CN104831407A - Compound warm down feather composite fiber and producing method thereof - Google Patents
Compound warm down feather composite fiber and producing method thereof Download PDFInfo
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Abstract
The invention discloses compound warm down feather composite fiber which is characterized by comprising the following raw materials: 14-17 parts of duck down, 16-19 parts of chicken feather fragments, 8-12 parts of jute pulp fiber, 9-11 parts of black bamboo charcoal fiber, 4-6 parts of nano seaweed powder, 2-4 parts of konjac gum, 2-3 parts of expanded vermiculite, 3-4 parts of chlorinated paraffin, 1.1-2.1 parts of costustoot, 0.7-1.2 parts of honeysuckle, 0.8-1.4 parts of semen cassiae torae, 8-11 parts of waxberry bark, 10-14 parts of dry flos sophorae, 100-110 parts of 1-butyl-3-methyl imidazole dimethyl phosphate, 105-120 parts of 1-butyl 3-methyl imidazole acetate, 3-5 parts of an additive and a moderate amount of water; by effective compounding of the components, the prepared compound warm down feather composite fiber has good warmth retention property, flame retardant effect, green environmental protection, spinnability and tailorability, and enormous market demand potential.
Description
Technical field
The present invention relates to nonwoven material technical field, be specifically related to a kind of composite heat insulation eider down composite fibre and preparation method thereof.
Background technology
Eider down is the long belly goose, duck, becomes the fine hair of a reed catkins shape, slabbing be feather.Because eider down is a kind of animal protein fiber, higher than cotton (vegetative fiber element) heat insulating ability, and ten million leg-of-mutton tiny pore that eider down nodular fibrous gathers, can the convergent-divergent with temperature Change, produce temperature adjustment function, Absorbable rod human body distributes the hot gas of flowing, the invasion of isolated cool ambient air, because eider down has the superperformance that the softly warming of this uniqueness and moisture absorption disperse, determine the health care that eider down is good, eiderdown quilt be widely used in clothes, wadded a quilt with cotton, the fields such as filler of weaving.
Natural down is used to there is many defects in prior art: one, because eider down content in feather is little, usually only to account for 20-25%, thus make the use cost of eider down too high; Two, eider down makes moist because of the humidity of environment, preserves the improper raw mite that easily goes mouldy; Three, intensity is poor, can make eider down pulverizing, conglomeration, reduce warmth retention property, affect attractive in appearance more than washed; Four, the frequent static electrification of eider down in prior art, brings inconvenience; Five, existing eider down does not have the characteristics such as fire-retardant, antibacterial, water-fastness, there is the hidden danger such as safety, so develop a kind of existing environmental protection, health care, the warmth retention property being conducive to again the health of people is strong, high strength, fire-retardant, antibacterial, laundry-resistant eider down composite fibre can solve the deficiencies in the prior art smoothly.
Summary of the invention
Object of the present invention is just to provide a kind of composite heat insulation eider down composite fibre and preparation method thereof, to overcome the deficiencies in the prior art.
The object of the present invention is achieved like this:
A kind of composite heat insulation eider down composite fibre, it is characterized in that, be made up of the raw material of following weight portion: duck's down 14-17, chicken feather fragment 16-19, jute pulp fibres 8-12, black bamboo Carbon fibe 9-11, nanometer seawood meal 4-6, konjac glucomannan 2-4, expanded vermiculite 2-3, chlorinated paraffin wax 3-4, banksia rose 1.1-2.1, honeysuckle 0.7-1.2, Cassia occidentalis 0.8-1.4, Chinese waxmyrtle bark 8-11, dry sophora flower 10-14,1-butyl-3-methylimidazole dimethyl phosphate 100-110,1-butyl-3-N-Methylimidazoleacetic salt 105-120, auxiliary agent 3-5, suitable quantity of water.
Described auxiliary agent is made up of following raw materials in part by weight: kaolin 2-3, menthol 0.2-0.4, rilanit special polyoxyethylene ether 3-5, dimethicone 2-4, carboxymethyl cellulose 1-2, imidazoline quaternary ammonium salt 0.4-0.7, tarragon 1-3, Asian puccoon 2-3, water 100, its preparation method is by tarragon, Asian puccoon boiling 3-5 hour obtained the concentrated liquid of tradition Chinese medicine, filter, kaolin is added in filtrate, soak 10-12 hour, add other residual componentss again and add thermal agitation, grinding 20-30 minute, to obtain final product.
