CN105154228B - Cigarette is with plant flavone essence cigarette pearl and preparation method thereof - Google Patents
Cigarette is with plant flavone essence cigarette pearl and preparation method thereof Download PDFInfo
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- CN105154228B CN105154228B CN201510337696.1A CN201510337696A CN105154228B CN 105154228 B CN105154228 B CN 105154228B CN 201510337696 A CN201510337696 A CN 201510337696A CN 105154228 B CN105154228 B CN 105154228B
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- cigarette
- plant flavone
- essence
- flavone essence
- pearl
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- 229930003944 flavone Natural products 0.000 title claims abstract description 68
- 235000011949 flavones Nutrition 0.000 title claims abstract description 68
- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 61
- VHBFFQKBGNRLFZ-UHFFFAOYSA-N vitamin p Natural products O1C2=CC=CC=C2C(=O)C=C1C1=CC=CC=C1 VHBFFQKBGNRLFZ-UHFFFAOYSA-N 0.000 title claims abstract description 58
- GAMYVSCDDLXAQW-AOIWZFSPSA-N Thermopsosid Natural products O(C)c1c(O)ccc(C=2Oc3c(c(O)cc(O[C@H]4[C@H](O)[C@@H](O)[C@H](O)[C@H](CO)O4)c3)C(=O)C=2)c1 GAMYVSCDDLXAQW-AOIWZFSPSA-N 0.000 title claims abstract description 57
- 150000002212 flavone derivatives Chemical class 0.000 title claims abstract description 52
- 238000002360 preparation method Methods 0.000 title claims abstract description 10
- 241000196324 Embryophyta Species 0.000 claims abstract description 54
- IYRMWMYZSQPJKC-UHFFFAOYSA-N kaempferol Chemical compound C1=CC(O)=CC=C1C1=C(O)C(=O)C2=C(O)C=C(O)C=C2O1 IYRMWMYZSQPJKC-UHFFFAOYSA-N 0.000 claims abstract description 18
- 239000011122 softwood Substances 0.000 claims abstract description 15
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 11
- PFTAWBLQPZVEMU-DZGCQCFKSA-N (+)-catechin Chemical compound C1([C@H]2OC3=CC(O)=CC(O)=C3C[C@@H]2O)=CC=C(O)C(O)=C1 PFTAWBLQPZVEMU-DZGCQCFKSA-N 0.000 claims abstract description 9
- 239000001100 (2S)-5,7-dihydroxy-2-(3-hydroxy-4-methoxyphenyl)chroman-4-one Substances 0.000 claims abstract description 9
- UBSCDKPKWHYZNX-UHFFFAOYSA-N Demethoxycapillarisin Natural products C1=CC(O)=CC=C1OC1=CC(=O)C2=C(O)C=C(O)C=C2O1 UBSCDKPKWHYZNX-UHFFFAOYSA-N 0.000 claims abstract description 9
- 238000004090 dissolution Methods 0.000 claims abstract description 9
- AIONOLUJZLIMTK-AWEZNQCLSA-N hesperetin Chemical compound C1=C(O)C(OC)=CC=C1[C@H]1OC2=CC(O)=CC(O)=C2C(=O)C1 AIONOLUJZLIMTK-AWEZNQCLSA-N 0.000 claims abstract description 9
- AIONOLUJZLIMTK-UHFFFAOYSA-N hesperetin Natural products C1=C(O)C(OC)=CC=C1C1OC2=CC(O)=CC(O)=C2C(=O)C1 AIONOLUJZLIMTK-UHFFFAOYSA-N 0.000 claims abstract description 9
- 229960001587 hesperetin Drugs 0.000 claims abstract description 9
- 235000010209 hesperetin Nutrition 0.000 claims abstract description 9
- FTODBIPDTXRIGS-UHFFFAOYSA-N homoeriodictyol Natural products C1=C(O)C(OC)=CC(C2OC3=CC(O)=CC(O)=C3C(=O)C2)=C1 FTODBIPDTXRIGS-UHFFFAOYSA-N 0.000 claims abstract description 9
- MWDZOUNAPSSOEL-UHFFFAOYSA-N kaempferol Natural products OC1=C(C(=O)c2cc(O)cc(O)c2O1)c3ccc(O)cc3 MWDZOUNAPSSOEL-UHFFFAOYSA-N 0.000 claims abstract description 9
- 235000008777 kaempferol Nutrition 0.000 claims abstract description 9
- UXOUKMQIEVGVLY-UHFFFAOYSA-N morin Natural products OC1=CC(O)=CC(C2=C(C(=O)C3=C(O)C=C(O)C=C3O2)O)=C1 UXOUKMQIEVGVLY-UHFFFAOYSA-N 0.000 claims abstract description 9
- 238000003756 stirring Methods 0.000 claims abstract description 9
