CN104606115B - Rose honey and its application - Google Patents
Rose honey and its application Download PDFInfo
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- CN104606115B CN104606115B CN201510034016.9A CN201510034016A CN104606115B CN 104606115 B CN104606115 B CN 104606115B CN 201510034016 A CN201510034016 A CN 201510034016A CN 104606115 B CN104606115 B CN 104606115B
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- 150000004670 unsaturated fatty acids Chemical class 0.000 description 1
- 235000021122 unsaturated fatty acids Nutrition 0.000 description 1
- 229930003231 vitamin Natural products 0.000 description 1
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- Cosmetics (AREA)
Abstract
The present invention relates to a kind of rose honey and its new applications, more specifically, the cosmetics that rose honey is used for anti-oxidant, moisturizing, increases skin barrier, improve wrinkle and elasticity of skin.Rose honey in the present invention, preparation process is mixed using rosaceae rose rose with honey, after impregnating at low temperature, then the rose honey obtained is extracted using vacuum drying technique, as natural free radical scavenger, moisturizer and aging ingredient, it can be used as enhancing skin barrier, moisturizing, improve wrinkle microgroove, improve the effect of moisturizings, anti-aging cosmetics such as elasticity of skin additive.
Description
Technical field
The present invention relates to a kind of rose honey and its new applications, more specifically, rose honey is used for anti-oxidant, moisturizing, increase
Skin barrier, the cosmetics for improving wrinkle and elasticity of skin.
Background technique
According to the free radical causes of senescence of Harman, excessive free radical is the major reason for causing biological aging.Activity
Oxygen radical is generation during physiological metabolism in vivo, under normal circumstances, the polyphenoils and reductase of human body itself
It, can be by these harmful active oxygens certainly including vitamin C, vitamin E, lipoic acid, glutathione, superoxide dismutase etc.
It is changed into harmless water or oxygen by base.Due to the environmental pollution of ultraviolet radioactive, air pollution and chemical substance in environment etc.
Object stimulating organism body constantly generates free radicals, and internal excessive active oxygen radical and unsaturated fatty acid effect generate malonaldehyde
Equal substances, malonaldehyde will produce brown pigment with the effects of protein on cell membrane, be deposited in skin and become as various color spots.It crosses
The free radical of amount can also make collagenous fibres, elastomer in skin crosslink and be denaturalized, become fragile, follow the string, and work as skin
It when water deficient, is easy to make elastic fibers break, the skin ageing phenomenons such as dark line, microgroove, wrinkle occurs.Although having in human body
The Antioxidative Defense System of equilibrium state between oxidative and anti-oxidative is able to maintain that, to slow down the production of active oxygen and free radical
It is raw, if but long-term excessive exposure in the sun, then the free radical largely generated in human body will lead to the antioxygen chemoprevention of skin
Imperial ability reduces, and causes injury of skin, such as light aging, creasy surface, the imbalance of cutaneous immunisation power etc..Antioxidant is that have to catch
The substance of free radical ability is caught, the living radical in skin can be removed, mitigating skin oxidative caused by free radical stress damage
Wound, so as to improve the skin aging as caused by oxidative stress etc..It is intracorporal clear the biology such as vitamin E, vitamin C has been currently known
Except free radical type antioxidant, in addition, there are also artificial synthesized antioxidant such as propylgallates, TBHQ, BHT and butyl hydroxyl
Base anisole because the problem of safety, antioxidants of these synthesis in use by additive amount, use scope in terms of
Various limitations, consumer also select also have a misgiving when the product containing these artificial synthesized antioxidants, therefore, exploitation pair
Human-body safety, natural antioxidant is increasingly taken seriously.
Adult skin moisture storage capacity accounts for the 18%~20% of whole body, and moisture of skin is for keeping good physiological function and being good for
Health maintains the appearance of skin beauty to be all very important.The excessive of internal water can be prevented to scatter and disappear.Air-conditioning, environmental pollution,
Seasonal conversion bring temperature change and pressure and skin aging, metabolism, which such as slow down at the factors, can all cause skin moisture to be lost,
Enable skin it is coarse, it is dim it is mute, form dry line, cause many skin problems.If skin is chronically at the state of water shortage, skin can be reduced
The protective capability of skin, self-repairing capability when being damaged can also decline, or even the premature ageings such as microgroove, wrinkle occur and show
As.
