CN105907106A - Candy package wax and preparation method thereof - Google Patents
Candy package wax and preparation method thereof Download PDFInfo
- Publication number
- CN105907106A CN105907106A CN201610016523.4A CN201610016523A CN105907106A CN 105907106 A CN105907106 A CN 105907106A CN 201610016523 A CN201610016523 A CN 201610016523A CN 105907106 A CN105907106 A CN 105907106A
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- China
- Prior art keywords
- wax
- ethylene
- candy wrapping
- candy
- copolymer
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L91/00—Compositions of oils, fats or waxes; Compositions of derivatives thereof
- C08L91/06—Waxes
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
- B65D—CONTAINERS FOR STORAGE OR TRANSPORT OF ARTICLES OR MATERIALS, e.g. BAGS, BARRELS, BOTTLES, BOXES, CANS, CARTONS, CRATES, DRUMS, JARS, TANKS, HOPPERS, FORWARDING CONTAINERS; ACCESSORIES, CLOSURES, OR FITTINGS THEREFOR; PACKAGING ELEMENTS; PACKAGES
- B65D65/00—Wrappers or flexible covers; Packaging materials of special type or form
- B65D65/38—Packaging materials of special type or form
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L23/00—Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers
- C08L23/02—Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers not modified by chemical after-treatment
- C08L23/18—Homopolymers or copolymers of hydrocarbons having four or more carbon atoms
- C08L23/20—Homopolymers or copolymers of hydrocarbons having four or more carbon atoms having four to nine carbon atoms
- C08L23/22—Copolymers of isobutene; Butyl rubber ; Homo- or copolymers of other iso-olefins
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/02—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
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- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Laminated Bodies (AREA)
- Confectionery (AREA)
Abstract
The invention discloses candy package wax. The candy package wax is prepared from 10-40% by mass of a tackifier, 1-10% by mass of a plasticizer, 0.1-5% by mass of a flexibilizer, 0.2-10% by mass of a film forming agent, 1-5% by mass of a stabilizing agent and the balance wax. A preparation method of the candy package wax comprises heating to melt wax, adding the tackifier, the plasticizer, the flexibilizer, the film forming agent and the stabilizing agent into the wax, heating the mixture to a temperature of 180 DEG C or more, carrying out stirring at a rotation rate of 10-30r/min until uniform mixing after complete melting of the raw materials and carrying out cooling molding to obtain the candy package wax. The candy package wax has good adhesion, temperature resistance and coating performances. The candy package wax can be simply operated, can be directly put into a wax melting cylinder of a candy packaging machine, is free of a blending process, has stable quality, can form a clean and flat candy package and can form a thin coating with good adhesion. The preparation method has simple processes and is convenient for operation and large-scale production.
Description
Technical field
The present invention relates to packaging material field, particularly relate to a kind of candy wrapping wax and preparation method thereof.
Background technology
For a long time, candy wrapping mostly with paper as packaging material, the especially product such as chewing gum and bubble gum,
At wrapping paper sealing part, the glue typically allocated with PUR and paraffin adheres to, on the one hand, PUR has many
Kind, manufacturer is not easy to select.Two, the technology of the master worker of allotment packaging glue is the most unbalanced, so,
The product quality fluctuation of manufacturer is bigger.The most viscous, it is not easy to strip off, or do not stick, easily come unglued.
Some is unreasonable with paraffin proportioning due to PUR, coats uneven, affects outward appearance.
Summary of the invention
It is an object of the invention to propose a kind of candy wrapping wax, described candy wrapping wax has well
Adhesive force and heat resistance, coating property is good.Simple to operate, only candy wrapping wax need to be directly placed into
The wax melting tank of candy wrapper, it is not necessary to additionally allocate, steady quality, the packaging external appearance of candy is clean,
Smooth, coating is thin but bonding is good.
The second object of the present invention is to provide the preparation method of a kind of candy wrapping wax, and the method technique is simple,
Easy to operate, it is simple to large-scale production.
The technical scheme is that and be achieved in that: a kind of candy wrapping wax, described candy wrapping wax is main
It is prepared from by the raw material of following mass fraction: the plasticizer of tackifier, 1%～10%, 0.1%～5% of 10%～40%
The stabilizer of the film forming agent of toughener, 0.2%～10%, 1%～5%, surplus be wax.
