃ in the steam distillation process;
in the step a1), the time of steam distillation is 2-3 h;
in the step a1), the output speed of distillate is 20-40 parts by weight per hour for every 100-200 parts by weight of Wuyi rock tea;
in the step a2), performing oil-water separation on the distillate through an oil-water separator;
in the step a2), the yield of the Wuyi rock tea essential oil is 0.005-0.01 wt%.
In one embodiment, the composition of any of the present invention, wherein step b1) or b2) has one or more of the following characteristics:
in the step b1), mixing the Wuyi rock tea leaves and/or residues left after extraction of the Wuyi rock tea with ethanol or ethanol water solution according to the weight ratio of 1: 8-10;
the concentration of the ethanol aqueous solution in the step b1) is 90-99 wt%;
in the step b2), the density of the alcohol extract of the Wuyi rock tea is 1.05-1.10 g/cm3
In the step b2), the yield of the alcohol extract of the Wuyi rock tea is 10-15 wt%.
In one embodiment, the composition of any of the present invention, wherein step c1) or c2) has one or more of the following characteristics:
in the step c1), mixing the Wuyi rock tea leaves and/or residues left after extraction of the Wuyi rock tea with water according to the weight ratio of 1: 8-10;
in the step c2), the density of the Wuyi rock tea aqueous extract is 1.00-1.10g/cm 3;
in the step c2), the yield of the Wuyi rock tea water extract is 10-15 wt%.
In one embodiment, the composition of any one of the present invention, wherein the residue after extraction of wuyiyan tea is: preparing the solid residue of Wuyi cliff tea left after Wuyi cliff tea essential oil preparation, the solid residue of Wuyi cliff tea left after Wuyi cliff tea alcohol extract preparation or the solid residue of Wuyi cliff tea left after Wuyi cliff tea water extract preparation.
In one embodiment, the composition of any one of the present invention, wherein the wuyi yan tea is one or more varieties of tea selected from dahongpao, mingxia, cinnamon, narcissus, chia;
preferably, the Wuyi Yancha includes tea of cinnamon variety and tea of at least one of dahongpao, Mingxiang, narcissus and Qizhong;
preferably, the Wuyi rock tea is a cinnamon variety tea.
The second aspect of the invention provides a Wuyi rock tea essence which comprises the composition and formula essence of any one of the invention;
the formula essence consists of the following substances in percentage by weight: 0.3 to 0.7 percent of acetic acid, 0.5 to 1.5 percent of phenylacetic acid, 0.3 to 0.7 percent of ethyl laurate, 0.1 to 0.3 percent of cinnamyl cinnamate, 0.03 to 0.07 percent of geranyl acetate, 0.3 to 0.7 percent of citronellyl acetate, 0.05 to 0.15 percent of linalool, 0.03 to 0.07 percent of heliotropin, 0.1 to 0.3 percent of cinnamyl alcohol, 0.3 to 0.7 percent of farnesol, 0.01 to 0.02 percent of maltol, 0.03 to 0.07 percent of ethyl maltol, 0.03 to 0.07 percent of furanone, 0.03 to 0.07 percent of megastigmatrienone, 0.01 to 0.02 percent of 2, 5-dimethyl pyrazine, 0.01 to 0.03 percent of 2-acetyl pyrazine, 2,3, 5-trimethyl pyrazine, 0.03 to 0.07 percent of lemon oil, 0.01 to 0.03 percent of sweet orange oil, 0.7 percent of peruvian apple juice, 2.3 to 2 percent of apple juice extract, 3 to 2 percent of cinnamon extract, 3 to 0.07 percent of cinnamon extract, 2 to 2 percent of liquorice extract, 3 percent of cinnamon extract, 2 to 0.3 percent of cinnamon extract, 2, 0.3 to 0.7 percent of benzoin paste, 20 to 30 percent of propylene glycol and the balance of ethanol water solution (such as ethanol water solution with the ethanol concentration of 50 to 95 percent by weight);
preferably, the weight ratio of the composition to the formula essence is 10-25: 6-8, preferably 15-20: 6-8.