Skin elasticity is the one of the important signs that for judging skin aging, collagenous fibres, the elasticity of skin elasticity and skin corium
Fiber is related with reticular fibre, and skin elasticity is also in close relations with skin moisture content, when cuticula is rich in moisture, skin bullet
Property it is preferable, cuticula exsiccation can lead to skin elasticity decline, skin occur it is dry, tight and crack phenomena such as.
Skin barrier can prevent loss of moist and external environment from invading, and skin barrier reduction is the important original of skin sensitivity
Cause.When by skin physiology pathological change and such environmental effects, when skin barrier function is damaged, skin will appear sensitive, dry
The symptoms such as dry, itch, the disease incidence such as some skin diseases such as eczema increase.After skin barrier function is destroyed, it can also make to stimulate
Ingredient quickly penetrates into skin, increases and stimulation and anaphylactoid probability occurs.Skin barrier function is usually with percutaneous moisture stream
(TEWL) is lost to measure.TEWL reflects evaporation of the moisture from skin surface, is inversely proportional in any case with skin hydration effect,
It is the outstanding feature of skin barrier function.
Moisturizing constituents, which have, keeps moisture of skin, delays, prevents the effect of moisture evaporation, to maintenance and repairs skin screen
Hinder function, reduction skin appearance is significant, is widely used in cosmetics.There are many moisturizing ingredient type, wherein with
Based on polyalcohol, vaseline, such as glycerol, silicone oil, vaseline, white oil, lanolin, urea are the most commonly used, major defect be using
Skin often has greasy feeling afterwards, some preparations (such as lanolin, urea) have peculiar smell, some are also easy to cause skin allergy etc..And
From natural plants the substance with moisturizing effect or composition with high security, it is low in cost, just
Increasingly obtain the attention of skin care industry.
Rose honey is the traditional beauty treatment Gu method of Minorities in Yunnan, is mixed using rose with honey, by low temperature dipping, is mentioned
The essence for taking the Hua Yumi of acquisition has effects that moisturizing and nutrition skin.Rich in sugar such as fructose, glucose in rose honey
Class, the flavones ingredients such as procyanidine.The rose that rose honey uses is rosaceae rose, before 5-6 month full-bloom stage, is adopted
Pluck sufficiently expand but unopened bud for.Its pharmacological property of rose is mild, fragrance is sweet, have toxin-expelling and face nourishing, the promoting flow of qi and blood circulation,
Having one's ideas straightened out silt, adjusts the effect of body at soothing liver-qi stagnation.It is just on the books in Ming Dynasty's " food book on Chinese herbal medicine ": " the main sharp lung spleen of rose, benefit
Liver and gallbladder, the gas for the evil that exorcises evil spirits, the fragrance of food is sweet and refreshing, makes us refreshing refreshing ".Rose can extract aromatic oil, be fine perfumery.It is civil that there are also make
Make the tradition such as rose liter (cider), rose candy, such as washes water clothes open with rose sugaring, it is not only sweet and dilitious, but also can the promoting flow of qi and blood circulation；With
Rose bubble wine clothes, relaxing tendons and activating collaterals can control arthralgia.Rose, smell just is made in rose with the method for distillation from ancient times
Fragrance, it is significant in efficacy.Existing patent report, by Flos Rosae Rugosae petal extract (containing tannin, anthocyanin and flavone compound) and
Honey mixing can be used for the inflammation during gingivitis is especially teethed, which is considered as mild astringent reconciliation
Congested medicine.
The rose honey that the present invention uses is by mixing rose with honey, after impregnating at low temperature, then dry using vacuum
Dry technology is prepared " rose honey ".Both containing anti-oxidation active substance in rose such as procyanidine, rutin etc. in rose honey
Polyphenols and Flavonoid substances, also containing fructose, glucose, flavonoids and the flavanols compounds and human body in honey
The minerals such as essential amino acid, protein, vitamin, potassium, magnesium, zinc, manganese, phosphorus and microelement.
The cosmetic active raw material with oxidation and removing free radicals, moisture-keeping function from natural plants has safety
Property it is high, it is low in cost the advantages that, just increasingly obtain the attention of skin care industry.The invention reside in provide a kind of natural freedom
Base scavenger, moisturizer and aging ingredient can be used as enhancing skin barrier, moisturizing, improve wrinkle microgroove, improve elasticity of skin
The effect of waiting moisturizings and anti-aging cosmetics additive.
