CN104760440B - A kind of anti-fake marble paper and its printing method - Google Patents
A kind of anti-fake marble paper and its printing method Download PDFInfo
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Abstract
The present invention relates to a kind of anti-fake marble paper and its printing method, which includes the following steps：1st, word and/or pattern are made；2nd, film is made；3rd, printing screen version is made；4th, non-gold stamping word and/or pattern are printed；5th, upper isolation resin；6th, upper gold stamping bottom ink：Using the screen printing plate made in step 3, using UV resin, primary method is printed according to same color, the group of different colours is printed on same base stock respectively, UV ink, the optical curing of UV ink under ultraviolet light irradiation；7th, it transfers gold stamping：Anti-fake electrochemical aluminum foil is transferred in respectively on the UV ink that step 6 obtains with gilding press；8th, upper isolation gloss oil；9th, upper tearable laminate cover.The present invention provides a kind of with marble paper printing method anti-fraud functional, that printing is simple, production efficiency is high, the anti-fake marble paper of gained can be widely applied on the packing box of all kinds of cosmetics, daily necessities, cigarette, wine and food etc., substantially increase the application range of marble paper.
Description
Technical field
The invention belongs to anti-fake printing fields, and in particular to a kind of anti-fake marble paper and its printing method.
Background technology
Marble paper has the characteristics that performances and the bright colors such as intensity big, high temperature resistant, rub resistance, product be widely used in ceramics,
On the products such as glass ornaments.With commercialization society it is growing, not only marble paper printing method needs to improve, while its function
It is also required to give generalization.In the prior art, the printing process of marble paper needs multinomial drying process more, time-consuming longer, reduces
Productivity effect, and traditional marble paper is printed on the gold stamping step of transfer mostly using not having anti-fraud functional electrochemical aluminum foil, at present
After traditional electrochemical aluminum foil is gold stamping, color immobilizes, and still keeps the gold scalded；When being subject to anti-fake if necessary, then
Antiforge function is not had, it is easy to counterfeit by people.
Therefore, those skilled in the art need to provide it is a kind of with it is anti-fraud functional, printing is simple, improves production efficiency
Anti-fake marble paper and its printing method.
Invention content
For above-mentioned deficiency, the technical problem to be solved in the present invention is to provide one kind to have anti-fraud functional, printing letter
Anti-fake marble paper and its printing method single, that improve production efficiency.
To achieve these goals, the invention is realized by the following technical scheme：
A kind of printing method of anti-fake marble paper, the printing method include the following steps：
(1), word and/or pattern are made；
(2), film is made：According to the word and/or pattern of the different colours that step (1) makes, according to same color
The method for making same film, makes film respectively；
(3), printing screen version is made：According to the film that the word of different colours and/or pattern make, according to same face
The method that color makes same printing screen version makes printing screen version respectively；
(4) non-gold stamping word and/or pattern are printed：It, will be non-gold stamping using the screen printing plate made in step (3)
Word and/or pattern are printed on dry membranelle base stock；
(5), one layer of isolation resin, institute are printed in the side for being printed with non-gold stamping word and/or pattern of membranelle base stock
Stating isolation resin is used to prevent word and/or pattern on membranelle base stock from coming off；
(6), upper gold stamping bottom ink：Using the screen printing plate made in step (3), using UV resins, according to same color
Print primary method, the pattern of different colours be printed on same membranelle base stock respectively, UV ink, ultraviolet light shine
Penetrate lower optical curing of UV ink；
(7), gold stamping word and/or pattern are transferred：According to the gold stamping word of different colours and/or the needs of pattern, according to
Same color prints primary method, with gilding press by the electrochemical aluminum foil with anti-fake word and/or security pattern 110~
At 140 DEG C, the pressure of 3~4 normal atmospheres is transferred in respectively on the UV ink that step (6) obtains；
(8), upper isolation gloss oil：After completing above-mentioned pattern printing, one layer of isolation gold stamping face oil is applied；
(9), upper tearable laminate cover.