- 239000000853 adhesive Substances 0.000 claims abstract description 8
- 230000001070 adhesive effect Effects 0.000 claims abstract description 8
- 238000000034 method Methods 0.000 claims description 7
- 238000001035 drying Methods 0.000 claims description 6
- 239000002245 particle Substances 0.000 claims description 3
- 229920002134 Carboxymethyl cellulose Polymers 0.000 claims description 2
- 229920002153 Hydroxypropyl cellulose Polymers 0.000 claims description 2
- WHNWPMSKXPGLAX-UHFFFAOYSA-N N-Vinyl-2-pyrrolidone Chemical compound C=CN1CCCC1=O WHNWPMSKXPGLAX-UHFFFAOYSA-N 0.000 claims description 2
- 239000001768 carboxy methyl cellulose Substances 0.000 claims description 2
- 235000010948 carboxy methyl cellulose Nutrition 0.000 claims description 2
- 239000008112 carboxymethyl-cellulose Substances 0.000 claims description 2
- 239000001863 hydroxypropyl cellulose Substances 0.000 claims description 2
- 235000010977 hydroxypropyl cellulose Nutrition 0.000 claims description 2
- 239000001866 hydroxypropyl methyl cellulose Substances 0.000 claims description 2
- 229920003088 hydroxypropyl methyl cellulose Polymers 0.000 claims description 2
- 235000010979 hydroxypropyl methyl cellulose Nutrition 0.000 claims description 2
- UFVKGYZPFZQRLF-UHFFFAOYSA-N hydroxypropyl methyl cellulose Chemical compound OC1C(O)C(OC)OC(CO)C1OC1C(O)C(O)C(OC2C(C(O)C(OC3C(C(O)C(O)C(CO)O3)O)C(CO)O2)O)C(CO)O1 UFVKGYZPFZQRLF-UHFFFAOYSA-N 0.000 claims description 2
- 235000013855 polyvinylpyrrolidone Nutrition 0.000 claims description 2
- 229920000036 polyvinylpyrrolidone Polymers 0.000 claims description 2
- 229940069328 povidone Drugs 0.000 claims description 2
- 244000080767 Areca catechu Species 0.000 claims 1
- 235000006226 Areca catechu Nutrition 0.000 claims 1
- 150000002576 ketones Chemical class 0.000 claims 1
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 abstract description 35
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 abstract description 13
- 239000003546 flue gas Substances 0.000 abstract description 13
- 150000002213 flavones Chemical class 0.000 abstract description 11
- ADRVNXBAWSRFAJ-UHFFFAOYSA-N catechin Natural products OC1Cc2cc(O)cc(O)c2OC1c3ccc(O)c(O)c3 ADRVNXBAWSRFAJ-UHFFFAOYSA-N 0.000 abstract description 8
- 235000005487 catechin Nutrition 0.000 abstract description 8
- 229950001002 cianidanol Drugs 0.000 abstract description 8
- 230000000694 effects Effects 0.000 abstract description 8
- 239000000126 substance Substances 0.000 abstract description 8
- 150000003254 radicals Chemical class 0.000 abstract description 6
- 239000000779 smoke Substances 0.000 abstract description 6
- 230000008901 benefit Effects 0.000 abstract description 4
- 241001044671 Piper tuberculatum Species 0.000 abstract description 2
- 230000009467 reduction Effects 0.000 abstract description 2
- 230000035943 smell Effects 0.000 abstract description 2
- -1 flavone compound Chemical class 0.000 description 16
- 229960003742 phenol Drugs 0.000 description 15
- 150000002989 phenols Chemical class 0.000 description 8
- 239000011230 binding agent Substances 0.000 description 6
- 239000012530 fluid Substances 0.000 description 6
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 6
- 230000000391 smoking effect Effects 0.000 description 5
- YCIMNLLNPGFGHC-UHFFFAOYSA-N catechol Chemical compound OC1=CC=CC=C1O YCIMNLLNPGFGHC-UHFFFAOYSA-N 0.000 description 4
- 229930003935 flavonoid Natural products 0.000 description 4