Summary of the invention
The invention reside in providing a kind of rose honey, as natural free radical scavenger, moisturizer and anti-ageing experienced
Point, it can be used as the function for enhancing skin barrier, moisturizing, improving wrinkle microgroove, improving the moisturizings and anti-aging cosmetics such as elasticity of skin
Imitate additive.
This rose honey is prepared by the following method:
(1) roseleaf is crushed or is shredded, and is mixed with honey by the weight ratio of 1:2~10；
(2) 0~30 DEG C impregnate 5~30 days, remove petal；
(3) the nectar vacuum drying after removing petal, obtains rose honey.
Preferably, the honey in step (1) is wild sophorae honey, clover honey or snow rouge lotus honey；Roseleaf is non-standard-sized sheet
The roseleaf acquired when putting；The weight ratio of roseleaf and honey is 1:2~10.
In obtained rose honey, the content of fructose and glucose is 60.0%~87.9%, and the content of procyanidine is
1.0%~2.0%；The pH value of rose honey is 3.50~4.99.
Above-mentioned rose honey can be used as preparing cosmetics, especially have senile-resistant efficacy or moisture-keeping efficacy cosmetics, anti-ageing
Old effect is to improve wrinkle, elasticity of skin, increase skin barrier and anti-oxidant.Wherein the additive amount of rose honey be 0.1%~
10%, preferably 0.1%~5%, it is weight percentage.
Above-mentioned rose honey can be used as preparing Dermatologic preparation composition, such as creams, lotion, Essence or toner, wherein
The content of rose honey is 0.1%~10%, preferably 0.1%~5%, is weight percentage.
The cosmetics containing rose honey of invention have enhancing skin barrier, moisturizing, improve wrinkle microgroove, improve skin bullet
Moisturizings and the senile-resistant efficacies such as property.
Rose honey in the present invention, preparation process are mixed using rose with honey, and rose used can be rose
Section rose rose (Rosa rugosa Thunb.), thorn rose (Rosa acicularis Lindl.), Rosa bella
(Rosa davurica Pall.) etc., specifically preferred according to the invention is rose (the Rosa rugosa of Yunnan land race
Thunb.), honey used can be commercially available common honey, it is currently preferred be Yunnan local products wild sophorae honey,
Chinese milk vetch nectar and snow rouge lotus honey.Then rose uses vacuum drying with after honey at depressed temperatures, or at room temperature time of infusion
Technology extracts the rose honey obtained can be used as enhancing as natural free radical scavenger, moisturizer and aging ingredient
Skin barrier, moisturizing improve wrinkle microgroove, improve the effect of moisturizings such as elasticity of skin and anti-aging cosmetics additive.
Specific embodiment
The preparation of 1 rose honey of embodiment
Batch 1: the roseleaf 1000g of the non-Full-open of collected by hand, after chopping, according to roseleaf and wild sophorae honey 1:
3 weight ratio is uniformly mixed, and 4 DEG C of dippings isolated petal, petal can be used for other products, will remove petal after 14 days
The sticky rose honey finished product of aubergine is obtained after nectar vacuum drying afterwards, there is rose aroma.
Batch 2: the roseleaf 500g of the non-Full-open of collected by hand, after crushing, according to roseleaf and Chinese milk vetch nectar
The weight ratio of 1:2 is uniformly mixed, and 0 DEG C of dipping isolated petal after 28 days, and petal can be used for other products, and removal is spent
Rose honey finished product is obtained after nectar vacuum drying after valve.
Batch 3: the roseleaf 800g of the non-Full-open of collected by hand, according to the weight of roseleaf and snow rouge lotus honey 1:10
Ratio is mixed directly, and (20 DEG C~25 DEG C) of room temperature impregnate 7 days, isolate petal, and petal can be used for other products, will
Rose honey finished product is obtained after nectar vacuum drying after removal petal.
The detection of 2 rose honey physical and chemical index of embodiment
Using pH value measuring method (one annex VII G of Chinese Pharmacopoeia version in 2010), detect according to batch 1 in embodiment 1
The pH value of the rose honey sample (being configured to 10wt% aqueous solution) of~3 methods preparation.