Preferably, the resin of being isolated is modified acroleic acid high molecular polymer, the modified acroleic acid high molecular polymerization
Object includes four monomeric acrylic AA, methyl methacrylate MMA, butyl acrylate BA, hydroxypropyl acrylate HPA, further includes
Initiator benzoyl peroxide BPO, curing agent and solvent, the quality proportioning of four monomers is MMA:BA:AA:HPA=
37.5:37.5:12.5:12.5；The dosage of initiator benzoyl peroxide BPO is the 1.75% of four monomer gross mass；Curing
The dosage of agent is the 3% of four monomer gross mass；The mass ratio of the gross mass of the solvent and four monomers is 1:L, solvent are
The mass ratio of the mixed liquor of n-butanol and water, n-butanol and water is 2:1；
The preparation process that resin is isolated is as follows：
1), first be respectively connected into the reaction vessel for being configured with blender and reflux condensing tube four monomeric acrylic AA,
Methyl methacrylate MMA, butyl acrylate BA, hydroxypropyl acrylate HPA, solvent and initiator, the acrylic acid AA, methyl
Methyl acrylate MMA, butyl acrylate BA, hydroxypropyl acrylate HPA addition be respectively its respectively quality 1/3, solvent
Addition be the 1/2 of its quality, the addition of initiator is the 1/4 of its quality, and the addition of curing agent is the 1/ of its quality
3, it starts blender and is warming up to 100 DEG C, react 15min；
2), continue the mixture of dropwise addition residual monomer and initiator into reaction vessel, the addition of wherein initiator is
The 1/2 of its quality, the addition of curing agent are 1/3, time for adding 3h of its quality, continue to stir 0.5h after dripping off；
3) remaining solvent, initiator and curing agent, are added in into reaction vessel again, continues to be stirred to react 3h, be cooled to
40~50 DEG C, under stiring the solution into reaction vessel ammonium hydroxide is added to be neutralized to pH=8~9, the reaction was continued 0.5h to get to this
Resin is isolated.
Preferably, the curing agent is DETA, that is, diethylenetriamine.
Preferably, the ultraviolet curing wavelength in step (5) be 300~420nm, and hardening time continue 2~6s.
Preferably, the proportioning of the UV resins is：5~8 parts of urethane acrylate, epoxy acrylate 6~10
Part, 20~22 parts of coloring pigment, is filled out 30~48 parts of polyester acrylate, 10~20 parts of photo-sensitive monomer, 1~7 part of photoinitiator
1~4 part of material.
Preferably, the electrochemical aluminum foil is made of successively base membrane layer, release layer, dyed layer, aluminium layer, glue-line, described release
Layer is printed on by coating process on base membrane layer, and dyed layer is printed on by coating process on release layer, and the aluminium layer passes through plating
Aluminium technique is attached to dyed layer, and anti-fake word and/or security pattern are printed on by imprint process on aluminium layer and dyed layer, described
Glue-line is printed on by coating process on aluminium layer.
Further, the base membrane layer use biaxial stretching polyester film PET, the basement membrane layer thickness be 16 μm, it is described from
Type layer, dyed layer, aluminium layer three general thickness be 3 μm.
The second technical problem to be solved by the present invention is to provide a kind of anti-fake marble paper made of above-mentioned printing process.
The beneficial effects of the present invention are：
1), required common language and/or pattern first (namely are not needed to gold stamping text by the present invention using water-transfer printing paper
Word and/or pattern) it is transferred on stock, recycle gilding press by anti-fake electrochemical aluminum foil at 110~140 DEG C, 3~4 marks
It is transferred in respectively under quasi- atmospheric pressure on the UV ink after photocuring, you can obtain gold stamping pattern, then upper isolation gloss oil and can again
Laminate cover is torn, wherein isolation gloss oil has low-corrosiveness, therefore gold stamping face coat will not be destroyed, and is had with tearable laminate cover
There is good separation property, and tearable laminate cover is then transferred to convenient for water on body, after taking the film off by low-temperature bake, you can
Retain the word and/or pattern of complete display on body.
