CN105749084B - It is a kind of with antibacterial, disinfection medical fluid and its application - Google Patents
It is a kind of with antibacterial, disinfection medical fluid and its application Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/09—Lichens
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/28—Asteraceae or Compositae (Aster or Sunflower family), e.g. chamomile, feverfew, yarrow or echinacea
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/88—Liliopsida (monocotyledons)
- A61K36/904—Stemonaceae (Stemona family), e.g. croomia
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L15/00—Chemical aspects of, or use of materials for, bandages, dressings or absorbent pads
- A61L15/16—Bandages, dressings or absorbent pads for physiological fluids such as urine or blood, e.g. sanitary towels, tampons
- A61L15/42—Use of materials characterised by their function or physical properties
- A61L15/44—Medicaments
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L15/00—Chemical aspects of, or use of materials for, bandages, dressings or absorbent pads
- A61L15/16—Bandages, dressings or absorbent pads for physiological fluids such as urine or blood, e.g. sanitary towels, tampons
- A61L15/42—Use of materials characterised by their function or physical properties
- A61L15/46—Deodorants or malodour counteractants, e.g. to inhibit the formation of ammonia or bacteria
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/33—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones
- A61K2236/333—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones using mixed solvents, e.g. 70% EtOH
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/39—Complex extraction schemes, e.g. fractionation or repeated extraction steps
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/50—Methods involving additional extraction steps
- A61K2236/51—Concentration or drying of the extract, e.g. Lyophilisation, freeze-drying or spray-drying
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L2300/00—Biologically active materials used in bandages, wound dressings, absorbent pads or medical devices
- A61L2300/40—Biologically active materials used in bandages, wound dressings, absorbent pads or medical devices characterised by a specific therapeutic activity or mode of action
- A61L2300/404—Biocides, antimicrobial agents, antiseptic agents
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Abstract
The present invention relates to a kind of with antibacterial, disinfection medical fluid and its application；The medical fluid includes the active constituent of following parts by weight: 8-12 parts of Cortex Dictamni extract, 12-18 parts of Radix Stemonae extract, 10-15 parts of Herba Senecionis Scandentis extract, 6-10 parts of extractive of usnea.The active constituent of medical fluid of the present invention is natural extract, and biodegradability is good, is not polluted to environment；And property is mild, and it is skin friendly, it is nonirritant, there is ideal antibacterial, sterilization and antiinflammation.Medical fluid of the present invention has broad application prospects in hygienic articles, especially in the application of towel of going to the lavatory (wet tissue, dry towel), embodies ideal antibacterial, sterilization and anti-inflammatory effects.
Description
Technical field
The present invention relates to a kind of with antibacterial, disinfection medical fluid, while being related to above-mentioned medical fluid and preparing hygienic articles
In application.
Background technique
As attention degree of the masses for personal hygiene aggravates, with antibacterial, disinfection hygienic articles at present
As much-sought-after item.Such as:
Chinese patent CN1062467C discloses a kind of clean-preserving agent, borneol, the original pharmaceutical content for being 1-3 ‰ by weight ratio
For every milliliter 0.3-0.5 grams, the alcohol composition that remaining is 10-15% concentration, crude drug in whole includes climbing groundsel, cortex dictamni, radix saposhnikoviae, Chinese mugwort
Leaf, frutus cnidii, Chinese gall, borneol, which is added, when preparation, after primary medicinal alcohol is soaked, leaked can be prepared by.Keep a public place clean above-mentioned
First woven fabric is penetrated into agent can be made into moist-retaining tissues, can be used in preventing and treating skin disease and gynaecological disease.
Although above-mentioned clean-preserving agent has preferable antibacterial, disinfection and antiinflammation, found in practical application, exist with
Lower Railway Project:
1) women is small after an action of the bowels, and private parts itself is due to there are urine left, needing to inhale using the excellent paper handkerchief of the water imbibition of dry state
Urine, clean is received, and the small requirement for absorbing urine cleaning private parts after an action of the bowels is not achieved in wet tissue.
2) borneol has refrigerant experience sense, and human body is also easy to produce dependence, and the reproductive system for being harmful to women is used for a long time
Health.
China application 104013558 A of CN discloses a kind of wet tissue sterilization and anticorrosion compositional liquor, preparation method and its usage.
The wet tissue sterilization and anticorrosion compositional liquor by following weight percentage material composition: 16 a heatable brick bed base pyridinium chloride 4-15%；Solvent
10-30%；Solubilizer 5-20%；3 p-chlorophenyl -1,2 propylene glycol 2%-10%；Chamomile extracting solution 0.02%-1.5%；
Extract solution from aloe 0.02%-1.5%；Appropriate citric acid, remaining is RO water.This application points out that resulting wet tissue sterilization and anticorrosion is multiple
With the wet tissue being prepared after liquid dilution, mildly nothing is irritated, harmless, and has sterilization, and conditioning improves skin properties, right
Skin-friendliness reaches optimum efficiency, both will not be too viscous, will not be too dry, there is skin-moisturizing, skin antioxidation.However, in reality
It is found in, the application range of above-mentioned sterilization and anticorrosion compositional liquor is relatively narrow, ideal can not especially go to the lavatory towel for women.
Therefore, need to be proposed a kind of antibacterial, significant medical fluid of disinfection, in order to make hygienic articles, especially female
Sex hygiene product (towel of such as going to the lavatory).
Summary of the invention
To overcome the above disadvantages, the present invention provides a kind of with antibacterial, disinfection medical fluid；The medical fluid includes
The active constituent of following parts by weight: 8-12 parts of Cortex Dictamni extract, 12-18 parts of Radix Stemonae extract, Herba Senecionis Scandentis extract 10-15
Part, 6-10 parts of extractive of usnea.