- 235000017173 flavonoids Nutrition 0.000 description 4
- 239000002304 perfume Substances 0.000 description 4
- 235000013824 polyphenols Nutrition 0.000 description 4
- 238000011160 research Methods 0.000 description 4
- 238000010521 absorption reaction Methods 0.000 description 3
- 230000003064 anti-oxidating effect Effects 0.000 description 3
- 230000003078 antioxidant effect Effects 0.000 description 3
- 150000002215 flavonoids Chemical class 0.000 description 3
- 239000004615 ingredient Substances 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- 239000001301 oxygen Substances 0.000 description 3
- 229910052760 oxygen Inorganic materials 0.000 description 3
- QIGBRXMKCJKVMJ-UHFFFAOYSA-N Hydroquinone Chemical compound OC1=CC=C(O)C=C1 QIGBRXMKCJKVMJ-UHFFFAOYSA-N 0.000 description 2
- 241000208125 Nicotiana Species 0.000 description 2
- 235000002637 Nicotiana tabacum Nutrition 0.000 description 2
- 102000019197 Superoxide Dismutase Human genes 0.000 description 2
- 108010012715 Superoxide dismutase Proteins 0.000 description 2
- 230000001093 anti-cancer Effects 0.000 description 2
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- 231100000315 carcinogenic Toxicity 0.000 description 2
- 230000008859 change Effects 0.000 description 2
- MLUCVPSAIODCQM-NSCUHMNNSA-N crotonaldehyde Chemical compound C\C=C\C=O MLUCVPSAIODCQM-NSCUHMNNSA-N 0.000 description 2
- MLUCVPSAIODCQM-UHFFFAOYSA-N crotonaldehyde Natural products CC=CC=O MLUCVPSAIODCQM-UHFFFAOYSA-N 0.000 description 2
- 230000007423 decrease Effects 0.000 description 2
- 230000007812 deficiency Effects 0.000 description 2
- 230000007613 environmental effect Effects 0.000 description 2
- 239000000796 flavoring agent Substances 0.000 description 2
- 125000004435 hydrogen atom Chemical group [H]* 0.000 description 2
- 230000003647 oxidation Effects 0.000 description 2
- 238000007254 oxidation reaction Methods 0.000 description 2
- GHMLBKRAJCXXBS-UHFFFAOYSA-N resorcinol Chemical compound OC1=CC=CC(O)=C1 GHMLBKRAJCXXBS-UHFFFAOYSA-N 0.000 description 2
- 206010002383 Angina Pectoris Diseases 0.000 description 1
- 208000024172 Cardiovascular disease Diseases 0.000 description 1
- 238000002965 ELISA Methods 0.000 description 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
- 206010020772 Hypertension Diseases 0.000 description 1
- 102000004882 Lipase Human genes 0.000 description 1
- 108090001060 Lipase Proteins 0.000 description 1
- 239000004367 Lipase Substances 0.000 description 1
- WSMYVTOQOOLQHP-UHFFFAOYSA-N Malondialdehyde Chemical compound O=CCC=O WSMYVTOQOOLQHP-UHFFFAOYSA-N 0.000 description 1
- 241000124008 Mammalia Species 0.000 description 1
- 208000004880 Polyuria Diseases 0.000 description 1
- 239000003463 adsorbent Substances 0.000 description 1
- 230000008485 antagonism Effects 0.000 description 1
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- 230000002019 anti-mutation Effects 0.000 description 1
- 239000003963 antioxidant agent Substances 0.000 description 1
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- 206010003119 arrhythmia Diseases 0.000 description 1
- 230000006793 arrhythmia Effects 0.000 description 1
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- 235000013355 food flavoring agent Nutrition 0.000 description 1
- 239000003205 fragrance Substances 0.000 description 1
- 239000000446 fuel Substances 0.000 description 1
- 150000002240 furans Chemical class 0.000 description 1
