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BR8404372A - PROCESS FOR THE PREPARATION OF IODINE AND ITS COMPOUNDS OF CARBONILATION PRODUCTS ACETIC ACID, ACETANIDRID OR ETHYLIDENE DIACETATE, OBTAINED IN THE CARBONILATION OF DIMETHYL ETH, METHYL ACETATE - Google Patents

PROCESS FOR THE PREPARATION OF IODINE AND ITS COMPOUNDS OF CARBONILATION PRODUCTS ACETIC ACID, ACETANIDRID OR ETHYLIDENE DIACETATE, OBTAINED IN THE CARBONILATION OF DIMETHYL ETH, METHYL ACETATE

Info

Publication number
BR8404372A
BR8404372A BR8404372A BR8404372A BR8404372A BR 8404372 A BR8404372 A BR 8404372A BR 8404372 A BR8404372 A BR 8404372A BR 8404372 A BR8404372 A BR 8404372A BR 8404372 A BR8404372 A BR 8404372A
Authority
BR
Brazil
Prior art keywords
carbonilation
iodine
compounds
acetic acid
methyl acetate
Prior art date
Application number
BR8404372A
Other languages
Portuguese (pt)
Inventor
Heinz Erpenbach
Klaus Gehrmann
Alexander Ohorodnik
Winfried Lork
Herbert Joest
Original Assignee
Hoechst Ag
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Hoechst Ag filed Critical Hoechst Ag
Publication of BR8404372A publication Critical patent/BR8404372A/en

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42Separation; Purification; Stabilisation; Use of additives
    • C07C51/487Separation; Purification; Stabilisation; Use of additives by treatment giving rise to chemical modification
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/54Preparation of carboxylic acid anhydrides
    • C07C51/573Separation; Purification; Stabilisation; Use of additives
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00Preparation of carboxylic acid esters
    • C07C67/48Separation; Purification; Stabilisation; Use of additives
    • C07C67/60Separation; Purification; Stabilisation; Use of additives by treatment giving rise to chemical modification

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Catalysts (AREA)
  • Furan Compounds (AREA)
  • Carbon And Carbon Compounds (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)

Abstract

1. Process for separating iodine and its compounds from the carbonylation products acetic acid, acetic anhydride or ethylidene diacetate obtained by subjecting dimethylether, methyl acetate or methanol to carbonylation, characterized in that, in order to reduce the quantity of total iodine contaminating the carbonylation products to less than 20 ppb iodine, the carbonylation products are treated at temperatures of 50 to 200 degrees C with hydrogen in the presence of at least one noble metal selected from group VIII of the Periodic System of the elements, and separated from the noble metal.
BR8404372A 1983-09-01 1984-08-31 PROCESS FOR THE PREPARATION OF IODINE AND ITS COMPOUNDS OF CARBONILATION PRODUCTS ACETIC ACID, ACETANIDRID OR ETHYLIDENE DIACETATE, OBTAINED IN THE CARBONILATION OF DIMETHYL ETH, METHYL ACETATE BR8404372A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE19833331548 DE3331548A1 (en) 1983-09-01 1983-09-01 METHOD FOR SEPARATING IODINE AND ITS COMPOUNDS FROM CARBONYLATION PRODUCTS OBTAINED FROM CARBONYLATING DIMETHYL ETHER, METHYL ACETATE OR METHANOL

Publications (1)

Publication Number Publication Date
BR8404372A true BR8404372A (en) 1985-07-30

Family

ID=6207989

Family Applications (1)

Application Number Title Priority Date Filing Date
BR8404372A BR8404372A (en) 1983-09-01 1984-08-31 PROCESS FOR THE PREPARATION OF IODINE AND ITS COMPOUNDS OF CARBONILATION PRODUCTS ACETIC ACID, ACETANIDRID OR ETHYLIDENE DIACETATE, OBTAINED IN THE CARBONILATION OF DIMETHYL ETH, METHYL ACETATE

Country Status (9)

Country Link
EP (1) EP0143179B1 (en)
JP (1) JPS6072837A (en)
AT (1) ATE22550T1 (en)
AU (1) AU568675B2 (en)
BR (1) BR8404372A (en)
CA (1) CA1234149A (en)
DE (2) DE3331548A1 (en)
MX (1) MX160501A (en)
ZA (1) ZA846823B (en)

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4792420A (en) * 1985-07-24 1988-12-20 Eastman Kodak Company Purification of carboxylic acid anhydrides
DE3534070A1 (en) * 1985-09-25 1987-04-02 Hoechst Ag METHOD FOR SEPARATING IODINE AND ITS COMPOUNDS FROM CARBONYLATION PRODUCTS OBTAINED FROM CARBONYLATING DIMETHYL ETHER, METHYL ACETATE OR METHANOL
DE3612504A1 (en) * 1985-09-30 1987-04-09 Hoechst Ag METHOD FOR SEPARATING IODINE AND ITS COMPOUNDS FROM CARBONYLATING PRODUCTS CONTAINING CARBBONYLATION OF DIMETHYL ETHER, METHYL ACETATE OR METHANOL
GB8822661D0 (en) * 1988-09-27 1988-11-02 Bp Chem Int Ltd Removal of iodine/iodide impurities
CA2088973C (en) * 1990-08-15 1998-09-29 Brent A. Tennant Process for the purification of acetic anhydride and acetic acid

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4246195A (en) * 1978-10-06 1981-01-20 Halcon Research And Development Corporation Purification of carbonylation products
DE3137782A1 (en) * 1981-09-23 1983-03-31 Hoechst Ag, 6230 Frankfurt METHOD FOR RECOVERY OF IODINE COMPOUNDS FROM THE EXHAUST GAS FROM CARBONYLATION REACTIONS
DE3149094A1 (en) * 1981-12-11 1983-06-16 Hoechst Ag, 6230 Frankfurt METHOD FOR REMOVING ACETONE FROM REACTION MIXTURES FROM CARBONYLATION REACTIONS
DE3329781A1 (en) * 1983-08-18 1985-02-28 Hoechst Ag, 6230 Frankfurt METHOD FOR SEPARATING IODINE AND ITS COMPOUNDS FROM CARBONYLATION PRODUCTS OBTAINED FROM CARBONYLATING DIMETHYL ETHER, METHYL ACETATE OR METHANOL
DE3534070A1 (en) * 1985-09-25 1987-04-02 Hoechst Ag METHOD FOR SEPARATING IODINE AND ITS COMPOUNDS FROM CARBONYLATION PRODUCTS OBTAINED FROM CARBONYLATING DIMETHYL ETHER, METHYL ACETATE OR METHANOL

Also Published As

Publication number Publication date
DE3460873D1 (en) 1986-11-06
AU568675B2 (en) 1988-01-07
EP0143179B1 (en) 1986-10-01
ZA846823B (en) 1985-05-29
MX160501A (en) 1990-03-12
JPH0528212B2 (en) 1993-04-23
AU3263784A (en) 1985-03-07
CA1234149A (en) 1988-03-15
ATE22550T1 (en) 1986-10-15
DE3331548A1 (en) 1985-03-21
EP0143179A1 (en) 1985-06-05
JPS6072837A (en) 1985-04-24

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Legal Events

Date Code Title Description
B21A Patent or certificate of addition expired [chapter 21.1 patent gazette]

Free format text: PATENTE EXTINTA EM 31/08/99