Above-mentioned parts by weight are μ g, mg, g, one of kg well known in the art, or are its multiple, such as 1/100,1/10,10
Times, 100 times etc..
Preferably, the medical fluid includes the active constituent of following parts by weight: 10 parts of Cortex Dictamni extract, Radix Stemonae extract 15
Part, 12 parts of Herba Senecionis Scandentis extract, 8 parts of extractive of usnea.
Medical fluid of the present invention provides active constituent with cortex dictamni, the tuber of stemona, climbing groundsel, sunglo combination, wherein cortex dictamni
The main component of extract is dictamine, and the main component of Radix Stemonae extract is stemonine, and Herba Senecionis Scandentis extract main component is
Senecionine, the main active of extractive of usnea are usnic acid, above-mentioned active constituent compatible use, it is ensured that medical fluid matter
Amount.
Ordinary commercial products can be used in above-mentioned active constituent, in order to ensure medical fluid/towel of going to the lavatory is antibacterial, the effect of disinfection,
Cortex Dictamni extract of the present invention, Radix Stemonae extract, Herba Senecionis Scandentis extract, extractive of usnea preferably pass through side as described below
Method is extracted to obtain.
The extracting method of the Cortex Dictamni extract is as follows: by cortex dictamni grinding and sieving (preferably 30 mesh), according to 1:15-
The solid-liquid ratio (g:ml) of 1:20 extracts 80-90min with the EtOH Sonicate of volume fraction 85%~95%, and concentrated extracting solution is at leaching
Cream (preferably relative density be 1.1-1.3 medicinal extract) to get；Wherein, preferably the frequency of ultrasonic extraction is 20-60kHz, and power is
400-1200W。
It is preferred that cortex dictamni is smashed it through 30 meshes, according to the solid-liquid ratio (g:ml) of 1:16-1:19, volume fraction is used
The EtOH Sonicate of 88%-92% extracts 83-87min, concentrated extracting solution at the medicinal extract of relative density 1.1-1.3 to get.Wherein,
The frequency of ultrasonic extraction is 40kHz, power 500W.
Using said extracted method, the recovery rate of effective component dictamine can be made to greatly improve, make the suppression in prescription
Bacterium bactericidal effect is also improved simultaneously.
The extracting method of the Radix Stemonae extract is as follows: by tuber of stemona grinding and sieving (preferably 30 mesh), according to 1:10-1:20
Solid-liquid ratio (g:ml), 12.5-14.5h, concentrated extracting solution are extracted at 50-60 DEG C with the ethyl alcohol of mass fraction 70%-80%
At medicinal extract (preferably relative density be 1.1-1.3 medicinal extract) to get；
Using said extracted method, the amount of total alkaloids of sessile stemona root is up to 9-10mg/g in extracting solution, it is ensured that prescription has good
Good restraining and sterilizing bacteria effect.
It is preferred that the tuber of stemona is smashed it through 30 meshes, according to the solid-liquid ratio (g:ml) of 1:15-1:20, with mass fraction 72%-
78% ethyl alcohol extracts 12.6-14.2h at 55-58 DEG C, concentrated extracting solution at the medicinal extract that relative density is 1.1-1.3 to obtain the final product；
Using said extracted method, the amount of total alkaloids of sessile stemona root is further improved up to 9.5-10mg/g in extracting solution
The restraining and sterilizing bacteria effect of prescription.
The extracting method of the Herba Senecionis Scandentis extract is as follows: climbing groundsel is put in 55-65 DEG C of insulating box dry 0.5-2h,
Grinding and sieving (preferably 30 meshes)；2-4 is extracted at 55-65 DEG C with the 50-70% ethyl alcohol for being equivalent to 10-14 times of its quality
Secondary, extraction time is 1-3h every time, respectively combined extract and be condensed into medicinal extract (preferably relative density be 1.1-1.3 leaching
Cream)；
It is preferred that climbing groundsel is put in 60 DEG C of insulating boxs dry 1h, 30 meshes are smashed it through；With being equivalent to 12 times of its quality
60% ethyl alcohol extracts 3 times at 60 DEG C, and extraction time is 2h, 1.5h, 1h every time, combined extract and is condensed into relatively close respectively
Degree be 1.1-1.3 medicinal extract to get.
Using said extracted method, the recovery rate of effective component senecionine can be made to greatly improve, other have antibacterial function
The phenolic acid compound recovery rate of effect can also be promoted, so that the restraining and sterilizing bacteria effect in prescription is also improved simultaneously.
The extracting method of the extractive of usnea is as follows: by sunglo grinding and sieving (preferably 30 mesh), according to 1:15-1:25
Solid-liquid ratio, extracted 1-5 times at 60-90 DEG C with the ethyl alcohol of volume fraction 90%-95%, extraction time is 1-4h every time, point
Other combined extract and be condensed into medicinal extract (preferably relative density be 1.1-1.3 medicinal extract) to get；
It is preferred that sunglo is smashed it through 30 meshes, according to the solid-liquid ratio of 1:18-1:22, existed with the ethyl alcohol of volume fraction 95%
Extracted 2-4 times at 65-75 DEG C, extraction time is 2-4h every time, respectively combined extract and be condensed into relative density be 1.1-1.3
Medicinal extract to get；
Using said extracted method, the recovery rate of effective component usnic acid can be made to greatly improve, make the suppression in prescription
Bacterium bactericidal effect is also improved simultaneously.
Medical fluid of the present invention still further comprises solvent in addition to above-mentioned active constituent, i.e., the described medical fluid by activity at
Dispersion is formed in a solvent.It is preferred that the dosage of the solvent is 200-900 parts by weight.
