BR8404372A - PROCESS FOR THE PREPARATION OF IODINE AND ITS COMPOUNDS OF CARBONILATION PRODUCTS ACETIC ACID, ACETANIDRID OR ETHYLIDENE DIACETATE, OBTAINED IN THE CARBONILATION OF DIMETHYL ETH, METHYL ACETATE - Google Patents
PROCESS FOR THE PREPARATION OF IODINE AND ITS COMPOUNDS OF CARBONILATION PRODUCTS ACETIC ACID, ACETANIDRID OR ETHYLIDENE DIACETATE, OBTAINED IN THE CARBONILATION OF DIMETHYL ETH, METHYL ACETATEInfo
- Publication number
- BR8404372A BR8404372A BR8404372A BR8404372A BR8404372A BR 8404372 A BR8404372 A BR 8404372A BR 8404372 A BR8404372 A BR 8404372A BR 8404372 A BR8404372 A BR 8404372A BR 8404372 A BR8404372 A BR 8404372A
- Authority
- BR
- Brazil
- Prior art keywords
- carbonilation
- iodine
- compounds
- acetic acid
- methyl acetate
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/42—Separation; Purification; Stabilisation; Use of additives
- C07C51/487—Separation; Purification; Stabilisation; Use of additives by treatment giving rise to chemical modification
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/54—Preparation of carboxylic acid anhydrides
- C07C51/573—Separation; Purification; Stabilisation; Use of additives
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C67/00—Preparation of carboxylic acid esters
- C07C67/48—Separation; Purification; Stabilisation; Use of additives
- C07C67/60—Separation; Purification; Stabilisation; Use of additives by treatment giving rise to chemical modification
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Catalysts (AREA)
- Furan Compounds (AREA)
- Carbon And Carbon Compounds (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Abstract
1. Process for separating iodine and its compounds from the carbonylation products acetic acid, acetic anhydride or ethylidene diacetate obtained by subjecting dimethylether, methyl acetate or methanol to carbonylation, characterized in that, in order to reduce the quantity of total iodine contaminating the carbonylation products to less than 20 ppb iodine, the carbonylation products are treated at temperatures of 50 to 200 degrees C with hydrogen in the presence of at least one noble metal selected from group VIII of the Periodic System of the elements, and separated from the noble metal.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE19833331548 DE3331548A1 (en) | 1983-09-01 | 1983-09-01 | METHOD FOR SEPARATING IODINE AND ITS COMPOUNDS FROM CARBONYLATION PRODUCTS OBTAINED FROM CARBONYLATING DIMETHYL ETHER, METHYL ACETATE OR METHANOL |
Publications (1)
Publication Number | Publication Date |
---|---|
BR8404372A true BR8404372A (en) | 1985-07-30 |
Family
ID=6207989
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
BR8404372A BR8404372A (en) | 1983-09-01 | 1984-08-31 | PROCESS FOR THE PREPARATION OF IODINE AND ITS COMPOUNDS OF CARBONILATION PRODUCTS ACETIC ACID, ACETANIDRID OR ETHYLIDENE DIACETATE, OBTAINED IN THE CARBONILATION OF DIMETHYL ETH, METHYL ACETATE |
Country Status (9)
Country | Link |
---|---|
EP (1) | EP0143179B1 (en) |
JP (1) | JPS6072837A (en) |
AT (1) | ATE22550T1 (en) |
AU (1) | AU568675B2 (en) |
BR (1) | BR8404372A (en) |
CA (1) | CA1234149A (en) |
DE (2) | DE3331548A1 (en) |
