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BR112016026394A2 - processo para produzir um reagente de fosfato de cálcio, partícula de reagente de fosfato de cálcio, e, método de purificação de um efluente líquido - Google Patents

processo para produzir um reagente de fosfato de cálcio, partícula de reagente de fosfato de cálcio, e, método de purificação de um efluente líquido

Info

Publication number
BR112016026394A2
BR112016026394A2 BR112016026394A BR112016026394A BR112016026394A2 BR 112016026394 A2 BR112016026394 A2 BR 112016026394A2 BR 112016026394 A BR112016026394 A BR 112016026394A BR 112016026394 A BR112016026394 A BR 112016026394A BR 112016026394 A2 BR112016026394 A2 BR 112016026394A2
Authority
BR
Brazil
Prior art keywords
calcium phosphate
phosphate reagent
calcium
purifying
produce
Prior art date
Application number
BR112016026394A
Other languages
English (en)
Other versions
BR112016026394A8 (pt
BR112016026394B1 (pt
Inventor
Patrick Perrin
Olivier Jacques F J G Bodson
Thierry Delplanche
Dirk Breugelmans
Original Assignee
Solvay
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Solvay filed Critical Solvay
Publication of BR112016026394A2 publication Critical patent/BR112016026394A2/pt
Publication of BR112016026394A8 publication Critical patent/BR112016026394A8/pt
Publication of BR112016026394B1 publication Critical patent/BR112016026394B1/pt

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B25/00—Phosphorus; Compounds thereof
    • C01B25/16—Oxyacids of phosphorus; Salts thereof
    • C01B25/26—Phosphates
    • C01B25/32—Phosphates of magnesium, calcium, strontium, or barium
    • C01B25/322—Preparation by neutralisation of orthophosphoric acid
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/04—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising compounds of alkali metals, alkaline earth metals or magnesium
    • B01J20/041—Oxides or hydroxides
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/04—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising compounds of alkali metals, alkaline earth metals or magnesium
    • B01J20/043—Carbonates or bicarbonates, e.g. limestone, dolomite, aragonite
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/04—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising compounds of alkali metals, alkaline earth metals or magnesium
    • B01J20/048—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising compounds of alkali metals, alkaline earth metals or magnesium containing phosphorus, e.g. phosphates, apatites, hydroxyapatites
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/28—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
    • B01J20/28002—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their physical properties
    • B01J20/28004—Sorbent size or size distribution, e.g. particle size
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/28—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
    • B01J20/28014—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their form
    • B01J20/28016—Particle form
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/28—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
    • B01J20/28054—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J20/28057—Surface area, e.g. B.E.T specific surface area
    • B01J20/28061—Surface area, e.g. B.E.T specific surface area being in the range 100-500 m2/g
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30—Processes for preparing, regenerating, or reactivating
    • B01J20/3085—Chemical treatments not covered by groups B01J20/3007 - B01J20/3078
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00—Treatment of water, waste water, or sewage
    • C02F1/28—Treatment of water, waste water, or sewage by sorption
    • C02F1/281—Treatment of water, waste water, or sewage by sorption using inorganic sorbents
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C01P2004/61—Micrometer sized, i.e. from 1-100 micrometer
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/12—Surface area
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F2101/00—Nature of the contaminant
    • C02F2101/10—Inorganic compounds
    • C02F2101/20—Heavy metals or heavy metal compounds
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F2301/00—General aspects of water treatment
    • C02F2301/04—Flow arrangements
    • C02F2301/046—Recirculation with an external loop
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F2303/00—Specific treatment goals
    • C02F2303/16—Regeneration of sorbents, filters

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Analytical Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Hydrology & Water Resources (AREA)
  • Water Supply & Treatment (AREA)
  • Environmental & Geological Engineering (AREA)
  • Engineering & Computer Science (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Removal Of Specific Substances (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)
  • Water Treatment By Sorption (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
  • Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)

Abstract

processo para produzir um reagente de fosfato de cálcio, partícula de reagente de fosfato de cálcio, e, método de purificação de um efluente líquido. este pedido se refere a um processo para produzir um reagente de fosfato de cálcio, de acordo com o qual: - em uma primeira etapa, é feito uso de uma fonte de cálcio e uma fonte de íons fosfato em água, em uma razão molar que é ajustada de modo a obter uma razão molar ca/p de entre 0,5 a 1,6, e a fonte de cálcio é reagida com os íons fosfato a um ph de entre 2 e 8, a fim de obter uma suspensão (a) de fosfato de cálcio, e ? - em uma segunda etapa, são adicionados à suspensão (a) um composto alcalino compreendendo íons hidróxido a fim de definir um ph de mais de 8 e uma fonte adicional de cálcio a fim de obter uma suspensão (b) de reagente de fosfato de cálcio tendo uma razão molar ca/p de mais de 1,6. adicionalmente, o pedido se refere a um método para purificar um efluente líquido contendo elementos metálicos e/ou elementos não metálicos com o reagente de fosfato de cálcio obtenível por esse processo.
BR112016026394-4A 2014-05-16 2015-05-18 Processo para produzir um reagente de fosfato de cálcio BR112016026394B1 (pt)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
FR1454383A FR3021045B1 (fr) 2014-05-16 2014-05-16 Procede de production d'un reactif phosphocalcique, reactif obtenu et son utilisation
FR1454383 2014-05-16
PCT/EP2015/060923 WO2015173437A1 (en) 2014-05-16 2015-05-18 Process for producing a calcium phosphate reactant, reactant obtained and use thereof in the purification of liquid effluents