Specifically, medical fluid of the present invention is used as solvent with ethanol water, water, propylene glycol, glycerine etc., with more advantageous
In dispersion of active ingredients, it is ensured that medical fluid/towel of going to the lavatory quality.
When the solvent is ethanol water, volumetric concentration is advisable in 50-75%, preferably 60-70%.
It further include spice additive in medical fluid of the present invention, the odor additive includes pure natural spice or artificial fragrant
Material.
Wherein, the pure natural spice is selected from one or more of elscholtiza, borneol, oriental wormwood, peppermint hydrosol and yellow wormwood artemisia；Institute
It states plants essential oil and is selected from Chinese torreya essential oil, mother chrysanthemum flower essential oil, daphne odera essential oil, pinecone essential oil, mugwort oil, thyme essential oil, You Jia
One or more of sharp essential oil, tea tree ethereal oil and camphor tree essential oil.
Preferably, various plants essential oils and chemical synthesis essence, especially Elsholtzia cilita essential oil, argy wormwood may be selected in the artificial flavors
Oil, daphne odera essential oil and camphor tree essential oil, such essential oil is preferably to be added medical fluid of the present invention, further to adjust gas
Taste increases effect.
The dosage of above-mentioned spice additive, which is subject to, can make the medical fluid form pleasant fragrance, when selection plants essential oil
When, ideal dosage is 0.1%-0.3%, can specifically be adjusted according to actual conditions.
Invention also provides above-mentioned medical fluids to prepare the application in hygienic articles.
Above-mentioned hygienic articles include wet tissue or dry towel, preferably go to the lavatory towel, sanitary napkin or disinfecting paper etc., towel of more preferably going to the lavatory.
Towel of the present invention of going to the lavatory is wet tissue or dry towel, and the base fabric is selected from non-woven fabrics or domestic paper, the domestic paper
It is preferred that wettable domestic paper.Wherein, domestic paper refers to paper for daily use, refer to for look after it is personal at home, it is outgoing it is equal used in all kinds of defend
Raw wiping paper, including roll toilet paper, extraction-type toilet paper, Boxed facial tissue, pocket face-tissue, paper handkerchief, napkin paper, wiping hand
Paper, kitchen towels.Wettable domestic paper refers to that wet strength is preferable in domestic paper, can wipe at home and not allow in the case where getting wet
Easily rupturable paper.
When the towel of going to the lavatory is wet tissue, non-woven fabrics or domestic paper is may be selected in the base fabric, i.e., the medical fluid is infiltrated institute
Stating base fabric can be obtained towel wet tissue of going to the lavatory.This field conventional technology can be used in the preparation method for towel wet tissue of going to the lavatory, in order to
Obtain the optimal towel wet tissue of going to the lavatory of effect, the present invention is preferably during towel wet tissue is gone to the lavatory in infiltration, use of the medical fluid with respect to base fabric
Amount is 4-6ml/g, after infiltration, drains the moisture for towel of going to the lavatory, reaches the wet tissue water content of this field routine.For
Medical fluid is set preferably to play antibacterial, disinfection, the infiltration amount that the present invention preferably controls final products Chinese medicine liquid is 4.5-
5.5g/g being advisable.
When the towel of going to the lavatory is dry towel, domestic paper is may be selected in the base fabric, the needle slurry of the preferably described domestic paper
Usage amount is 85% or more, and moisture is less than 9.0%.
Alternatively, the index of the ideal domestic paper at least meets 3 of following index or more (preferably meeting): thickness
For 0.05-0.07mm, longitudinal dry tensile strength is 2000-3200mN, and lateral dry tensile strength is 290-370mN, elongation 9%-11%,
2mm~5mm hole eye number≤6/m2, single layer transverse direction suction range is not less than 20mm/100s, and the double-deck transverse direction suction range is not less than
40mm/100s。
Preferably, the wettable domestic paper with a thickness of 0.05-0.06mm, longitudinal dry tensile strength is 2480-3000mN,
Lateral dry tensile strength is 290-320mN, elongation 10%-11%, 2mm~5mm hole eye number≤6/m2, single layer transverse direction suction range
Not less than 20mm/100s, the double-deck transverse direction suction range is not less than 40mm/100s.
The life stationery base fabric that the present invention can select further includes such as permanent wettable water paper handkerchief of peace product promise.
The present invention goes to the lavatory the medicine liquid spray the dry towel of towel to obtain the final product on base fabric (and can be described as body paper), the specific spray of medical fluid
The amount of spilling can be by those skilled in the art depending on the conventional selection of this field, foundation actual conditions, and medical fluid of the present invention exists
Fountain height in base fabric is preferably 0.006-0.008ml/g, and what this fountain height was prepared go to the lavatory, and towel medicine liquid spray is uniform, humidity
It is suitable for being easy to use.
In addition, above-mentioned base fabric has preferably covered one layer of smears, such base fabric softness moisturizing, while water imbibition on its surface
It is good, more skin-friendly strong with the towel water lock ability of going to the lavatory that this base fabric is prepared.The smears can be selected from commonly used in the art
Substance plays optimal effect in order to enable smears can preferably cooperate with medical fluid described herein, and the present invention is preferred
Above-mentioned smears is selected from one of moisturizer, softening agent, creams or a variety of, and (smears is opposite for its further preferred coating weight
In the mass percent dosage of base fabric) it is 18-25%.Wherein, the moisturizer be selected from glycerol, polyglycereol, transparent Bronsted acid sodium,
One or more of aloe extract.