Further, described candy wrapping wax is mainly prepared from by the raw material of following mass fraction: 20%～30%
The stabilizer of the film forming agent of the toughener of the plasticizer of tackifier, 3%～7%, 0.1%～5%, 3%～7%, 2%～4%,
Surplus is wax.
Further, described candy wrapping wax is mainly prepared from by the raw material of following mass fraction: the thickening of 25%
Agent, the plasticizer of 5%, the toughener of 3%, the film forming agent of 5%, the stabilizer of 3%, surplus are wax.
Further, the one during described wax is paraffin, microwax, ceresine, Fischer Tropsch waxes and polyolefin-wax
Or it is multiple.
Further, described tackifier are hydrocarbon resin, polybutene, polyisobutene, group aliphatic resin, ring grease
Diene resin, Petropols, ester gum, rosin resin, aromatic resin, aliphatic-aromatic are common
One or more in poly resin and random polyolefin.
Further, described plasticizer is petrolatum, polybutadiene, phthalic acid ester, glycolate, ore deposit
One or more in thing oil and polybutene.
Further, described toughener is butyl rubber, linear saturated polyester, PEPA and two isocyanic acids
Ester polymer, ethylene-propylene copolymer, ethylene-vinyl acetate copolymer, propene-1-butene copolymer, ethene
-vinyl acetate-propylene copolymer, ene-propylene-butene mixed polymer, ethylene-acrylic acid copolymer, second
Alkene-octene copolymer, ethylene-stryene-propylene copolymer, ethylene-stryene-butylene copolymer and butylene-
One or more in styrol copolymer.
Further, described film forming agent is polyethylene, polypropylene, ethylene-vinyl acetate copolymer, ethene-the third
Olefin(e) acid ethyl ester EVA, ethylene-acrylic acid copolymer body, ethylene isobutyl acrylate EVA, polytetramethylene glycol
Modified polyester resin, epoxy resin or polyurethane resin, ethylene-propylene-1-butene polymers, styrene-
Butadiene-styrene block copolymer, SIS, PPG,
In polyisocyanates, styrene-ethylene butylene-styrene and styrene ethylene-propylene-styrene
One or more.
Further, described stabilizer be BHT, 2, tri-grades of butyl-4-methylphenols of 6-,
Double (tri-grades of butyl-4-hydroxy phenyls of 3,5-) thioether, methyl polysiloxane, four [β-(tri-grades of butyl of 3,5-
-4-hydroxy phenyl) propionic acid] pentaerythritol ester, double Lauryl Alcohol ester, double ten four carbon alcohols esters, double octadecanol ester
With one or more in β-(3,5-di-tert-butyl-hydroxy phenyl) propionic acid positive octadecanol ester.
The preparation method of a kind of candy wrapping wax, comprises the steps:
First wax is added heat fusing, be then added thereto to tackifier, plasticizer, toughener, film forming agent and steady
Determining agent, liter high-temperature, to more than 180 DEG C, stirs with the rotating speeds of 10～30 revs/min, treats that raw material is completely melt
After, stirring is to mixing, and cooling is molded, and prepares described candy wrapping wax.
The invention have the benefit that candy wrapping wax of the present invention, by tackifier, plasticizer,
Toughener, rationally the selecting and compatibility of film forming agent so that the tack of described candy wrapping wax, coating and
Elastic (antifungal gene ability) is more satisfactory, and so, Wax-coated layer is thin and uniform, smooth, and cohesive force is fitted
In, also will not come unglued when environment temperature is at about 70 DEG C.Described candy wrapping wax has good attachment
Power and heat resistance, coating property is good.Simple to operate, only candy wrapping wax need to be directly placed into candy bag
The wax melting tank of installation, it is not necessary to additionally allocating, steady quality, the packaging external appearance of candy is clean, smooth,
Coating is thin but bonding is good.The method technique is simple, easy to operate, it is simple to large-scale production.
Candy wrapping wax of the present invention is by rationally selecting and compatibility raw material so that it is have good attachment
There is while power good stripping performance, wrapping paper will not be torn, it addition, according to subscriber equipment situation
(having the equipment of Germany's production, the equipment of Korea S's production and home equipment) and the speed of equipment regulation, only need
Just it is adapted to high or low for wax cylinder temperature tune, there is the biggest using value.
