CN106165965B - A kind of nano-negative ion bristle and preparation process - Google Patents

Abstract

The invention discloses a kind of nano-negative ion bristle and preparation processes, calculate by weight, including following component thermoplastic polyester granulate, and 25 grams to 60 grams；Nanometer anion powder solution, 19 grams to 30 grams；Couplant, 1.5 grams to 10 grams；Nano-magnetic powder, 1.5 grams to 5 grams；Coral nano powder, 1.5 grams to 2 grams；Nano pearl powder, 1.5 grams to 3 grams.Preparation process of the invention is simple, it is cheap, it is proved by statistics, antibacterial effect of the invention has antibacterial effect of 99% or more a possibility that higher than normal bristles, have the function of to promote blood circulation, stimulate cytothesis, anti-aging etc. to the skin of human body, economic value is high.

Description

A kind of nano-negative ion bristle and preparation process

Technical field

The present invention relates to bristle preparation process, prescription, antimicrobial technology field more particularly to a kind of nano-negative ion bristle and Preparation process.

Background technique

Nanometer anion powder is to pass through nanotechnology elaborate by natural material.Scientific investigations showed that nano-negative ion Powder keeps energetic to human body and has great help to the improvement of human residential environment.

Nano-negative ion gram has good effect, also has good effect especially for health care, beauty treatment fields.? Hairbrush used in the field of cleaning chemical products such as beauty, face cleaning, beauty treatment fields, due to direct and human body skin contact, matter Amount and skin effect, health effect, health-care effect, it is just most important for user, when hairbrush is used for a long time, or even can be to trouble Person causes subtle influence, and existing hairbrush, antibacterial ability are weaker, which solves.

Summary of the invention

A kind of nano-negative ion bristle is provided it is an object of the invention to overcome the deficiency of the above-mentioned prior art, the present invention The anti-microbial property of the cilium of enhancing hairbrush is carried out using nano silver technology, antibacterial effect is outstanding, has spectrum antibacterial effect, drop The population density and type of microorganism on low hairbrush, clean and hygienic, very useful convenience.

To achieve the above object, the present invention provides a kind of nano-negative ion bristle, calculates by weight, including following component:

Thermoplastic polyester particle, 25 grams to 60 grams；

Nanometer anion powder solution, 19 grams to 30 grams；

Couplant, 1.5 grams to 10 grams；

Nano-magnetic powder, 1.5 grams to 5 grams；

Coral nano powder, 1.5 grams to 2 grams；

Nano pearl powder, 1.5 grams to 3 grams.

Preferably, it calculates by weight, also comprises the following components: hyaluronic acid, 1 gram to 3 grams.

Preferably, it calculates by weight, also comprises the following components: the Chinese herbal medicine extract dry powder with fungistatic effect, 0.2 gram To 0.5 gram.

Preferably, it calculates by weight, also comprises the following components: natural perfume material, 0.1 gram to 0.2 gram.

Preferably, it calculates by weight, also comprises the following components: polynucleotide extract dry powder, 0.01 gram to 0.03 gram.

Preferably, it calculates by weight, also comprises the following components: soft agent, 1 gram to 10 grams.

Preferably, it calculates by weight, the thermoplastic polyester particle is PBT particle.

The present invention provides a kind of preparation process of nano-negative ion bristle, includes the following steps:

By weight mixer is added in PBT particle, nano-magnetic powder, coral nano powder, Nano pearl powder by S801；Add Enter 30% nanometer anion powder solution；Drying, passes through equipment high temperature fusion wire drawing of reeling off raw silk from cocoons；

S802 is cut into chunks according to customization size, burns a mao peak using sodium hydroxide, then cleaned using organic acid；

S803 is put into the dyeing of dye vat equipment, the couplant of 30% nanometer anion powder solution and 30% is added after fixation 80 to 110 degree heat preservation 30 minutes is warming up to by high temperature dye vat；

S804 is cleaned again, is dehydrated, toasting 100 minutes and dry into 110 degree of oven.