Invention also provides the preparation methods of above-mentioned towel of going to the lavatory, as one of technical solution of the present invention, when described
When towel of going to the lavatory is wet tissue, preparation method specifically comprises the following steps:
(1) 8-12 parts of Cortex Dictamni extract, 12-18 parts of Radix Stemonae extract, 10-15 parts of Herba Senecionis Scandentis extract, sunglo is taken to mention
Take 6-10 parts of object, it is spare；
(2) each component in step (1) is dissolved in partial solvent, is stirred evenly；
(3) step (2) acquired solution is filtered, deposit is removed, takes supernatant, further add solvent thereto, it is fixed
Hold to 700-900 parts；Or it is further added in the supernatant and adds solvent constant volume again after spice additive and disappear to get antibacterial
Poison liquid；
(4) by the antibacterial disinfection medical fluid infiltration base fabric to get.
Preferably, step (4) Chinese medicine liquid is 4-6ml/g with respect to the dosage of base fabric.
Preferably, the solvent is 50-75% ethanol solution or water.
Wherein, step (2) is predissolve step, and the 8-12% of the partial solvent preferred solvent total volume, predissolve has
The abundant dissolution for helping active constituent, improves the quality of medical fluid.
As another technical solution of the invention, when the towel of going to the lavatory is dry towel, preparation method specifically include as
Lower step:
(1) 8-12 parts of Cortex Dictamni extract, 12-18 parts of Radix Stemonae extract, 10-15 parts of Herba Senecionis Scandentis extract, sunglo is taken to mention
Take 6-10 parts of object, it is spare；
(2) each component in step (1) is dissolved in partial solvent, is stirred evenly；
(3) step (2) acquired solution is filtered, deposit is removed, takes supernatant, further add solvent thereto, it is fixed
Hold to 200-400 parts；Or it is further added in the supernatant and adds solvent constant volume again after spice additive and disappear to get antibacterial
Poison liquid；
(4) by the antibacterial disinfection medical fluid be sprayed at scrim surfaces to get.
Fountain height of the medical fluid of the present invention in base fabric is preferably 0.006-0.008ml/g,
Preferably, the solvent is 50-75% ethanol solution or glycerine.
Step (2) is predissolve step, and the 8-12% of the partial solvent preferred solvent total volume, predissolve helps to live
The abundant dissolution of property ingredient, improves the quality of medical fluid.
Currently, life paper conversion mainly includes two processes: preceding processing and post-processing.Preceding processing refers to that body paper produces, rear to add
Work refer to the body paper after cutting is embossed, the processing such as Amscomatic.The present invention is in order to enable final products are more soft wet
Profit, pro-skin sense is stronger, and each layer of paper handkerchief is tightly combined, and is easy to use, and in this application, has been especially added with completely new middle processing skill
Art, which is to carry out roller coating or spray treatment to body paper using smears before post-processing, in addition, changing existing
" being first embossed, rear to fold " mode, using completely new " first folding, rear to be embossed " mode.
Concrete operations are as follows: in step (4), first base fabric is coated using smears, is then cut into base fabric specified
Breadth, then folded, be embossed, fold and embossing process in by the antibacterial disinfection medical fluid or antibacterial disinfection medical fluid
It is sprayed on the surface of base fabric with fragrance, finally product is packed, is sterilized.
The specification of towel of the present invention of going to the lavatory can be adjusted according to actual conditions, optimal size are as follows: 10cm × 14cm, thickness
16 layers, white embossing, with the fragrance tasteless, the fragrant and a variety of different type of Chinese medicine is light.
Towel of the present invention of going to the lavatory has the advantage that
(1) Cortex Dictamni extract in the present invention, Radix Stemonae extract, four kinds of Herba Senecionis Scandentis extract, extractive of usnea ingredients
Be used in combination, there is heat-clearing and damp-drying drug, eliminate dampness with aromatics, restraining and sterilizing bacteria, can prevent microorganism infection, when use have cleaning, it is comfortable,
Health-care effect.
(2) medical fluid tool of the invention is antibacterial, sterilization and antiinflammation, to skin and vaginal mucosa without any irritation and
Side effect, it is fragrant odour, easy to carry.
(3) go to the lavatory towel soft comfortable, good water absorption, the fungistatic effect prepared using medical fluid of the present invention is significant and has
The features such as easily disperse.
(4) the advantages that medical fluid of the present invention and towel of going to the lavatory are provided with low in cost, long shelf-life, high stability.
Detailed description of the invention
Fig. 1 is the preparation technology flow chart of towel dry towel of the invention of going to the lavatory.
Specific embodiment
The following examples are used to illustrate the present invention, but are not intended to limit the scope of the present invention..
All raw materials of the present invention are known commercially available product, and the detection method being related to or operation are such as without special
Explanation is the common detection methods or operation of this field.Cortex Dictamni extract involved in following embodiment, a thousand li light extraction
Object, Radix Stemonae extract extract by the following method.
Cortex Dictamni extract: smashing it through 30 meshes for cortex dictamni, according to the solid-liquid ratio (g:ml) of 1:18, uses volume fraction
90% EtOH Sonicate extracts 85min, and concentrated extracting solution is at the medicinal extract of relative density 1.1-1.3 to get, wherein ultrasonic extraction
Frequency be 40kHz, power 500W.
Herba Senecionis Scandentis extract: climbing groundsel is put in 60 DEG C of insulating boxs dry 1h, smashes it through 30 meshes；With being equivalent to it
12 times of 60% ethyl alcohol of quality extracts 3 times at 60 DEG C, and extraction time is respectively 2h, 1.5h, 1h, combined extract and is concentrated respectively
At relative density be 1.1-1.3 medicinal extract to get.
Radix Stemonae extract: smashing it through 30 meshes for the tuber of stemona, according to the solid-liquid ratio (g:ml) of 1:18, with mass fraction 75%
Ethyl alcohol extract 13.5h at 55-58 DEG C, concentrated extracting solution at the medicinal extract that relative density is 1.1-1.3 to obtain the final product.