Detailed description of the invention
For being more fully understood that the present invention, below by following example, the present invention made the most concrete elaboration,
But it is not to be construed as limitation of the invention, those skilled in the art is made according to foregoing invention content
Some nonessential improvement and adjustment, be also considered as being within the scope of the present invention.
Embodiment 1
A kind of candy wrapping wax, is prepared from by the raw material of following mass fraction:
Tackifier 10%, plasticizer 1%, toughener 0.1%, film forming agent 0.2%, stabilizer 1%, surplus are wax.
Described tackifier are random polystyrene；
Described plasticizer is polybutadiene；
Described toughener is butyl rubber；
Described film forming agent is polyethylene；
Described stabilizer is DBPC 2,6 ditertiary butyl p cresol；
Described wax is paraffin；
Preparation method is as follows:
First wax is added heat fusing, be then added thereto to tackifier, plasticizer, toughener, film forming agent and steady
Determining agent, liter high-temperature, to 180 DEG C, stirs with the rotating speeds of 10 revs/min, after raw material is completely melt, with
The rotating speed mix and blend of 30 revs/min prepares described candy wrapping wax to mixing in 4 hours.
Embodiment 2
A kind of candy wrapping wax, is prepared from by the raw material of following mass fraction:
Tackifier 40%, plasticizer 10%, toughener 5%, film forming agent 10%, stabilizer 5%, surplus are wax.
Described tackifier are polyisobutene；
Described plasticizer is Methyl Benzene-o-dicarboxylate；
Described toughener is ethylene-propylene copolymer；
Described film forming agent is polypropylene；
Described stabilizer is tri-grades of butyl-4-methylphenols of 2,6-；
Described wax is microwax；
Preparation method is as follows:
First wax is added heat fusing, be then added thereto to tackifier, plasticizer, toughener, film forming agent and steady
Determining agent, liter high-temperature, to 250 DEG C, stirs with the rotating speeds of 30 revs/min, after raw material is completely melt, with
The rotating speed mix and blend of 60 revs/min prepares described candy wrapping wax to mixing in 2 hours.
Embodiment 3
A kind of candy wrapping wax, is prepared from by the raw material of following mass fraction:
Tackifier 20%, plasticizer 3%, toughener 2%, film forming agent 3%, stabilizer 2%, surplus are wax.
Described tackifier are random polypropylene；
Described plasticizer is mineral oil；
Described toughener is propene-1-butene copolymer；
Described film forming agent is ethylene-acrylic acid copolymer body；
Described stabilizer is double (tri-grades of butyl-4-hydroxy phenyls of 3,5-) thioethers；
Described wax is Fischer Tropsch waxes；
Preparation method is as follows:
First wax is added heat fusing, be then added thereto to tackifier, plasticizer, toughener, film forming agent and steady
Determining agent, liter high-temperature, to more than 180 DEG C, stirs with the rotating speeds of 10～30 revs/min, treats that raw material is completely melt
After, stirring is to mixing, and cooling is molded, and prepares described candy wrapping wax.
Embodiment 4
A kind of candy wrapping wax, is prepared from by the raw material of following mass fraction:
Tackifier 30%, plasticizer 7%, toughener 4%, film forming agent 7%, stabilizer 4%, surplus are wax.
Described tackifier are random polypropylene 10%, polyisobutene 5% and random polystyrene 15%；
Described plasticizer is mineral oil 1%, Methyl Benzene-o-dicarboxylate 2% and ethyl phthalate 4%；
Described toughener is that propene-1-butene copolymer 1%, ethylene-propylene copolymer 1% and butylene-styrene are total to
Polymers 2%；
Described film forming agent is ethylene-acrylic acid copolymer body 1%, diisocyanate 2%, triisocyanate 4%；
Described stabilizer is that double (tri-grades of butyl-4-hydroxy phenyls of 3,5-) thioether 1%, 2,6-di-t-butyl are to first
1% and 2,6-tri-grade of butyl-4-methylphenol 2% of phenol；
Described wax such as is at the paraffin of quality, Tissuemat E and the polypropylene wax mixture；
Preparation method is as follows:
First wax is added heat fusing, be then added thereto to tackifier, plasticizer, toughener, film forming agent and steady
Determining agent, liter high-temperature, to more than 180 DEG C, stirs with the rotating speeds of 10～30 revs/min, treats that raw material is completely melt
After, stirring is to mixing, and cooling is molded, and prepares described candy wrapping wax.