Preferably, include the following steps:

S801, by weight, by PBT particle, nano-magnetic powder, coral nano powder, Nano pearl powder, hyaluronic acid, in Mixer is added in herb extracts dry powder, natural perfume material, polynucleotide extract dry powder, soft agent；30% nano-negative ion is added Powder solution mixes 40 minutes；Drying 1.5 hours, passes through equipment high temperature fusion wire drawing of reeling off raw silk from cocoons；

S802 is cut into chunks according to customization size, burns a mao peak using sodium hydroxide, then cleaned using organic acid, then Subtract material process equipment with laser and further modifies hair peak；

S803 is put into the dyeing of dye vat equipment, the couplant of 30% nanometer anion powder solution and 30% is added after fixation 80 to 110 degree heat preservation 30 minutes is warming up to by high temperature dye vat；

S804 is cleaned again, is dehydrated, toasting 100 minutes and dry into 110 degree of oven.

The beneficial effects of the present invention are:

1, preparation process of the invention is simple, cheap, its antibacterial ability of the products such as hairbrush prepared by this technique goes out Crowd, facilitates the clean hygiene of user, and avoids skin infection.

2, by setting nano-magnetic powder, hairbrush of the invention also has the effect of magnetic therapy physical therapy to the skin of human body.Pass through Coral nano powder, which is arranged, can penetrate to the skin the element of coral surface when using hairbrush；By the way that pearl powder is arranged, Nano pearl powder can be protruded into Skin Cell.Play good whitening effect.By the way that Chinese herbal medicine extract dry powder is arranged, when When the micro sweat of hairbrush and body surface contacts, medicinal herb components can be penetrated into skin, such as with the Chinese herbal medicine of whitening composition Component.By the way that natural perfume material is added, bristle of the invention has good fragrant breath.It, can by mixing polynucleotide extract In use, to supplement a certain amount of polynucleotide material for skin, play good health-care effect.

3, it is proved by statistics, antibacterial effect of the invention has antibacterial of 99% or more a possibility that higher than normal bristles Effect, anti-microbial property are superior.

4, the used bristle of cosmetic brush is all filling material, made by traditional handicraft currently on the market, with the development of society, Pursuit of the mankind to quality of the life, the attention to safety, we pass through research and development in 2 years, have devised nano-negative ion bristle, It will be suitable for the fields such as cosmetic brush, wig makeups tool, accessory.

Nano-negative ion bristle active constituent containing anion of the invention, is widely used in medical treatment, and prove it is safe and efficient, it is right No skin irritation, it is nontoxic, without allergic reaction, in use, has to the skin of human body and promote blood circulation, stimulate carefully The functions such as born of the same parents' regeneration, anti-aging, economic value are high.The present invention demonstrates its antibacterial effect by statistics.

Detailed description of the invention

Fig. 1 is the experiment effect figure of one embodiment of the invention, and abscissa represents group, and 1 to 4 group respectively represents hairbrush D Group, hairbrush A group, hairbrush B group, hairbrush C group；Ordinate represents microorganism concn rank, and 10 grades represent highest.

Specific embodiment

Embodiment one: formula and preparation process

	A(grams of prescription)	B(grams of prescription)	C(grams of prescription)
				PBT particle	25	50	60
Nanometer silver antimicrobial liquid	19	25	30
				Nano-magnetic powder	1.5	3	5
Coral nano powder	1.5	1.5	2
				Nano pearl powder	1.5	2	3
Hyaluronic acid	1.5	1.5	2
				Chinese herbal medicine extract dry powder with fungistatic effect	0.2	0.3	0.5
Natural perfume material	0.1	0.15	0.2
				Polynucleotide extract dry powder	0.01	0.02	0.03
Soft agent	2	5	10
				Couplant	1.5	5	20

Preparation process is as follows: S801, by weight, by PBT particle, nano-magnetic powder, coral nano powder, nano-pearl Mixer is added in powder, hyaluronic acid, Chinese herbal medicine extract dry powder, natural perfume material, polynucleotide extract dry powder, soft agent；It is added 30% nanometer anion powder solution mixes 40 minutes；Drying 1.5 hours, passes through equipment high temperature fusion wire drawing of reeling off raw silk from cocoons；S802, root It cuts into chunks according to customization size, burns a mao peak using sodium hydroxide, then cleaned using organic acid, then subtract material processing with laser and set Standby further finishing hair peak；S803 is put into the dyeing of dye vat equipment, adds 30% nanometer anion powder solution and 30% after fixation Couplant by high temperature dye vat be warming up to 80 to 110 degree heat preservation 30 minutes；S804 is cleaned again, is dehydrated, into oven 110 Degree baking is dried for 100 minutes.Wherein, organic acid is citric acid.Nanometer anion powder solution is mass concentration expression.