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- 231100000025 genetic toxicology Toxicity 0.000 description 1
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- 239000001257 hydrogen Substances 0.000 description 1
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- 125000004356 hydroxy functional group Chemical group O* 0.000 description 1
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- IWDCLRJOBJJRNH-UHFFFAOYSA-N p-cresol Chemical class CC1=CC=C(O)C=C1 IWDCLRJOBJJRNH-UHFFFAOYSA-N 0.000 description 1
- 150000002978 peroxides Chemical class 0.000 description 1
- KHUXNRRPPZOJPT-UHFFFAOYSA-N phenoxy radical Chemical compound O=C1C=C[CH]C=C1 KHUXNRRPPZOJPT-UHFFFAOYSA-N 0.000 description 1
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- Manufacture Of Tobacco Products (AREA)
Abstract
The present invention discloses a kind of cigarette plant flavone essence cigarette pearl and preparation method thereof, weigh the adhesive that weight is plant flavone essence weight 0.1%~1%, it is added in flavones essence after adhesive water dissolution, it stirs evenly and softwood is made, it first passes through extruder and is extruded into elongated strip, then it is round as a ball by spheronizator, obtain plant flavone essence cigarette pearl after dry；The weight percentages of components of the plant flavone essence includes catechin 40%~70%, cyanidenon 10%~30%, hesperetin 10%~30%, Kaempferol 5%~20%.The plant flavone essence cigarette pearl of the present invention has significant advantage in terms of phenol in smoke is reduced, and it is 8~25% that phenol reduced rate, which can reach 15~45%, free radical reduced rate,；The plant flavone essence cigarette pearl of the present invention has excellent natural breath, is brought to cigarette and comfortably smells fragrant feeling, and when cigarette is aspirated, certain reduction effect can be also generated to other harmful substances matter in flue gas.
Description
Technical field
The invention belongs to technical field of cigarettes, and in particular to a kind of cigarette is with plant flavone essence cigarette pearl and preparation method thereof.
Background technology
Natural plants are widely used in tobacco aromaticss, wherein being much containing Flavonoid substances.According to Flavonoid substances
Molecular characterization and interelectric active force power, Primary Study find such substance burning crack after can generate
Furans and its derivative, these substances are the main aroma components in flue gas, can be brought camerlsed to flue gas, it is fragrant and sweet,
Roasting perfume, increases perfume quantity and aroma quality.Therefore in the allotment of essence spice for cigarette, there is the use of many flavonoids perfume materials.
Many researchs also indicate that, flavone compound has multiple biological activities, except using its antibacterial, anti-inflammatory, anti-mutation,
Outside the effects that decompression, clearing heat and detoxicating, calm, diuresis, in anti-oxidant, anticancer, anti-cancer, lipase etc. is inhibited also to have notable effect
Fruit.It is the scavenger of most of oxygen radicals, thus the vigor of energy increased SOD (superoxide dismutase), reduces MDA (fat
Matter peroxide malonaldehyde) and OX-LDL (OxLDL ELISA) generation.It can increase coronary flow, to experiment
Myocardial inyaretion has antagonism；There is protective effect to acute myocardial ischemia；Have to treatment coronary heart diseases and angina pectoris, hypertension etc.