In one embodiment, the wuyiyan tea flavor of any one of the present inventions, wherein the formula flavor consists of the following materials in weight percentage: 0.4 to 0.6 percent of acetic acid, 0.8 to 1.2 percent of phenylacetic acid, 0.4 to 0.6 percent of ethyl laurate, 0.1 to 0.3 percent of cinnamyl cinnamate, 0.04 to 0.06 percent of geranyl acetate, 0.4 to 0.6 percent of citronellyl acetate, 0.08 to 0.12 percent of linalool, 0.04 to 0.06 percent of heliotropin, 0.1 to 0.3 percent of cinnamyl alcohol, 0.4 to 0.6 percent of farnesol, 0.01 to 0.02 percent of maltol, 0.04 to 0.06 percent of ethyl maltol, 0.04 to 0.06 percent of furanone, 0.04 to 0.06 percent of megastigmatrienone, 0.01 to 0.03 percent of 2, 5-dimethyl pyrazine, 0.01 to 0.03 percent of 2-acetyl pyrazine, 2,3, 5-trimethyl pyrazine, 0.04 to 0.06 percent of lemon oil, 0.01 to 0.03 percent of sweet orange oil, 0.6 percent of secret orange oil, 1 to 2 percent of apple juice, 1 to 3 percent of apple juice extract, 1 to 1 percent of 1 to 0.6 percent of cinnamon extract, 1 to 0.06 percent of liquorice extract, 1 to 0.4 percent of cinnamon extract, 1 to 0.06 percent, 0.4-0.6% of benzoin paste, 20-30% of propylene glycol and the balance of ethanol (for example, ethanol solution with the ethanol concentration of 50-99 wt%).
In a third aspect, the invention provides a composition according to any one of the invention, or a wuyiyan tea flavor according to any one of the invention, for use in flavoring a cigarette or an electronic cigarette.
The fourth aspect of the invention provides an electronic cigarette liquid containing the composition of any one of the invention or the wuyiyan tea essence of any one of the invention.
In one embodiment, the electronic cigarette liquid of any of the present inventions further comprises an electronic cigarette liquid adjuvant;
preferably, the electronic cigarette liquid auxiliary material is one or more selected from the following substances: glycerol, propylene glycol, ethanol water solution (the concentration is preferably 60-80 weight percent), diethylene glycol, triethylene glycol, sorbitol, tobacco extract and nicotine;
preferably, each 100 parts of the electronic cigarette liquid contains 20-50 parts of Wuyi rock tea essence, 5-10 parts of glycerol and the balance of propylene glycol.
The fifth aspect of the invention provides an electronic cigarette, or an electronic cigarette cartridge, containing the electronic cigarette liquid according to any one of the invention.
In the present invention, unless otherwise specified, the ethanol solution is an aqueous ethanol solution, and the concentration thereof is a weight% concentration.
In one embodiment, the wuyi rock tea is the wuyi rock tea specified in GBT 18745-.
In one embodiment, the Wuyi cliff tea is one or more selected from the group consisting of clovershrub, Minabies, cinnamon, narcissus, chia, preferably cinnamon.
In one embodiment, the wuyiyan tea is finished wuyiyan tea (tea subjected to the whole tea making process) or a tea process processed in one or more steps during the tea making process, such as a green-making or green-removing product of wuyiyan tea green.
In one embodiment, the wuyiyan tea extract is wuyiyan tea essential oil, wuyiyan tea alcohol extract, and/or wuyiyan tea water extract.
Accordingly, the present invention may provide one or more of the following advantages:
(1) the composition containing the Wuyi rock tea extract has the fragrance characteristics of Wuyi rock tea, has pure and long fragrance, is mellow and fragrant, and is particularly suitable for flavoring cigarettes/electronic cigarettes;
(2) the composition containing the Wuyi rock tea extract is reasonably compounded with the formula essence, so that the Wuyi rock tea essence has pure and long-lasting fragrance and is mellow and fragrant, and is particularly suitable for flavoring cigarettes/electronic cigarettes;
(3) the composition containing the Wuyi rock tea extract or the Wuyi rock tea essence is used for flavoring the electronic cigarette, not only endows the electronic cigarette with the characteristics of pure and long-lasting and mellow and fragrant Wuyi rock tea fragrance, but also enriches and coordinates the fragrance of the electronic cigarette, ensures that the cigarette fragrance is fine and soft during smoking, has better fullness and thickness, and obviously improves the smoking quality and the sensory comfort of the electronic cigarette.