The present invention carries out photocuring using ultraviolet light, does not need to time-consuming and lengthy and tedious drying course, printing is greatly saved
Time improves printing production efficiency；Silk-screen printing transfer word and/or pattern are first passed through simultaneously, then are shifted by gilding press
Gold stamping pattern, not only printing efficiency is high, and enriches the print content of marble paper, increases product category.
2), the present invention uses UV ink, not only saves the time, while also more save ink, and printing environment is also more pure and fresh,
Smell is small, reduces the pollution to environment, and does not contain the heavy metals harmful object such as lead, cadmium, lithium, be conducive to environmental protection and
Consumer health；And the good curability of UV ink surface layers and conjunctiva can not only improve post-press finishing characteristic, but also
Improve the presentation quality of product；In addition, UV ink also has good high temperature resistant, water-fast and alcohol resistance energy.
3), present invention employs anti-fake electrochemical aluminum foils, and the anti-fake electrochemical aluminum foil is i.e. with anti-fake word and/or anti-fake figure
The electrochemical aluminum foil of case, electrochemical aluminum foil in the present invention using anti-counterfeiting information is printed on electrochemical aluminum foil by the way of coining, thus
So that after gold stamping security pattern brightness is higher and complete display, there is preferable stereo visual effect, antifalse effect is good.
4), the laminate cover in the present invention both economized on resources preferably using tearable polystyrene film, and in turn avoided causing
Environmental pollution.
5) the isolation resin property index, in the present invention is as follows：Viscosity (25% solid content) is 40s, and fineness ＜ 20pm
Color power be 98%, glossiness 75%, alkali resistant performance be three-level, stable storing.So as to further improve in the present invention
The clarity and stability of pattern.
Specific embodiment
To make the object, technical solutions and advantages of the present invention clearer, the present invention is made into one with reference to embodiment
Step ground detailed description.
Gold stamping face oil is purchased from Wuxi City prosperity printing material factory, model 58-130 in the present embodiment；Ultraviolet curing agent
Model HR-206-1050zw, UV lamp wavelength are 300~410nm, and main wave crest is 365nm.
Embodiment 1
UV resins and isolation resin are prepared first, and UV resins press mass fraction, by 5 parts of urethane acrylate, ring
6 parts of oxypropylene acid esters, 45 parts of polyester acrylate, 15 parts of photo-sensitive monomer, 5 parts of photoinitiator, 20 parts of coloring pigment, filler 4
Part.
Then, according to the following steps, a kind of method of anti-fake marble paper is printed：
(1), pattern-making：Utilize the pattern of two kinds of colors of computer photograph (red, blue).
(2), film is made：According to the pattern for the different colours that step (1) makes, same phenanthrene is made according to same color
The method of forest tract makes two films respectively；
(3), printing screen version is made：Two printing screen plates are made, wherein, red needs are gold stamping, and blue does not need to
It is gold stamping；
(4), dry commercially available water-soluble membranelle base stock printing is taken not need to gold stamping pattern；It is made using in step (3)
Screen printing plate, with light water transfer ink, the blue color patterns for not needing to be gold stamping are printed on base stock, republish one layer of guarantor
The unlikely isolation resin to come off of pattern on river bottom protection paper, the isolation resin is modified acroleic acid high molecular polymer；
(5), upper gold stamping bottom ink：Using the screen printing plate made in step (3), using UV resins, by red pattern
The isolation resin side of membranelle base stock in step (4) is printed on to get UV ink；
(6), dry gold stamping bottom ink：The optical curing of UV ink under ultraviolet light irradiation, light consolidate speed up to 4000/hour；
(7), it transfers gold stamping：Using gilding press by the electrochemical aluminum foil with anti-fake word and security pattern at 110 DEG C, four
A normal atmosphere pressure is transferred on the UV ink that step (6) obtains；
(8), upper isolation gloss oil：After completing above-mentioned pattern printing, one layer of gold stamping face oil is applied；
(9), dry isolation gloss oil：Photocuring drying is carried out using UV-light photocuring machine, with the ultraviolet light of 365nm wavelength,
Kept for hardening time continue 3s.