Remarkable result；To reducing diastolic pressure, prevention arrhythmia cordis, cardiovascular disease and promoting blood circulation and removing blood stasis also play an important role.
Phenolic compound is a kind of compound common in nature, in water, fuel, vehicle exhaust, air, wine and cigarette
There is the presence of phenolic compound in flue gas.The phenolic compounds in cigarette smoke reported has more than 50 kinds, wherein most important phenol
Class compound includes phenol, catechol, resorcinol, hydroquinone, 7 kinds of ingredients such as o, m, p- cresols.
Phenolic compound can be directly entered blood circulation by the contact with skin, mucous membrane, cause protein denaturation, thin
Born of the same parents destroy and lose vigor.And induced by alkyl hydroxybenzene has endocrine disrupting activity, and the reproduction of mammal and aquatile is sent out
It educates and impacts, be referred to as phenols environmental estrogens, there is part phenols component genotoxicity and carcinogenic or promotion mutagenesis to make
With.More than 7 kinds of phenols components be put into EPA harmful components lists, catechol is classified as 2B grades of carcinogenic components by IARC.Zheng
State Bureau's key research project " cigarette harmfulness Research on Index System " project that state tobacco research institute undertakes is harmful by studying
The relationship of ingredient burst size and flue gas biological activity, it is that influence cigarette mainstream flue gas harmfulness is most important harmful to find phenol
One of ingredient.
At present, the method for phenol in flue gas is reduced mainly using the method for absorption, because phenol is present in flue gas
In granule phase substance, it can be retained down from flue gas by the method for physical absorption.The adsorbent of prior art application is mainly table
The larger porous material of area while absorption, retention phenol, can also adsorb the aroma component of part and flue gas water in flue gas
Point, cause easily to generate stimulation, perfume quantity deficiency, aroma quality decline during cigarette smoking, seriously affect cigarette smoking quality.
The cigarette pearl containing essence and flavoring agent is put into filter tip in the prior art, which can make cigarette in aspiration procedure
In it is more raw fragrant, strengthen fragrance or characteristic, smoker made to obtain more comfortably experiencing.This cigarette pearl can only simply make cigarette
It is raw fragrant in aspiration procedure, it is impossible to play the harmful substance for reducing and being generated during smoking cigarette.
Invention content
In view of the deficiencies of the prior art, the present invention provides a kind of cigarette for phenol being blocked to generate using antioxidation and uses plant
Flavones essence cigarette pearl and preparation method thereof has the function that reduce phenol in smoke.
Technical solution is used by the present invention solves above-mentioned technical problem：A kind of cigarette plant flavone essence cigarette pearl is provided
Preparation method, the preparation method is as follows：
The adhesive that weight is plant flavone essence weight 0.1%~1% is weighed, plant is added to after adhesive water dissolution
In object flavones essence, stir evenly and softwood be made, then by extrusion-spheronizator on softwood, first pass through extruder be extruded into it is elongated
Strip, it is then round as a ball by spheronizator, obtain that particle size range is 0.5mm~4mm, heap density is 1.2g/ml~1.8g/ after dry
The plant flavone essence cigarette pearl of ml；
Wherein：The weight percentages of components of the plant flavone essence is as follows：
Further, the DNA purity of the catechin, cyanidenon, hesperetin and Kaempferol is 80~95%.
Further, described adhesive is povidone, hydroxypropyl cellulose, hydroxypropyl methyl cellulose and carboxymethyl cellulose
It is one or more in element.
Further, the particle size range of the cigarette pearl is 0.8mm~1.5mm, and heap density is 1.4g/ml~1.6g/ml.