Detailed Description
The technical solution of the present invention is further described in detail by the following examples. The exemplary embodiments of the present invention and the description thereof are provided for the purpose of explanation and are not to be construed as limiting the invention.
The formulations/fragrances used in the following examples and comparative examples are supplied by Huabao formulation fragrance (Shanghai) Co., Ltd.
The wuyiyan tea extracts (wuyiyan tea essential oil, wuyiyan tea alcohol extract and wuyiyan tea water extract) in the following examples and comparative examples were prepared by the following methods:
a) preparing Wuyi rock tea essential oil:
steam distilling Wuyi rock tea (Cinnamomum cassia) with steam distilling kettle. The lower part of the steam distillation kettle is provided with a steam inlet, the upper part of the steam distillation kettle is provided with a steam outlet, and perforated sieve plates for placing the to-be-distilled substance and penetrating steam are arranged in the steam distillation kettle and between the steam inlet and the steam outlet. 200kg of Wuyi rock tea is placed on a sieve plate of a steam distillation kettle, steam (with the temperature of about 102-110 ℃) enters the distillation kettle from the lower part of the distillation kettle, fully contacts with the Wuyi rock tea through the sieve plate, is led out from a steam outlet at the upper part, is condensed by a condenser and is collected, and the collected distillate is obtained. The temperature of the condenser is-5-10 ℃, the distilling speed of the distillate is 20-40 Kg/h, and the distilling time is 2-3 h. And (3) separating oil and water of the distillate from an oil-water separator to obtain an oil phase, namely the Wuyi rock tea essential oil. The yield of the essential oil is 0.005-0.01 wt%.
b) Preparing alcohol extract of Wuyi cliff tea:
b1) mixing the solid residue of Wuyi cliff tea left after preparing Wuyi cliff tea essential oil with 95 wt% ethanol according to the weight ratio of 1:10, carrying out hot reflux extraction at the extraction temperature of 60-70 ℃ for 1-2h, and then filtering to obtain an ethanol extract; repeating the above extraction steps once for the residue after filtration, and then combining the ethanol extract obtained by the two extractions;
b2) and distilling the ethanol extract under reduced pressure, wherein the vacuum degree (absolute pressure) of the reduced pressure distillation is 40-60 mbar, the temperature of the reduced pressure distillation is 45-55 ℃, and the obtained distillation residue is the Wuyi rock tea alcohol extract. The yield of the Wuyi rock tea alcohol extract is 10-15 wt%.
c) Preparing the Wuyi rock tea water extract:
c1) mixing the solid residue of Wuyi cliff tea left after preparing the Wuyi cliff tea alcohol extract with water according to the weight ratio of 1:10, carrying out hot reflux extraction at the extraction temperature of 80-90 ℃ for 1-2h, and then filtering to obtain a water extract; repeating the above extraction steps once for the residue after filtration, and then combining the water extract obtained by the two extractions;
c2) and distilling the water extract under reduced pressure, wherein the vacuum degree of the reduced pressure distillation is 40-60 mbar, the temperature of the reduced pressure distillation is 50-60 ℃, and the obtained distillation residue is the water extract of the Wuyi rock tea. The yield of Wuyi rock tea water extract is 10-15 wt%.
