Hedge balls nano-structure of a mixed-ligand lead(II) coordination polymer; thermal, structural and X-ray powder diffraction studies

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Hedge balls nano-structure of a mixed-ligand lead(II) coordination polymer; thermal, structural and X-ray powder diffraction studies†

Homa Sadeghzadeh^a and Ali Morsali*^a

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* Corresponding authors

^a Department of Chemistry, Faculty of Sciences, Tarbiat Modares University, P.O. Box 14115-175, Tehran, Islamic Republic of Iran

Abstract

Hedge balls nano-structure of a new Pb(II) two-dimensional coordination polymer, [Pb(3-pyc)(N₃)H₂O]_n (1), {3-Hpyc = 3-pyridinecarboxylic acid} was synthesized by a sonochemical method. The new nano-structure was characterized by scanning electron microscopy, X-ray powder diffraction, IR spectroscopy and elemental analyses. Compound 1 was structurally characterized by single-crystal X-ray diffraction and consists of two-dimensional polymeric units. The thermal stability of compound 1 was studied by thermal gravimetric and differential thermal analyses and comparison.

$Graphical abstract: Hedge balls nano-structure of a mixed-ligand lead(II) coordination polymer; thermal, structural and X-ray powder diffraction studies$

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Article information

DOI: https://doi.org/10.1039/B917819H
Article type: Communication
Submitted: 28 Aug 2009
Accepted: 25 Sep 2009
First published: 07 Oct 2009

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CrystEngComm, 2010,12, 370-372

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