Further, it in temperature is 4~6 hours dry under the conditions of 60 DEG C~80 DEG C that the drying, which is,.
A kind of cigarette is plant prepared by method described above with plant flavone essence cigarette pearl, the plant flavone essence cigarette pearl
Flavones essence cigarette pearl.
It is analyzed according to organic chemistry basic theories, influences to be most importantly hydroxyl in the oxidation resistant factor of flavone compound
Change degree and hydroxy position, phenolic hydroxyl group are the chief active group of flavone compound antioxidation, while find flavonoids
Hydroxyl activity difference on each ring is larger, is mainly manifested in：B rings are the main work of flavone compound oxidation and removing free radicals
Property position, when the ring is there are during ortho-phenolic hydroxyl structure, antioxidant activity greatly enhances；When hydroxyl on c rings and unsaturated double-bond phase
Lian Shi, c ring also have stronger antioxidant activity；The phenolic hydroxyl group of A rings is most weak.Phenolic hydroxyl group in flavones structure is lived with hydrogen supply
Property, hydrogen atom can be supplied to active oxygen radical, form the Phenoxy radical of stable low activity, so as to avoid these activity
Oxygen radical generates phenolic compound to the attack of aromatic rings.Phenolic hydroxyl group number in flavones molecule is more, it is possible to provide to
The hydrogen atom combined with living radical is more, and therefore, flavone compound can utilize the life of antioxidation blocking phenol
Into so as to have the function of preferably to reduce phenol release amount in flue gas.
The present invention has the following advantages：
1st, plant flavone essence cigarette pearl of the invention has significant advantage in terms of phenol in smoke is reduced, and phenol reduced rate can
To reach 15~45%, free radical reduced rate as 8~25%, natural, environmental protection meets requirement of the consumer to health, low evil；
2nd, plant flavone essence cigarette pearl of the invention has excellent natural breath, is brought to cigarette and comfortably smells fragrant sense
Feel, when cigarette is aspirated, certain reduction effect can be also generated to other harmful substances matter in flue gas, and will not be to cigarette smoking product
Matter has a negative impact, and further improves cigarette smoking quality；
3rd, plant flavone flavor of raw material of the present invention derives from a wealth of sources, of low cost, easy to utilize.
Specific embodiment
In order to make the purpose , technical scheme and advantage of the present invention be clearer, with reference to embodiments, to the present invention
It is further elaborated.The specific embodiments described herein are merely illustrative of the present invention, is not used to limit this hair
It is bright.
Embodiment 1
Plant flavone essence according to ratio in table 1 is mixed, weighs the hydroxypropyl that weight is plant flavone essence weight 0.1%
Ylmethyl cellulosic binders with being added in plant flavone essence after 400ml water dissolutions, stir evenly and softwood are made, then
By extrusion-spheronizator on softwood, first pass through extruder and be extruded into elongated strip, then round as a ball by spheronizator, upper fluid bed exists
The plant flavone essence cigarette pearl that grain size is 0.5mm, heap density is 1.8g/ml is obtained after temperature is 6 hours dry under the conditions of being 60 DEG C.
Table 1
| Flavones type | Catechin | Cyanidenon | Hesperetin | Kaempferol |
| Weight percent | 40% | 15% | 25% | 20% |
Embodiment 2
Plant flavone essence according to ratio in table 2 is mixed, weighs the hydroxypropyl that weight is plant flavone essence weight 0.5%
Ylmethyl cellulosic binders with being added in plant flavone essence after 450ml water dissolutions, stir evenly and softwood are made, then
By extrusion-spheronizator on softwood, first pass through extruder and be extruded into elongated strip, then round as a ball by spheronizator, upper fluid bed exists
The plant flavone essence cigarette that grain size is 0.8mm, heap density is 1.6g/ml is obtained after temperature is 5.5 hours dry under the conditions of being 65 DEG C
Pearl.