Using method (the measurement side of Fructose in Honey, glucose, sucrose, maltose content as defined in GB/T 18932.22
Method-liquid chromatogram differential pulse polarograpll method), measure fructose, glucose content in rose honey.Determination step are as follows: 5g sample is weighed,
It is accurate to 0.001g.It is placed in 100mL beaker, 30mL water is added, be completely dissolved sample with glass bar stirring, be transferred to
In 100mL volumetric flask, beaker then is washed three times with 10mL again and is transferred in above-mentioned 100mL volumetric flask, is settled to acetonitrile
Volume mixes.Sample liquid is filtered in sample bottle for liquid chromatogram measuring with 0.45 μm of filter membrane.Liquid phase chromatogram condition are as follows: chromatography
Column is 10 μm of X300mmX3.9mm (i.d) of carbohydrate analysis column, and mobile phase is acetonitrile: water (77:23), flow velocity 1.0mL/
Min, column temperature are 25 DEG C, and detector cell temperature is 35 DEG C, and sample volume is 15 μ L.It is warded off with the fruit of preparation, glucose standards solution is drawn
For system using peak height as ordinate, concentration of standard solution is the standard curve of abscissa, guarantees the sound of fructose, glucose in sample solution
Should be worth should all be in the range of linearity of standard working curve, and sample solution is measured with the isometric sample introduction of standard solution.
Rose honey procyanidins content is measured using spectrophotometry: taking procyanidine reference substance appropriate, it is accurately weighed,
Add dehydrated alcohol that the solution that every 1mL contains 50 μ g is made.Pipette respectively above-mentioned procyanidine reference substance solution 2.00,4.00,6.00,
8.00,10.00mL is added dehydrated alcohol, is settled to scale, sufficiently shakes up after stoppering, exist respectively in 10.0mL volumetric flask
At 280nm, using dehydrated alcohol as blank determination absorbance value, using concentration as abscissa, absorbance value is that ordinate draws mark
Directrix curve.Precision weighs rose honey sample 1g to 50mL volumetric flask, adds 10mL purified water, ultrasonic (power 300W, frequency 50kHz)
Processing 10 minutes, room temperature is let cool, and dehydrated alcohol is added to be settled to scale, and ultrasound 15 minutes takes supernatant after standing cooling 30 minutes
0.5 μm of organic filter membrane is crossed, filtrate is taken.Rose honey sample solution is taken to measure absorbance value according to reference substance measuring method, according to mark
The content of directrix curve calculating rose honey sample procyanidins.
Table 1
The test of 3 rose honey antioxidant activity of embodiment
Using the work for the rose honey oxidation and removing free radicals that the measurement of DPPH method is prepared according to 1 method of batch in embodiment 1
Property, it is control with wild sophorae honey.Determination step are as follows: the wild sophorae honey that rose honey and unused rose impregnate is used into deionized water respectively
It is configured to aqueous solution, pipettes 2mL in 10mL tool plug test tube, 2mL DPPH ethanol solution (2 × 10 is added-4Mol/L), sufficiently mixed
It is even, it is stored at room temperature, the absorbance A of spectrophotometric determination 517nm wavelength is used after 30min517(using ethyl alcohol as reference)；It surveys simultaneously
Determine 2mL DPPH solution and the mixed absorbance A of 2mL ethyl alcoholcAnd 2mL extracting solution and the mixed suction of 2mL ethanol solution
Luminosity A0, it is measured in parallel three times, is averaged.Measurement result is as shown in table 1.
2 rose honey antioxidant activity of table
As can be seen from Table 2, rose honey has excellent radicals scavenging effect, and antioxidant activity is impregnated better than unused rose
Honey, can be used as effective antioxidant, can by rose honey cooperate in external preparation, as prevent skin ageing, maintain
The antioxidant activity object of the skin state of young healthy uses.
It is as a result similar to batch 1 compared with the honey of unused roseleaf dipping using the rose honey of batch 2 and 3,1
Under the concentration of~10mg/ml, the ability for removing free radical is 7~16 times of the common honey of same concentration.
The moisturizing determination of activity (external weight method) of 4 rose honey of embodiment
Test sample: taking 1 batch of above-described embodiment, 1 rose honey respectively, is configured to 5% (w/v) solution with deionized water.