(10), the tearable laminate cover of last layer：Using the tearable laminate cover of polystyrene.
(11), dry tearable laminate cover.Using heat drying, 35 DEG C of temperature, 3 hours time.
By above step to get the marble paper of two kinds of colors (red, blue) pattern.
Embodiment 2
UV resins and isolation resin are prepared first, and UV resins press mass fraction, by 6 parts of urethane acrylate, ring
8 parts of oxypropylene acid esters, 42 parts of polyester acrylate, 14 parts of photo-sensitive monomer, 4 parts of photoinitiator, 22 parts of coloring pigment, filler 4
Part.
Then, according to the following steps, a kind of method of anti-fake marble paper is printed：
(1), pattern-making：Utilize the pattern of three kinds of colors of computer photograph (red, blue, green).
(2), film is made：According to the pattern for the different colours that step (1) makes, same phenanthrene is made according to same color
The method of forest tract makes three films respectively；
(3), printing screen version is made：Make three printing screen plates, wherein, red, blue needs are gold stamping, it is green not
It needs gold stamping；
(4), dry commercially available water-soluble membranelle base stock printing is taken not need to gold stamping pattern；It is made using in step (3)
Screen printing plate, with light water transfer ink, the green pattern for not needing to be gold stamping is printed on base stock, republishes one layer of guarantor
The unlikely isolation resin to come off of pattern on river bottom protection paper, the isolation resin is modified acroleic acid high molecular polymer；
(5), the first upper gold stamping bottom ink：It, will be red using UV resins using the screen printing plate made in step (3)
Pattern be printed on the isolation resin side of membranelle base stock in step (4), UV ink；
(6), dry gold stamping bottom ink：The optical curing of UV ink under ultraviolet light irradiation, light consolidate speed up to 4000/hour；
(7), it transfers gold stamping：Using gilding press by the electrochemical aluminum foil with anti-fake word and security pattern at 140 DEG C, four
A normal atmosphere pressure is transferred on the UV ink that step (6) obtains；
(8), upper second gold stamping bottom ink：It, will be blue using UV resins using the screen printing plate made in step (3)
Pattern be printed on base stock, UV ink；
(9), dry gold stamping bottom ink：The optical curing of UV ink under ultraviolet light irradiation, light consolidate speed up to 4000/hour；
(10), it transfers gold stamping：Using gilding press by the electrochemical aluminum foil with anti-fake word and security pattern at 130 DEG C,
Three normal atmosphere pressures are transferred on the UV ink that step (9) obtains；
(11), upper isolation gloss oil：After completing above-mentioned pattern printing, one layer of gold stamping face oil is applied；
(12), dry isolation gloss oil：Photocuring drying is carried out using UV-light photocuring machine, with the ultraviolet light of 365nm wavelength,
Kept for hardening time continue 4s.
(13), the tearable laminate cover of last layer：Using the tearable laminate cover of polystyrene.
(14), dry tearable laminate cover.Using heat drying, 35 DEG C of temperature, 3 hours time.
By above step to get the marble paper of two kinds of colors (red, blue, green) pattern.
Embodiment 3
UV resins and isolation resin are prepared first, and UV resins press mass fraction, by 7 parts of urethane acrylate, ring
7 parts of oxypropylene acid esters, 43 parts of polyester acrylate, 16 parts of photo-sensitive monomer, 3 parts of photoinitiator, 21 parts of coloring pigment, filler 3
Part.
Then, according to the following steps, a kind of method of anti-fake marble paper is printed：
(1), pattern-making：Utilize the pattern of three kinds of colors of computer photograph (red, blue, green).