MX (1) | MX160501A (en) |
ZA (1) | ZA846823B (en) |
Families Citing this family (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4792420A (en) * | 1985-07-24 | 1988-12-20 | Eastman Kodak Company | Purification of carboxylic acid anhydrides |
DE3534070A1 (en) * | 1985-09-25 | 1987-04-02 | Hoechst Ag | METHOD FOR SEPARATING IODINE AND ITS COMPOUNDS FROM CARBONYLATION PRODUCTS OBTAINED FROM CARBONYLATING DIMETHYL ETHER, METHYL ACETATE OR METHANOL |
DE3612504A1 (en) * | 1985-09-30 | 1987-04-09 | Hoechst Ag | METHOD FOR SEPARATING IODINE AND ITS COMPOUNDS FROM CARBONYLATING PRODUCTS CONTAINING CARBBONYLATION OF DIMETHYL ETHER, METHYL ACETATE OR METHANOL |
GB8822661D0 (en) * | 1988-09-27 | 1988-11-02 | Bp Chem Int Ltd | Removal of iodine/iodide impurities |
CA2088973C (en) * | 1990-08-15 | 1998-09-29 | Brent A. Tennant | Process for the purification of acetic anhydride and acetic acid |
Family Cites Families (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4246195A (en) * | 1978-10-06 | 1981-01-20 | Halcon Research And Development Corporation | Purification of carbonylation products |
DE3137782A1 (en) * | 1981-09-23 | 1983-03-31 | Hoechst Ag, 6230 Frankfurt | METHOD FOR RECOVERY OF IODINE COMPOUNDS FROM THE EXHAUST GAS FROM CARBONYLATION REACTIONS |
DE3149094A1 (en) * | 1981-12-11 | 1983-06-16 | Hoechst Ag, 6230 Frankfurt | METHOD FOR REMOVING ACETONE FROM REACTION MIXTURES FROM CARBONYLATION REACTIONS |
DE3329781A1 (en) * | 1983-08-18 | 1985-02-28 | Hoechst Ag, 6230 Frankfurt | METHOD FOR SEPARATING IODINE AND ITS COMPOUNDS FROM CARBONYLATION PRODUCTS OBTAINED FROM CARBONYLATING DIMETHYL ETHER, METHYL ACETATE OR METHANOL |
DE3534070A1 (en) * | 1985-09-25 | 1987-04-02 | Hoechst Ag | METHOD FOR SEPARATING IODINE AND ITS COMPOUNDS FROM CARBONYLATION PRODUCTS OBTAINED FROM CARBONYLATING DIMETHYL ETHER, METHYL ACETATE OR METHANOL |
-
1983
- 1983-09-01 DE DE19833331548 patent/DE3331548A1/en not_active Withdrawn
-
1984
- 1984-08-04 AT AT84109285T patent/ATE22550T1/en not_active IP Right Cessation
- 1984-08-04 EP EP84109285A patent/EP0143179B1/en not_active Expired
- 1984-08-04 DE DE8484109285T patent/DE3460873D1/en not_active Expired
- 1984-08-30 CA CA000462141A patent/CA1234149A/en not_active Expired
- 1984-08-31 JP JP59180842A patent/JPS6072837A/en active Granted
- 1984-08-31 MX MX202587A patent/MX160501A/en unknown
- 1984-08-31 AU AU32637/84A patent/AU568675B2/en not_active Ceased
- 1984-08-31 BR BR8404372A patent/BR8404372A/en not_active IP Right Cessation
- 1984-08-31 ZA ZA846823A patent/ZA846823B/en unknown
Also Published As
Publication number | Publication date |
---|---|
DE3460873D1 (en) | 1986-11-06 |
AU568675B2 (en) | 1988-01-07 |
EP0143179B1 (en) | 1986-10-01 |
ZA846823B (en) | 1985-05-29 |
MX160501A (en) | 1990-03-12 |
JPH0528212B2 (en) | 1993-04-23 |
AU3263784A (en) | 1985-03-07 |
CA1234149A (en) | 1988-03-15 |
ATE22550T1 (en) | 1986-10-15 |
DE3331548A1 (en) | 1985-03-21 |
EP0143179A1 (en) | 1985-06-05 |
JPS6072837A (en) | 1985-04-24 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
B21A | Patent or certificate of addition expired [chapter 21.1 patent gazette] |
Free format text: PATENTE EXTINTA EM 31/08/99 |