Control sample: deionized water, 5% glycerol.
Test method: its moisturizing activity is measured with external weighing moisturizing method, the glass slide of same specification is selected, in upper face paste
One layer of medical air-permeable adhesive tape, draws each 50 μ L of test sample under room temperature, and even application is subsequently placed in phase on breathable adhesive tape
To dry in the drier that humidity is 60% (potassium acetate saturated solution), the reduction of weighing sample quality after 24 hours, parallel survey
Determine three times, to be averaged, calculate the moisturizing rate of sample.
The sample quality * 100% before sample quality/placement after moisturizing rate (%)=placement 24 hours
Test result is as shown in table 3:
Table 3
| Sample ID | Moisturizing rate (%) for 24 hours |
| Rose honey | 5.94 |
| Deionized water | 1.48 |
| 5% glycerol | 5.11 |
As seen from the above table, rose honey is compared with glycerol, and under the same conditions, moistening effect is better than glycerol.
It is detected using the rose honey of 1 batch 2 and 3 of embodiment, moistening effect is also superior to glycerol.
Skin preparations for extenal use of the embodiment 5 containing rose honey
Prepared rose honey, the preparation for skin preparations for extenal use in Example 1.The skin preparations for extenal use is preferably changed
Cosmetic compositions, such as toner, Essence, creams etc..Weight percent of the rose honey in skin preparations for extenal use is 0.1
~10%, preferably 1~5%.The embodiment for the concrete application that the following are rose honeys in skin preparations for extenal use."-" in following table
Indicate no added.
(1) containing the toner of rose honey
1 batch of Example, 1 rose honey is used to prepare the toner with anti-aging, moisture-keeping function, and the toner contains
Some components are as shown in table 4:
Table 4
(2) containing the Essence of rose honey
1 batch of Example, 1 rose honey is used to prepare the Essence with anti-aging, moisture-keeping function, and the Essence contains
Some components are as shown in table 5:
Table 5
(3) lotion and frost containing rose honey
1 batch of Example, 1 rose honey is used to prepare with anti-aging, the lotion of moisture-keeping function and frost, the lotion and
The component that frost contains is as shown in table 6:
Table 6
The moisture-keeping efficacy Journal of Sex Research of skin preparations for extenal use of the embodiment 6 containing rose honey
It is tested by normal individual trial, is formulated toner, the embodiment 5 that 2# contains rose honey to examine and evaluate embodiment 5
The Essence and embodiment 5 that formula 6# contains rose honey are formulated whether the frost that 14# contains rose honey has to human skin moisturizing
The effect of effect.
It requires to choose healthy volunteer 64 according to research, wherein 14 people of male, 50 people of women, the age 22~53 years old, put down
Equal 33 ± 8 years old age.Two groups are randomly divided into, every group of 32 people, using subject's cheek, eye as test position.Stop after on-test
With other cosmetics, only uses toner, the formula of embodiment 5 6# that the formula of embodiment 5 2# contains rose honey and contain rose honey
Essence and embodiment 5 are formulated face/frost that 14# contains rose honey.The usage amount of every group of sample presses 2mg/cm2It uses, daily
Once in the morning and once at night.
Skin water loss TEWL is very important parameter to the function of assessment skin barrier, has obtained in the world
Extensive approval.Skin barrier function is more intact, and the content of moisture will be higher, represents the numerical value that skin moisture is lost TEWL
It is lower.In the development process of cosmetics, moisturizing cosmetic can be evaluated by the numerical value that test skin moisture is lost TEWL
Whether effect, the barrier function that can also be applied to monitoring skin have been destroyed.
The measurement of moisture content of skin passes through capacitance measurement human body using the Cornemeter (CM825) of CK company of Germany
The water content of keratoderma, each point measurement three times, are averaged.The measurement of skin water loss (TEWL) uses Germany CK
The Tewameter (TM300) of company is based on Fick diffusion principle, is formed between two points by cuticula moisture loss
Vapor barometric gradient, directly measures the moisture value distributed through epidermis, and each point measurement three times, is averaged.Before test,
It is 21.9 ± 0.1 DEG C in room temperature after asking subject to clean tested position using unified cleaning solution, relative humidity 49.9 ±
It is tested after waiting for peacefully 30 minutes in 0.1% environment.