Extractive of usnea: smashing it through 30 meshes for sunglo, according to the solid-liquid ratio of 1:20, with the ethyl alcohol of volume fraction 95%
It is extracted 4 times at 70 DEG C, extraction time is respectively 4h, 3h, 2.5-3h, 2h, combined extract and is condensed into relative density respectively
For 1.1-1.3 medicinal extract to get.
Although a kind of above-mentioned specific embodiment for being only exemplified by each extract, it will be appreciated by those skilled in the art that
Be be not limited to other extracting methods (method especially in the limited range of the present invention) of ad hoc fashion similarly can be with
It realizes essentially identical extraction effect, can be used for realizing the present invention, this is no longer particularly limited.
Only as explaining, such as Cortex Dictamni extract obtained may be equally applied to the present invention in accordance with the following methods:
Cortex Dictamni extract: smashing it through 30 meshes for cortex dictamni, according to the solid-liquid ratio (g:ml) of 1:16 or 1:19, uses body
Fraction 88 or 92% EtOH Sonicate extract 83-87min, concentrated extracting solution at the medicinal extract of relative density 1.1~1.3 to get,
Wherein, the frequency of ultrasonic extraction is 60kHz, power 400W.
The parameter of wettable domestic paper used in following embodiment is as follows: with a thickness of 0.05-0.06mm, longitudinal dry tensile strength
For 2480-3000mN, lateral dry tensile strength is 290-320mN, elongation 10%-11%, 2mm~5mm hole eye number≤6/m2, single
The lateral suction range of layer is not less than 20mm/100s, and the double-deck transverse direction suction range is not less than 40mm/100s.
It will be appreciated by persons skilled in the art that other suitable paper products can in addition to above-mentioned preferred wettable domestic paper
It is equally used for realizing the present invention.
Embodiment 1
It present embodiments provides a kind of with antibacterial, disinfection medical fluid；The specific prescription of the medical fluid is as follows: shaggy-fruited dittany
8 parts of bark extract, 12 parts of Radix Stemonae extract, 10 parts of Herba Senecionis Scandentis extract, 6 parts of extractive of usnea, 1 part of daphne odera essential oil, water 800
Part.
Embodiment 2
It present embodiments provides a kind of with antibacterial, disinfection medical fluid；The specific prescription of the medical fluid is as follows: shaggy-fruited dittany
10 parts of bark extract, 15 parts of Radix Stemonae extract, 12 parts of Herba Senecionis Scandentis extract, 8 parts of extractive of usnea, 1 part of daphne odera essential oil, 60%
300 parts of ethyl alcohol.
Embodiment 3
It present embodiments provides a kind of with antibacterial, disinfection medical fluid；The specific prescription of the medical fluid is as follows: shaggy-fruited dittany
12 parts of bark extract, 18 parts of Radix Stemonae extract, 15 parts of Herba Senecionis Scandentis extract, 10 parts of extractive of usnea, 300 parts of glycerine.
Embodiment 4
It present embodiments provides a kind of with antibacterial, disinfection medical fluid；The specific prescription of the medical fluid is as follows: shaggy-fruited dittany
10 parts of bark extract, 16 parts of Radix Stemonae extract, 15 parts of Herba Senecionis Scandentis extract, 9 parts of extractive of usnea, 70% 300 parts of ethyl alcohol.
Embodiment 5
A kind of method prepared described in embodiment 1 with antibacterial, disinfection towel of going to the lavatory is present embodiments provided, specifically
Include the following steps:
(1) Cortex Dictamni extract, Herba Senecionis Scandentis extract, Radix Stemonae extract, extractive of usnea are dissolved in 80 parts of water, are stirred
Uniformly；
(2) step (1) acquired solution is filtered, deposit is removed, takes supernatant, daphne odera essential oil is added thereto, so
After add remaining water, be uniformly mixed up to antibacterial disinfection medical fluid；
(3) non-woven fabrics that the antibacterial disinfection medical fluid infiltration is cut into suitable dimension, is packed to obtain the final product.
Wherein, go to the lavatory towel Chinese medicine liquid infiltration amount be 4-6g/g.
Embodiment 6
A kind of method prepared described in embodiment 2 with antibacterial, disinfection towel of going to the lavatory is present embodiments provided, specifically
Include the following steps (as shown in Figure 1):
(1) Cortex Dictamni extract, Herba Senecionis Scandentis extract, Radix Stemonae extract, extractive of usnea are dissolved in 30 part of 60% ethyl alcohol
In, it stirs evenly；
(2) step (1) acquired solution is filtered, deposit is removed, takes supernatant, daphne odera essential oil is added thereto, is mended
Add remaining ethyl alcohol, is uniformly mixed up to antibacterial disinfection medical fluid；
(3) first wettable domestic paper (and can claim body paper) is coated with using rolling method using glycerol (coating weight 20%), then
Paper product is cut into 10cm × 14cm breadth, then folded, be embossed, by the antibacterial disinfection in folding and embossing process
Medical fluid (fountain height 0.006-0.008ml/g) is sprayed on the surface of paper product, is finally packed to product, ethylene oxide sterilizing
To obtain the final product.
Embodiment 7
A kind of method prepared described in embodiment 3 with antibacterial, disinfection towel of going to the lavatory is present embodiments provided, specifically
Include the following steps:
(1) Cortex Dictamni extract, Herba Senecionis Scandentis extract, Radix Stemonae extract, extractive of usnea are dissolved in 36 parts of glycerine,
It stirs evenly；
(2) step (1) acquired solution is filtered, deposit is removed, takes supernatant, add remaining glycerine, is uniformly mixed
Up to antibacterial disinfection medical fluid；
(3) first wettable domestic paper is coated with using polyglycereol (coating weight 18%) using rolling method, then cuts paper product
It at 10cm × 14cm breadth, then folded, be embossed, be sprayed on the antibacterial disinfection medical fluid in embossing process folding
The surface (fountain height 0.006-0.008ml/g) of paper product, finally product is packed, ethylene oxide sterilizing to obtain the final product.