Embodiment 5
A kind of candy wrapping wax, is prepared from by the raw material of following mass fraction:
Tackifier 25%, plasticizer 5%, toughener 3%, film forming agent 5%, stabilizer 3%, surplus are wax.
Described tackifier are polyisobutene；
Described plasticizer is mineral oil；
Described toughener is butyl rubber；
Described film forming agent is polyethylene；
Described stabilizer is dimethyl polysiloxane；
Described wax is paraffin, microwax mixture, and wherein the mass ratio of paraffin and microwax is 9:1；
Preparation method is as follows:
First wax is added heat fusing, be then added thereto to tackifier, plasticizer, toughener, film forming agent and steady
Determining agent, liter high-temperature, to more than 180 DEG C, stirs with the rotating speeds of 10～30 revs/min, treats that raw material is completely melt
After, stirring is to mixing, and cooling is molded, and prepares described candy wrapping wax.
The requirement of raw materials all for the present invention, all must use food-grade or packaging for foodstuff level raw material.
It addition, the physicochemical properties of embodiment of the present invention 1-5 gained candy wrapping wax are as follows:
The foregoing is only presently preferred embodiments of the present invention, not in order to limit the present invention, all at this
Within bright spirit and principle, any modification, equivalent substitution and improvement etc. made, should be included in this
Within bright protection domain.
Claims (9)
1. a candy wrapping wax, it is characterized in that, described candy wrapping wax is mainly prepared from by the raw material of following mass fraction: the stabilizer of the film forming agent of the toughener of the plasticizer of tackifier, 1%～10%, 0.1%～5%, 0.2%～10%, 1%～5%, the surplus of 10%～40% are wax.
2. candy wrapping wax as claimed in claim 1, it is characterized in that, described candy wrapping wax is mainly prepared from by the raw material of following mass fraction: the stabilizer of the film forming agent of the toughener of the plasticizer of tackifier, 3%～7%, 0.1%～5%, 3%～7%, 2%～4%, the surplus of 20%～30% are wax.
3. candy wrapping wax as claimed in claim 1, it is characterized in that, described candy wrapping wax is mainly prepared from by the raw material of following mass fraction: the tackifier of 25%, the plasticizer of 5%, the toughener of 3%, the film forming agent of 5%, the stabilizer of 3%, surplus are wax.
4. candy wrapping wax as claimed in claim 1, it is characterised in that: described wax is one or more in paraffin, microwax, ceresine, Fischer Tropsch waxes and polyolefin-wax.
5. candy wrapping wax as claimed in claim 1, it is characterised in that: described tackifier are one or more in hydrocarbon resin, polybutene, polyisobutene, Petropols, ester gum, rosin resin, group aliphatic resin, ring grease diene resin, aromatic resin, aliphatic-aromatic copolymer resins and random polyolefin；Described plasticizer is one or more in petrolatum, polybutadiene, phthalic acid ester, glycolate, mineral oil and polybutene.
A kind of candy wrapping wax the most according to claim 1, it is characterised in that: described toughener is butyl rubber, linear saturated polyester, PEPA and one or more in diisocyanate polymer, ethylene-propylene copolymer, ethylene-vinyl acetate copolymer, propene-1-butene copolymer, ethene-vinyl acetate-propylene copolymer, ene-propylene-butene mixed polymer, ethylene-acrylic acid copolymer, ethylene-octene copolymer, ethylene-stryene-propylene copolymer, ethylene-stryene-butylene copolymer and butylene-styrene copolymers.
A kind of candy wrapping wax the most according to claim 1, it is characterized in that: described film forming agent is polyethylene, polypropylene, ethylene-vinyl acetate copolymer, ethylene-ethylacrylate EVA, ethylene-acrylic acid copolymer body, ethylene isobutyl acrylate EVA, the polyester resin that polytetramethylene glycol is modified, epoxy resin or polyurethane resin, ethylene-propylene-1-butene polymers, SBS, SIS, PPG, polyisocyanates, one or more in styrene-ethylene butylene-styrene and styrene ethylene-propylene-styrene.