(II) the formula essence in the following examples consists of the following substances in percentage by weight: 0.50% of acetic acid, 1.00% of phenylacetic acid, 0.50% of ethyl laurate, 0.20% of lauryl cinnamate, 0.05% of geranyl acetate, 0.50% of citronellyl acetate, 0.10% of linalool, 0.05% of heliotropin, 0.20% of cinnamyl alcohol, 0.50% of farnesol, 0.01% of maltol, 0.05% of ethyl maltol, 0.05% of furanone, 0.05% of megastigmatrienone, 0.01% of 2, 5-dimethylpyrazine, 0.02% of 2-acetylpyrazine, 0.05% of 2,3, 5-trimethylpyrazine, 0.02% of lemon oil, 0.50% of sweet orange oil, 1.50% of apple juice, 2.50% of hawthorn tincture, 1.50% of Yunyan extract, 3.50% of Zimbabwe extract, 1.50% of licorice extract, 0.50% of Peru extract, 0.50% of benzoin extract, 25.00% of propylene glycol, and the balance of an aqueous. The substances are mixed according to a certain proportion and stirred for 30min at normal temperature, so that the components are fully and uniformly mixed to obtain the formula essence.
(III) examples 1 to 6 and comparative examples 1 to 3
Examples 1 to 6 include:
1. the composition containing the Wuyi cliff tea extract is prepared by mixing and proportioning the Wuyi cliff tea essential oil, the Wuyi cliff tea alcohol extract and the Wuyi cliff tea water extract to obtain the composition α 1- α 5.
2. The proportion of the Wuyi rock tea essence is that the composition is compounded with the formula essence to obtain the Wuyi rock tea essence β 1- β 5 with the characteristics of the Wuyi rock tea essence.
3. The electronic cigarette liquid is prepared by mixing the Wuyi rock tea essence β 1- β 5 with electronic cigarette liquid auxiliary materials (propylene glycol and glycerol) to obtain electronic cigarette liquid A1-A5, and mixing the composition β 5 with the electronic cigarette liquid auxiliary materials (propylene glycol and glycerol) to obtain electronic cigarette liquid A6.
Comparative examples 1 to 4 include:
1. mixing the Wuyi rock tea essence formula, the formula essence and electronic cigarette liquid auxiliary materials (propylene glycol and glycerol) to obtain the electronic cigarette liquid B1.
2. Mixing the Wuyi rock tea essential oil with electronic cigarette auxiliary materials (propylene glycol and glycerol) to obtain electronic cigarette liquid B2.
3. And mixing the formula essence with the electronic cigarette auxiliary materials (propylene glycol and glycerol) to obtain the electronic cigarette liquid B3.
The composition, the Wuyi rock tea essence and the electronic cigarette liquid contained in the embodiment are sequentially shown in the following tables 1-3:
TABLE 1 composition containing extract of WUYIYANCHA
Containing a composition Wuyi rock tea essential oil Wuyi rock tea alcohol extract Wuyi rock tea water extract
α1 1.5 5.5 7.1
α2 2.5 8.5 11.0
α3 1.0 4.5 5.5
α4 2.0 7.0 9.5
α5 2.0 7.5 9.0
Unit: parts by weight
TABLE 2 Wuyi rock tea essence
Unit: parts by weight
TABLE 3 electronic cigarette liquid
Unit: by weight%
(IV) evaluation of sensory quality
The electronic cigarette tobacco liquids A1-A6 of examples 1-6 and the electronic cigarette tobacco liquids B1-B3 of comparative examples 1-3 were added to electronic cigarettes for sensory quality evaluation. The sensory quality evaluation method of the electronic cigarette adopts GB 5606.4-2005 part IV of cigarettes: the evaluation method of sensory technical requirements was found to have an evaluation index of "gloss" of 11 persons, and the specific evaluation results are shown in table 4.
TABLE 4 sensory quality evaluation results
As can be seen from table 4, the electronic cigarette liquids a 1-a 6 have significantly improved aroma, coordination, miscellaneous odor, irritation, and aftertaste, higher sensory quality scores, and improved smoking quality and sensory comfort, as compared with the electronic cigarette liquids B1-B3.