Embodiment 8
A kind of method prepared described in embodiment 4 with antibacterial, disinfection towel of going to the lavatory is present embodiments provided, specifically
Include the following steps:
(1) Cortex Dictamni extract, Herba Senecionis Scandentis extract, Radix Stemonae extract, extractive of usnea are dissolved in 24 part of 70% ethyl alcohol
In, it stirs evenly；
(2) step (1) acquired solution is filtered, deposit is removed, takes supernatant, add remaining ethyl alcohol, is uniformly mixed i.e.
Obtain antibacterial disinfection medical fluid；
(3) first wettable domestic paper is used using softening agent SME-4 (polyoxyethylene stearic acid ester, coating weight 25%) and is sprayed
Method coating, then cuts into 10cm × 14cm breadth for paper product, is then folded, is embossed, will in folding and embossing process
The antibacterial disinfection medical fluid is sprayed on the surface (fountain height 0.006-0.008ml/g) of paper product, is finally packed, is gone out to product
Bacterium to obtain the final product.
Below by way of fungistatic effect, the stability etc. for testing medical fluid of the present invention and towel of going to the lavatory, the present invention is protected
Technical solution be further described.
The experiment of one fungistatic effect of experimental example
1, medical fluid fungistatic effect is tested
1.1 experiment reagents (see Table 1 for details):
Table 1:
Licorice, camomile extract and aloe extract etc. can be right by commercially available in above-mentioned control group
Preparation according to Fructus Gleditsiae Abnormalis extract in group 6 can refer to China application CN103340816.
1.2 experimental method
Experimental strain: staphylococcus aureus, Candida albicans, Escherichia coli, Pseudomonas aeruginosa, hemolytic streptococcus；Tool
Regulation of the body experimental procedure with reference to " 15979-2002 disposable sanitary articles sanitary standard ".
1.3 experimental result
Experimental result is shown in Table 2:
Table 2: bacteriostasis rate (%)
Above-mentioned experiment is repeated with the medical fluid of other embodiments of the present invention, obtains essentially identical experiment conclusion.
2, wet tissue fungistatic effect is tested
2.1 experiment reagents (see Table 3 for details):
Table 3:
| Experimental group 1 | The preparation-obtained wet tissue of embodiment 5 (the infiltration amount of medical fluid is 5g/g, and liquid formula is with embodiment 1) |
| Compare blank group | With experimental group 1, difference is only that wet tissue preparation method: infiltrating non-woven fabrics using physiological saline |
| Control group 1 | With experimental group 1, difference is only that wet tissue preparation method: using the active constituent of control group 1 |
| Control group 2 | With experimental group 1, difference is only that wet tissue preparation method: using the active constituent of control group 2 |
| Control group 3 | With experimental group 1, difference is only that wet tissue preparation method: using the active constituent of control group 3 |
| Control group 4 | With experimental group 1, difference is only that wet tissue preparation method: using the active constituent of control group 4 |
| Control group 5 | With experimental group 1, difference is only that wet tissue preparation method: using the active constituent of control group 5 |
| Control group 6 | With experimental group 1, difference is only that wet tissue preparation method: using the active constituent of control group 6 |
2.2 experimental methods:
With 2.1.
2.3 experimental result
See Table 4 for details for experimental result.
Table 4: bacteriostasis rate (%)
3, dry towel fungistatic effect experiment
3.1 experiment reagents (see Table 5 for details):
Table 5:
| Experimental group 1 | The preparation-obtained dry towel of embodiment 6 (liquid formula is with embodiment 2) |
| Compare blank group | With experimental group 1, difference is only that dry towel preparation method: using the active constituent of blank control group |
| Control group 1 | With experimental group 1, difference is only that dry towel preparation method: using the active constituent of control group 1 |
| Control group 2 | With experimental group 1, difference is only that dry towel preparation method: using the active constituent of control group 2 |
| Control group 3 | With experimental group 1, difference is only that dry towel preparation method: using the active constituent of control group 3 |
| Control group 4 | With experimental group 1, difference is only that dry towel preparation method: using the active constituent of control group 4 |
| Control group 5 | With experimental group 1, difference is only that dry towel preparation method: using the active constituent of control group 5 |
| Control group 6 | With experimental group 1, difference is only that dry towel preparation method: using the active constituent of control group 6 |
3.2 experimental methods: with 2.2；
3.3 experimental result
See Table 6 for details for experimental result.
Table 6: bacteriostasis rate (%)
4, wet tissue and the experiment of the long-time stability of dry towel
Experimental subjects: the table 3 after placing 3,6,12 and 24 months after preparation respectively and wet tissue and dry towel in table 5；
Experimental method: with 2.2 and 3.2；
Experimental result is shown in Table 7.
Table 7: bacteriostasis rate (%)
Two wet tissue of experimental example, dry towel skin irritation test
Laboratory sample: dry towel in wet tissue and table 2 in table 1
Experimental method: experiment before rabbit back spinal diamond wool is cut for 24 hours, unhairing range or so give 5cm × 5cm, one
For testing, skin is cleaned for compareing, using warm water in side for side, then wipes laboratory sample on a side test skin,
Wiping 1 time daily, 1h observes skin wound repair after wiping, and continuous wiping 30 days records experimental result.
Experimental result: as shown in table 8.