(2), film is made：According to the pattern for the different colours that step (1) makes, same phenanthrene is made according to same color
The method of forest tract makes three films respectively；
(3), printing screen version is made：Make three printing screen plates, wherein, red, blue needs are gold stamping, it is green not
It needs gold stamping；
(4), dry commercially available water-soluble membranelle base stock printing is taken not need to gold stamping pattern；It is made using in step (3)
Screen printing plate, with light water transfer ink, the green pattern for not needing to be gold stamping is printed on base stock, republishes one layer of guarantor
The unlikely isolation resin to come off of pattern on river bottom protection paper, the isolation resin is modified acroleic acid high molecular polymer；
(5), the first upper gold stamping bottom ink：It, will be red using UV resins using the screen printing plate made in step (3)
Pattern be printed on the isolation resin side of membranelle base stock in step (4), UV ink；
(6), dry gold stamping bottom ink：The optical curing of UV ink under ultraviolet light irradiation, light consolidate speed up to 4000/hour；
(7), it transfers gold stamping：Using gilding press by the electrochemical aluminum foil with security pattern at 120 DEG C, four normal atmospheres
Pressure is transferred on the UV ink that step (6) obtains；
(8), upper second gold stamping bottom ink：It, will be blue using UV base oils using the screen printing plate made in step (3)
Pattern be printed on base stock, UV ink；
(9), dry gold stamping bottom ink：The optical curing of UV ink under ultraviolet light irradiation, light consolidate speed up to 4000/hour；
(10), it transfers gold stamping：Using gilding press by the electrochemical aluminum foil with security pattern at 120 DEG C, four standards it is big
It is transferred under air pressure on the UV ink that step (9) obtains；
(11), upper isolation gloss oil：After completing above-mentioned pattern printing, one layer of gold stamping face oil is applied；
(12), dry isolation gloss oil：Photocuring drying is carried out using UV-light photocuring machine, with the ultraviolet light of 365nm wavelength,
Kept for hardening time continue 4s.
(13), the tearable laminate cover of last layer：Using the tearable laminate cover of polystyrene.
(14), dry tearable laminate cover.Using heat drying, 35 DEG C of temperature, 3 hours time.
By above step to get the marble paper of two kinds of colors (red, blue, green) pattern.
It should be noted that the present invention includes but are not limited to above-described embodiment.For the wherein adjustment of UV base oils ratio,
Selection, the alternation of signs of photo solidification machine type or change of anti-fake mode of gold stamping face oil etc. all belong to the scope of protection of the present invention.
Claims (7)
1. a kind of printing method of anti-fake marble paper, which is characterized in that the printing method includes the following steps：
（1）, make word and/or pattern；
（2）, make film：According to step（1）The word and/or pattern of the different colours of making, make according to same color
The method of same film, makes film respectively；
（3）, make printing screen version：According to the film that the word of different colours and/or pattern make, according to same color system
Make the method for same printing screen version, make printing screen version respectively；
（4）, printing non-gold stamping word and/or pattern：Using step（3）The printing screen version of middle making, by non-gold stamping text
Word and/or pattern are printed on dry membranelle base stock；
（5）, one layer of isolation resin liquid is printed in the side for being printed with non-gold stamping word and/or pattern of membranelle base stock, it is described
Isolation resin liquid is used to prevent word and/or pattern on membranelle base stock from coming off；
（6）, upper gold stamping bottom ink：Using step（3）The printing screen version of middle making, using UV ink, prints according to same color
The pattern of different colours is printed on same membranelle base stock by primary method respectively, the optical curing of UV oil under ultraviolet light irradiation
Ink；
（7）, the gold stamping word of transfer and/or pattern：According to the gold stamping word of different colours and/or the needs of pattern, according to same
The primary method of color printing, with gilding press by the electrochemical aluminum foil with anti-fake word and/or security pattern at 110~140 DEG C