Table 2
| Flavones type | Catechin | Cyanidenon | Hesperetin | Kaempferol |
| Weight percent | 50% | 15% | 15% | 20% |
Embodiment 3
Plant flavone essence according to ratio in table 3 is mixed, weighs the carboxylic first that weight is plant flavone essence weight 0.8%
Base cellulosic binders with being added in plant flavone essence after 500ml water dissolutions, stir evenly and softwood are made, then will be soft
Extrusion-spheronizator on material first passes through extruder and is extruded into elongated strip, and then round as a ball by spheronizator, upper fluid bed is in temperature
Drying obtains the plant flavone essence cigarette pearl that grain size is 1.0mm, heap density is 1.6g/ml after 6 hours under the conditions of being 70 DEG C.
Table 3
| Flavones type | Catechin | Cyanidenon | Hesperetin | Kaempferol |
| Weight percent | 60% | 20% | 10% | 10% |
Embodiment 4
Plant flavone essence according to ratio in table 4 is mixed, weighs the carboxylic first that weight is plant flavone essence weight 0.8%
Base cellulosic binders with being added in plant flavone essence after 500ml water dissolutions, stir evenly and softwood are made, then will be soft
Extrusion-spheronizator on material first passes through extruder and is extruded into elongated strip, and then round as a ball by spheronizator, upper fluid bed is in temperature
Drying obtains the plant flavone essence cigarette pearl that grain size is 1.5mm, heap density is 1.4g/ml after 6 hours under the conditions of being 75 DEG C.
Table 4
| Flavones type | Catechin | Cyanidenon | Hesperetin | Kaempferol |
| Weight percent | 65% | 15% | 10% | 10% |
Embodiment 5
Plant flavone essence according to ratio in table 5 is mixed, weighs the hydroxypropyl that weight is plant flavone essence weight 1%
Cellulosic binders with being added in plant flavone essence after 550ml water dissolutions, stir evenly and softwood are made, then by softwood
Upper extrusion-spheronizator first passes through extruder and is extruded into elongated strip, and then round as a ball by spheronizator, upper fluid bed is in temperature
Drying obtains the plant flavone essence cigarette pearl that grain size is 1.5mm, heap density is 1.4g/ml after 5 hours under the conditions of 70 DEG C.
Table 5
| Flavones type | Catechin | Cyanidenon | Hesperetin | Kaempferol |
| Weight percent | 60% | 20% | 15% | 5% |
Embodiment 6
Plant flavone essence according to ratio in table 6 is mixed, weighs the hydroxypropyl that weight is plant flavone essence weight 1%
Cellulosic binders with being added in plant flavone essence after 550ml water dissolutions, stir evenly and softwood are made, then by softwood
Upper extrusion-spheronizator first passes through extruder and is extruded into elongated strip, and then round as a ball by spheronizator, upper fluid bed is in temperature
Drying obtains the plant flavone essence cigarette pearl that grain size is 1.5mm, heap density is 1.4g/ml after 4 hours under the conditions of 80 DEG C.
Table 6
| Flavones type | Catechin | Cyanidenon | Hesperetin | Kaempferol |
| Weight percent | 50% | 25% | 15% | 10% |
Plant flavone essence cigarette pearl prepared in above 6 embodiments is added in cigarette filter stick, then to system
Into cigarette carry out detection of exhaust gas compositions, and carry out phenol reduced rate and compare, be specifically shown in the following table 7
Table 7
The smoke components mainly reduced have phenol, crotonaldehyde, free radical, while smoke hazard index also becomes in decline
Gesture, specific reduced rate result see the table below 8
Table 8
| Sample number into spectrum | Phenol | Crotonaldehyde | Index | Free radical |
| Embodiment 1 | 14.7% | 13.5% | 14.1% | 9.2% |
| Embodiment 2 | 20.2% | 15.5% | 12.8% | 13.3% |
| Embodiment 3 | 30.2% | 12.8% | 15.4% | 16.4% |
| Embodiment 4 | 36.4% | 32.4% | 19.2% | 21.1% |
| Embodiment 5 | 41.9% | 29.1% | 17.9% | 20.7% |
| Embodiment 6 | 39.5% | 28.4% | 15.4% | 22.2% |
Plant flavone essence cigarette pearl prepared in above 6 embodiments is added in cigarette filter stick, then to system
Into cigarette carry out sensory evaluation, as a result such as table 9
Table 9
The above description is merely a specific embodiment, but protection scope of the present invention is not limited thereto, any
Belong to those skilled in the art in the technical scope disclosed by the present invention, the change or replacement that can be readily occurred in all should
It is included within the scope of the present invention.Therefore, protection scope of the present invention should be subject to the protection scope in claims.