8 skin irritation test result of table:
Three wet tissue of experimental example, the experiment of dry towel vaginal irritation
Laboratory sample: dry towel in wet tissue and table 2 in table 1
Experimental method: taking SD rat, and female, regular grade, weight 220-240g is randomly divided into 16 groups, every group 4.Reference
3.8 in disinfection technology standard (third edition) 1999.11, dry towel, wet tissue are placed in animal intravaginal, contacted with vagina mucosa
2h, puts to death animal after 12h, takes out vagina local organization, and observation is whether there is or not congested, oedema phenomenon, referring to disinfection technology standard (the
Three editions) the standards of grading scoring of skin wound repair intensity and skin irritatin strength grading in 1999.11, it carries out to vagina mucosa
The evaluation of stimulus intensity.
Experimental result: 9 are shown in Table.
9 vaginal irritation experimental result of table:
Wet tissue of the present invention, dry towel are 0 to rat vagina mucosal irritation reaction top mean value, belong to nonirritant,
Shelf-life is 36 months or more.
Experimental example four is gone to the lavatory towel comprehensive quality test experiments
1, by carrying out test discovery to towel of going to the lavatory described in embodiment 6~8, the towel of going to the lavatory being related in above-described embodiment
Dry towel can reach index as shown in table 10, and properties are superior to GB/T 20808-2011 to the regulation of super soft paper.
It goes to the lavatory described in 10 embodiment 6-8 of table the product index of the dry towel of towel
2, to embodiment 6 go to the lavatory towel and common commercially available towel products compare, three control groups, control group are set
The 1 nose noble's face tissue produced for Japanese king's paper industry, control group 2 is a tissue of Ni Piao company production, and control group 3 is
Heng An group heart chief minister's seal tea family of languages column paper handkerchief, as a result as shown in table 11.
Table 11 is gone to the lavatory towel product actual measurement physical index and correlation data
As can be seen from Table 11, the present invention goes to the lavatory, and towel moisture content is suitable, and pliability is good, and has good dry drawing
Power and wet tensile strength, entire product sense of touch is soft and moist, and pro-skin sense is strong.
Experimental example five is gone to the lavatory towel material test experiments
The present invention further compared going to the lavatory the material of towel and conventional paper handkerchief, and specific targets are as follows:
1, body-sensing
Body-sensing refers to comfort when consumer's physical examination product, and the comfort of product is better, and body-sensing is better.Material
Body-sensing comfort be realized by improving 3 indexs of moisture feeling of the flexibility of paper, surface sophistication and paper, and then reach with
Nowadays the domestic paper that women generally uses is compared, and has apparent sense of touch otherness.
(1) flexibility
The pliability of domestic paper includes bulk softness and Surface softness.Bulk softness refers to when people with the hands squeeze
Platen towel Shi Suoneng experiences the softness of paper；Surface softness refers to finger tip slight amount, and touches paper back and forth and felt
Softness by paper.According to GB/T 20808-2011 to the regulation of super soft paper, single-part stationery pliability is necessary≤40mN.
(2) surface sophistication
Currently without specific detection means, mainly by user's finger tip slight amount, and paper is touched back and forth and is felt
Judged by the softness of paper, belongs to an importance in body-sensing.
(3) moisture feeling
Moisture feeling belongs to the new concept in domestic paper, is put forward for the first time for the application.According to GB/T 20808-2011 to super soft paper
Regulation, delivery moisture be≤9%.
2, water imbibition
Mainly measured by lateral suction range, according to GB/T 20808-2011 to the regulation of super soft paper, single-part stationery
Lateral suction range is greater than 20mm/100s.
3, breaking up property
For tissue Related product, breaking up property is mainly influenced by the additive amount of wet strength agent.Good paper product can reach
It abandons after to use in closestool, does not block closestool and sewer, it is degradable, it is free from environmental pollution.
4, toughness
Lateral tensile index and longitudinal wet tensile index are better than GB/T 20808-2011 to the regulation of super soft paper, to reach
To that will not be broken easily when body paper normal use use, deform.
It is found by comparison, its pliability of currently marketed paper handkerchief is of the present invention small generally between 38-40mN
Solution its pliability of towel is 30 ± 2mN, belongs to the high-class product in super soft paper；The moisture of paper handkerchief is commonly 7% or so on Vehicles Collected from Market,
The present invention goes to the lavatory, and towel water conservation moisture pick-up properties is good, and paper handkerchief moisture content remains between 15-18%, and exquisiteness is good, and sense of touch is soft
Profit, pro-skin sense are strong；In addition, the present invention goes to the lavatory, the water imbibition of towel also meets national standard, and has good easily disperse, uses
After abandon in closestool, do not block closestool and sewer, it is degradable, it is free from environmental pollution.
In addition to this, table 12 has also listed other differences of go to the lavatory towel and conventional paper handkerchief of the invention.
Table 12 is gone to the lavatory the difference of towel and conventional paper handkerchief
Experimental example six is gone to the lavatory towel market questionnaire investigation
The present invention has carried out questionnaire investigation to towel of going to the lavatory simultaneously, as a result as shown in table 13: having 70.29% women to think very
Like going to the lavatory the texture of towel, 26.43% women waits and see.Generally speaking, the public to the degree of recognition of product close to 80%,
There are extraordinary market prospects.
Degree of recognition of 13 public of table to towel product of going to the lavatory at this stage
The above shows and describes the basic principles and main features of the present invention and the advantages of the present invention.The technology of the industry
Personnel are it should be appreciated that the present invention is not limited to the above embodiments, and the above embodiments and description only describe this
The principle of invention, without departing from the spirit and scope of the present invention, various changes and improvements may be made to the invention, this is to this
It is for the technical staff of field it will be apparent that these changes and improvements all fall within the protetion scope of the claimed invention.This hair
Bright claimed range is defined by the appending claims and its equivalent thereof.