7 moisture-keeping efficacy Journal of Sex Research (eye) of table
8 moisture-keeping efficacy Journal of Sex Research (face) of table
From table 7 and table 8 it is found that rose honey toner and Essence can dramatically increase the water content of keratoderma, reduce
Amount through cuticula moisture loss, has good moisture-keeping efficacy, and the lotion containing rose honey and frost also have identical effect.
The rose honey of batch 1 in the formula of embodiment 5 is replaced with the rose honey of batch 2 and batch 3, effect is similar.
The assessment of improvement wrinkle effect of skin preparations for extenal use of the embodiment 7 containing rose honey
It is tested by normal individual trial, is formulated toner, the embodiment 7 that 2# contains rose honey to examine and evaluate embodiment 6
The Essence and embodiment 8 that formula 6# contains rose honey are formulated whether the frost that 14# contains rose honey has improvement wrinkle of skin
Effect.
It requires to choose healthy volunteer 64 according to research, wherein 14 people of male, 50 people of women, the age 22~53 years old, put down
Equal 33 ± 8 years old age.Two groups are randomly divided into, every group of 32 people, using subject's cheek, eye as test position.Stop after on-test
With other cosmetics, only uses toner, the formula of embodiment 5 6# that the formula of embodiment 5 2# contains rose honey and contain rose honey
Essence and embodiment 5 are formulated the frost that 14# contains rose honey, and the usage amount of every group of sample presses 2mg/cm2It uses, daily morning and evening
It is each primary.
The measurement of wrinkle of skin uses the VISIA face imaging system of U.S. Canfield company, carries out to test position
After taking pictures, then with software photo is analyzed, the parameters such as quantity, depth of available skin lines.Before test, it is desirable that by
Examination person is 21.9 ± 0.1 DEG C in room temperature, is tested after waiting for peacefully 30 minutes in the environment of relative humidity 49.9 ± 0.1%.
Table 9 improves wrinkle research
As known from Table 9, using 1 week, 2 weeks and 4 weeks after rose honey toner and Essence compared with basic value 0 week,
Eye and face wrinkles' quantity are decreased obviously, and have the function of that good improvement wrinkle, the lotion containing rose honey and frost also have
Identical effect.
The rose honey of batch 1 in the formula of embodiment 5 is replaced with the rose honey of batch 2 and batch 3, effect is similar.
The assessment of improvement skin elasticity effect of skin preparations for extenal use of the embodiment 8 containing rose honey
It is tested by normal individual trial, is formulated toner, the embodiment 7 that 2# contains rose honey to examine and evaluate embodiment 5
The Essence and embodiment 5 that formula 5# contains rose honey are formulated whether the frost that 14# contains rose honey has improvement skin elasticity
Effect.
It requires to choose healthy volunteer 30, the age 25~30 years old according to research.Using subject's arm as test position, examination
Other cosmetics are deactivated after testing beginning, toner, the formula of embodiment 7 6# that the formula of embodiment 6 2# contains rose honey is only used and contains
There are the Essence of rose honey and embodiment 8 to be formulated the frost that 14# contains rose honey, the usage amount of every group of sample presses 2mg/cm2Make
With, it is each primary daily morning and evening, it is used continuously 20 days.
The measurement of skin elasticity based on suction and is stretched former using the skin elasticity tester MPA580 of CK company of Germany
Reason generates a negative pressure in one fc-specific test FC probe of skin inspiration in tested skin surface, and skin is sucked into test
Depth in probe is measured by a contactless optic testing system.Test probe in including light transmitter and
The ratio (emitting the ratio between light and reception light) of receiver, light is directly proportional with the depth of skin is inhaled into, and then passes through MPA software point
Analyse the elastic property to determine skin.Before test, it is desirable that subject is 21.9 ± 0.1 DEG C in room temperature, relative humidity 49.9 ±
It is tested after waiting for peacefully 30 minutes in 0.1% environment.
Table 10 improves skin elasticity research
As known from Table 10, after using rose honey cosmetics 20 days compared with basic value, skin elasticity increases, and having improves
The effect of elasticity of skin.
The rose honey of batch 1 in the formula of embodiment 5 is replaced with the rose honey of batch 2 and batch 3, effect is similar.