Under, the pressure of 3~4 normal atmospheres be transferred in step respectively（6）On the UV ink of obtained membranelle base stock；
（8）, upper isolation gloss oil：After completing above-mentioned pattern printing, one layer of isolation gold stamping face oil is applied；
（9）, upper tearable laminate cover；
The isolation resin liquid includes modified acroleic acid high molecular polymer, and the modified acroleic acid high molecular polymer includes four
A monomer, four monomers are respectively：Acrylic acid AA, methyl methacrylate MMA, butyl acrylate BA, hydroxypropyl acrylate
HPA further includes initiator benzoyl peroxide BPO, curing agent and solvent, and the quality proportioning of four monomers is MMA:
BA:AA:HPA=37.5:37.5:12.5:12.5；The dosage of initiator benzoyl peroxide BPO is four monomer gross mass
1.75%, the dosage of curing agent is the 3% of four monomer gross mass；The mass ratio of the gross mass of the solvent and four monomers is 1:
The mass ratio of l, mixed liquor of the solvent for n-butanol and water, n-butanol and water is 2:1；
The preparation process that resin liquid is isolated is as follows：
1）, first four monomers are respectively connected into the reaction vessel for being configured with blender and reflux condensing tube：Acrylic acid AA, methyl
Methyl acrylate MMA, butyl acrylate BA, hydroxypropyl acrylate HPA, solvent and initiator, the acrylic acid AA, metering system
Sour methyl esters MMA, butyl acrylate BA, hydroxypropyl acrylate HPA addition be respectively its respectively quality 1/3, solvent plus
Enter 1/2 that amount is its quality, the addition of initiator is the 1/4 of its quality, and the addition of curing agent is the 1/3 of its quality, is opened
Dynamic blender is warming up to 100 DEG C, reacts 15min；
2）, continue into reaction vessel that the addition of residual monomer and the mixture of initiator and curing agent, wherein initiator is added dropwise
1/2 for its quality is measured, the addition of curing agent is 1/3, time for adding 3h of its quality, continues to stir 0.5h after dripping off；
3）, remaining solvent, initiator and curing agent are added in into reaction vessel again, continue to be stirred to react 3h, be cooled to 40~
50 DEG C, under stiring the solution into reaction vessel ammonium hydroxide is added to be neutralized to pH=8~9, the reaction was continued 0.5h is to get to this isolation
Resin liquid；
The proportioning of the UV ink is：5~8 parts of urethane acrylate, 6~10 parts of epoxy acrylate, polyester
30~48 parts of acid esters, 10~20 parts of photo-sensitive monomer, 1~7 part of photoinitiator, 20~22 parts of coloring pigment, 1~4 part of filler.
A kind of 2. printing method of anti-fake marble paper according to claim 1, which is characterized in that step（6）In ultraviolet light
Curing wavelength be 300~420nm, and hardening time continue 2~6s.
3. the printing method of a kind of anti-fake marble paper according to claim 1, which is characterized in that the electrochemical aluminum foil is by basement membrane
Layer, release layer, dyed layer, aluminium layer, glue-line are formed successively, and the release layer is printed on by coating process on base membrane layer, coloring
Layer is printed on by coating process on release layer, and the aluminium layer is attached to dyed layer by aluminum plating process, anti-fake word and/or anti-
Pseudo- pattern is printed on by imprint process on aluminium layer and dyed layer, and the glue-line is printed on by coating process on aluminium layer.
4. the printing method of a kind of anti-fake marble paper according to claim 1, which is characterized in that the curing agent is DETA.
5. the printing method of a kind of anti-fake marble paper according to claim 3, which is characterized in that the base membrane layer is using two-way
Oriented polyester film PET, the thickness of the base membrane layer are 16 μm, the release layer, dyed layer, aluminium layer three overall thickness be 3 μm.
6. the printing method of a kind of anti-fake marble paper according to claim 1, which is characterized in that the tearable laminate cover is
The tearable laminate cover of polystyrene.
7. a kind of anti-fake marble paper prepared by claim 1~6 any one.
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| CN109733105A (en) * | 2019-01-20 | 2019-05-10 | 邱晖 | A kind of ceramic marble paper production method |
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