Claims (13)
1. a kind of with antibacterial, disinfection medical fluid, it is characterised in that: by weight, the active constituent of the medical fluid is such as
Under: 8-12 parts of Cortex Dictamni extract, 12-18 parts of Radix Stemonae extract, 10-15 parts of Herba Senecionis Scandentis extract, 6-10 parts of extractive of usnea；
The extracting method of the Cortex Dictamni extract is as follows: by cortex dictamni grinding and sieving, according to the solid-liquid ratio of 1:15-1:20,
Extract 80-90min with the EtOH Sonicate of volume fraction 85%~95%, concentrated extracting solution at medicinal extract to get；
The extracting method of the Radix Stemonae extract is as follows: tuber of stemona grinding and sieving is used according to the solid-liquid ratio of 1:10-1:20
The ethyl alcohol of 70%-80% extracts 12.5-14.5h at 50-60 DEG C, concentrated extracting solution at medicinal extract to get；
The extracting method of the Herba Senecionis Scandentis extract is as follows: climbing groundsel being put in 55-65 DEG C of insulating box dry 0.5-2h, is crushed
After be sieved；It is extracted 2-4 times at 55-65 DEG C with the 50-70% ethyl alcohol for being equivalent to 10-14 times of its quality, extraction time is every time
1-3h combined extract and is condensed into medicinal extract respectively；
The extracting method of the extractive of usnea is as follows: sunglo grinding and sieving is used body according to the solid-liquid ratio of 1:15-1:25
The ethyl alcohol of fraction 90%-95% extracts 1-5 times at 60-90 DEG C, and extraction time is 1-4h every time, and difference combined extract is simultaneously
Be condensed into medicinal extract to get.
2. medical fluid as described in claim 1, it is characterised in that: by weight, the active constituent of the medical fluid is as follows: shaggy-fruited dittany
10 parts of bark extract, 15 parts of Radix Stemonae extract, 12 parts of Herba Senecionis Scandentis extract, 8 parts of extractive of usnea.
3. medical fluid as claimed in claim 1 or 2, it is characterised in that: the extracting method of the Cortex Dictamni extract is as follows: will be white
Fresh hide smashes it through 30 meshes, according to the solid-liquid ratio of 1:16-1:19, extracts 83- with the EtOH Sonicate of volume fraction 88%-92%
87min, concentrated extracting solution at the medicinal extract of relative density 1.1-1.3 to get.
4. medical fluid as claimed in claim 1 or 2, it is characterised in that: the extracting method of the Radix Stemonae extract is as follows: by the tuber of stemona
30 meshes are smashed it through, according to the solid-liquid ratio of 1:15-1:20, are extracted at 55-58 DEG C with the ethyl alcohol of mass fraction 72%-78%
12.6-14.2h, concentrated extracting solution at relative density be 1.1-1.3 medicinal extract to obtain the final product.
5. medical fluid as claimed in claim 1 or 2, it is characterised in that: climbing groundsel is put in 60 DEG C of insulating boxs dry 1h, is crushed
30 meshes are crossed afterwards；Extracted 3 times at 60 DEG C with 12 times of 60% ethyl alcohol of its quality is equivalent to, extraction time be respectively 2h, 1.5h,
1h, respectively combined extract and be condensed into relative density be 1.1-1.3 medicinal extract to get.
6. medical fluid as claimed in claim 1 or 2, it is characterised in that: the extracting method of the extractive of usnea is as follows: by sunglo
30 meshes are smashed it through, according to the solid-liquid ratio of 1:18-1:22, extract 2-4 at 65-75 DEG C with the ethyl alcohol of volume fraction 95%
Secondary, extraction time is 2-4h every time, respectively combined extract and be condensed into relative density be 1.1-1.3 medicinal extract to get.
7. medical fluid as claimed in claim 1 or 2, it is characterised in that: the medical fluid is with ethanol water, water, propylene glycol or third
Glycol is as solvent.
8. medical fluid as claimed in claim 7, it is characterised in that: the dosage of the solvent is 200-900 parts by weight.
9. medical fluid as claimed in claim 1 or 2, it is characterised in that: it further include spice additive in the medical fluid, the fragrance
Additive includes pure natural spice or artificial flavors.
10. medical fluid as claimed in claim 9, it is characterised in that: the pure natural spice is selected from elscholtiza, borneol, oriental wormwood, peppermint
One or more of hydrosol and yellow wormwood artemisia；The artificial flavors include plants essential oil and chemical synthesis essence；The plants essential oil
Selected from Chinese torreya essential oil, mother chrysanthemum flower essential oil, daphne odera essential oil, pinecone essential oil, mugwort oil, thyme essential oil, eucalyptus quintessence oil, tea tree
One or more of essential oil and camphor tree essential oil.
11. any one of the claim 1-10 medical fluid is preparing the application in hygienic articles.
12. application according to claim 11, it is characterised in that: the hygienic articles are wet tissue or dry towel.
13. application according to claim 12, it is characterised in that: the hygienic articles are go to the lavatory towel, sanitary napkin or disinfection
Paper.
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|---|---|---|---|---|
| CN101167934A (en) * | 2007-10-17 | 2008-04-30 | 广西仙草堂制药有限责任公司 | 'Jinsong' itching-relieving lotion |
| CN103800510A (en) * | 2014-02-18 | 2014-05-21 | 扈建民 | External washing liquor composition and preparation method thereof |
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| CN101167934A (en) * | 2007-10-17 | 2008-04-30 | 广西仙草堂制药有限责任公司 | 'Jinsong' itching-relieving lotion |
| CN104666516A (en) * | 2013-11-29 | 2015-06-03 | 康普药业股份有限公司 | Anti-inflammatory leucorrhoea arresting washing liquor |
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