A kind of candy wrapping wax the most according to claim 1, it is characterized in that: described stabilizer is 2,6-BHT, 2, tri-grades of butyl-4-methylphenols of 6-, double (3, tri-grades of butyl-4-hydroxy phenyls of 5-) thioether, methyl polysiloxane, four [β-(3, tri-grades of butyl-4-hydroxy phenyls of 5-) propionic acid] pentaerythritol ester, double Lauryl Alcohol ester, double ten four carbon alcohols esters, one or more in double octadecanol ester and β-(3,5-di-tert-butyl-hydroxy phenyl) propionic acid positive octadecanol ester.
9. the preparation method of the candy wrapping wax as described in claim 1-8 is arbitrary, it is characterised in that comprise the steps:
First wax is added heat fusing, be then added thereto to tackifier, plasticizer, toughener, film forming agent and stabilizer, rise high-temperature to more than 180 DEG C, stirring with the rotating speeds of 10～30 revs/min, after raw material is completely melt, stirring is to mixing, cooling shaping, prepares described candy wrapping wax.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610016523.4A CN105907106A (en) | 2016-01-08 | 2016-01-08 | Candy package wax and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610016523.4A CN105907106A (en) | 2016-01-08 | 2016-01-08 | Candy package wax and preparation method thereof |
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| CN105907106A true CN105907106A (en) | 2016-08-31 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
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| CN201610016523.4A Pending CN105907106A (en) | 2016-01-08 | 2016-01-08 | Candy package wax and preparation method thereof |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109628018A (en) * | 2018-11-29 | 2019-04-16 | 山东康威通信技术股份有限公司 | A method of oxidation PE wax is applied to circuit board sealing protection |
| CN110066631A (en) * | 2019-05-27 | 2019-07-30 | 广州市德馨蜡制品有限公司 | Pack wax and preparation method thereof |
| CN110437798A (en) * | 2019-08-07 | 2019-11-12 | 广州市德馨蜡制品有限公司 | It is packed for bonding wax and its preparation method and application |
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| CN101678925A (en) * | 2007-05-10 | 2010-03-24 | 国际壳牌研究有限公司 | Paraffin wax composition |
| CN102030995A (en) * | 2010-09-21 | 2011-04-27 | 北京同仁堂股份有限公司 | Packed wax composition as Chinese herbal honeyed pill |
| CN105017784A (en) * | 2015-08-20 | 2015-11-04 | 广州市德馨蜡制品有限公司 | Epilating wax for living stock and preparation method of epilating wax |
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2016
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| CN101045854A (en) * | 2007-04-24 | 2007-10-03 | 上海泰尔精蜡有限公司 | Antiskid wax for board and manufacturing method thereof |
| CN101678925A (en) * | 2007-05-10 | 2010-03-24 | 国际壳牌研究有限公司 | Paraffin wax composition |
| CN102030995A (en) * | 2010-09-21 | 2011-04-27 | 北京同仁堂股份有限公司 | Packed wax composition as Chinese herbal honeyed pill |
| CN105017784A (en) * | 2015-08-20 | 2015-11-04 | 广州市德馨蜡制品有限公司 | Epilating wax for living stock and preparation method of epilating wax |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109628018A (en) * | 2018-11-29 | 2019-04-16 | 山东康威通信技术股份有限公司 | A method of oxidation PE wax is applied to circuit board sealing protection |
| CN110066631A (en) * | 2019-05-27 | 2019-07-30 | 广州市德馨蜡制品有限公司 | Pack wax and preparation method thereof |
| CN110437798A (en) * | 2019-08-07 | 2019-11-12 | 广州市德馨蜡制品有限公司 | It is packed for bonding wax and its preparation method and application |
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Address after: 510000 Guangdong Province, Guangzhou city Zengcheng District Xian Cun Zhen Ji Gang Cun Sha Jiao Dang (soil) plant (No. A-3) Applicant after: GUANGZHOU DEXIN WAX PRODUCTS CO., LTD. Address before: Wo Zhen Bai Tang Cun Baiyun District of Guangzhou City, Guangdong province 510000 Songyuan Street No. 6 Applicant before: GUANGZHOU DEXIN WAX PRODUCTS CO., LTD. |
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Application publication date: 20160831 |