Embodiment two: antibacterial effect experimental design

Take microorganism nature culture (containing human body surface, such as the multiple-microorganism of facial surface)；Prepare various trainings Support the suspension of object；Hairbrush A, hairbrush B, hairbrush C are prepared respectively with component A, component B, component C, and are selected commercially available general Logical hairbrush D, it is ensured that the specification of four kinds of hairbrush is identical.Certain time is impregnated in suspension with hairbrush, such as 30 minutes, 60 minutes, 180 minutes.Hairbrush is taken out, is cleaned with slow tap water.It dries, then, hairbrush is carried out to ultrasound in the container for determining volume Wave cleans (cleaning solution constant volume), and after cleaning, liquid in extracting container is counted with cell counting board under the microscope Number, the number of cell is classified, is divided into 1 to 10 grade, 1 grade of density is minimum, 10 grades of density highests.Every group of hairbrush selects 20 hairs It brushes, totally four groups, totally 80 hairbrush.10 grades of concentration are defined as the cell concentration after suspension directly dilutes.With point otherwise, directly The expression microorganism residual quantity of sight.Certainly the antibacterial for microorganisms such as Escherichia coli, staphylococcus aureuses can also be verified Performance.

Embodiment three: experimental result

	Hairbrush D group	Hairbrush A group	Hairbrush B group	Hairbrush C group
					1	9.75	6.79	4.05	1.29
2	9.44	6.53	4.65	1.17
					3	9.43	5.80	5.40	2.39
4	9.65	6.37	4.36	1.73
					5	9.50	5.38	4.49	2.41
6	9.55	6.30	4.16	2.96
					7	9.42	5.10	5.45	2.34
8	9.29	6.45	5.00	1.59
					9	9.45	6.39	4.70	1.42
10	9.49	5.19	5.26	1.51
					11	9.17	6.77	5.50	1.44
12	9.80	5.29	4.43	1.21
					13	9.20	6.52	4.91	1.68
14	9.26	6.20	4.69	1.90
					15	9.69	5.74	4.18	2.65
16	9.70	6.04	5.27	1.29
					17	9.23	5.10	4.36	1.39
18	9.57	5.23	4.66	2.36
					19	9.34	5.38	5.44	2.96
20	9.23	5.27	4.19	2.30
					Maximum value	9.80	6.79	5.50	2.96
Minimum value	9.17	5.10	4.05	1.17
					Average value	9.46	5.89	4.76	1.90
Standard deviation	0.1877574	0.589412346	0.47656	0.57773

Above-mentioned experimental result is the experimental data obtained in the experimental design of embodiment two, and soaking time uses 30 points Clock.

Example IV: statistics conclusion

Referring to Fig. 1, Fig. 1 is data processing figure, from Fig. 1, it has also been discovered that 1 to 4 groups (i.e. D group, A group, B group, C Group), average value successively reduces (bacteria containing amount is horizontal).

In addition, carrying out statistical test (T inspection), P=1.9811E-18 < 0.01 between A group and D group illustrates in A group and D Group has significant difference, that is to say, that in statistics, the antibacterial ability of its antibacterial ability of the hairbrush of A group and D group has 99% A possibility that there is significant difference, wherein D group is control group, and the antibacterial ability of A group is significantly better than the antibacterial ability of D group.

Progress T inspection between B group and D group, P=2.552E-24 < 0.01, progress T inspection between C group and D, P= It is significant to illustrate that the antibacterial ability of B group, the antibacterial ability of C group and D group has 99% a possibility that have for 4.73419E-26 < 0.01 The difference of property, B group, C group antibacterial ability be significantly better than the antibacterial ability of D group.

