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CN105367087A - Magnesia refractory material binder and preparation method thereof - Google Patents

Magnesia refractory material binder and preparation method thereof Download PDF

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Publication number
CN105367087A
CN105367087A CN201410411800.2A CN201410411800A CN105367087A CN 105367087 A CN105367087 A CN 105367087A CN 201410411800 A CN201410411800 A CN 201410411800A CN 105367087 A CN105367087 A CN 105367087A
Authority
CN
China
Prior art keywords
binder
preparation
magnesia refractory
refractory material
solvent
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201410411800.2A
Other languages
Chinese (zh)
Inventor
张磊
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Qingdao Weiye Forging Machinery Co Ltd
Original Assignee
Qingdao Weiye Forging Machinery Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Qingdao Weiye Forging Machinery Co Ltd filed Critical Qingdao Weiye Forging Machinery Co Ltd
Priority to CN201410411800.2A priority Critical patent/CN105367087A/en
Publication of CN105367087A publication Critical patent/CN105367087A/en
Pending legal-status Critical Current

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Abstract

The invention relates to a magnesia refractory material binder and a preparation method thereof. The magnesia refractory material binder comprises 40-70wt% of phenolic resin, 10-30wt% of aromatic polyester, 5-25wt% of a solvent and 5-25wt% of a reinforcing agent. The preparation method greatly reduces the production cost, and has obvious economic and social benefits. The binder has stable and reliable quality; and an examination result shows that the performance indexes of the binder reach standards of present binders, and the solid content and the carbon residue are obviously higher than those of present refractory material binders, so the performance indexes of refractory materials are improved.

Description

A kind of binder for making magnesia refractory and preparation method thereof
Technical field
The present invention relates to technical field of refractory materials, particularly relate to a kind of binder for making magnesia refractory and preparation method thereof.
Background technology
At present, domestic existing binder for fire-resistant materials, general employing thermoplasticity or heat-reactive phenolic resin, producer generally reflects that its production cost is higher, and due to bonding agent kind single, the different needs that high, medium and low magnesite refractory is produced can not be met, all adopt high-grade thermoplasticity or heat-reactive phenolic resin bonding agent at present, expensive, so, research and develop the magnesite refractory bonding agent of different class, imperative.
Summary of the invention
The object of this invention is to provide the series product of binder for magnesium carbonaceous fire-resistant material, greatly reduce production cost, and be divided into high, medium and low, can according to carbonic refractory material in magnesium texture need select, its constant product quality, can meet the production requirement of carbonic refractory material in magnesium texture.
For achieving the above object, technical scheme of the present invention is described below:
A kind of binder for making magnesia refractory and preparation method thereof, is made up of by weight proportion following material:
Resol 40-70%
Fragrance aromatic polyester 10-30%
Solvent 5-25%
Toughener 5-25%.
Described manufacture method is: phenol and formaldehyde are after catalyzed polycondensation reaction terminates, form resol, then add aromatic polyester to carry out heating, stir, dewater, moisture is made to reach less than 10%, after moisture is qualified, use solvent adjustment viscosity again, viscosity controls at 1-30PaS according to the requirement of user.
Described solvent refers to one or more mixing in alcohols, ester class, benzene class or tarry cut, and described toughener is tetramethylolmethane.
Compared with prior art, the invention has the beneficial effects as follows: the series product providing binder for magnesium carbonaceous fire-resistant material, production cost significantly reduces, and has obvious economic benefit and social benefit.Stable and reliable product quality, by inspection, the performance index of this bonding agent reach the standard of now educating bonding agent, and solids content and remaining carbon are apparently higher than existing binder for fire-resistant materials, and the performance index of refractory materials are also increased.
Embodiment
Embodiment 1
A kind of binder for making magnesia refractory and preparation method thereof, is made up of by weight proportion following material:
Resol 55%
Fragrance aromatic polyester 25%
Solvent 10%
Toughener 10%.
Described solvent refers to alcohols and benzene class mixture, and described toughener is tetramethylolmethane.
Described manufacture method is: phenol and formaldehyde are after catalyzed polycondensation reaction terminates, form resol, then add aromatic polyester to carry out heating, stir, dewater, moisture is made to reach less than 10%, after moisture is qualified, use solvent adjustment viscosity again, viscosity controls at 1-30PaS according to the requirement of user.
Embodiment 2
A kind of binder for making magnesia refractory and preparation method thereof, is made up of by weight proportion following material:
Resol 60%
Fragrance aromatic polyester 15%
Solvent 10%
Toughener 15%.
Described solvent refers to the mixture of ester class, benzene class and tarry cut, and described toughener is tetramethylolmethane.
Described manufacture method is: phenol and formaldehyde are after catalyzed polycondensation reaction terminates, form resol, then add aromatic polyester to carry out heating, stir, dewater, moisture is made to reach less than 10%, after moisture is qualified, use solvent adjustment viscosity again, viscosity controls at 1-30PaS according to the requirement of user.

Claims (3)

1. binder for making magnesia refractory and preparation method thereof, is characterized in that it is made up of by weight proportion following material:
Resol 40-70%
Fragrance aromatic polyester 10-30%
Solvent 5-25%
Toughener 5-25%.
2. a kind of binder for making magnesia refractory according to claim l and preparation method thereof agent, it is characterized in that described manufacture method is: phenol and formaldehyde are after catalyzed polycondensation reaction terminates, form resol, then add aromatic polyester to carry out heating, stir, dewater, moisture is made to reach less than 10%, after moisture is qualified, use solvent adjustment viscosity again, viscosity controls at 1-30PaS according to the requirement of user.
3. a kind of binder for making magnesia refractory according to claim l, is characterized in that: described solvent refers to one or more mixing in alcohols, ester class, benzene class or tarry cut, and described toughener is tetramethylolmethane.
CN201410411800.2A 2014-08-21 2014-08-21 Magnesia refractory material binder and preparation method thereof Pending CN105367087A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201410411800.2A CN105367087A (en) 2014-08-21 2014-08-21 Magnesia refractory material binder and preparation method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201410411800.2A CN105367087A (en) 2014-08-21 2014-08-21 Magnesia refractory material binder and preparation method thereof

Publications (1)

Publication Number Publication Date
CN105367087A true CN105367087A (en) 2016-03-02

Family

ID=55369792

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201410411800.2A Pending CN105367087A (en) 2014-08-21 2014-08-21 Magnesia refractory material binder and preparation method thereof

Country Status (1)

Country Link
CN (1) CN105367087A (en)

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Legal Events

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C06 Publication
PB01 Publication
WD01 Invention patent application deemed withdrawn after publication

Application publication date: 20160302

WD01 Invention patent application deemed withdrawn after publication