Subjective assessment of 9 consumer of embodiment to the skin preparations for extenal use containing rose honey
Subjective assessment is carried out after testing by normal individual trial, contains rose honey to examine and evaluate the formula of embodiment 6 2#
Toner, embodiment 7 are formulated the Essence that 6# contains rose honey and embodiment 8 is formulated whether the frost that 14# contains rose honey has
Moisturizing, the effect for improving wrinkle microgroove, improving elasticity of skin.Selection healthy volunteer 31 is required according to studying, the age 25~
It 30 years old, is paid a return visit within product indwelling 28 days, asking using the various subjective sensations after product is carried out to the subject for participating in test
Volume investigation, scoring account for the ratio of all respondents using 5 points of systems, 3 points of statistics or more.
11 rose honey cosmetics of table use rear subjective assessment statistical result
Such as 11 statistical result showed of table, after continuous use 28 days, embodiment 5 is formulated the toner that 2# contains rose honey, matches
The frost that the Essence and formula 14# that square 6# contains rose honey contain rose honey is equal in TOP3 (T3B) performance of whole testing attributes
It has been more than 85%.Especially make skin more 15 testing attribute TOP3 performances such as moisturizing, moist, increase elasticity, microgroove desalination
Reach 90% or more.The result shows that the work that rose honey cosmetics have moisturizing, improve wrinkle microgroove, improve elasticity of skin
With.
The rose honey of batch 1 in the formula of embodiment 5 is replaced with the rose honey of batch 2 and batch 3, effect is similar.
Claims (10)
1. a kind of application of rose honey in terms of preparing cosmetics, which is characterized in that the rose honey is made by the following method
It is standby:
(1) roseleaf is crushed or is shredded, and is mixed with honey by the weight ratio of 1:2~10；
(2) 0~30 DEG C impregnate 5~30 days, remove petal；
(3) the nectar vacuum drying after removing petal, obtains rose honey；
The content of fructose and glucose is 60.0wt%~87.9wt% in the rose honey, and the content of procyanidine is
0.1wt%~0.2wt%；The pH value of the rose honey is 3.50~4.99；The rose honey has senile-resistant efficacy or moisturizing
Effect；
Honey in the step (1) is wild sophorae honey, clover honey or snow rouge lotus honey.
2. application according to claim 1, which is characterized in that the weight ratio of roseleaf and honey is 1:2 in step (1)
~10.
3. application according to claim 1, which is characterized in that acquired when the non-Full-open of roseleaf in step (1)
Roseleaf.
4. application according to claim 1, which is characterized in that the application is that the rose honey is being prepared with anti-aging
Application in terms of effect or moisture-keeping efficacy cosmetics.
5. application according to claim 1, which is characterized in that the additive amount of the rose honey be 0.1wt%~
10wt%.
6. application according to claim 1, which is characterized in that the additive amount of the rose honey is 0.1wt%~5wt%.
7. application according to claim 4, which is characterized in that the senile-resistant efficacy is to improve wrinkle, elasticity of skin, increasing
Add skin barrier and anti-oxidant.
8. application according to claim 1, which is characterized in that the application is that the rose honey is combined in skin preparations for extenal use
Application in object.
9. application according to claim 8, which is characterized in that content of the rose honey in Dermatologic preparation composition
For 0.1wt%~10wt%.
10. application according to claim 8, which is characterized in that the rose honey containing in Dermatologic preparation composition
Amount is 0.1wt%~5wt%.
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| CN104146198A (en) * | 2014-07-28 | 2014-11-19 | 王泰朕 | Honey capable of eliminating toxicants and beautifying skin, and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102940604A (en) * | 2012-12-10 | 2013-02-27 | 汤燕 | Skin whitening traditional Chinese medicine facial mask |
| CN104146198A (en) * | 2014-07-28 | 2014-11-19 | 王泰朕 | Honey capable of eliminating toxicants and beautifying skin, and preparation method thereof |
Non-Patent Citations (1)
| Title |
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| 如何自制养颜玫瑰蜜;匿名;《http://jingyan.baidu.com/article/8275fc86b6186746a03cf6ed.html》;http://jingyan.baidu.com/article/8275fc86b6186746a03cf6ed.html;20140722;第1-3页. |
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