The sensory quality evaluation result of the electronic cigarette liquid shows that: the electronic cigarette liquid A1-A6 is used for electronic cigarettes, so that the electronic cigarettes are endowed with the characteristics of being clear, long-lasting, mellow and fragrant Wuyi rock tea fragrance, and the electronic cigarettes have good fragrance, coordination, miscellaneous gas, irritation and aftertaste during smoking, and good smoking quality and sensory comfort. Particularly, the electronic cigarette liquid A5 has the most abundant, coordinated, fine and soft aroma, better fullness and thickness, more comfortable mouthfeel and highest sensory evaluation score.
In contrast, the formula of the wuyiyan tea extract of the electronic cigarette liquid B1 is different from the formula of the electronic cigarette liquid B1, and the sensory quality evaluation score is low; the electronic cigarette liquid B2 and B3 only contain Wuyi rock tea essential oil and formula essence respectively, the fragrance is slightly thin, the miscellaneous gas is slightly high, and the sensory quality evaluation score is low.
Accordingly, the above-described embodiments of the present invention may have one or more of the following advantages:
(1) the composition containing the Wuyi rock tea extract has the fragrance characteristics of Wuyi rock tea, has pure and long fragrance, is mellow and fragrant, and is particularly suitable for flavoring cigarettes/electronic cigarettes;
(2) the composition containing the Wuyi rock tea extract is reasonably compounded with the formula essence, so that the Wuyi rock tea essence has pure and long-lasting fragrance and is mellow and fragrant, and is particularly suitable for flavoring cigarettes/electronic cigarettes;
(3) the composition containing the Wuyi rock tea extract or the Wuyi rock tea essence is used for flavoring the electronic cigarette, not only endows the electronic cigarette with the characteristics of pure and long-lasting and mellow and fragrant Wuyi rock tea fragrance, but also enriches and coordinates the fragrance of the electronic cigarette, ensures that the cigarette fragrance is fine and soft during smoking, has better fullness and thickness, and obviously improves the smoking quality and the sensory comfort of the electronic cigarette.
Finally, it should be noted that: the above examples are only intended to illustrate the technical solution of the present invention and not to limit it; although the present invention has been described in detail with reference to preferred embodiments, those skilled in the art will understand that: modifications to the specific embodiments of the invention or equivalent substitutions for parts of the technical features may be made; without departing from the spirit of the present invention, it is intended to cover all aspects of the invention as defined by the appended claims.

Claims (27)

1. A composition comprising an extract of WUYIYANCHA comprising, by weight:
1-4 parts of Wuyi rock tea essential oil;
5-10 parts of Wuyi cliff tea alcohol extract;
5-12 parts of Wuyi rock tea water extract; wherein,
the Wuyi rock tea essential oil is prepared by the following steps a1) to a 2):
a1) performing steam distillation on the distilled Wuyi rock tea, collecting distillate, and performing water distillation on the distillate;
a2) performing oil-water separation on the distillate to obtain an oil phase which is the Wuyi rock tea essential oil;
the Wuyi cliff tea alcohol extract is prepared by the following steps b1) to b 2):
b1) mixing the residue of WUYIYAN tea and/or WUYIYAN tea with ethanol or ethanol water solution, extracting under reflux at 60-70 deg.C for 1-2 hr, filtering to obtain ethanol extractive solution,
b2) distilling the ethanol extract under reduced pressure, wherein the vacuum degree of the reduced pressure distillation is 40-60 mbar, the temperature of the reduced pressure distillation is 45-55 ℃, and the obtained distillation residue is the Wuyi rock tea alcohol extract;
the Wuyi rock tea aqueous extract is prepared by the following steps c1) to c 2):
c1) mixing the Wuyi rock tea leaves and/or residues left after extraction of the Wuyi rock tea with water according to the weight ratio of 1: 8-10, carrying out hot reflux extraction at the extraction temperature of 80-90 ℃ for 1-2h, then filtering to obtain a water extract,
c2) and distilling the water extract under reduced pressure, wherein the vacuum degree of the reduced pressure distillation is 40-60 mbar, the temperature of the reduced pressure distillation is 50-60 ℃, and the obtained distillation residue is the water extract of the Wuyi rock tea.