Publications (3)

Publication Number Publication Date
BR112016026394A2 true BR112016026394A2 (pt) 2017-08-15
BR112016026394A8 BR112016026394A8 (pt) 2020-10-20
BR112016026394B1 BR112016026394B1 (pt) 2024-02-06

Family

ID=51210619

Family Applications (1)

Application Number Title Priority Date Filing Date
BR112016026394-4A BR112016026394B1 (pt) 2014-05-16 2015-05-18 Processo para produzir um reagente de fosfato de cálcio

Country Status (14)

Country Link
US (2) US10814303B2 (pt)
EP (1) EP3142784B1 (pt)
KR (1) KR20170008261A (pt)
CN (1) CN106660794B (pt)
AU (1) AU2015261392B2 (pt)
BR (1) BR112016026394B1 (pt)
CA (1) CA2948573C (pt)
CL (1) CL2016002909A1 (pt)
EA (1) EA201692311A1 (pt)
ES (1) ES2909061T3 (pt)
FR (1) FR3021045B1 (pt)
MX (2) MX2016015088A (pt)
PL (1) PL3142784T3 (pt)
WO (1) WO2015173437A1 (pt)

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CN107847856A (zh) 2015-06-03 2018-03-27 索尔维公司 使用包含磷灰石的磷酸钙反应物来处理被金属或有机化合物污染的气体的方法
EP3551330A1 (en) 2016-12-07 2019-10-16 Solvay SA Copper supported catalyst comprising a ca-deficient hydroxyapatite for waste gas nox removal
EP3664935A1 (en) 2017-08-09 2020-06-17 Solvay SA Iron supported catalyst comprising a ca-deficient hydroxyapatite for waste gas treatment
WO2019106175A1 (en) 2017-11-30 2019-06-06 Solvay Sa Hydroxyapatite composite comprising activated carbon for use in removal of contaminants from effluents and method of making
WO2019106176A1 (en) 2017-11-30 2019-06-06 Solvay Sa Removal of contaminants from water effluent using a hydroxyapatite composite
US11472706B2 (en) 2017-11-30 2022-10-18 Solvay Sa Hydroxyapatite composite for use in removal of contaminants from effluents and methods of making
CN108163956B (zh) * 2018-02-13 2020-10-27 南京师范大学 一种利用双相磷酸钙在去除水中重金属铅的应用
US20200399127A1 (en) * 2018-03-06 2020-12-24 Basearth Co., Ltd. Method for producing calcium phosphate, and harmful gas- and odor-removing composition containing calcium phosphate obtained thereby
WO2019207075A1 (en) 2018-04-25 2019-10-31 Solvay Sa Removal of stable metal-cyanide complexes and metallic ions from water stream
EP3604234A1 (en) 2018-08-02 2020-02-05 Solvay Sa Removal of stable metal-cyanide complexes and metallic ions from water effluent
WO2020127627A1 (en) 2018-12-20 2020-06-25 Solvay Sa A particulate material comprising a hydroxyapatite and a metal sulfide and its use for removing contaminants from a fluid
WO2020128021A1 (en) 2018-12-20 2020-06-25 Solvay Sa Particles comprising hydroxyapatite, process for making and their use
EP3927667A1 (en) 2019-02-22 2021-12-29 Solvay Sa Method for the removal of at least one contaminant from an aqueous liquor or a gas
CN112062672B (zh) * 2020-09-18 2022-04-19 南昌航空大学 一种镧配合物及其制备方法和应用
CN112675805B (zh) * 2021-01-25 2022-04-19 西北师范大学 一种羟基磷灰石纳米线复合二硫化钼吸附剂的制备方法
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Also Published As

Publication number Publication date
CA2948573A1 (en) 2015-11-19
US10814303B2 (en) 2020-10-27
WO2015173437A1 (en) 2015-11-19
BR112016026394A8 (pt) 2020-10-20
ES2909061T3 (es) 2022-05-05
PL3142784T3 (pl) 2022-04-19
CL2016002909A1 (es) 2017-09-01
US20200330955A1 (en) 2020-10-22
CN106660794B (zh) 2019-02-12
EA201692311A1 (ru) 2017-04-28
AU2015261392B2 (en) 2019-02-28
CA2948573C (en) 2022-08-30
EP3142784B1 (en) 2021-12-29
MX2016015088A (es) 2017-05-30
EP3142784A1 (en) 2017-03-22
MX2022003153A (es) 2022-04-11
KR20170008261A (ko) 2017-01-23
FR3021045B1 (fr) 2020-02-21
FR3021045A1 (fr) 2015-11-20
CN106660794A (zh) 2017-05-10
US11498049B2 (en) 2022-11-15
BR112016026394B1 (pt) 2024-02-06
AU2015261392A1 (en) 2016-12-15
US20170080401A1 (en) 2017-03-23

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