The preparation method of described a kind of composite heat insulation eider down composite fibre, is characterized in that comprising the following steps:
(1) by the banksia rose, honeysuckle, Cassia occidentalis, Chinese waxmyrtle bark, dry sophora flower boiling 3-5 hour, filter, get filter residue and dry pulverizing, add 10% sulfuric acid heating stirring reaction 1-2 hour of filter residue powder 20 times of quality in mass ratio, add the NaOH heating stirring reaction 1-2 hour of filter residue powder 2 times of quality again, filter, with clear water washing to clean, add the grinding of the expanded vermiculite after high-temperature calcination 20-30 minute;
(2) duck's down, chicken feather fragment, black bamboo Carbon fibe are dropped in above-mentioned filtrate and soak 10-13 hour, after pulling oven dry, degreasing, ultra-fine grinding out, spray into vaporific chlorinated paraffin wax and the mixing of nanometer seawood meal ultrasonic wave;
(3) take 1-butyl-3-methylimidazole dimethyl phosphate, 1-butyl-3-N-Methylimidazoleacetic salt drops in reactor and stirs and evenly mixs, add jute pulp fibres, step (1), (2) product grinding 20-40 minute, be heated to 100-120 DEG C, add other residual components stirring reaction 50-70 minute, obtained spinning solution;
(4) finally obtained spinning solution carried out spinning, winding, boundling, stretching and get final product.
The present invention has following beneficial effect: the present invention is by effective for various component compound, and obtained eider down composite fibre warmth retention property is good, flame retardant effect is excellent, environmental protection, has spinnability and Scalability, and raw material resources of the present invention enriches, and the market demand potential is very big.
Detailed description of the invention
Described a kind of composite heat insulation eider down composite fibre, it is characterized in that, be made up of the raw material of following weight portion: duck's down 16, chicken feather fragment 17, jute pulp fibres 8, black bamboo Carbon fibe 10, nanometer seawood meal 6, konjac glucomannan 3, expanded vermiculite 2, chlorinated paraffin wax 3, the banksia rose 1.8, honeysuckle 0.7, Cassia occidentalis 1.4, Chinese waxmyrtle bark 8, dry sophora flower 10,1-butyl-3-methylimidazole dimethyl phosphate 100,1-butyl-3-N-Methylimidazoleacetic salt 120, auxiliary agent 3, suitable quantity of water.
Described auxiliary agent is made up of following raw materials in part by weight: kaolin 2, menthol 0.2, rilanit special polyoxyethylene ether 5, dimethicone 4, carboxymethyl cellulose 1, imidazoline quaternary ammonium salt 0.4, tarragon 1, Asian puccoon 2, water 100, its preparation method is by tarragon, Asian puccoon boiling 3-5 hour obtained the concentrated liquid of tradition Chinese medicine, filter, kaolin is added in filtrate, soak 10-12 hour, add other residual componentss again and add thermal agitation, grinding 20-30 minute, to obtain final product.
Preparation method comprises the following steps:
(1) by the banksia rose, honeysuckle, Cassia occidentalis, Chinese waxmyrtle bark, dry sophora flower boiling 3-5 hour, filter, get filter residue and dry pulverizing, add 10% sulfuric acid heating stirring reaction 1-2 hour of filter residue powder 20 times of quality in mass ratio, add the NaOH heating stirring reaction 1-2 hour of filter residue powder 2 times of quality again, filter, with clear water washing to clean, add the grinding of the expanded vermiculite after high-temperature calcination 20-30 minute;
(2) duck's down, chicken feather fragment, black bamboo Carbon fibe are dropped in above-mentioned filtrate and soak 10-13 hour, after pulling oven dry, degreasing, ultra-fine grinding out, spray into vaporific chlorinated paraffin wax and the mixing of nanometer seawood meal ultrasonic wave;
(3) take 1-butyl-3-methylimidazole dimethyl phosphate, 1-butyl-3-N-Methylimidazoleacetic salt drops in reactor and stirs and evenly mixs, add jute pulp fibres, step (1), (2) product grinding 20-40 minute, be heated to 100-120 DEG C, add other residual components stirring reaction 50-70 minute, obtained spinning solution;
(4) finally obtained spinning solution carried out spinning, winding, boundling, stretching and get final product.
The technical parameter index of the eider down composite fibre using the present invention to produce is as follows:
(1) light weight, warming, environmental protection;
(2) bacteriostasis rate of finished product to Escherichia coli, staphylococcus aureus, Candida albicans is all greater than 99%;
(3) after 30 washings, antibiotic rate still reaches 95%.
Claims (2)
1. a composite heat insulation eider down composite fibre, it is characterized in that, be made up of the raw material of following weight portion: duck's down 14-17, chicken feather fragment 16-19, jute pulp fibres 8-12, black bamboo Carbon fibe 9-11, nanometer seawood meal 4-6, konjac glucomannan 2-4, expanded vermiculite 2-3, chlorinated paraffin wax 3-4, banksia rose 1.1-2.1, honeysuckle 0.7-1.2, Cassia occidentalis 0.8-1.4, Chinese waxmyrtle bark 8-11, dry sophora flower 10-14,1-butyl-3-methylimidazole dimethyl phosphate 100-110,1-butyl-3-N-Methylimidazoleacetic salt 105-120, auxiliary agent 3-5, suitable quantity of water; Described auxiliary agent is made up of following raw materials in part by weight: kaolin 2-3, menthol 0.2-0.4, rilanit special polyoxyethylene ether 3-5, dimethicone 2-4, carboxymethyl cellulose 1-2, imidazoline quaternary ammonium salt 0.4-0.7, tarragon 1-3, Asian puccoon 2-3, water 100, its preparation method is by tarragon, Asian puccoon boiling 3-5 hour obtained the concentrated liquid of tradition Chinese medicine, filter, kaolin is added in filtrate, soak 10-12 hour, add other residual componentss again and add thermal agitation, grinding 20-30 minute, to obtain final product.