2. The composition of claim 1, wherein step b1) comprises repeating the above extraction steps once for the residue remaining after filtration, and then combining the ethanol extracts obtained from the two extractions.
3. The composition according to claim 1, step c1) comprising repeating the extraction step once for the residue remaining after filtration and then combining the aqueous extracts obtained in two steps.
4. The composition according to any one of claims 1 to 3, wherein the Wuyi rock tea essential oil is 2 to 3 parts.
5. The composition according to any one of claims 1 to 3, wherein the Wuyi cliff tea alcohol extract is 7 to 8 parts.
6. The composition according to any one of claims 1 to 3, wherein the Wuyi mountain rock tea aqueous extract is 8 to 10 parts.
7. The composition of any one of claims 1 to 3, wherein the step a1) or a2) is characterized by one or more of the following features:
in the step a1), the temperature of steam is 102-110 ℃ in the steam distillation process;
in the step a1), the time of steam distillation is 2-3 h;
in the step a1), the output speed of distillate is 20-40 parts by weight per hour for every 100-200 parts by weight of Wuyi rock tea;
in the step a2), performing oil-water separation on the distillate through an oil-water separator;
in the step a2), the yield of the Wuyi rock tea essential oil is 0.005-0.01 wt%.
8. The composition of any one of claims 1 to 3, wherein step b1) or b2) is characterized by one or more of the following:
in the step b1), mixing the Wuyi rock tea leaves and/or residues left after extraction of the Wuyi rock tea with ethanol or ethanol water solution according to the weight ratio of 1: 8-10;
the concentration of the ethanol aqueous solution in the step b1) is 90-99 wt%;
in the step b2), the density of the alcohol extract of the Wuyi rock tea is 1.05-1.10 g/cm3
In the step b2), the yield of the alcohol extract of the Wuyi rock tea is 10-15 wt%.
9. The composition of any one of claims 1 to 3, wherein step c1) or c2) is characterized by one or more of the following:
in the step c1), mixing the Wuyi rock tea leaves and/or residues left after extraction of the Wuyi rock tea with water according to the weight ratio of 1: 8-10;
in the step c2), the density of the Wuyi rock tea aqueous extract is 1.00-1.10g/cm 3;
in the step c2), the yield of the Wuyi rock tea water extract is 10-15 wt%.
10. The composition according to any one of claims 1 to 3, wherein the residue after extraction of Wuyi mountain tea is: preparing the solid residue of Wuyi cliff tea left after Wuyi cliff tea essential oil preparation, the solid residue of Wuyi cliff tea left after Wuyi cliff tea alcohol extract preparation or the solid residue of Wuyi cliff tea left after Wuyi cliff tea water extract preparation.
11. The composition according to any one of claims 1 to 3, wherein the Wuyi Yancha is one or more selected from Dahongpao, Ming fir, cinnamon, narcissus and Qizhong tea.
12. The composition of claim 11, wherein the Wuyi Yancha comprises a cinnamon variety of Camellia sinensis and at least one of Dahongpao, Ming fir, Narcissus tazetta, and Qizhong variety of Camellia sinensis.
13. The composition of claim 11, wherein the Wuyi rock tea is a cinnamon variety tea
14. A wuyiyan tea flavor comprising the composition of any one of claims 1 to 13 and a formula flavor;
the formula essence consists of the following substances in percentage by weight: 0.3 to 0.7 percent of acetic acid, 0.5 to 1.5 percent of phenylacetic acid, 0.3 to 0.7 percent of ethyl laurate, 0.1 to 0.3 percent of cinnamyl cinnamate, 0.03 to 0.07 percent of geranyl acetate, 0.3 to 0.7 percent of citronellyl acetate, 0.05 to 0.15 percent of linalool, 0.03 to 0.07 percent of heliotropin, 0.1 to 0.3 percent of cinnamyl alcohol, 0.3 to 0.7 percent of farnesol, 0.01 to 0.02 percent of maltol, 0.03 to 0.07 percent of ethyl maltol, 0.03 to 0.07 percent of furanone, 0.03 to 0.07 percent of megastigmatrienone, 0.01 to 0.02 percent of 2, 5-dimethyl pyrazine, 0.01 to 0.03 percent of 2-acetyl pyrazine, 2,3, 5-trimethyl pyrazine, 0.03 to 0.07 percent of lemon oil, 0.01 to 0.03 percent of sweet orange oil, 0.7 percent of peruvian apple juice, 2.3 to 2 percent of apple juice extract, 3 to 2 percent of cinnamon extract, 3 to 0.07 percent of cinnamon extract, 2 to 2 percent of liquorice extract, 3 percent of cinnamon extract, 2 to 0.3 percent of cinnamon extract, 2, 0.3 to 0.7 percent of benzoin paste, 20 to 30 percent of propylene glycol and the balance of ethanol water solution.