Although the embodiments of the present invention has been shown and described above, it is to be understood that above-described embodiment is example Property, it is not considered as limiting the invention, those skilled in the art are not departing from the principle of the present invention and objective In the case where can make changes, modifications, alterations, and variations to the above described embodiments within the scope of the invention.

Claims (8)

1. a kind of nano-negative ion bristle, which is characterized in that calculate by weight, including following component:

Thermoplastic polyester particle, 25 grams to 60 grams；

Nanometer anion powder solution, 19 grams to 30 grams；

Couplant, 1.5 grams to 10 grams；

Nano-magnetic powder, 1.5 grams to 5 grams；

Coral nano powder, 1.5 grams to 2 grams；

Nano pearl powder, 1.5 grams to 3 grams；

The thermoplastic polyester particle is PBT particle；

By weight, mixer is added in PBT particle, nano-magnetic powder, coral nano powder, Nano pearl powder；Addition 30% is received Rice negative ion powder solution；Drying, passes through equipment high temperature fusion wire drawing of reeling off raw silk from cocoons；It is cut into chunks according to customization size, utilizes sodium hydroxide A mao peak is burnt, is then cleaned using organic acid；It is put into the dyeing of dye vat equipment, it is molten to add 30% nanometer anion powder after fixation Liquid and 30% couplant by high temperature dye vat be warming up to 80 to 110 degree heat preservation 30 minutes；It cleans, be dehydrated, into oven again 110 degree dry for baking 100 minutes.

2. nano-negative ion bristle according to claim 1, which is characterized in that calculate by weight, also comprise the following components: Hyaluronic acid, 1 gram to 3 grams.

3. nano-negative ion bristle according to claim 2, which is characterized in that calculate by weight, further include such as the following group Point: the Chinese herbal medicine extract dry powder with fungistatic effect, 0 .2 grams to 0 .5 grams.

4. nano-negative ion bristle according to claim 3, which is characterized in that calculate by weight, also comprise the following components: Natural perfume material, 0.1 gram to 0.2 gram.

5. nano-negative ion bristle according to claim 4, which is characterized in that calculate by weight, also comprise the following components: Polynucleotide extract dry powder, 0.01 gram to 0.03 gram.

6. nano-negative ion bristle according to claim 5, which is characterized in that calculate by weight, also comprise the following components: Soft agent, 2 grams to 10 grams.

7. a kind of preparation process of nano-negative ion bristle according to claim 6, which is characterized in that including walking as follows It is rapid:

By weight mixer is added in PBT particle, nano-magnetic powder, coral nano powder, Nano pearl powder by S801；It is added 30% nanometer anion powder solution；Drying, passes through equipment high temperature fusion wire drawing of reeling off raw silk from cocoons；

S802 is cut into chunks according to customization size, burns a mao peak using sodium hydroxide, then cleaned using organic acid；S803 is put into The dyeing of dye vat equipment, 30% nanometer anion powder solution is added after fixation and 30% couplant is warming up to by high temperature dye vat 80 to 110 degree heat preservations 30 minutes；

S804 is cleaned again, is dehydrated, toasting 100 minutes and dry into 110 degree of oven.

8. a kind of preparation process of nano-negative ion bristle according to claim 7, which is characterized in that including walking as follows It is rapid:

S801, by weight, by PBT particle, nano-magnetic powder, coral nano powder, Nano pearl powder, hyaluronic acid, Chinese herbal medicine Mixer is added in extract dry powder, natural perfume material, polynucleotide extract dry powder, soft agent；The nanometer anion powder of addition 30% is molten Liquid mixes 40 minutes；Drying 1.5 hours, passes through equipment high temperature fusion wire drawing of reeling off raw silk from cocoons；

S802 is cut into chunks according to customization size, burns a mao peak using sodium hydroxide, then cleaned using organic acid, then with sharp Light subtracts material process equipment and further modifies hair peak；

S803 is put into the dyeing of dye vat equipment, and 30% nanometer anion powder solution is added after fixation and 30% couplant passes through High temperature dye vat is warming up to 80 to 110 degree heat preservation 30 minutes；

S804 is cleaned again, is dehydrated, toasting 100 minutes and dry into 110 degree of oven.