Claims (3)
1. a kind of cigarette preparation method of plant flavone essence cigarette pearl, it is characterised in that：The preparation method is as follows：
The adhesive that weight is plant flavone essence weight 0.1%~1% is weighed, plant Huang is added to after adhesive water dissolution
It in ketone essence, stirs evenly and softwood is made, then by extrusion-spheronizator on softwood, first pass through extruder and be extruded into elongated item
Shape, it is then round as a ball by spheronizator, obtain that particle size range is 0.5mm~4mm, heap density is 1.2g/ml~1.8g/ml after dry
Plant flavone essence cigarette pearl；
Wherein：The weight percentages of components of the plant flavone essence is as follows：
Described adhesive be povidone, hydroxypropyl cellulose, hydroxypropyl methyl cellulose and carboxymethyl cellulose in one kind or
It is a variety of；It in temperature is 4~6 hours dry under the conditions of 60 DEG C~80 DEG C that the drying, which is,.
2. the cigarette according to claim 1 preparation method of plant flavone essence cigarette pearl, it is characterised in that：The catechu
Element, cyanidenon, hesperetin and Kaempferol DNA purity be 80~95%.
3. a kind of cigarette is with plant flavone essence cigarette pearl, it is characterised in that：The plant flavone essence cigarette pearl is described in claim 1
Plant flavone essence cigarette pearl prepared by method.
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|---|---|---|---|---|
| CN101016288A (en) * | 2007-03-06 | 2007-08-15 | 川渝中烟工业公司 | Method of stabilizing bioactivity of flavones substance |
| CN101653290A (en) * | 2009-08-26 | 2010-02-24 | 甘全军 | Cigarette containing rosmarinic acid and preparation method thereof |
| CN101864694A (en) * | 2010-06-13 | 2010-10-20 | 玉溪市星源油墨厂 | Tea flavonoids containing water-based coating for cigarette plug wrap paper |
| CN102061174A (en) * | 2010-10-29 | 2011-05-18 | 华南农业大学 | Squalene and tea polyphenol composition and application thereof in cigarettes |
| CN104068467A (en) * | 2014-07-01 | 2014-10-01 | 安徽中烟工业有限责任公司 | Electronic cigarette liquid rich in plant flavone |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101016288A (en) * | 2007-03-06 | 2007-08-15 | 川渝中烟工业公司 | Method of stabilizing bioactivity of flavones substance |
| CN101653290A (en) * | 2009-08-26 | 2010-02-24 | 甘全军 | Cigarette containing rosmarinic acid and preparation method thereof |
| CN101864694A (en) * | 2010-06-13 | 2010-10-20 | 玉溪市星源油墨厂 | Tea flavonoids containing water-based coating for cigarette plug wrap paper |
| CN102061174A (en) * | 2010-10-29 | 2011-05-18 | 华南农业大学 | Squalene and tea polyphenol composition and application thereof in cigarettes |
| CN104068467A (en) * | 2014-07-01 | 2014-10-01 | 安徽中烟工业有限责任公司 | Electronic cigarette liquid rich in plant flavone |
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