15. The wuyiyan tea flavor according to claim 14, wherein the ethanol aqueous solution is an ethanol aqueous solution having an ethanol concentration of 50 to 95% by weight.
16. The wuyiyan tea flavor according to claim 14, wherein the weight ratio of the composition to the formula flavor is 10-25: 6-8.
17. The Wuyi rock tea essence according to claim 14, wherein the weight ratio of the composition to the formula essence is 15-20: 6-8.
18. The wuyiyan tea flavor according to claim 14, wherein the formula is composed of the following materials in weight percent: 0.4 to 0.6 percent of acetic acid, 0.8 to 1.2 percent of phenylacetic acid, 0.4 to 0.6 percent of ethyl laurate, 0.1 to 0.3 percent of cinnamyl cinnamate, 0.04 to 0.06 percent of geranyl acetate, 0.4 to 0.6 percent of citronellyl acetate, 0.08 to 0.12 percent of linalool, 0.04 to 0.06 percent of heliotropin, 0.1 to 0.3 percent of cinnamyl alcohol, 0.4 to 0.6 percent of farnesol, 0.01 to 0.02 percent of maltol, 0.04 to 0.06 percent of ethyl maltol, 0.04 to 0.06 percent of furanone, 0.04 to 0.06 percent of megastigmatrienone, 0.01 to 0.03 percent of 2, 5-dimethyl pyrazine, 0.01 to 0.03 percent of 2-acetyl pyrazine, 2,3, 5-trimethyl pyrazine, 0.04 to 0.06 percent of lemon oil, 0.01 to 0.03 percent of sweet orange oil, 0.6 percent of secret orange oil, 1 to 2 percent of apple juice, 1 to 3 percent of apple juice extract, 1 to 1 percent of 1 to 0.6 percent of cinnamon extract, 1 to 0.06 percent of liquorice extract, 1 to 0.4 percent of cinnamon extract, 1 to 0.06 percent, 0.4-0.6% of benzoin paste, 20-30% of propylene glycol and the balance of ethanol.
19. Use of a composition according to any one of claims 1 to 13 for perfuming a cigarette or e-cigarette.
20. The wuyiyan tea flavor of any one of claims 14 to 18, for use in flavoring a cigarette or e-cigarette.
21. An electronic cigarette liquid containing the composition of any one of claims 1 to 13 or the wuyiyan tea flavor of claims 14 to 18.
22. The e-cigarette liquid of claim 21, further comprising an e-cigarette liquid adjunct.
23. The e-cigarette liquid of claim 22, the e-cigarette liquid accessory being one or more selected from the group consisting of: glycerol, propylene glycol, ethanol water solution, diethylene glycol, triethylene glycol, sorbitol, tobacco extract, and nicotine.
24. The e-cigarette liquid of claim 23, wherein the aqueous ethanol solution has a concentration of 60-80 wt.%.
25. The electronic cigarette liquid of claim 22, wherein per 100 parts by weight of the electronic cigarette liquid comprises 20-50 parts by weight of Wuyi mountain rock tea essence, 5-10 parts by weight of glycerol and the balance of propylene glycol
26. An electronic cigarette comprising the electronic cigarette liquid of any one of claims 21 to 25.
27. An electronic cigarette cartridge containing the electronic cigarette liquid of any one of claims 21 to 25.
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