2. the preparation method of a kind of composite heat insulation eider down composite fibre according to claim 1, is characterized in that comprising the following steps:
(1) by the banksia rose, honeysuckle, Cassia occidentalis, Chinese waxmyrtle bark, dry sophora flower boiling 3-5 hour, filter, get filter residue and dry pulverizing, add 10% sulfuric acid heating stirring reaction 1-2 hour of filter residue powder 20 times of quality in mass ratio, add the NaOH heating stirring reaction 1-2 hour of filter residue powder 2 times of quality again, filter, with clear water washing to clean, add the grinding of the expanded vermiculite after high-temperature calcination 20-30 minute;
(2) duck's down, chicken feather fragment, black bamboo Carbon fibe are dropped in above-mentioned filtrate and soak 10-13 hour, after pulling oven dry, degreasing, ultra-fine grinding out, spray into vaporific chlorinated paraffin wax and the mixing of nanometer seawood meal ultrasonic wave;
(3) take 1-butyl-3-methylimidazole dimethyl phosphate, 1-butyl-3-N-Methylimidazoleacetic salt drops in reactor and stirs and evenly mixs, add jute pulp fibres, step (1), (2) product grinding 20-40 minute, be heated to 100-120 DEG C, add other residual components stirring reaction 50-70 minute, obtained spinning solution;
(4) finally obtained spinning solution carried out spinning, winding, boundling, stretching and get final product.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201510143138.1A CN104831407A (en) | 2015-03-30 | 2015-03-30 | Compound warm down feather composite fiber and producing method thereof |
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| CN201510143138.1A CN104831407A (en) | 2015-03-30 | 2015-03-30 | Compound warm down feather composite fiber and producing method thereof |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105821516A (en) * | 2016-04-28 | 2016-08-03 | 安徽华强羽绒有限公司 | Anti-static down feather composite fibers compounded by nanometer goose down powder/ultrafine chicken feather powder and manufacture method thereof |
| CN105821517A (en) * | 2016-04-28 | 2016-08-03 | 安徽华强羽绒有限公司 | Multilayer composite setting down feather composite fibers and manufacture method thereof |
| CN105839219A (en) * | 2016-05-14 | 2016-08-10 | 陆建益 | Antibacterial and anti-ultraviolet sea mud polypropylene fibers and preparation method thereof |
| CN106436294A (en) * | 2016-09-21 | 2017-02-22 | 东莞市联洲知识产权运营管理有限公司 | Waxberry-based multifunctional textile finishing agent and preparation method thereof |
| CN115072649A (en) * | 2021-03-15 | 2022-09-20 | 天辰创新材料科技股份有限公司 | Filling material structure and manufacturing method thereof |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104264277A (en) * | 2014-09-09 | 2015-01-07 | 安徽省含山县富强羽绒制品有限公司 | Mothproof down feather composite fiber and preparation method thereof |
-
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- 2015-03-30 CN CN201510143138.1A patent/CN104831407A/en active Pending
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104264277A (en) * | 2014-09-09 | 2015-01-07 | 安徽省含山县富强羽绒制品有限公司 | Mothproof down feather composite fiber and preparation method thereof |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105821516A (en) * | 2016-04-28 | 2016-08-03 | 安徽华强羽绒有限公司 | Anti-static down feather composite fibers compounded by nanometer goose down powder/ultrafine chicken feather powder and manufacture method thereof |
| CN105821517A (en) * | 2016-04-28 | 2016-08-03 | 安徽华强羽绒有限公司 | Multilayer composite setting down feather composite fibers and manufacture method thereof |
| CN105839219A (en) * | 2016-05-14 | 2016-08-10 | 陆建益 | Antibacterial and anti-ultraviolet sea mud polypropylene fibers and preparation method thereof |
| CN106436294A (en) * | 2016-09-21 | 2017-02-22 | 东莞市联洲知识产权运营管理有限公司 | Waxberry-based multifunctional textile finishing agent and preparation method thereof |
| CN115072649A (en) * | 2021-03-15 | 2022-09-20 | 天辰创新材料科技股份有限公司 | Filling material structure and manufacturing method thereof |
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Application publication date: 20150812 |